Metrohm 886 User Manual

886 Professional Thermostat/Reactor
Manual
8.886.8002EN
Metrohm AG CH-9100 Herisau Switzerland Phone +41 71 353 85 85 Fax +41 71 353 89 01 info@metrohm.com www.metrohm.com
886 Professional Thermostat/Reactor
2.886.0110 / 2.866.0210
Manual
8.886.8002EN 11.2011 zst
Teachware Metrohm AG CH-9100 Herisau teachware@metrohm.com
This documentation is protected by copyright. All rights reserved.
Although all the information given in this documentation has been checked with great care, errors cannot be entirely excluded. Should you notice any mistakes please send us your comments using the address given above.
Documentation in additional languages can be found on
http://products.metrohm.com under Literature/Technical documenta-
tion.
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Table of contents

1 Introduction 1
1.1 Instrument description ......................................................... 1
1.2 Intended use ......................................................................... 2
1.3 About the documentation ................................................... 2
1.4 Symbols and conventions .................................................... 3
1.5 Safety instructions ................................................................ 4
1.5.1 General notes on safety ........................................................... 4
1.5.2 Electrical safety ........................................................................ 4
1.5.3 Tubing and capillary connections ............................................. 5
1.5.4 Flammable solvents and chemicals ........................................... 5
1.5.5 Recycling and disposal ............................................................. 5
2 Overview of the instrument 7
Table of contents
2.1 Front ...................................................................................... 7
2.2 Rear ........................................................................................ 8
2.3 Accessories for 2.886.0110 Professional Reactor ............. 9
2.4 Accessories for 2.886.0210 Professional Thermostat ....... 9
3 Installation 10
3.1 Setting up the instrument .................................................. 10
3.1.1 Packaging .............................................................................. 10
3.1.2 Checks .................................................................................. 10
3.1.3 Location ................................................................................ 10
3.2 Proposed setup ................................................................... 10
3.2.1 2.886.0110 Professional Reactor ........................................... 10
3.2.2 2.886.0210 Professional Thermostat ...................................... 11
3.3 Mounting base tray and bottle holder (optional) ............ 12
3.3.1 Removing / mounting the base tray ....................................... 12
3.3.2 Removing / mounting the bottle holder ................................. 14
3.4 Capillary connections in the IC system ............................. 17
3.5 Installations on the rear of the instrument ...................... 19
3.5.1 Connecting the leak sensor .................................................... 19
3.6 Capillary and cable feed-throughs .................................... 20
3.7 Opening / closing oven door ............................................. 21
3.8 Installing accessories .......................................................... 22
3.8.1 2.886.0110 Professional Reactor ........................................... 22
3.8.2 2.886.0210 Professional Thermostat ...................................... 29
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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III
Table of contents
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3.9 Connecting the instrument ................................................ 35
3.9.1 Connecting the instrument to the PC ..................................... 35
3.9.2 Connecting the instrument to mains supply ........................... 35
4 Start-up 36
5 Operation 37
6 Handling and maintenance 38
6.1 General notes ...................................................................... 38
6.1.1 Care ...................................................................................... 38
6.1.2 Maintenance by Metrohm Service .......................................... 38
6.1.3 Operation .............................................................................. 38
6.1.4 Shutting down ...................................................................... 39
6.2 Door ..................................................................................... 39
7 Quality Management and validation with Metrohm 40
8 Troubleshooting 41
8.1 Problems and their solutions ............................................. 41
9 Technical specifications 42
9.1 Reference conditions .......................................................... 42
9.2 Instrument ........................................................................... 42
9.3 Leak sensor ......................................................................... 42
9.4 Ambient conditions ............................................................ 42
9.5 Housing ............................................................................... 43
9.6 Reactor / Column thermostat ............................................ 43
9.7 Mains connection ............................................................... 44
9.8 Interfaces ............................................................................. 44
9.9 Safety specification ............................................................ 45
9.10 Electromagnetic compatibility (EMC) ................................ 45
9.11 Weight ................................................................................. 45
10 Warranty (guarantee) 46
11 Accessories 47
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IV
11.1 Scope of delivery ................................................................ 47
11.1.1 2.886.0110 Professional Reactor ........................................... 47
11.1.2 2.886.0210 Professional Thermostat ...................................... 50
11.2 Optional accessories ........................................................... 52
11.2.1 2.886.0110 Professional Reactor ........................................... 52
11.2.2 2.886.0210 Professional Thermostat ...................................... 55
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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Index 58
Table of contents
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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V

