Teachware
Metrohm AG
CH-9100 Herisau
teachware@metrohm.com
This documentation is protected by copyright. All rights reserved.
Although all the information given in this documentation has been
checked with great care, errors cannot be entirely excluded. Should you
notice any mistakes please send us your comments using the address
given above.
Documentation in additional languages can be found on
Figure 6823 Membrane Pump Unit via the Remote Box and 731 Relay Box .. 11
Table of figures
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1 Introduction
1.1 Instrument description
The 823 Membrane Pump Unit is a versatile membrane pump. It was
designed specifically for the production operation and laboratory environment and enables a wide range of applications. Particularly when used in
a Metrohm automation system with Sample Processor and various analysis
instruments, it is of indisputable service in processing large sample series
in the complete titration area and in various measuring applications or
other analytical tasks.
The 823 Membrane Pump Unit uses the membrane pump principle (seeChapter 2.1, page 6) and is suitable for pumping all types of liquid
media.
Note
1 Introduction
The 823 Membrane Pump Unit is not suitable for pumping liquids with
solids content.
The flow rate of at least 450 mL/min opens up a wide range of applications.
1.1.1 Model versions
The 823 Membrane Pump Unit is available in the following three versions:
2.823.0010
2.823.0020823 Membrane Pump
2.823.0030823 Membrane Pump
Each version includes different accessories according to its use (see Chap-ter 9, page 23).
823 Membrane Pump
Unit
Unit
Unit
with aspiration equipment
with rinsing equipment
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1.2 About the documentation
1.1.2 Connectors
The 823 Membrane Pump Unit needs 16 - 24 V DC voltage.
Power is supplied to the pump via the direct connection to a Sample Processor (e.g. 814 or 815) or to the 731 Relay Box (connection via adapter
cable 6.2160.010).
1.1.3 Intended use
The 823 Membrane Pump Unit is designed for usage in automated systems in analytical laboratories.
This instrument is suitable for pumping chemicals and flammable samples.
Use of the 823 Membrane Pump Unit therefore requires the user to have
basic knowledge and experience in handling toxic and caustic substances.
Knowledge with respect to the application of the fire prevention measures
prescribed for laboratories is also mandatory.
1.2 About the documentation
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Caution
Please read through this documentation carefully before putting the
instrument into operation. The documentation contains information
and warnings which the user must follow in order to ensure safe operation of the instrument.
1.2.1 Symbols and conventions
The following symbols and formatting may appear in this documentation:
MethodDialog text, parameter in the software
File ▶ NewMenu or menu item
Cross-reference to figure legend
The first number refers to the figure number, the second to the instrument part in the figure.
Instruction step
Carry out these steps in the sequence shown.
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[Next]Button or key
Warning
This symbol draws attention to a possible life hazard
or risk of injury.
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1 Introduction
Warning
This symbol draws attention to a possible hazard due
to electrical current.
Warning
This symbol draws attention to a possible hazard due
to heat or hot instrument parts.
Warning
This symbol draws attention to a possible biological
hazard.
Caution
This symbol draws attention to a possible damage of
instruments or instrument parts.
Note
This symbol marks additional information and tips.
1.3 Safety instructions
1.3.1 General notes on safety
Warning
This instrument may only be operated in accordance with the specifications in this documentation.
This instrument has left the factory in a flawless state in terms of technical
safety. To maintain this state and ensure non-hazardous operation of the
instrument, the following instructions must be observed carefully.
1.3.2 Electrical safety
The electrical safety when working with the instrument is ensured as part
of the international standard IEC 61010.
Warning
Only personnel qualified by Metrohm are authorized to carry out service
work on electronic components.
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1.3 Safety instructions
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Warning
Never open the housing of the instrument. The instrument could be
damaged by this. There is also a risk of serious injury if live components
are touched.
There are no parts inside the housing which can be serviced or replaced
by the user.
Mains voltage
Warning
An incorrect mains voltage can damage the instrument.
Only operate this instrument with a mains voltage specified for it (see
rear panel of the instrument).
Protection against electrostatic charges
Warning
Electronic components are sensitive to electrostatic charges and can be
destroyed by discharges.
