Hanna Instruments HI 9032 User Manual

4.7 (7)

Instruction Manual

HI 9032

Microprocessor Bench

Conductivity/TDS/NaCl

Fertilizer/°C/°F Meter

with RS 232

These Instruments are in Compliance with the CE Directives

h t t p : / / w w w . h a n n a i n s t . c o m

Dear Customer,

Thank you for choosing a Hanna Instruments Product.

Please read this instruction manual carefully before using the instrument.

This manual will provide you with all the necessary information for the correct use of the instrument, as well as a precise idea of its versatility in a wide range of applications.

This instrument is in compliance with CSA, UL and (EN 50081-1 and EN 50082-1) directives.

TABLE OF CONTENTS

Preliminary Examination .............................

3

General Description .....................................

3

The Front Panel ..........................................

 

 

5

Liquid Crystal Displays................................

7

The Rear Panel ...........................................

 

 

8

Specifications ...........................................

 

 

10

Operational Guide

......................................

11

Conductivity Calibration .............................

21

NaCl Calibration ........................................

 

 

31

Fertilizer Calibration ..................................

35

Setting Temperature ..................................

40

Setting Temperature .................Coefficient

42

Setting TDS Factor ...................................

45

Programs ..................................................

 

 

47

Interface with PC

.......................................

 

54

Probe Maintenance ...................................

59

Accessories ..............................................

 

 

60

Warranty ...................................................

 

 

62

CE Declaration of Conformity ....................

63

 

 

ISO 9000

Certified

 

e

 

 

ins rum

 

n s Company since 1992

PRELIMINARY EXAMINATION

Remove the instrument from the packing material and examine it to make sure that no damage has occurred during shipping. If there is any damage, notify your Dealer.

Each HI 9032 bench meter is supplied complete with:

HI 7669/2W Temperature Probe

HI 7686 Conductivity Probe

External Power Supply (HI710005 or

HI710006)

HI 76405 Electrode Holder

Dust Cover

Note: Save all packing material until you are sure that the instrument functions correctly. All defective items must be returned in the original package together with the supplied accessories.

GENERAL DESCRIPTION

Hanna Instruments HI 9032 is a micropro- cessor-based, bench-top, conductivity meter designed for the laboratory stringent demands, with the ability to perform five types of measurements:

Conductivity (4 different ranges: 0.0 to

399.9S/cm, 399 to 3999 S/cm, 3.99 to

39.99mS/cm, 39.9 to 99.9 mS/cm)

Fertilizer Concentration (F1 or F2 in the range 0.00 to 39.9 g/l)

NaCl of sea water saturation (range 0.0 to 130.0%)

Temperature (range 0.0 to 50.0°C)

Total Dissolved Solids (3 different ranges:

0.0to 199.9 ppm, 0 to 1999 ppm, 0.00 to

19.99g/l).

2

3

HI 9032 automatically recognizes buffers @ 84 S/cm, 1413 S/cm, 12.88 mS/cm, 80.0 mS/cm.

Commands are easily accessible through the user-friendly keyboard:

Through the COND key the meter is set in the conductivity range, TDS key selects Total Dissolved Solids measurements, NaCl key sets the range to NaCl measurement, and the FERT key selects 1st or 2nd fertilizer measurements.

Temperature compensation can be either automatic or manual. It can be selected through the key ATC / MTC respectively.

A temperature coefficient factor (for conductivity measurements) can be also selected through the %TC key (from 0.0 to 3.0%).

The TDS factor (for TDS measurements) can be selected through the FTR key (from 0.01 to 0.99).

The unit includes memory storages for all calibration data even after the unit is shut off.

HI 9032 is equipped with two liquid crystal displays:

A large one in two sections (primary and secondary LCD) indicates conductivity, TDS, NaCl, Fertilizer and temperature coefficient %;

A smaller one indicates temperature.

The meter also incorporates a standard R232C output to allow serial communication with a host computer; a series of programs can be selected for the setting of the R232C baud rate.