Table of figures

Table of figures
Figure 1 Front ................................................................................................. 7
Figure 2 Rear .................................................................................................. 8
Figure 3 6.2845.100 Reactor plate .................................................................. 9
Figure 4 6.2845.600 Column plate ................................................................. 9
Figure 5 Proposed Setup – Professional Reactor ........................................... 11
Figure 6 Proposed setup – Professional Thermostat ....................................... 12
Figure 7 Connection of capillaries with pressure screws ................................ 17
Figure 8 Connecting the leak sensor ............................................................ 20
Figure 9 Capillary feed-throughs – oven ........................................................ 20
Figure 10 Capillary feed-throughs – instrument ............................................... 21
Figure 11 Front – open ................................................................................... 22
Figure 12 Feeding capillaries into the oven – reactor ....................................... 24
Figure 13 Reactor plate – capillaries connected ............................................... 24
Figure 14 Feeding capillaries into the oven – thermostat ................................. 30
Figure 15 Connecting the columns ................................................................. 31
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886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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1 Introduction

1.1 Instrument description

The 886 Professional Thermostat / Reactor is an instrument of the Metrohm Professional line of instruments, which was conceived to be used for two different functions.
The main function of the 886 Professional Thermostat / Reactor is detec­tion preparation in an IC system with photometric detection. In IC systems with photometric detection, a post-column derivatization (PCR) is required for most applications. An IC system with photometric detection consists of an 850 Professional IC instrument, the 886 Professional Thermostat / Reactor, and the 887 Professional UV/VIS Detector. Additionally, 872 extension modules can be used to transfer reagent solutions and/or for sample preparation.

1 Introduction

The second function of the 886 Professional Thermostat / Reactor is that of a column thermostat. A 872 Extension Module – IC Module together with an 886 Professional Thermostat / Reactor provide all the functions of an IC instrument. By adding a suitable detector, an isocratic analytical sys­tem can be built without a dedicated IC instrument.
The 886 Professional Thermostat / Reactor is available in two model ver­sions each with different set of accessories, to support each function:
2.886.0110 Professiopost columnnal Reactor
For the use as a pre-column or post-column reactor. 886 Professional Thermostat / Reactor with accessory set 6.2845.100 consisting of a reactor plate with one reactor. For sophisticated applications, the reac­tor plate can be equipped with up to four reactors.
2.886.0210 Professional Thermostat
For the use as a column thermostat: 886 Professional Thermostat / Reactor with accessories set 6.2845.600 consisting of a column plate with a fitted column block for two separation columns and a preheat­ing capillary.
These accessories sets can be inserted into the the oven of the 886 Profes­sional Thermostat / Reactor, which can be heated up to 150 °C as a maxi­mum.
The oven of the 886 Professional Thermostat / Reactor can be heated up to maximum 150 °C if it is empty. With the accessories for the Professio­nal Reactor (6.2845.100) inserted, the maximum temperature is 120 °C; with the accessories for the Professional Thermostat (6.2845.600) inser­ted, 80 °C.
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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1.2 Intended use

The 886 Professional Thermostat / Reactor is operated with MagIC Net software. It is connected via a USB cable to a PC on which MagIC Net is installed. The software automatically recognizes the instrument and checks its functional readiness. MagIC Net controls and monitors the instrument, and documents heating power and reagent flow rates in a database.
Additional information on operating the software can be found in the document "Tutorial for MagIC Net" or in the online help.
1.2 Intended use
The main function of the 886 Professional Thermostat / Reactor is post­column derivatization (PCR). In the process, chemicals are brought to a reaction in a heated atmosphere. It is also possible to perform pre-column reactions.
This instrument is suitable for processing chemicals and flammable sam­ples. The usage of the 886 Professional Thermostat / Reactor therefore requires that the user has basic knowledge and experience in the handling of toxic and caustic substances. Knowledge with respect to the applica­tion of the fire prevention measures prescribed for laboratories is also mandatory.
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1.3 About the documentation