Do not fail to pull the mains cable out of the mains connection socket
before you set up or disconnect electrical plug connections at the rear
of the instrument.
1.3.3 Tubing and capillary connections
Caution
Leaks in tubing and capillary connections are a safety risk. Tighten all
connections well by hand. Avoid applying excessive force to tubing
connections. Damaged tubing ends lead to leakage. Appropriate tools
can be used to loosen connections.
Check the connections regularly for leakage. If the instrument is used
mainly in unattended operation, then weekly inspections are mandatory.
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1.3.4 Flammable solvents and chemicals
Warning
All relevant safety measures are to be observed when working with
flammable solvents and chemicals.
■Set up the instrument in a well-ventilated location (e.g. fume cup-
board).
■Keep all sources of flame far from the workplace.
■Clean up spilled liquids and solids immediately.
■Follow the safety instructions of the chemical manufacturer.
1.3.5 Recycling and disposal
This product is covered by European Directive 2002/96/EC, WEEE – Waste
from Electrical and Electronic Equipment.
The correct disposal of your old equipment will help to prevent negative
effects on the environment and public health.
1 Introduction
More details about the disposal of your old equipment can be obtained
from your local authorities, from waste disposal companies or from your
local dealer.
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2.1 Mode of operation of the membrane pump
12
3
4
5
6
2 Overview of the instrument
Figure 1Front 823 Membrane Pump Unit
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Status LED
1
For displaying the operating state.
Membrane pump
3
With arrows to indicate the flow direction.
Outlet connector
5
With union nut for the drainage tubing.
Inlet connector
2
With union nut for the aspiration tubing.
Pressurizing valve
4
Connection cable
6
With M8 plug for connection to a Sample
Processor.
2.1 Mode of operation of the membrane pump
Outlet valve
1
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6
Figure 2
Mode of operation of the membrane pump
Inlet valve
2
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2 Overview of the instrument
Pump chamber
3
Eccentric
5
PTFE membrane
4
Principle
The membrane pump is located in the pump head. The membrane made
of PTFE 4 is moved up and down by an eccentric 5. This results in a periodic volume change of the pump chamber 3. On the downstroke, the
medium to be pumped is therefore aspirated through the inlet valve 2. On
the upstroke, the membrane forces the medium out of the pump chamber
through the outlet valve 1.
The following features characterize the membrane pump:
■Self-aspirating, due to the ingenious membrane technology.
■Dry run safe, i.e., the pump is not damaged if gases are pumped
instead of liquids.
■Operational in any position.
■Small-sized and thus space-saving.
■High chemical resistance:
As chemically resistant materials such as PTFE, PP and FFPM are used in
all parts that come into contact with the media, nearly all neutral and
aggressive media may be pumped.
Note
If you use particularly aggressive media, make sure that the above-mentioned materials are resistant to them prior to using the instrument.
In addition, the membrane pump has a very long lifetime. The only
expendable parts are the membrane and the valve plates.
The dosing accuracy of the membrane pump is considerably further
increased by a valve at the pump outlet. This valve has the following three
functions:
■Pressurizing function
When media are pumped into systems with fluctuating pressures, into
a vacuum or from an overpressure area, the pressurizing valve ensures
a constant backpressure.
■Overflow function
The valve prevents an excessive rise in pressure in the system on the
pressure side.
■Anti-injector function
When the pump is used for dosing into piping systems with high flow
rates, the pressurizing valve prevents an injector effect (aspiration of
ambient air as a result of the underpressure).
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3.1 Setting up the instrument
3 Installation
3.1 Setting up the instrument
3.1.1 Packaging
The instrument is supplied in highly protective special packaging together
with the separately packed accessories. Keep this packaging, as only this
ensures safe transportation of the instrument.
3.1.2 Checks
Immediately after receipt, check whether the shipment has arrived complete and without damage by comparing it with the delivery note.
3.1.3 Location
The instrument has been developed for operation indoors and may not be
used in explosive environments.
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Place the instrument in a location of the laboratory which is suitable for
operation, free of vibrations, protected from corrosive atmosphere, and
contamination by chemicals.
