Metrohm 865 User Manual
865 Dosimat plus
Manual
8.865.8005EN
Metrohm AG
CH-9100 Herisau
Switzerland
Phone +41 71 353 85 85
Fax +41 71 353 89 01
info@metrohm.com
www.metrohm.com
865 Dosimat plus
Manual
8.865.8005EN 09.2011 dm
Teachware
Metrohm AG
CH-9100 Herisau
teachware@metrohm.com
This documentation is protected by copyright. All rights reserved.
Although all the information given in this documentation has been
checked with great care, errors cannot be entirely excluded. Should you
notice any mistakes please send us your comments using the address
given above.
Documentation in additional languages can be found on
http://products.metrohm.com under Literature/Technical documenta-
tion.
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Table of contents
1 Introduction 1
1.1 Instrument description ......................................................... 1
1.1.1 Dosing modes ......................................................................... 1
1.1.2 Connectors .............................................................................. 1
1.2 Intended use ......................................................................... 2
1.3 About the documentation ................................................... 2
1.3.1 Symbols and conventions ........................................................ 2
1.4 Safety instructions ................................................................ 3
1.4.1 General notes on safety ........................................................... 3
1.4.2 Electrical safety ........................................................................ 3
1.4.3 Tubing connections ................................................................. 4
1.4.4 Flammable solvents and chemicals ........................................... 5
1.5 Recycling and disposal ......................................................... 5
Table of contents
2 Overview of the instrument 6
2.1 865 Dosimat plus ................................................................. 6
2.2 Manual Dosing Controller .................................................... 8
3 Installation 9
3.1 Setting up the instrument .................................................... 9
3.1.1 Packaging ................................................................................ 9
3.1.2 Checks .................................................................................... 9
3.1.3 Location .................................................................................. 9
3.2 Connecting a stirrer .............................................................. 9
3.3 Connecting the Manual Dosing Controller ....................... 10
3.4 Connecting a balance ......................................................... 10
3.5 Connecting a keyboard, printer and other USB devi-
ces ........................................................................................ 11
3.6 Connecting instruments to the remote connector .......... 13
3.7 Connecting the 805 Dosimat ............................................. 14
3.8 Attaching the exchange unit ............................................. 15
865 Dosimat plus
4 Operation 16
4.1 Switching the instrument on and off ............................... 16
4.2 Fundamentals of operation ............................................... 17
4.2.1 The keypad ............................................................................ 17
4.2.2 Structure of the dialog windows ............................................ 18
4.2.3 Navigating in the dialog ......................................................... 18
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III
Table of contents
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4.2.4 Entering text and numbers ..................................................... 19
4.2.5 Selecting from a selection list ................................................. 20
4.3 Methods .............................................................................. 20
4.3.1 Method templates ................................................................. 20
4.3.2 Creating a new method ......................................................... 21
4.3.3 Saving a method ................................................................... 21
4.3.4 Loading a method ................................................................. 22
4.3.5 Exporting a method ............................................................... 23
4.4 Stirrer operation ................................................................. 24
4.5 Entering sample data ......................................................... 25
4.6 Preparing the buret unit (PREP) ........................................ 25
4.7 Printing a report manually ................................................. 26
5 System settings 28
5.1 Basic settings ...................................................................... 28
5.2 Managing solutions ............................................................ 31
5.2.1 General ................................................................................. 31
5.2.2 Editing the solution data ........................................................ 31
5.3 File management ................................................................ 33
5.4 Configuring external devices ............................................. 34
5.5 Instrument diagnosis .......................................................... 37
5.5.1 Loading program versions and language files ......................... 37
5.5.2 Diagnosis functions ............................................................... 38
6 Parameters and dosing modes 39
6.1 Manual dosing (DOS) ......................................................... 39
6.1.1 General description ................................................................ 39
6.1.2 Selecting a solution ............................................................... 40
6.1.3 Dosing parameters ................................................................ 40
6.1.4 Calculation ............................................................................ 41
6.1.5 Reports .................................................................................. 43
6.1.6 Pulse control .......................................................................... 43
6.2 Extended dosing (XDOS) .................................................... 44
6.2.1 General description ................................................................ 44
6.2.2 Selecting a solution ............................................................... 45
6.2.3 Selecting the operating mode ................................................ 45
6.2.4 Dosing parameters ................................................................ 47
6.2.5 Reports .................................................................................. 48
6.3 Creating solutions (CNT D) ................................................ 49
6.3.1 General description ................................................................ 49
6.3.2 Selecting a solution ............................................................... 51
6.3.3 Definition of the target solution ............................................. 51
6.3.4 Dosing parameters ................................................................ 52