This manual describes both model versions of the 886 Professional Ther­mostat / Reactor. Chapters which are valid for both model versions are not especially marked. Chapters, however, which are only valid for one of the model versions are marked in the title with the number and name of the corresponding model version (e.g. "Installing the 2.886.0110 Professional Reactor" or "Installing the 2.886.0210 Professional Thermostat").
Caution
Please read through this documentation carefully before putting the instrument into operation. The documentation contains information and warnings which the user must follow in order to ensure safe opera­tion of the instrument.
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886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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1.4 Symbols and conventions

The following symbols and styles are used in this documentation:
Cross-reference to figure legend
The first number refers to the figure number, the second to the instrument part in the figure.
Instruction step
Carry out these steps in the sequence shown.
Warning
This symbol draws attention to a possible life hazard or risk of injury.
Warning
This symbol draws attention to a possible hazard due to electrical current.
1 Introduction
Warning
This symbol draws attention to a possible hazard due to heat or hot instrument parts.
Warning
This symbol draws attention to a possible biological hazard.
Caution
This symbol draws attention to a possible damage of instruments or instrument parts.
Note
This symbol marks additional information and tips.
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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1.5 Safety instructions

1.5 Safety instructions

1.5.1 General notes on safety

Warning
This instrument may only be operated in accordance with the specifica­tions in this documentation.
This instrument has left the factory in a flawless state in terms of technical safety. To maintain this state and ensure non-hazardous operation of the instrument, the following instructions must be observed carefully.

1.5.2 Electrical safety

The electrical safety when working with the instrument is ensured as part of the international standard IEC 61010.
Warning
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Only personnel qualified by Metrohm are authorized to carry out service work on electronic components.
Warning
Never open the housing of the instrument. The instrument could be damaged by this. There is also a risk of serious injury if live components are touched.
There are no parts inside the housing which can be serviced or replaced by the user.
Mains voltage
Warning
An incorrect mains voltage can damage the instrument.
Only operate this instrument with a mains voltage specified for it (see rear panel of the instrument).
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886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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Protection against electrostatic charges
Warning
Electronic components are sensitive to electrostatic charges and can be destroyed by discharges.
Always pull the mains cable out of the mains connection socket before connecting or disconnecting electrical appliances on the rear panel of the instrument.

1.5.3 Tubing and capillary connections

Caution
Leaks in tubing and capillary connections are a safety risk. Tighten all connections well by hand. Avoid applying excessive force to tubing connections. Damaged tubing ends lead to leakage. Appropriate tools can be used to loosen connections.
1 Introduction
Check the connections regularly for leakage. If the instrument is used mainly in unattended operation, then weekly inspections are manda­tory.

1.5.4 Flammable solvents and chemicals

Warning
All relevant safety measures are to be observed when working with flammable solvents and chemicals.
Set up the instrument in a well-ventilated location (e.g. laboratory
flue).
Keep all sources of flame far from the workplace. Clean up spilled fluids and solids immediately. Follow the safety instructions of the chemical manufacturer.

1.5.5 Recycling and disposal

This product is covered by European Directive 2002/96/EC, WEEE – Waste from Electrical and Electronic Equipment.
The correct disposal of your old equipment will help to prevent negative effects on the environment and public health.
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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1.5 Safety instructions
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More details about the disposal of your old equipment can be obtained from your local authorities, from waste disposal companies or from your local dealer.
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886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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1 2
3
2
1
2 Overview of the instrument

2.1 Front

2 Overview of the instrument

Figure 1 Front
1
3
Capillary feed-throughs
For feeding through the capillaries into the oven.
Oven door
Knurled screws
2
For opening and closing the oven door.
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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2.2 Rear