The instrument should be protected against excessive temperature fluctuations and direct sunlight.
3.2 Installing the inlet tubing and outlet tubing
As the inlet tubing and outlet tubing, two different tubing types are available. Both tubings are included in the scope of delivery:
■PVC tubing (6.1801.120), 2 x 2 m
■PTFE tubing (6.1812.000), 1 x 4 m
Note
Which of the two tubings to use depends largely on the solvent used.
PVC tubing is more flexible and has the advantage of making less noise
during the pumping operation. It must be noted that the PVC tubing is
not resistant to solvents.
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Install the inlet tubing and outlet tubing as follows:
Cut the inlet tubing and outlet tubing to the suitable length.
1
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Connect the tubings to the tubing olives of the pump tubing using
2
union nuts.
Figure 3Connecting the tubings
Note
To fasten PTFE tubings in place, you have to widen their openings
(e.g. using a Phillips screwdriver). You can use a piece of sandpaper to make the PTFE tubing easier to handle.
3 Installation
Screw the union nuts tightly to ensure a secure tubing connection.
3
Figure 4Screwing the union nuts tightly
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3.3 Connecting the membrane pump
12
3.3 Connecting the membrane pump
Warning
Follow the instructions listed below for connecting to a control device.
The instrument can be damaged if operated with the wrong supply
voltage.
Voltage
The 823 Membrane Pump Unit needs 16 - 24 V DC voltage. It can be connected directly to Sample Processor models 814, 815, 855 or 864.
When using the 823 Membrane Pump Unit in an automation system with
remote control, we recommend using a 731 Relay Box for the power supply.
3.3.1 Connection to a Sample Processor
■Plug the M8 plug into the socket on the Sample Processor provided for
this purpose.
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Sample Processor 814, 815, 855, 864
1
Instruments with Pump Connector.
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Figure 5
823 Membrane Pump Unit connected directly to the Sample
Processor
823 Membrane Pump Unit
2
Membrane pump with M8 plug.
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3
45
6
Note
The 823 Membrane Pump Unit is not suitable for use in conjunction
with the 824 Easy Sample Changer processor.
3.3.2 Connection to the 731 Relay Box
Connect the 823 Membrane Pump Unit with connection via the Remote
Box (6.2148.010) and the 731 Relay Box to a remote interface.
■Connect the M8 plug of the 772 Pump Unit to the corresponding
socket on the adapter cable.
■Plug the adapter cable into low-voltage DC current output DC1 or DC2
of the 731 Relay Box.
3 Installation
Figure 6
Sample Processor 814, 815, 855, 864
1
Connection to remote interface.
Remote cable (6.2125.100)
3
Adapter cable (6.2160.010)
5
823 Membrane Pump Unit via the Remote Box and 731 Relay
Box
Remote Box (6.2148.010)
2
731 Relay Box (2.731.0010)
4
823 Membrane Pump Unit
6
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3.3 Connecting the membrane pump
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Note
Ensure the correct polarity of the banana plugs. The red plug (positive
pole) belongs in the red socket, the black plug (negative pole) belongs
in the black socket.
Note
For information on controlling the 823 Membrane Pump Unit using the
731 Relay Box and a suitable control device, refer to the manual of the
731 Relay Box.
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4 Operation
4 Operation
The 823 Membrane Pump Unit does not have its own operating units. It is
operated and controlled via the main instrument in the linked system.
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5.1 General notes
5 Operation and maintenance
5.1 General notes
5.1.1 Care
The 823 Membrane Pump Unit requires appropriate care. Excess contamination of the instrument may result in functional disruptions and a reduction in the lifetime of the sturdy mechanics and electronics.
Spilled chemicals and solvents should be removed immediately. Above all,
the plug connections on the rear of the instrument (in particular the mains
connection socket) should be protected from contamination.
Caution
Although this is extensively prevented by design measures, the mains
plug should be unplugged immediately if aggressive media have penetrated the inside of the instrument, so as to avoid serious damage to
the instrument electronics. In such cases, Metrohm Service must be
informed.
