OPERATING INSTRUCTIONS FOR
Model 3110
Portable Trace & Percent
Oxygen Analyzer
P/N M82155 12/05/11
DANGER
Toxic gases and or flammable liquids may be present in this monitoring system. Personal protective equipment may be required when servicing this instrument.
Hazardous voltages exist on certain components internally which may persist for a time even after the power is turned off and disconnected.
Only authorized personnel should conduct maintenance and/or servicing. Before conducting any maintenance or servicing, consult with authorized supervisor/manager.
Teledyne Analytical Instruments
Model 3110
Copyright © 2011 Teledyne Instruments/ Analytical Instruments
All Rights Reserved. No part of this manual may be reproduced, transmitted, transcribed, stored in a retrieval system, or translated into any other language or computer language in whole or in part, in any form or by any means, whether it be electronic, mechanical, magnetic, optical, manual, or otherwise, without the prior written consent of Teledyne Instruments/Analytical Instruments, 16830 Chestnut Street, City of Industry, CA 917491580.
Warranty
This equipment is sold subject to the mutual agreement that it is warranted by us free from defects of material and of construction, and that our liability shall be limited to replacing or repairing at our factory (without charge, except for transportation), or at customer plant at our option, any material or construction in which defects become apparent within one year from the date of shipment, except in cases where quotations or acknowledgements provide for a shorter period. Components manufactured by others bear the warranty of their manufacturer. This warranty does not cover defects caused by wear, accident, misuse, neglect or repairs other than those performed by TI/AI or an authorized service center. We assume no liability for direct or indirect damages of any kind and the purchaser by the acceptance of the equipment will assume all liability for any damage which may result from its use or misuse.
We reserve the right to employ any suitable material in the manufacture of our apparatus, and to make any alterations in the dimensions, shape or weight of any parts, in so far as such alterations do not adversely affect our warranty.
Important Notice
This instrument provides measurement readings to its user, and serves as a tool by which valuable data can be gathered. The information provided by the instrument may assist the user in eliminating potential hazards caused by his process; however, it is essential that all personnel involved in the use of the instrument or its interface, with the process being measured, be properly trained in the process itself, as well as all instrumentation related to it.
The safety of personnel is ultimately the responsibility of those who control process conditions. While this instrument may be able to provide early warning of imminent danger, it has no control over process conditions, and it can be misused. In particular, any alarm or control systems installed must be tested and understood, both as to how they operate and as to how they can be defeated. Any safeguards required such as locks, labels, or redundancy, must be provided by the user or specifically requested of TI/AI at the time the order is placed.
Therefore, the purchaser must be aware of the hazardous process conditions. The purchaser is responsible for the training of personnel, for providing hazard warning methods and instrumentation per the appropriate standards, and for ensuring that hazard warning devices and instrumentation are maintained and operated properly.
Teledyne Instruments/ Analytical Instruments, the manufacturer of this instrument, cannot accept responsibility for conditions beyond its knowledge and control. No statement expressed or implied by this document or any information disseminated by the manufacturer or its agents, is to be construed as a warranty of adequate safety control under the user’s process conditions.
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Portable Trace Oxygen Analyzer
Safety Messages
Your safety and the safety of others is very important. We have provided many important safety messages in this manual. Please read these messages carefully.
A safety message alerts you to potential hazards that could hurt you or others. Each safety message is associated with a safety alert symbol. These symbols are found in the manual and inside the instrument. The definition of these symbols is described below:
GENERAL WARNING/CAUTION: Refer to the instructions for details on the specific danger. These cautions warn of specific procedures which if not followed could cause bodily Injury and/or damage the instrument.