6.3.5 Reports .................................................................................. 53
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IV
865 Dosimat plus
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7 Handling and maintenance 59
8 Appendix 61
Table of contents
6.4 Pipetting and diluting (LQT) .............................................. 54
6.4.1 General description ................................................................ 54
6.4.2 Selecting a solution ............................................................... 56
6.4.3 Definitions of the sample transfer .......................................... 56
6.4.4 Dosing parameters ................................................................ 57
6.4.5 Reports .................................................................................. 57
7.1 General ................................................................................ 59
7.2 Quality Management and validation with Metrohm ....... 59
8.1 Exchange unit ..................................................................... 61
8.1.1 Maximum dosing and filling rate ............................................ 61
8.1.2 Parameters for the preparing (PREP) ....................................... 61
8.2 Stirring rate ......................................................................... 62
8.3 Balance ................................................................................ 62
8.4 USB devices ......................................................................... 63
8.4.1 Numerical USB keypad 6.2147.000 ........................................ 63
8.4.2 Key assignment of a USB keyboard ........................................ 64
8.4.3 Printer ................................................................................... 64
8.5 System initialization ........................................................... 65
8.6 Remote interface ................................................................ 66
8.6.1 Pin assignment of the remote interface .................................. 66
8.6.2 Status diagram of the remote interface .................................. 67
8.7 Pulse control ....................................................................... 69
8.8 Remote control via an RS-232 connection ....................... 70
8.8.1 Commands and variables ....................................................... 71
9 Technical specifications 74
9.1 Dosing drive ........................................................................ 74
9.2 Interfaces ............................................................................. 74
9.3 Mains connection ............................................................... 74
9.4 Safety specification ............................................................ 75
9.5 Electromagnetic compatibility (EMC) ................................ 75
9.6 Ambient temperature ......................................................... 75
9.7 Reference conditions .......................................................... 76
9.8 Dimensions .......................................................................... 76
865 Dosimat plus
10 Conformity and warranty 77
10.1 Declaration of Conformity ................................................. 77
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V
Table of contents
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10.2 Quality Management Principles ........................................ 78
10.3 Warranty (guarantee) ......................................................... 79
11 Accessories 80
11.1 Scope of delivery 865 Dosimat plus 2.865.0010 ............. 80
11.2 Optional accessories ........................................................... 82
Index 86
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VI
865 Dosimat plus
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Table of figures
Figure 1 Front 865 Dosimat plus ..................................................................... 6
Figure 2 Rear 865 Dosimat plus ...................................................................... 7
Figure 3 Manual Dosing Controller 6.2107.100 ............................................... 8
Figure 4 Connecting a stirrer ........................................................................... 9
Figure 5 Connecting the Manual Dosing Controller ....................................... 10
Figure 6 Connecting a balance ...................................................................... 10
Figure 7 Connecting USB devices .................................................................. 11
Figure 8 Connecting the USB stick ................................................................ 12
Figure 9 Connecting the 6.2147.000 USB keyboard with USB stick and
printer ............................................................................................. 13
Figure 10 Connecting the USB hub with USB stick, printer and the 6.2148.030
RS-232/USB Box (for connecting balances). ..................................... 13
Figure 11 Connecting a remote cable ............................................................. 13
Figure 12 Connecting the 805 Dosimat ........................................................... 14
Figure 13 MSB connector on the 801 Stirrer ................................................... 14
Figure 14 Attaching the exchange unit ........................................................... 15
Figure 15 Keypad 865 Dosimat plus ................................................................ 17
Figure 16 Directory structure on the USB stick ................................................. 34
Figure 17 Dosing ramp, two examples ............................................................ 41
Figure 18 Tandem operation ........................................................................... 46
Figure 19 Rotational speed depending on stirring rate .................................... 62
Figure 20 Pin assignment of remote socket and plug ...................................... 66
Figure 21 Remote status diagram DOS ............................................................ 67
Figure 22 Remote status diagram DOS with pulse control ............................... 68
Figure 23 Remote status diagram XDOS .......................................................... 68
Figure 24 Remote status diagram CNT_D ........................................................ 68
Figure 25 Remote status diagram LQT ............................................................. 69
Figure 26 Connecting the RS-232/USB Box to the PC ...................................... 71
Table of figures
865 Dosimat plus
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VII
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1 Introduction
1.1 Instrument description
The 865 Dosimat plus is a universally utilizable dosing instrument. Methods can be generated and stored under a new name. When a USB memory stick is connected as an external storage medium, then the methods
can be exported to that USB memory stick. This function makes it possible
for you to copy methods quickly and easily from one instrument to
another. The remote connector enables the integration of the instrument
in a Metrohm automation system.
