Metrohm 823 User Manual

823 Membrane Pump Unit
Manual
8.823.8001EN
Metrohm AG CH-9100 Herisau Switzerland Phone +41 71 353 85 85 Fax +41 71 353 89 01 info@metrohm.com www.metrohm.com
823 Membrane Pump Unit
8.823.8001EN
Manual
06.2012 fpe
Teachware Metrohm AG CH-9100 Herisau teachware@metrohm.com
This documentation is protected by copyright. All rights reserved.
Although all the information given in this documentation has been checked with great care, errors cannot be entirely excluded. Should you notice any mistakes please send us your comments using the address given above.
Documentation in additional languages can be found on
http://documents.metrohm.com.
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Table of contents

1 Introduction 1
1.1 Instrument description ......................................................... 1
1.1.1 Model versions ........................................................................ 1
1.1.2 Connectors .............................................................................. 2
1.1.3 Intended use ........................................................................... 2
1.2 About the documentation ................................................... 2
1.2.1 Symbols and conventions ........................................................ 2
1.3 Safety instructions ................................................................ 3
1.3.1 General notes on safety ........................................................... 3
1.3.2 Electrical safety ........................................................................ 3
1.3.3 Tubing and capillary connections ............................................. 4
1.3.4 Flammable solvents and chemicals ........................................... 5
1.3.5 Recycling and disposal ............................................................. 5
2 Overview of the instrument 6
Table of contents
2.1 Mode of operation of the membrane pump ...................... 6
3 Installation 8
3.1 Setting up the instrument .................................................... 8
3.1.1 Packaging ................................................................................ 8
3.1.2 Checks .................................................................................... 8
3.1.3 Location .................................................................................. 8
3.2 Installing the inlet tubing and outlet tubing ...................... 8
3.3 Connecting the membrane pump ..................................... 10
3.3.1 Connection to a Sample Processor ......................................... 10
3.3.2 Connection to the 731 Relay Box .......................................... 11
4 Operation 13
5 Operation and maintenance 14
5.1 General notes ...................................................................... 14
5.1.1 Care ...................................................................................... 14
5.1.2 Maintenance by Metrohm Service .......................................... 14
5.2 Tubings ................................................................................ 15
5.3 Quality Management and validation with Metrohm ....... 15
6 Troubleshooting 16
6.1 Problems ............................................................................. 16
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Table of contents
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7 Technical specifications 17
7.1 Membrane pump ................................................................ 17
7.2 Power supply ...................................................................... 17
7.3 Interfaces and connectors ................................................. 17
7.4 Safety specifications ........................................................... 17
7.5 Electromagnetic compatibility (EMC) ................................ 18
7.6 Ambient temperature ......................................................... 18
7.7 Reference conditions .......................................................... 18
7.8 Dimensions/material ........................................................... 19
8 Conformity and warranty 20
8.1 Quality Management Principles ........................................ 20
8.2 Warranty (Guarantee) ........................................................ 21
9 Accessories 23
9.1 Scope of delivery per model version ................................. 23
9.1.1 823 Membrane Pump Unit .................................................... 23
9.1.2 823 Membrane Pump Unit with aspiration equipment ........... 24
9.1.3 823 Membrane Pump Unit with rinsing equipment ................ 26
9.2 Optional accessories ........................................................... 28
9.2.1 823 Membrane Pump Unit .................................................... 28
9.2.2 823 Membrane Pump Unit with aspiration equipment ........... 28
9.2.3 823 Membrane Pump Unit with rinsing equipment ................ 29
Index 30
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Table of figures

Figure 1 Front 823 Membrane Pump Unit ....................................................... 6
Figure 2 Mode of operation of the membrane pump ...................................... 6
Figure 3 Connecting the tubings ..................................................................... 9
Figure 4 Screwing the union nuts tightly ......................................................... 9
Figure 5 823 Membrane Pump Unit connected directly to the Sample Pro-
cessor ............................................................................................. 10
Figure 6 823 Membrane Pump Unit via the Remote Box and 731 Relay Box .. 11
Table of figures
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1 Introduction