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CAUTION: HOT SURFACE WARNING: This warning is |
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specific to heated components within the instrument. Failure |
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to heed the warning could result in serious burns to skin and |
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underlying tissue. |
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WARNING: ELECTRICAL SHOCK HAZARD: Dangerous |
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voltages appear within this instrument. This warning is |
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specific to an electrical hazard existing at or nearby the |
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component or procedure under discussion. Failure to heed this |
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warning could result in injury and/or death from |
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electrocution. |
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Technician Symbol: All operations marked with this symbol |
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are to be performed by qualified maintenance personnel only. |
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NOTE: Additional information and comments regarding a |
specific component or procedure are highlighted in the form |
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of a note. |
CAUTION: THE ANALYZER SHOULD ONLY BE USED FOR THE PURPOSE AND IN THE MANNER DESCRIBED IN THIS MANUAL.
IF YOU USE THE ANALYZER IN A MANNER OTHER THAN THAT FOR WHICH IT WAS INTENDED, UNPREDICTABLE BEHAVIOR COULD RESULT
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Model 3110
POSSIBLY ACCOMPANIED WITH HAZARDOUS CONSEQUENCES.
This manual provides information designed to guide you through the installation, calibration operation and maintenance of your new analyzer. Please read this manual and keep it available.
Occasionally, some instruments are customized for a particular application or features and/or options added per customer requests. Please check the front of this manual for any additional information in the form of an Addendum which discusses specific information, procedures, cautions and warnings that may be peculiar to your instrument.
Manuals do get lost. Additional manuals can be obtained from TAI at the address given in the Appendix. Some of our manuals are available in electronic form via the internet. Please visit our website at: www.teledyne-ai.com.
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Portable Trace Oxygen Analyzer
Table of Contents |
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List of Figures.............................................................................. |
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Introduction ................................................................................... |
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1.1 |
Introduction |
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1.2 |
Features |
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1.3 |
Method of Analysis |
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1.4 |
Micro-Fuel Cell |
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1.4.1 Cell Warranty |
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1.5 |
Accuracy and Response |
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1.6 |
Signal Output |
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1.7 |
Compact Packaging |
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Installation ..................................................................................... |
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2.1 |
Charging the Batteries |
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2.2 |
Gas Connections |
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2.3 |
Sensor Installation |
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2.3.1 Installing a Percent Sensor |
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2.3.2 Installing a Trace Sensor |
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2.4 |
Calibration |
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2.4.1 Calibration Using Air for Percent Analysis |
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2.4.2 Calibration Procedure for Trace Analysis |
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2.4.3 Bleeding the Regulator and Purging the Gas Line |
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2.5 |
Set the Sample Flowrate |
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2.6 |
External Signal |
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Operation ..................................................................................... |
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3.1 |
Front Panel Interface |
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3.1.1 ENTER Key |
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3.1.2 ESCAPE Key |
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3.1.3 UP/DOWN Keys |
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3.2 |
Operation and Setup Screens and Menus |
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3.2.1 POWER ON Screen |
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3.2.2 HOME Screen |
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Model 3110
3.2.3 DATE Screen |
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3.2.4 TIME Screen |
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3.2.5 AO Rng Screen |
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3.2.6 SPAN VALUE Screen |
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3.2.7 SPAN Screen |
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3.2.8 Filter Screen |
22 |
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3.2.9 LOG INTV Screen (Optional) |
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3.2.10 LOG RESET & START Screen (Optional) |
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3.2.11 LOG TRANSMIT Screen |
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3.2.12 POWER DOWN Screen |
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Maintenance & Troubleshooting................................................ |
27 |
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4.1 |
Routine Maintenance |
27 |
4.2 |
Opening the Instrument Case |
27 |
4.3 |
Replacing the Battery |
27 |
4.4 |
Battery Power Supply Service |
28 |
4.5 |
Cell Replacement |
29 |
4.6 |
Cell Warranty |
30 |
4.7 |
Temperature Compensation |
31 |
4.8 |
Leak Testing |
31 |
Appendix...................................................................................... |
35 |
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A.1 Specifications |
35 |
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A.2 Spare Parts List |
36 |
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Portable Trace Oxygen Analyzer
List of Figures |
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Figure 1-1: Model 3110 |
Portable Trace Oxygen Analyzer |
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Figure 2-1: Model 3110 |
Rear Panel ................................................ |
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Figure 3-1: Front Panel Keys......................................................... |
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Figure 3-2: Available Menus and Their Sequence......................... |
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Figure 4-1: Battery Charger Port on the Model 3110..................... |
29 |
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Figure 4-2: Effects of CO2 on B-2 Cell Life ................................... |
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Model 3110
DANGER
COMBUSTIBLE GAS USAGE
WARNING
This instrument is approved as an intrinsically safe gas analyzer for use in a Division 1 Group A-D hazardous area. Note that this approval does not apply to the non-conductive LCD window and micro-fuel cell. Also, although the analyzer is capable of being ranged up to 25% oxygen, the approval does not apply to oxygen exposure above 20.9%. This approval applies only to the equipment specified and installed in accordance with the information contained within this manual. It is the customer's responsibility to ensure safety especially when combustible gases are being analyzed since the potential of gas leaks always exist.