1.1.1 Dosing modes
The following dosing modes are supported:
￭ DOS
Manual dosing.
￭ XDOS
Fixed volume dosing, with freely selectable dosing criteria.
￭ CONT D
Preparing solutions.
￭ LQT
Pipetting and dilutiing.
1 Introduction
1.1.2 Connectors
The instrument is equipped with the following connectors:
￭ MSB connector (Metrohm Serial Bus)
￭ USB (OTG) connector
￭ Remote connector
For connecting a stirrer and an 805 Dosimat for tandem dosings.
The 6.2151.100 adapter allows you to connect, for example, a printer,
a USB memory stick or a USB keyboard. A printer can also be connec-
ted directly with the 6.2151.120 cable.
For connecting a Manual Dosing Controller, a Titrino plus or a sample
changer.
865 Dosimat plus
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1
1.2 Intended use
1.2 Intended use
The 865 Dosimat plus is designed for use in laboratories and production
plants. Its main area of application is the precise dosing of liquids. This
includes simple dosing according to specific criteria, the preparing of solutions, the pipetting of liquid samples and manual titrations.
The present instrument is suitable for dosing chemicals and flammable solvents. The usage of the 865 Dosimat plus therefore requires that the user
has basic knowledge and experience in the handling of poisonous and
caustic substances. Knowledge with respect to the application of the fire
prevention measures prescribed for laboratories or production plants is
also mandatory.
1.3 About the documentation
Caution
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Please read through this documentation carefully before putting the
instrument into operation. The documentation contains information
and warnings which have to be followed by the user in order to ensure
safe operation of the instrument.
1.3.1 Symbols and conventions
The following symbols and styles are used in this documentation:
Method Dialog text, parameter in the software
File ▶ New
[Next] Button or key
Cross-reference to figure legend
The first number refers to the figure number, the
second to the instrument part in the figure.
Instruction step
Carry out these steps in the sequence shown.
Menu or menu item
Warning
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2
This symbol draws attention to a possible life hazard
or risk of injury.
865 Dosimat plus
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1 Introduction
Warning
This symbol draws attention to a possible hazard due
to electrical current.
Warning
This symbol draws attention to a possible hazard due
to heat or hot instrument parts.
Warning
This symbol draws attention to a possible biological
hazard.
Caution
This symbol draws attention to a possible damage of
instruments or instrument parts.
Note
This symbol marks additional information and tips.
1.4 Safety instructions
1.4.1 General notes on safety
Warning
This instrument may only be operated in accordance with the specifications in this documentation.
This instrument has left the factory in a flawless state in terms of technical
safety. To maintain this state and ensure non-hazardous operation of the
instrument, the following instructions must be observed carefully.
1.4.2 Electrical safety
The electrical safety when working with the instrument is ensured as part
of the international standard IEC 61010.
Warning
Only personnel qualified by Metrohm are authorized to carry out service
work on electronic components.
865 Dosimat plus
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3
1.4 Safety instructions
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Warning
Never open the housing of the instrument. The instrument could be
damaged by this. There is also a risk of serious injury if live components
are touched.
There are no parts inside the housing which can be serviced or replaced
by the user.
Mains voltage
Warning
An incorrect mains voltage can damage the instrument.
Only operate this instrument with a mains voltage specified for it (see
rear panel of the instrument).
Protection against electrostatic charges
Electronic components are sensitive to electrostatic charges and can be
destroyed by discharges.
Always pull the mains cable out of the mains connection socket before
connecting or disconnecting electrical appliances on the rear panel of
the instrument.