1
2
3
4
5
6
7
8
2.2 Rear
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Figure 2 Rear
Leak sensor connection socket
1
For connecting the leak sensor.
PC connection socket
3
For connecting the instrument to the com­puter with the USB cable 6.2151.020.
MSB connection sockets
5
2 MSB connection sockets (labeled with MSB 1 and MSB 2) for connecting MSB devi­ces.
MSB = Metrohm Serial Bus
Mains switch
7
For switching the instrument on and off.
I = On
O = Off
Extension Module connection socket
2
To connect an extension module.
USB connection sockets
4
2 USB connection sockets (labeled with USB 1 and USB 2).
Service connection socket
6
Connector for service.
Mains connection socket
8
For plugging in the mains cable.
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886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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4
3
1
2
1
2
3
4
6
6
5
7
2 Overview of the instrument

2.3 Accessories for 2.886.0110 Professional Reactor

Figure 3 6.2845.100 Reactor plate
Heating plate
1
Reactor (6.2845.200)
3
Contact block
2
Connection between reactor plate and 886.
Y connector (6.2744.330)
4

2.4 Accessories for 2.886.0210 Professional Thermostat

Figure 4 6.2845.600 Column plate
Heating plate
1
Column holder
2
With column recognition chip.
Contact block
3
Connection between column plate and 886.
Knurled screw
5
For fixing the column.
Preheating capillary
7
Column block
4
With bore holes for maximum two columns of 150 mm length and a preheating capil­lary.
Knurled screw
6
For fixing the preheating capillary.
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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3.1 Setting up the instrument

3 Installation

3.1 Setting up the instrument

3.1.1 Packaging

The instrument is supplied in highly protective special packaging together with the separately packed accessories. Keep this packaging, as only this ensures safe transportation of the instrument.

3.1.2 Checks

Immediately after receipt, check whether the shipment has arrived com­plete and without damage by comparing it with the delivery note.

3.1.3 Location

The instrument has been developed for operation indoors and may not be used in explosive environments.
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Place the instrument in a location of the laboratory which is suitable for operation, free of vibrations, protected from corrosive atmosphere, and contamination by chemicals.
The instrument should be protected against excessive temperature fluctu­ations and direct sunlight.

3.2 Proposed setup

3.2.1 2.886.0110 Professional Reactor

An IC system with photometric detection and pre-column or post-column derivatization consists of the 886 Professional Thermostat / Reactor and:
any 850 Professional IC instrument, or
any 881 Compact IC pro instrument, or any 882 Compact IC plus instrument
the 887 Professional UV/VIS Detector optionally: an 872 Extension Module for transporting the reagent solu-
tion
optionally, if the reagent is pumped with a high pressure pump: a Met-
rosep BP 1 Guard/2.0 backpressure column (6.1015.100)
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An IC system with photometric detection and pre-column or post-column derivatization can be set up in in various combinations.
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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2.887.0010
2.886.0110
2.850.xxxx
2.872.xxxx
2.850.xxxx
2.872.xxxx
2.887.0010
2.886.0110
6.2061.100
6.2061.110
2.850.xxxx
2.881.xxxx
2.882.xxxx
2.887.0010
2.886.0110
2.872.xxxx
6.2061.110
6.2061.100
2.881.xxx
2.882.xxx
6.2061.120
2.872.xxxx
6.2061.100
2.887.0010
2.886.0110
6.2061.110
3 Installation
Figure 5 Proposed Setup – Professional Reactor
Note for proposed setup
If you want to set up the instruments in two stacks, we recommend you protect the instruments of the second stack and also order the following accessories:
6.2061.100 Bottle holder (ProfIC) 6.2061.110 Base tray with sensor for Professional IC systems
If you want to stack a 881 Compact IC pro or an 882 Compact IC plus instrument with a 886 Professional Thermostat / Reactor, the 887 Profes­sional UV/VIS Detector and/or a 872 Extension Module, you will require the 6.2061.120 System Connector to adapt the different support surfaces.