The customer should ensure that the principles of operating this equipment are well understood by the user. Misuse of this product in any manner, tampering with its components, or unauthorized substitution of any component may adversely affect the safety of this instrument.
Since the use of this instrument is beyond the control of Teledyne Analytical Instruments, referred as TAI, no responsibility by TAI, its affiliates, and agents for damage or injury from misuse or neglect of this equipment is implied or assumed.
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Portable Trace Oxygen Analyzer |
Introduction |
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Introduction
1.1 Introduction
The Teledyne Analytical Instruments (TAI) Model 3110 Portable Oxygen Analyzer is a portable, intrinsically safe oxygen analyzer capable of analyzing oxygen levels from 0-10 parts per million (ppm) oxygen to 25% oxygen (dependent on configuration). These units are rated as intrinsically safe and may be used in a Class I, Div 1, Group A- D hazardous environment. The instrument operates from internal rechargeable batteries and is supplied with a universal AC charge adapter. It features quick-disconnect fittings for sample connections and a rugged, lightweight housing with handle. This versatile instrument can be brought to the sample site and set up for analysis quickly and easily. Because of the intrinsically safe design, the instrument can be employed even in hazardous environments without compromise once calibrated. The Model 3110 incorporates a large standard feature list designed for versatile, accurate oxygen analysis for a wide range of applications. Figure 1-1 shows the standard Model 3110 Portable Trace Oxygen Analyzer.
The microprocessor based Model 3110 instrument provides one user settable analysis range in both trace and percent sensitivities. The range can be set from 0-10 ppm to 25% oxygen with lower ranges or percent sensitivity models available.
Sample oxygen is displayed on a 2-line 20 character alphanumeric LCD display mounted on the front panel. Four buttons are used to interface with the instrument and access all of the analyzer features.
Sample gas is introduced and vented via a pair of quick-disconnect fittings that feature integral shutoff valves which automatically close when the mating male fitting is withdrawn. The fittings are an integral part of the measuring cell manifold so that internal sample passage volume is at an absolute minimum.
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Introduction |
Model 3110 |
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Alphanumeric
LCD
User Interface
Buttons
Contrast
Adjustment
Low Battery
Indicator
Battery
Charging
Indicator
Figure 1-1: Model 3110 Portable Trace Oxygen Analyzer
1.2 Features
This instrument is designed to be versatile analytical instrument and to perform reliably and accurately in analyzing oxygen concentrations in gas mixtures from ppm levels through 25% oxygen. The following features are standard on the Model 3110:
Display: A 2-line 20 character alphanumeric LCD
on the front panel displays data and operational information through various screens. The contrast is adjustable for various lighting conditions.
Four-Button User Interface: Operation is performed using the
four front panel mounted buttons. These buttons are used to enter data, select items and move through operational screens that appear on the display.
Universal AC Charge Adapter: The batteries can be recharged
without removing them from the instrument. The charger operates over the range of 100-240 VAC.