1.4.3 Tubing connections
Leaks in tubing connections are a safety risk. Tighten all connections
well by hand. Avoid applying excessive force to tubing connections.
Damaged tubing ends lead to leakage. Appropriate tools can be used
to loosen connections.
Check the connections regularly for leaks.
Warning
Caution
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4
865 Dosimat plus
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1.4.4 Flammable solvents and chemicals
Warning
All relevant safety measures are to be observed when working with
flammable solvents and chemicals.
￭ Set up the instrument in a well-ventilated location.
￭ Keep all sources of flame far from the workplace.
￭ Clean up spilled fluids and solids immediately.
￭ Follow the safety instructions of the chemical manufacturer.
1.5 Recycling and disposal
This product is covered by European Directive 2002/96/EC, WEEE – Waste
from Electrical and Electronic Equipment.
The correct disposal of your old equipment will help to prevent negative
effects on the environment and public health.
1 Introduction
More details about the disposal of your old equipment can be obtained
from your local authorities, from waste disposal companies or from your
local dealer.
865 Dosimat plus
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5
2.1 865 Dosimat plus
2
5
4
3
1
2 Overview of the instrument
2.1 865 Dosimat plus
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Figure 1 Front 865 Dosimat plus
Piston rod
1
Of the dosing drive.
Coupling
3
For switching the flat stopcock.
Keypad
5
Contact pins
2
For the data chip.
Display
4
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6
865 Dosimat plus
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1
2
5
4
3
2 Overview of the instrument
Figure 2 Rear 865 Dosimat plus
Type plate
1
Contains specifications concerning mains
voltage and serial number.
USB (OTG) connector
3
For connecting printers, USB sticks, USB
hubs, etc.
Remote connector
5
For connecting the Manual Dosing Controller or instruments with a remote interface.
D-Sub, 9-pin.
Mains connection socket
2
MSB connector
4
Metrohm Serial Bus.
For connecting a stirrer or an 805 Dosimat.
Mini DIN, 9-pin.
865 Dosimat plus
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7
2.2 Manual Dosing Controller
1
2
3
4
2.2 Manual Dosing Controller
Figure 3 Manual Dosing Controller 6.2107.100
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Dosing key
1
To start the dosing.
Stop key/Fill key
3
For stopping and filling the dosing cylinder.
Status LED
2
Indicates the readiness of the instrument.
Connection cable
4
With 9-pin D-Sub plug.
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8
865 Dosimat plus
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3 Installation
3.1 Setting up the instrument
3.1.1 Packaging
The instrument is supplied in highly protective special packaging together
with the separately packed accessories. Keep this packaging, as only this
ensures safe transportation of the instrument.
3.1.2 Checks
Immediately after receipt, check whether the shipment has arrived complete and without damage by comparing it with the delivery note.
3.1.3 Location
The instrument has been developed for operation indoors and may not be
used in explosive environments.
3 Installation
Place the instrument in a location of the laboratory which is suitable for
operation, free of vibrations, protected from corrosive atmosphere, and
contamination by chemicals.
The instrument should be protected against excessive temperature fluctuations and direct sunlight.
3.2 Connecting a stirrer
You can connect the following stirrers:
￭ 801 Stirrer
￭ 803 Ti Stand
￭ 804 Ti Stand (requires rod stirrer)
865 Dosimat plus
Figure 4 Connecting a stirrer
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9
3.3 Connecting the Manual Dosing Controller
Caution
Make sure that the flat side of the plug matches the marking on the
socket.
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3.3 Connecting the Manual Dosing Controller
Figure 5 Connecting the Manual Dosing Controller
The Manual Dosing Controller is connected to the remote connector on
the rear of the instrument.
3.4 Connecting a balance
Balances are equipped with a serial RS-232 interface as a rule. To connect
a balance, you require a 6.2148.030 RS-232/USB Box.
Figure 6 Connecting a balance
When a 6.2151.020 USB cable is used, then the 6.2148.030 RS-232/USB
Box can be connected to the 865 Dosimat plus by means of a USB hub or
a 6.2151.100 adapter (see Chapter 3.5, page 11).
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10
Connect the 9-pin plug of the respective balance connecting cable to the
RS 232/1 connector. Consult the user manual of the balance in order to
select the correct connecting cable.