3.2.2 2.886.0210 Professional Thermostat

In order to build an isocratic IC analysis system without a dedicated IC instrument (850, 881, 882), you will require the 886 Professional Thermo­stat / Reactor and the following instruments:
a 2.872.0030 Extension Module – IC Module any detector (e.g. the 2.887.0010 Professional UV/VIS Detector) optionally an additional 872 Extension Module for sample preparation
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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3.3 Mounting base tray and bottle holder (optional)

6.2061.110
2.872.0030
2.886.0210
2.887.0010
6.2061.100
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For an isocratic IC analysis system with photometric detection (without dedicated IC instrument) we recommend the following set up:
Figure 6 Proposed setup – Professional Thermostat
3.3 Mounting base tray and bottle holder (optional)
The 6.2061.110 base tray and 6.2061.100 bottle holder protect IC instru­ments from dust, dirt and leaking fluids. If more than one instrument of the Professional IC family is used, these can be set up in one or more stacks. We recommend that a bottle holder and a base tray be mounted on/below each stack of instruments.
Bottle holder and base tray must be removed or mounted every time one of the following instruments is mounted on or under an 850 Professional IC instrument:
One or more 872 Extension Module. An 886 Professional Thermostat / Reactor. An 887 Professional UV/VIS Detector. or another instrument of the same support surface.

3.3.1 Removing / mounting the base tray

The base tray must be removed, in case you want to place another instru­ment under the IC instrument. Proceed as follows:
Removing the base tray
Before you can remove the base tray, the following preconditions must be met:
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The instrument is switched off. The bottle holder is cleared. All connections at the rear of the instrument are disconnected. There are no loose parts in the instrument.
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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1
2
3
3 Installation
To remove the base tray, you need the 6.2621.100 hexagon key 3 mm.
Tilt the instrument sideways and lay it down flat.
1
Loosen the cylinder screws with the 3 mm hexagon key and remove
2
them and their washers.
Remove base tray.
3
The base tray must always be mounted under the lowermost instrument of the stack. Proceed as follows:
Mounting the base tray
Before you can mount the base tray, the following preconditions must be met:
The instrument is switched off. The bottle holder is cleared. All connections at the rear of the instrument are disconnected. There are no loose parts in the instrument. The instrument is lying on it side, and the bottom surface is visible.
To mount the base tray, you need the 3 mm hexagon key (6.2621.100).
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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3.3 Mounting base tray and bottle holder (optional)
1
3
2
Attach the base tray so that the openings in the base tray match
1
exactly the screw threads in the bottom of the instrument.
Slide the four washers onto the four cylinder screws, insert the
2
screws and tighten them with the 3 mm hexagon key.
Set the instrument up on the base tray.
3
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Stack other instruments in the required order. Mount the 6.2061.100 bot­tle holder onto the topmost instrument (see "Mounting the bottle holder", page 15).

3.3.2 Removing / mounting the bottle holder

The bottle holder must be removed in case you want to mount another instrument on top of the IC instrument. Proceed as follows:
Removing the bottle holder
Before you can remove the bottle holder, the following preconditions must be met:
The instrument is switched off. The bottle holder is cleared. Drainage tubing is disconnected from the drainage tubing connection
of the bottle holder.
To remove the bottle holder, you need a 3 mm hexagon key (6.2621.100).
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886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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1
2 3
Remove the two covering stoppers.
1
Loosen the two cylinder screws with the 3 mm hexagon key and
2
remove them.
Remove the bottle holder.
3
3 Installation
Stack other instruments in the required order. Mount the 6.2061.100 bot­tle holder onto the topmost instrument (see "Mounting the bottle holder", page 15).
Proceed as follows:
Mounting the bottle holder
Before you can mount the bottle holder, the following preconditions must be met:
The instrument is switched off.
To mount the bottle holder, you need a 6.2621.100 hexagon key 3 mm.
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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3.3 Mounting base tray and bottle holder (optional)
1
2 3
Attach the bottle holder onto the topmost instrument so that the
1
openings in the bottle holder exactly match the screw threads on the top surface of the instrument.
Insert the two cylinder screws and tighten them with the 3 mm hexa-
2
gon key.
Insert covering stoppers .
3
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After having attached the bottle holder, all connections which were undone at the beginning of the process, must be reconnected. Proceed as follows:
Restoring the loosened connections
Connect the USB cable.
1
Connect the MSB cable.
2
Plug in the mains cable.
3
Reconnect drainage tubings (see manual of the IC instrument).
4
Possibly, a longer section of silicone tubing 6.186.020 must be cut to fit and mounted (see also the manual for the IC instrument).
If one of the instruments in the stack is equipped with a leak sensor
5
connection socket, connect the leak sensor (see manual of the IC instrument).
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886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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4
1
2 3