 

 

 

 

THE FRONT PANEL

 

 

 

 

 

 

 

CALIBRATION

 

 

 

 

 

 

 

 

 

 

ins rum n s

 

1

Select

 

Cond.

Fert.

NaCl

or

T.D.S.

 

 

 

 

 

2

Depress

CAL

 

 

 

 

 

 

 

 

 

 

 

e

 

3

Depress

0 ....

9 to enter calibration parameter

 

 

 

 

HI9032 microcomputer conductivity meter

4

Depress

ENTER

repeat

3 &

4

when necessary

 

 

 

 

 

 

 

 

(refer to instruction manual for details)

 

 

 

 

 

 

 

 

 

 

5

When

 

BUF on L.C.D. is blinking, place electrode in reference buffer

 

 

 

 

 

 

6

When

 

BUF displayed on L.C.D. & ~

on L.C.D. is blinking, equipment confirm that

 

 

 

 

 

 

 

buffer is within ±15% of theoritical set value, but reading is still not stable yet

 

 

LO BAT

 

 

m

 

When

 

 

& " CON" displayed on L.C.D., depress

CON

key to confirm for

 

1

 

 

S

7

 

BUF

 

SAMPLE

 

 

ppm

 

 

 

 

 

 

 

 

 

 

 

 

 

%

 

accepting the calibration

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

HOLD

 

 

gm

8

Equipment return to OPERATION mode for measurement

 

 

 

 

 

 

 

 

CONDUCTIVITY

TDS

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

FERTILIZER

NaCl

 

Main

Display

 

 

 

 

 

 

 

 

 

 

 

 

 

: The Result of measurement

 

 

 

 

CON

 

F1

°C

Sub.

Display

: Conditions of the measurement

 

 

 

 

 

Temp. Display

 

 

 

 

 

 

 

 

 

CAL

BUF

F2

%TC

: Temperature reading

 

 

 

 

 

 

 

 

 

 

 

 

 

 

(Keyboard entry is shown by the blinking of Decimal point)

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

ON

OFF

 

 

 

 

 

 

Cond.

 

Fert.

 

NaCl

 

 

 

 

2

TEMP.

 

HI

 

 

7

 

 

 

8

 

 

9

 

 

 

 

 

LO

 

 

T.D.S.

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

CAL

 

 

 

 

 

 

4

 

 

 

5

 

 

6

 

 

 

 

 

 

 

 

 

 

FTR

 

 

°F

 

°C

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

CON

 

 

 

 

 

 

1

 

 

 

2

 

 

3

 

 

 

 

 

 

 

 

 

 

ATC

 

 

%TC

 

PGM

 

 

 

 

 

 

 

 

 

 

MTC

 

 

 

 

 

 

 

ENTER

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

0

 

 

 

.

 

Clear

 

 

 

 

1.Large display for Conductivity, Fertilizer, NaCl and TDS

This large LCD displays the conductivity, fertilizer, NaCl and TDS reading. The corresponding symbol will be displayed along with the measured value.

A "----" signal will appear on this display to indicate an out of range condition.

2.Temperature display

This LCD displays the temperature measured by the HI7669/2W probe or the value that was manually set through the keyboard. Temperature can be selected between the Celsius and the Fahrenheit scale by pressing the °C or the °F key respectively.

If the probe is not connected when the meter is turned on, the "25°C" (or "77°F") symbol with a blinking decimal point will default.

3

4

4

5

If the temperature probe is discon- nected during operation, the decimal point will start blinking.

It will blink also if the temperature range is exceeded.

This LCD also displays the program # during programming.