865 Dosimat plus
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6.2151.100
3 Installation
The parameters for the RS-232 interface on the instrument must match
those on the balance (see "Editing the COM1 settings", page 35). Additionally consult the user manual of the balance.
3.5 Connecting a keyboard, printer and other USB devices
The 865 Dosimat plus has a USB (OTG) connector. Use the provided
6.2151.100 adapter USB MINI (OTG) - USB A for connecting USB devices
as e.g. printers, keyboards or USB sticks, see the following figure.
Figure 7 Connecting USB devices
Caution
Switch the instrument off before connecting or disconnecting a USB
device or a USB stick.
The 865 Dosimat plus can only recognize the device immediately after
switching on.
The following devices can be operated directly on the USB connector
with the 6.2151.100 adapter:
￭ USB sticks (for the backup or storing of methods)
￭ 6.2147.000 numerical USB keypad
￭ 6.2148.030 RS-232/USB Box (for connecting balances or for the
RS-232 remote control)
￭ USB hub (with or without an own power supply)
The 6.2147.000 numerical USB keypad serves for comfortable numerical input and for navigating in the dialog. In addition, it provides two USB
connectors. Connect additional USB devices to the keypad.
865 Dosimat plus
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11
3.5 Connecting a keyboard, printer and other USB devices
USB MINI (OTG)-USB
USB stick
6.2151.100
Note
Most of the USB devices need a so-called hub in order to work correctly.
A USB hub is a distributor to which several USB devices can be connected. USB hubs are available in specialty stores in a number of different
models.
The USB (OTG) connector of the 865 Dosimat plus has no such hub.
The 6.2147.000 numerical USB keypad has a USB hub and two USB
connectors.
The following devices can only be connected to a 6.2147.000
numerical keypad or to a USB hub:
￭ Printer (with USB connector, use the 6.2151.020 connecting cable)
￭ Barcode reader (with USB cable)
￭ Mouse (PC mouse with USB cable, for navigating in the dialog)
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The following devices can only be connected to a USB hub:
￭ PC keyboard (with USB cable, for the comfortable input of letters and
numbers)
￭ Keypad with numerical keypad (with USB cable)
If you wish to connect several different instruments without own
power supply, then you must possibly use a USB hub with own power
supply (self powered). The USB (OTG) connector of the 865 Dosimat plus
is not designed for supplying power to several devices with elevated electricity requirements.
Also observe the instructions in chapter 8.4, page 63.
Examples:
Figure 8 Connecting the USB stick
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12
865 Dosimat plus
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USB MINI (OTG)-USB
USB stick
Keypad
6.2147.000
6.2151.100
Printer
USB MINI (OTG)-USB
USB stick
USB-Hub
RS-232/USB Box
6.2148.030
6.2151.100
Printer
3 Installation
Figure 9 Connecting the 6.2147.000 USB keyboard with USB stick and
printer
3.6 Connecting instruments to the remote connector
Figure 10 Connecting the USB hub with USB stick, printer and the
6.2148.030 RS-232/USB Box (for connecting balances).
The 865 Dosimat plus can be integrated in an automation system with the
aid of a remote cable.
Figure 11 Connecting a remote cable
A variety of different connecting cables are available for connecting
Metrohm instruments (e.g. sample changers) (see Optional Accessories
chapter).
865 Dosimat plus
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13
3.7 Connecting the 805 Dosimat
3.7 Connecting the 805 Dosimat
For tandem operation (XDOS mode), an 805 Dosimat can be connected to
the MSB 1 socket on the rear of the 865 Dosimat plus.
Figure 12 Connecting the 805 Dosimat
Caution
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Make sure that the flat side of the plug matches the marking on the
socket.
If the MSB 1 connector is already occupied by a stirrer (e.g. 801 Stirrer),
then the 805 Dosimat can be connected to the MSB socket of the stirrer.
Figure 13 MSB connector on the 801 Stirrer
Caution
Make sure that the flat side of the plug matches the marking on the
socket.
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14
The 865 Dosimat plus must be switched off and then on again after connection.
865 Dosimat plus
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3.8 Attaching the exchange unit
3 Installation
Figure 14 Attaching the exchange unit
To attach the exchange unit, proceed as follows:
Slide the exchange unit from the front onto the 865 Dosimat plus
1
and push all the way to the rear.