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5.1.2 Maintenance by Metrohm Service
Maintenance of the 823 Membrane Pump Unit is best carried out as part
of an annual service, which is performed by specialist personnel of the
Metrohm company. If working frequently with caustic and corrosive
chemicals, a shorter maintenance interval could be necessary.
Metrohm Service offers every form of technical advice for maintenance
and service of all Metrohm instruments.
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5 Operation and maintenance
5.2 Tubings
The tubing requires regular inspection in order to work properly:
■Do not kink PTFE tubing.
■Ensure resistance to solvents .
■Check the tubing regularly for any damage.
5.3 Quality Management and validation with Metrohm
Quality Management
Metrohm offers you comprehensive support in implementing quality management measures for instruments and software. Further information on
this can be found in the brochure «Quality Management withMetrohm» available from your local Metrohm agent.
Validation
Please contact your local Metrohm agent for support in validating instruments and software. Here you can also obtain validation documentation
to provide help for carrying out the Installation Qualification (IQ) and
the Operational Qualification (OQ). IQ and OQ are also offered as a
service by the Metrohm agents. In addition, various application bulletins
are also available on the subject, which also contain Standard Operat-ing Procedures (SOP) for testing analytical measuring instruments for
reproducibility and correctness.
Maintenance
Electronic and mechanical functional groups in Metrohm instruments can
and should be checked as part of regular maintenance by specialist personnel from Metrohm. Please ask your local Metrohm agent regarding the
precise terms and conditions involved in concluding a corresponding
maintenance agreement.
Note
You can find information on the subjects of quality management, validation and maintenance as well as an overview of the documents currently available at www.metrohm.com/com/ under Support.
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6.1 Problems
6 Troubleshooting
6.1 Problems
ProblemCauseRemedy
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The liquid is not
aspirated, but just
"bubbles" instead.
The tubing connection of the inlet tubing and/or outlet
tubing is dripping.
The membrane
pump does not aspirate the solution.
The membrane
pump is pumping
too little or not at
all.
The inlet tubing and the
outlet tubing have been
switched.
The tubings are not
screwed on correctly.
The inlet valve or the outlet
valve is blocked.
The PTFE tubings are
kinked.
The membrane platelets
stick to each other. This
may occur if the membrane pump has not been
in use for an extended
period.
Switch the tubings so that the inlet tubing
goes into the solution and the outlet tubing
goes into the waste canister.
Check the screw connectors.
Contact Metrohm Service at your Metrohm
representative.
Straighten the kinked part or use flawless tubings.
Spray some water into the inlet valve with a
spray bottle, close the valve and allow to react
for some minutes.
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Too much air is trapped
between the membrane
platelets during aspirating
and pumping.
Contact Metrohm Service at your Metrohm
representative.
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7 Technical specifications
7.1 Membrane pump
Flow rate> 450 mL/min
7.2 Power supply
7 Technical specifications
Voltage
Power consumption
16 - 24 V DC
≤ 650 mA
7.3 Interfaces and connectors
The 823 Membrane Pump Unit does not have any control interfaces. It is
operated and controlled via the power supply.
7.4 Safety specifications
This instrument fulfills the following electrical safety requirements:
CE designation in accordance with the EU directives:
■2006/95/EC (Low Voltage Directive, LVD)
■2004/108/EC (EMC Directive, EMC)
Design and testing■EN/IEC/UL 61010-1
■CSA-C22.2 No. 61010-1
■Protection class III
■EN/IEC 60529
■Protection class IP20
Safety instructionsThis document contains safety instructions which have to be followed
by the user in order to ensure safe operation of the instrument.
Metrohm Ltd. holds the ISO 9001:2000 Certificate, registration number
10872-02, issued by SQS (Swiss Association for Quality and Management
Systems). Internal and external audits are carried out periodically to assure
that the standards defined by Metrohm’s QM Manual are maintained.
The steps involved in the design, manufacture and servicing of instruments
are fully documented and the resulting reports are archived for ten years.
The development of software for PCs and instruments is also duly documented and the documents and source codes are archived. Both remain
the possession of Metrohm. A non-disclosure agreement may be asked to
be provided by those requiring access to them.