3. Calibration Procedure

Briefly describes calibration procedure

4.Keyboard

Cond key, to select conductivity measurement mode

Fert. key, to select fertilizer measurement mode and to select Fertilizer #1 or #2 ("F1" or "F2")

NaCl key, to select NaCl measurement mode

T.D.S. key, to select total dissolved solids measurement mode

FTR key, to select the TDS factor for TDS measurements (see page 45)

°C key, to display temperature in the Celsius scale

°F key, to display temperature in the Fahrenheit scale

ATM/MTC key, to select automatic or manual temperature compensation

%T.C. key, to select the temperature coefficient for conductivity measurements or to select a different conductivity buffer during calibration (see page 21)

PGM key, used in programming

ON key, to switch the instrument on

OFF key, to switch the instrument off

CAL key, to enter or exit the calibration mode

CON key, to confirm calibration data

ENTER Key, to confirm/enter the numeric data entry

0 to 9 keys, numeric and decimal keys for numeric data input

Clear Key, to clear the numeric data entry

LIQUID CRYSTAL DISPLAYS

Large display for Conductivity, Fertilizer, NaCl

and TDS

Primary Display

LO BAT

 

 

mS

SAMPLE

 

 

ppm

 

 

%

 

 

 

HOLD

 

 

gm

 

 

 

CONDUCTIVITY

TDS

 

FERTILIZER

NaCl

 

CON

 

F1

°C

 

 

CAL

BUF

F2

%TC

Secondary Display

HI

LO

TEMP. display for temperature in °C or °F and program #

6

7

THE REAR PANEL

1.DIN female socket for the conductivity probe (HI7686)

2.Temperature probe socket for use with the

HI7669/2W

3.Reset button

4.Potentiometer for conductivity calibration (0.0µS)

5.RS 232C socket for serial communication.

6.DC Power Socket (for HI710005 or

HI710006).

Probes connection

Connect the supplied conductivity probe HI7686 securely to the DIN socket provided (#1) by aligning the pins with the socket, pushing the plug in and tightening the threaded ring.

For temperature measurements and automatic temperature compensation connect the temperature probe HI7669/2W to the °C socket (#2).

RESET button

The RESET button (#3) is used when the instrument displays erroneous messages due to strong electrical interference or when the instrument's power supply was disconnected before the meter was switched off. Press the

RESET button and restart the entire operation.

Power connection

Plug the 12VDC adapter (HI710005 or HI710006) into the DC socket (#6).

Plug the adapter into the mains.

Note: The instrument uses the following configuration.

+ -

It is recommendable to use Hanna HI710005 or HI710006 voltage adapters (supplied with the meters) that use the proper polarity configuration.

HI 9032 can also be used with other adapters. In this case, remember to check the correct polarity of your adapter before connecting it to the meter.

Note:

Make sure the main line is protected by a fuse.

If you need to unplug the instrument, press the OFF key before disconnecting the meter from the mains.

8

9

SPECIFICATIONS

MEASURE

 

COND.

0.0-399.9 / 399-3999 µS/cm

 

3.99-39.99 / 39.9-99.9 mS/cm

FERTILIZER

0.00 to 39.99 g/l

NaCl

0.0 to 130.0%

TDS

0.0-199.9 / 0-1999 ppm;

 

0.00 to 19.99 g/l

TEMP.

0.0 to 50.0°C / 32.0 to 122.0°F

 

 

RESOLUTION

 

COND.

0.1 µS/cm; 1 µS/cm;

FERTILIZER

0.01 mS/cm; 0.1 mS/cm

0.01 g/l

NaCl

0.1%

TDS

0.1 pmm; 1 ppm; 0.01 g/l

TEMP.

0.1°C / 0.1°F

 

 

ACCURACY

±1% full scale each range

(@20°C/ 68°F)

±0.5°C / ±1°F

TEMP.

excluding probe error

 

 

TYPICAL EMC

±1% full scale all 4 ranges

DEVIATION

±0.1°C / ±0.2°F

 

 

CALIBRATION

Automatic single point at 84µS,

1413 µS, 12.88 mS and 80.0

 

 

mS

T E M P E R A T U R E

Automatic or manual from

COMPENSATION

0 to 50°C (32 to 122°F) with

 

an adjustable ß from 0.0 to

 

3.0% per degree °C.