3.4 Capillary connections in the IC system

This chapter contains general information concerning the capillary con­nections in the IC instruments and systems.
Generally speaking, capillary connections between two components of an IC system are made up of one connection capillary and two pressure screws with which the capillary is connected to the respective compo­nents.
Pressure screws
3 Installation
Figure 7 Connection of capillaries with pressure screws
PEEK pressure screw (6.2744.014)
1
Use on the injection valve.
PEEK pressure screw, short
3
(6.2744.070)
For use on the high pressure pump, the purge valve, the inline filter, the pulsation absorber, the guard column and the separa­tion column.
In order to keep the dead volume as low as possible, capillary connec­tions should generally be as short as possible.
For an improved overview, capillary and tubing connections can be bundled with the 6.1815.010 spiral band.
Note
Note
Connection capillary
2
PEEK pressure screw, long
4
(6.2744.090)
Use on special components. Is not used on all instruments.
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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3.4 Capillary connections in the IC system
Connection capillaries
PEEK capillaries and PTFE capillaries are used in the IC system.
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PEEK capillaries (poly­etheretherketone)
PTFE capillaries (poly­tetrafluoroethylene)
PEEK capillaries are temperature-resistant up to 100°C, stable under pres­sure up to 400 bar, flexible, chemically inert and exhibit an extremely smooth surface. They can be readily cut down to the desired length with the 6.2621.080 capillary cutter.
Usage:
PEEK capillaries (6.1831.010) with an internal diameter of 0.25 mm for
the entire high pressure range.
PEEK capillaries (6.1831.030) with an internal diameter of 0.75 mm for
sample handling in the ultra trace range.
PTFE capillaries are transparent and enable visual tracing of the liquids to be pumped. They are chemically inert, flexible and temperature-resistant up to 80°C.
Usage:
PTFE capillaries (6.1803.0x0) are used for the low pressure range.
PTFE capillaries with internal diameter of 0.5 mm for sample handling. PTFE capillaries with internal diameter of 0.97 mm for sample handling
as well as for rinsing solutions (they do not have to be in the scope of delivery of the instrument).
Capillary connections
In order to achieve optimum analysis results, capillary connections in an IC system must be absolutely tight and free of dead volume. Dead volume occurs if two capillary ends connected to each other do not fit exactly, thus allowing liquid to escape. There are two possible reasons for this:
The capillaries do not have exactly cut edges. The two capillary ends do not completely meet.
One prerequisite for dead volume free capillary connection is, that both capillary ends are cut exactly plane. Therefore we recommend only to cut PEEK capillaries with the capillary cutter (6.2621.080).
Creating dead volume free capillary connections
To create dead volume free capillary connections, proceed as follows:
Slide the pressure screw over the capillary. Ensure that the capillary
1
protrudes 1–2 mm from the tip of the pressure screw.
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886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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3 Installation
Plug the capillary all the way into the connection or coupling until
2
the stop.
Only then start turning the pressure screw, while keeping the capil-
3
lary pressed in space.
Colored sleeves for PEEK capillaries
The enclosed set of varicolored sleeves for PEEK capillaries (6.2251.000) serves to easily differentiate the various flows of liquid in the system through color coding. Each capillary leading a given liquid (e. g. eluent) can be highlighted with sleeves of the same color.
To highlight a capillary, proceed as follows:
Slide a sleeve of a selected color over a capillary an move it to an
1
easily visible position.
If the capillary heats up, the sleeve shrinks and adapts to the form of the capillary.