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Portable Trace Oxygen Analyzer |
Introduction |
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LEDs: Two front panel-mounted LEDs are used
to indicate low battery condition and when the battery is recharging.
Contrast Control: This feature allows the user to easily
adjust the contrast of the display for optimum viewing under different lighting conditions. The adjustment is made using a front panel control dial.
Percent of Range Voltage Output: A 0-1 VDC output is
available that represents the percentage of the current analysis range.
Data Logger: The optional built-in data logging feature
allows the user to specify the time interval between data recording sets. The date, time, and oxygen concentration readings are stored in internal RAM at the user specified interval. The data set can be downloaded using the instrument’s 9-pin serial interface.
Real-time Clock: This feature allows the Model 3110 to date
and time stamp the data set recorded on the data logger. It uses a 24 hour clock.
Quick Disconnect Fittings: Dual self-sealing quick disconnect
fittings are installed for easy sample connections.
1.3 Method of Analysis
The sample oxygen is measured by a unique electrochemical transducer which functions as a fuel cell; in this instance, the fuel is oxygen. Oxygen diffusing into the cell reacts chemically to produce an electrical current that is proportional to the oxygen concentration in the gas phase immediately adjacent to the transducer’s sensing surface. The linear, but minute signal produced by the transducer from trace oxygen is amplified by a two-stage amplifier. Sensor output signal is digitized and fed to the microprocessor. Additional signal conditioning and temperature compensation are handled electronically and appropriate signals are directed to the display and output ports.
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Introduction |
Model 3110 |
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1.4 Micro-Fuel Cell
The micro-fuel cell (U.S. Pat. Nos. 3,767,552 and 3,668,101) is a sealed electrochemical transducer with no electrolyte to change or electrodes to clean. When the cell reaches the end of its useful life, it is thrown away and replaced. The life of the cell is warranted by TAI (see below).
The cell is specific for oxygen and is not sensitive to flowrate or reducing agents such as hydrocarbons, carbon monoxide, sulfur dioxide, etc. In the absence of oxygen, no current is produced; thus, no zeroing is required.
1.4.1 Cell Warranty
The Class B1, B2-C, A2C, B2C-XL, Insta-trace and NG series micro-fuel cells used in the Model 3110 carry a six (6) month warranty.
With regard to spare cells, service time starts when the cell is removed from its shipping package. You should stock only one spare cell per instrument at a time.
If a cell was working satisfactorily but ceases to function before the warranty period expires, you will receive credit on a pro-rated basis toward the purchase of a new cell.
If you have a warranty claim, return the cell in question to the factory for evaluation. If it is determined that failure is due to faulty workmanship or material, the cell will be replaced at no cost to you.
WARNING: EVIDENCE OF DAMAGE DUE TO TAMPERING OR MISHANDLING WILL RENDER THE CELL WARRANTY NULL AND VOID.
The Model 3110 is rated as intrinsically safe and may be used in a Class I, Div 1, Group A-D hazardous environments.
This safety feature does not apply when the instrument is being charged with the 100240 VAC external charge adapter. The instrument should be removed from hazardous areas when the batteries are being charged.
Note: Do not use the analyzer when the battery level is low.
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Portable Trace Oxygen Analyzer |
Introduction |
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1.5 Accuracy and Response
The Model 3110 provides monitoring accuracies of ±2% of full scale or ±1 ppm, whichever is greater, at constant temperature.
With a sample flowrate of 1 SCFH, a 90% response can be achieved in 10 seconds when analyzing in the percent range. At the trace levels (ppm analysis), a 90% response can be realized in 60 seconds or less. The response time on the 3110 is limited by the filter setting.
1.6 Signal Output
This analyzer includes a 0-1 VDC output as standard. This signal is suitable for driving external devices that have an input impedance of
10,000 or more. The signal output is available from a port on the rear panel.
1.7 Compact Packaging
The instrument is housed in 6 1/8" × 9 1/2" × 5 5/8" (156 × 241 × 143mm) aluminum case that is equipped with a carrying handle and foot pads.
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