 

 

TDS FACTOR

Adjustable from 0.01 to 0.99

 

 

ENVIRONMENT

0 to 50°C (32 to 122°F);

 

max. RH 95%

 

 

DIMENSIONS

230 x 170 x 70mm

 

(9.1 x 6.7 x 2.7")

 

 

SHIPPING WEIGHT

1.5 kg (3.3 lbs)

 

 

OPERATIONAL GUIDE

Make sure that the instrument has been calibrated before taking measurements (see calibration procedures on page 21 for conductivity, page 31 for NaCl and 35 for fertilizer).

Connect the conductivity probe to the meter securely by aligning the pins with the socket on the back of the meter, pushing the plug in and tightening the threaded ring.

Connect the temperature probe to the back of the meter for automatic temperature compensation or for temperature measurements.

If possible, to minimize any EMC interferences, use plastic beakers for the solutions.

TAKING CONDUCTIVITY, FERTILIZER, NaCl,

TDS MEASUREMENTS

With Automatic Temperature Compensation

Immerse the conductivity probe into the solution submerging the

holes of the sleeve in the sample.

Agitate the probe lightly in the solution to remove any air bubbles which may have been trapped inside the sleeve.

Immerse the temperature probe as close as possible to the conductivity probe.

10

11

ON

Switch the instrument on by pressing the ON key.

The meter automati-

 

cally defaults to the

 

 

mS

 

 

 

conductivity mea-

CONDUCTIVITY

 

surement mode with

 

 

 

 

2.0% as temperature

 

 

%TC

coefficient (on the

 

 

 

 

 

 

 

 

large LCD) and the

 

 

 

 

temperature in the

 

 

 

 

Celsius scale (on the TEMP. LCD).

 

Select a different measurement mode by pressing the following keys:

Fert.

• the Fert. key for fertilizer

#1

8

 

 

Fert.

• the Fert. key twice for fer-

8

tilizer #2

 

 

NaCl

• the NaCl key for NaCl of

9

sea water saturation.

 

 

T.D.S.

• the T.D.S. key for total

4

dissolved solids

 

 

Cond.

the Cond. key to enter the conductivity measurement 7 mode again.

Conductivity measurement mode

By pressing the Cond. key, the display will show "CONDUCTIVITY" to confirm the measurement mode.

Cond.

mS

CONDUCTIVITY

7

%TC

The meter will automatically default the temperature coefficient % value to 2.0% (shown on the secondary display) every time it is turned on.

Change the temperature coefficient to the value of the solution, by pressing the %TC key. The % value will start blinking on the secondary LCD.

mS

%TC

CONDUCTIVITY

.

%TC

Enter the desired value by pressing the numeric keys and then press the ENTER key to confirm the value.

The stored value will be displayed and it will stop blinking.

E.g. If you want to enter 2.5% as temperature coefficient value, proceed as follows:

Press the %TC key Press 2

Press .

Press 5

12

13

Press the ENTER key.

%TC

°F

%TC

 

 

 

 

ENTER

.

2

.

5

mS

CONDUCTIVITY

%TC

PGM

To clear the numeric entry,

Clear

press the CLEAR key.

See page 44 for the procedure to calculate the correct coefficient value.

If you need to take conductivity measurements without ATC, press the ATC/MTC key.

HI 9032 is an auto-ranging conductivity meter and the reading automatically

switches from one resolution to the next (from pure water @ 0.1 S/cm up to 99.9 mS/cm).

When using HI7686 together with HI7669/ 2W all readings are automatically compensated for any temperature difference. Wait for a few minutes for the temperature sensor to attain thermal equilibrium with the test solution before taking the measurement. If the temperature of the conductivity probe and the solution is drastically apart, a longer time should be allowed before taking readings.

Once the measurement reading stabilizes the measurement is complete.

If further measurements are desired, rinse the probe with a small amounts of the next sample and then proceed.

Fertilizer measurement mode

By pressing the Fert. key the display will show "FERTILIZER" to confirm the measurement mode and the secondary display will show "1", i.e. Fertilizer #1.