The implementation of the ISO 9001:2000 quality management system is
described in Metrohm’s QM Manual, which comprises detailed instructions on the following fields of activity:
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Instrument development
The organization of the instrument design, its planning and the intermediate controls are fully documented and traceable. Laboratory testing
accompanies all phases of instrument development.
Software development
Software development occurs in terms of the software life cycle. Tests are
performed to detect programming errors and to assess the program’s
functionality in a laboratory environment.
Components
All components used in the Metrohm instruments have to satisfy the quality standards that are defined and implemented for our products. Suppliers of components are audited by Metrohm as the need arises.
Manufacture
The measures put into practice in the production of our instruments guarantee a constant quality standard. Production planning and manufacturing
procedures, maintenance of production means and testing of components, intermediate and finished products are prescribed.
Customer support and service
Customer support involves all phases of instrument acquisition and use by
the customer, i.e. consulting to define the adequate equipment for the
analytical problem at hand, delivery of the equipment, user manuals, train-
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ing, after-sales service and processing of customer complaints. The
Metrohm service organization is equipped to support customers in implementing standards such as GLP, GMP, ISO 900X, in performing Operational Qualification and Performance Verification of the system components or in carrying out the System Validation for the quantitative determination of a substance in a given matrix.
8.2 Warranty (Guarantee)
Metrohm guarantees that the deliveries and services it provides are free of
errors in materials, design or manufacturing.
The general warranty period is 36 months (exclusions below) from the
date of delivery or 18 months in the event of continuous operation. The
warranty remains valid on the condition that the servicing is provided by a
Service Organization authorized by Metrohm at defined intervals and with
a defined scope.
The warranty period for anion suppressors is 120 months from the date of
delivery or 60 months in the event of continuous operation.
8 Conformity and warranty
The warranty period for IC separation columns is 90 days after start-up.
For third-party components that are recognizable as such, the manufacturer's warranty regulations apply.
Consumables and materials with limited storage life and glass breakage in
the case of electrodes or other glass parts are excluded from the warranty.
Warranty claims cannot be asserted if the customer has failed to meet his
payment obligations according to schedule.
During the warranty period, Metrohm undertakes either to replace free of
charge or to credit the purchaser for any assemblies or components that
can be shown to be faulty. Any transport or customs fees that may apply
are the ordering party’s responsibility.
The precondition for this is that the ordering party must use the Return
Material Authorization (RMA) to report the faulty part, along with specification of the article number, the article designation, an adequate error
description, the delivery date and (if applicable) the serial number or the
chip data, respectively. In addition, the ordering party undertakes to store
the faulty part for at least 24 months in accordance with current storage
directives (in compliance with ESD guidelines) and to hold it in readiness
for onsite inspection or for return shipment to Metrohm. Metrohm
reserves the right to invoice the ordering party for these articles, including
retroactively, in the event of noncompliance with these pre-conditions.
The original warranty periods for the original part apply to parts that are
replaced or repaired under the above-referenced warranties (no extension
of the warranty period).
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8.2 Warranty (Guarantee)
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Deficiencies arising from circumstances that are not the responsibility of
Metrohm, such as improper storage or improper use, etc., are expressly
excluded from the warranty.
Metrohm also offers a 120-month spare parts availability guarantee and a
60-month PC software support warranty, calculated from the date on
which the product is withdrawn from the market. The content of this warranty is the ability of the customer to obtain functioning spare parts or
appropriate software support at market prices during the time of the warranty period.
If Metrohm AG is unable to meet this obligation due to circumstances
beyond the control of Metrohm AG, then the ordering party shall be
offered alternative solutions at preferential conditions.
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9 Accessories
Note
Subject to change without notice.
9.1 Scope of delivery per model version
Note
After receiving the instrument, check the shipment to ensure that it is
complete. In doing so, check the version (order number) of your 823
Membrane Pump Unit.
9 Accessories
823 Membrane Pump Unit
2.823.0010
Qty.
Order no.Description
11.823.0010Membrane Pump Unit
Membrane pump for direct connection to Sample Processors.