3.5 Installations on the rear of the instrument

3.5.1 Connecting the leak sensor

The leak sensor detects escaping liquid which collects in the base tray of the instrument.
To activate the leak sensor, the leak sensor connector plug (8-2) must be connected, the instrument switched on and the leak sensor switched to active in the software.
Connecting the leak sensor
Pull the cable of the leak sensor (8-3) out of the rear of the base
1
tray.
Plug the leak sensor connector plug (8-2) into the leak sensor
connection socket (8-1) on the rear of the instrument.
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3.6 Capillary and cable feed-throughs

1
2
3
Figure 8 Connecting the leak sensor
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Leak sensor connection socket
1
Is labeled with "Leak Sensor".
Leak sensor connection cable
3
Is firmly mounted on the rear of the instru­ment.
Leak sensor connector plug
2
3.6 Capillary and cable feed-throughs
Several openings have been integrated for feeding through capillaries and cables. To feed through capillaries into the oven, two openings are provi­ded, one each left and right of the oven door. Up to five capillaries can be fed into the oven through each of the two capillary feed-throughs.
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20
Figure 9 Capillary feed-throughs – oven
To guide capillaries to or away from the instrument or to guide them between two instruments, use the capillary feed-throughs on top or at the
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3 Installation
bottom of the instrument. These are designed to guide capillaries between two instruments or between instrument an base plate or instru­ment an bottle holder.
Figure 10 Capillary feed-throughs – instrument

3.7 Opening / closing oven door

The heatable interior of the 886 Professional Thermostat / Reactor is closed with a well isolating oven door. In order to insert the required accessories into the oven, the oven door must be opened. Proceed as fol­lows:
Opening the oven door
Warning
Surfaces inside of the oven and the oven door can be hotter than 60 °C.
Risk of burns!
Let the oven cool down after use and open oven door carefully. Place oven door on a fire resistant surface.
Loosen the knurled screws on both sides of the oven door, and care-
1
fully remove oven door.
Place oven door on a fire resistant surface.
2
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3.8 Installing accessories

1
2
3
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Figure 11 Front – open
Oven door
1
Heating plate
3
2
Before the determination can be started, the oven door must be tightly closed. Proceed as follows:
Closing oven door
Place oven door onto opening. Make sure that no capillaries are
1
pinched.
Tighten both knurled screws at the front of the oven by hand.
2
3.8 Installing accessories