Fert.

gm

 

FERTILIZER

8

Select the second fertilizer ("2") by pressing the Fert. key again.

Fert.

gm

FERTILIZER

8

When using HI 7686 together with HI 7669/ 2W all readings are automatically compensated for any temperature difference. Wait for a few minutes for the temperature sensor to attain thermal equilibrium with the test solution before taking the measurement. If the temperature of the conductivity probe and the solution is drastically apart, a longer time should be allowed before taking readings.

Once the measurement reading stabilizes the measurement is complete.

If further measurements are desired, rinse the probe with a small amount of the next solution and test the sample.

14

15

Hanna Instruments HI 9032 User Manual

NaCl measurement mode

By pressing the NaCl key the display will show "NaCl" to confirm the measurement mode.

NaCl

%

NaCl

9

When using HI 7686 together with HI7669/ 2W all readings are automatically compensated for any temperature difference. Wait for a few minutes for the temperature sensor to attain thermal equilibrium with the test solution before taking the measurement. If the temperature of the conductivity probe and the solution is drastically apart, a longer time should be allowed before taking readings.

Once the measurement reading stabilizes the measurement is complete.

If further measurements are desired, rinse the probe with a small amount of the next solution and test the sample.

Total Dissolved Solids measurement mode

By pressing the TDS key the display will show "TDS" to confirm the measurement mode.

T.D.S.

ppm

 

TDS

4

 

The meter will automatically default the TDS factor value to 0.5 (shown on the secondary display) every time it is turned on.

Change the TDS factor to the value of the solution, by pressing the FTR key. The TDS factor value will start blinking on the secondary LCD.

FTR

ppm

 

TDS

1

 

Enter the desired value by pressing the numeric keys and then press the ENTER key to confirm the value.

The stored value will be displayed and it will stop blinking.

E.g. If you want to enter 0.9 as TDS factor, proceed as follows:

Press the FTR key Press .

Press 9

Press the ENTER key.

FTR

%TC

NaCl

 

 

ENTER

1

.

9

ppm

TDS

16

17

• To clear the numeric entry, PGM press the CLEAR key.

Clear

See page 45 for further information about the TDS factor.

HI9032 is an auto-ranging TDS meter, and the reading automatically switches from one resolution to the next (from 0.00mg/l up to 19.99 g/l).

When using HI 7686 together with HI7669/ 2W all readings are automatically compensated for any temperature difference. Wait for a few minutes for the temperature sensor to attain thermal equilibrium with the test solution before taking the measurement. If the temperature of the conductivity probe and the solution is drastically apart, a longer time should be allowed before taking readings.

Once the measurement reading stabilizes the measurement is complete.

If further measurements are desired, rinse the probe with a small amount of the next solution and test the sample.

With Manual Temperature Compensation

Immerse the HI7686 probe in the solution submerging the holes of the sleeve into the liquid. Tap the probe lightly on the bottom of the recipient to remove any air bubbles which may have being trapped inside the sleeve.

Take the temperature of the solution with a

Checktemp or a glass thermometer.

Press the ATC/MTC key and the decimal point will blink on the TEMP. display (both when in the Celsius and in the Fahrenheit scale).

ATC

MTC

0

°C

°F

Press the °C or

the °F key and

3

2

 

 

the temperature

 

 

value will start

 

 

blinking.

 

 

Enter the temperature of the solution by pressing the numeric keys and then press ENTER key to confirm the value. The stored value will be displayed and the decimal point will stop blinking.

E.g. If you want to enter 37.2°C as temperature value, proceed as follows:

Press 3 Press 7 Press . Press 2

Press the ENTER key and the display will

show "37.2°C".

°C

Cond

%TC

°F

 

 

 

ENTER

3

7

.

2

To clear the numeric entry,

PGM

 

press the CLEAR key.

Clear

The measurement reading displayed on the large LCD will be manually compensated for temperature variations.

18

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