It must snap in audibly.
865 Dosimat plus
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15
4.1 Switching the instrument on and off
4 Operation
4.1 Switching the instrument on and off
Switching on the instrument
Proceed as follows:
￭ Press the red [FILL] key.
1
The instrument is initialized and a system test performed. This
process takes some time.
￭ If a buret unit has been attached, then a request appears to carry
out the PREP function:
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All tubings and the cylinder are rinsed with the PREP (Preparing)
function. The preparing of the buret unit is described in chapter
"Preparing the buret unit (PREP)", page 25.
￭ Confirm the message with [OK].
The display of this message can be deactivated in the system settings (see "PREP warning", page 30).
The main dialog is displayed:
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865 Dosimat plus
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FILL
GO
Switching off the instrument
The instrument is switched off with the [FILL] key. The fact that the key
needs to be pressed down for an extended time prevents accidental
switch off.
Proceed as follows:
￭ Keep the red [FILL] key pressed down for at least 3 s.
1
A progress bar is displayed. If the key is released during this time,
then the instrument will not be switched off.
4.2 Fundamentals of operation
4.2.1 The keypad
4 Operation
Figure 15 Keypad 865 Dosimat plus
BACK Apply the input and exit the dialog.
⇧ ⇩ Move the selection bar either up or down by one
line at a time. Select the character to be entered
in the text editor.
⇦ ⇨ Select the character to be entered in the text and
number editor. Select the individual functions in
the function bar.
OK Confirm the selection.
FILL Stop an ongoing method run or a manual func-
tion. Switch the instrument on/off.
GO Start a method run or a manual function.
865 Dosimat plus
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4.2 Fundamentals of operation
4.2.2 Structure of the dialog windows
The current dialog title is displayed on the left-hand side of the title line.
The current status of the system is displayed in the upper right-hand corner:
ready The instrument is in normal status.
busy A method has been started.
hold A method has been paused.
Some dialogs have a so-called function bar on the bottom line. The functions contained therein can be selected with the arrow keys [⇦] or [⇨]
and executed with [OK].
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4.2.3 Navigating in the dialog
The selection bar is displayed in inverted style. Use the arrow keys [⇧] and
[⇩] to move the selection bar upward or downward one line at a time. If
a dialog text is marked with "＞", then additional settings are available in
a subordinate dialog. Use [OK] to access this dialog.
Example: System settings
Use the [BACK] key to return to the next higher level.
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865 Dosimat plus
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4.2.4 Entering text and numbers
In the editing dialog for text or numerical input you can select the individual characters with the arrow keys. Use [OK] to apply the character in the
input field. The following functions are available:
Editing function Description
4 Operation
Accept
Cancel
Clear
[BACK]
The modification is applied and the editing dialog
is exited.
The editing dialog is exited without applying the
modification.
The content of the input field is deleted completely.
The character left of the cursor is deleted (backspace).
Text editor only
The cursor within the input field is shifted to the
left by one character each time that [OK] is
pressed.
Text editor only
The cursor within the input field is shifted to the
right by one character each time that [OK] is
pressed.
The modification is applied and the editing dialog
is exited.
865 Dosimat plus
The [BACK] key has the same function as Accept.
A commercially available USB keyboard can be connected to make it easier to enter text and numbers. The key assignment on the PC keyboard is
described in chapter 8.4.2, page 64.
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4.3 Methods
4.2.5 Selecting from a selection list
In a selection list, select the individual entries with the arrow keys [⇧] and
[⇩]. Accept the selection with [OK] or [BACK].
4.3 Methods
4.3.1 Method templates
The 865 Dosimat plus contains method templates which are already configured and which can be adjusted to individual requirements.
The following method templates can be selected:
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DOS Manual interactive dosing with optional calcula-
tion of results.
For manual titrations.
XDOS Automatic dosing with freely selectable specifi-
cations.
The following specifications are possible:
￭ Volume and time
￭ Volume and dosing rate
￭ Dosing rate and time
CNT D Automatic preparation of solutions with speci-
fied content.
For standard solutions, sample solutions or dilutions.
LQT Liquid handling - sample transfer.
Pipetting with or without after-rinsing and/or
dilution.
You will find a detailed description of the methods in chapter .
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865 Dosimat plus
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