1.1 Instrument description

The 823 Membrane Pump Unit is a versatile membrane pump. It was designed specifically for the production operation and laboratory environ­ment and enables a wide range of applications. Particularly when used in a Metrohm automation system with Sample Processor and various analysis instruments, it is of indisputable service in processing large sample series in the complete titration area and in various measuring applications or other analytical tasks.
The 823 Membrane Pump Unit uses the membrane pump principle (see Chapter 2.1, page 6) and is suitable for pumping all types of liquid media.
Note

1 Introduction

The 823 Membrane Pump Unit is not suitable for pumping liquids with solids content.
The flow rate of at least 450 mL/min opens up a wide range of applica­tions.

1.1.1 Model versions

The 823 Membrane Pump Unit is available in the following three versions:
2.823.0010
2.823.0020 823 Membrane Pump
2.823.0030 823 Membrane Pump
Each version includes different accessories according to its use (see Chap- ter 9, page 23).
823 Membrane Pump Unit
Unit
Unit
with aspiration equip­ment
with rinsing equipment
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1.2 About the documentation

1.1.2 Connectors

The 823 Membrane Pump Unit needs 16 - 24 V DC voltage.
Power is supplied to the pump via the direct connection to a Sample Pro­cessor (e.g. 814 or 815) or to the 731 Relay Box (connection via adapter cable 6.2160.010).

1.1.3 Intended use

The 823 Membrane Pump Unit is designed for usage in automated sys­tems in analytical laboratories.
This instrument is suitable for pumping chemicals and flammable samples. Use of the 823 Membrane Pump Unit therefore requires the user to have basic knowledge and experience in handling toxic and caustic substances. Knowledge with respect to the application of the fire prevention measures prescribed for laboratories is also mandatory.
1.2 About the documentation
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Caution
Please read through this documentation carefully before putting the instrument into operation. The documentation contains information and warnings which the user must follow in order to ensure safe opera­tion of the instrument.

1.2.1 Symbols and conventions

The following symbols and formatting may appear in this documentation:
Method Dialog text, parameter in the software
File New Menu or menu item
Cross-reference to figure legend
The first number refers to the figure number, the sec­ond to the instrument part in the figure.
Instruction step
Carry out these steps in the sequence shown.
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[Next] Button or key
Warning
This symbol draws attention to a possible life hazard or risk of injury.
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1 Introduction
Warning
This symbol draws attention to a possible hazard due to electrical current.
Warning
This symbol draws attention to a possible hazard due to heat or hot instrument parts.
Warning
This symbol draws attention to a possible biological hazard.
Caution
This symbol draws attention to a possible damage of instruments or instrument parts.
Note
This symbol marks additional information and tips.

1.3 Safety instructions

1.3.1 General notes on safety

Warning
This instrument may only be operated in accordance with the specifica­tions in this documentation.
This instrument has left the factory in a flawless state in terms of technical safety. To maintain this state and ensure non-hazardous operation of the instrument, the following instructions must be observed carefully.

1.3.2 Electrical safety

The electrical safety when working with the instrument is ensured as part of the international standard IEC 61010.
Warning
Only personnel qualified by Metrohm are authorized to carry out service work on electronic components.
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1.3 Safety instructions
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Warning
Never open the housing of the instrument. The instrument could be damaged by this. There is also a risk of serious injury if live components are touched.
There are no parts inside the housing which can be serviced or replaced by the user.
Mains voltage
Warning
An incorrect mains voltage can damage the instrument.
Only operate this instrument with a mains voltage specified for it (see rear panel of the instrument).
Protection against electrostatic charges
Warning
Electronic components are sensitive to electrostatic charges and can be destroyed by discharges.
Do not fail to pull the mains cable out of the mains connection socket before you set up or disconnect electrical plug connections at the rear of the instrument.

1.3.3 Tubing and capillary connections

Caution
Leaks in tubing and capillary connections are a safety risk. Tighten all connections well by hand. Avoid applying excessive force to tubing connections. Damaged tubing ends lead to leakage. Appropriate tools can be used to loosen connections.
Check the connections regularly for leakage. If the instrument is used mainly in unattended operation, then weekly inspections are manda­tory.
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