3.8.1 2.886.0110 Professional Reactor

Equipped with the 6.2845.100 reactor plate, the 886 Professional Ther­mostat / Reactor provides the functionality of a pre- or post-column reac­tor.
Oven interior
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22
The easiest way to connect capillaries is outside the oven.
All capillaries must be fed into or out of the oven through the capillary feed-throughs at the right and left side of the oven door (see Figure 9, page 20).
If you have placed the 886 Professional Thermostat / Reactor under or next to the IC instrument, proceed as follows:
1. Feeding capillaries into the oven
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3 Installation
2. Connect capillaries to the reactor
3. Insert reactor plate
Start with "Feeding capillaries into the oven", page 24.
If you have placed the 886 Professional Thermostat / Reactor on top of the IC instrument, proceed as follows:
1. Connect capillaries to the reactor
2. Insert reactor plate
3. Guide capillaries out of the oven
Start with "Connect the capillaries", page 24
To deliver the reagent, you need either an additional high pressure pump or an additional peristaltic pump. If you deliver the reagent with a high pressure pump, you must install the 6.1015.100 Metrosep BP 1 Guard/2.0 backpressure column between the reactor and the pulsation absorber.
Note
In order to keep the dead volume as low as possible, make sure that capillary connections are as short as possible.
Always shorten capillaries with the 6.2621.080 capillary cutter to obtain flawless level cut capillary ends.
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3.8 Installing accessories
1
2
3
1
5
2
3
4
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Feeding capillaries into the oven
Figure 12 Feeding capillaries into the oven – reactor
Reactor inlet capillary
1
Reactor outlet capillary
3
Reagent inlet capillary
2
1
Feed capillaries into the oven
Guide the reactor inlet capillary, the reagent inlet capillary (section
of 6.1831.100), and the reactor outlet capillary through the two capillary feed-throughs on the right and left side of the oven door (see Figure 9, page 20) into the oven.
Connect the capillaries
Figure 13 Reactor plate – capillaries connected
Reactor inlet capillary
1
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Connection capillary
2
Section of PEEK capillary (6.1831.100).
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3 Installation
Reactor outlet capillary
3
Section of PEEK capillary (6.1831.100) or the PTFE capillary (6.1803.150)
Backpressure column
5
*
Metrosep BP 1 Guard/2.0 (6.1015.100)
*
In bromate determination with the tri-iodide method, the tri-iodide is partially absorbed by the PEEK capillary, which leads to peak widening and a lower detection limit. Therefore, for this application, we recommend to use the PTFE capillary (6.1803.150).
To connect the capillaries, you need the following accessories:
the long PEEK capillary (6.1831.100) the capillary cutter (6.2621.080) If the reagent is delivered via high pressure pump: the backpressure
column 6.1015.100 Metrosep BP 1 Guard/2.0
1
Connect the reactor inlet capillary
Attach the column outlet capillary (13-1) to one of the two Y con-
Connect the Y connector output and reactor input with a short
2
Connect the reagent inlet capillary
For reagent delivery, attach a section of the 6.1831.100 PEEK
Attach the backpressure column (13-5) at he other end. Attach another section of the 6.1831.100 PEEK capillary to the
3
Connect the reactor outlet capillary
Reagent inlet capillary
4
Section of PEEK capillary (6.1831.100)
nector inlets.
section of the 6.1831.100 PEEK capillary (13-2).
capillary to the second Y connector inlet.
other end of the backpressure column (13-4).
Attach a section of the 6.1831.100 PEEK capillary (13-3) at the
reactor output.
Inserting the reactor plate (6.2845.100)
To insert the reactor plate, you need the 6.2621.140 hexagon key 2.5 mm.
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3.8 Installing accessories
1 2
3
4
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1
Lowering the latches
Loosen the outer screws of both latches with the 6.2621.140 2.5 mm hexagon key turning them counterclockwise.
The latches open and unblock the insertion rails of the heating plate.
2
Insert reactor plate
Insert the reactor plate into the oven by fitting the two bolts at
the sides of the reaction plate into the insertion rails of the heat­ing plate.
Slide the reactor plate into the oven as far as it will go. Take care
not to jam or pinch the capillaries.
3
Lift the latches
Tighten the outer screws of both latches with the 6.2621.140 hexa­gon key 2.5 mm turning them clockwise.
The latches lift and fix the column holder on the heating plate.
4
Connect the capillaries to the system
In case the free capillary ends are not yet guided through the capil­lary feed-throughs, guide them out of the oven.
Connect the loose end of the reactor inlet capillary (13-1) with
the outlet of the separation column.
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3 Installation
Connect the loose end of the reactor outlet capillary (13-3) with
the detector inlet.
Connect the loose end of the reagent inlet capillary (13-4) with
either
– an unused high pressure pump (recommended), and make
sure that the 6.1015.100 Metrosep BP 1 Guard/2.0 back­pressure column is installed between the reactor and the pulsation absorber, or
– an unused peristaltic pump.
The reaction capillary inside the reactor is 2 m long and has a volume of 393 µL. This is sufficient for most applications. Should an application require a longer reaction time, or if the 886 Professional Thermostat / Reactor is used in a two channel IC system, the reactor plate can be equipped wit additional reactors (6.2845.200). A maximum of four reac­tors can be mounted on the reactor plate.
To mount additional reactors, proceed as follows:
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3.8 Installing accessories
1
6.2845.200
6.2845.200
2
6.2845.200
6.2845.200
6.2845.200
6.2845.200
3
6.2845.200
6.2845.200
6.2845.200
6.2845.200
4
6.2845.200
6.2845.200
6.2845.200
6.2845.200
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Optional: attaching additional reactors
To attach additional reactors, you need the following accessories:
6.2845.200 Reactor complete 6.2621.140 hexagon key 2.5 mm
1
Attach two reactors
The originally mounted reactor is attached to the reactor plate with four screws turned in from the bottom of the plate.
Remove the four screws using the 2.5 mm hexagon key. Reattach the reactor at the far end of the reactor plate. Attach a second reactor from the 6.2845.200 accessory set at the
front end of the reactor plate using the the included screws and the 2.5 mm hexagon key.
2
Attach additional reactors
Place two additional reactors on top of the other two.
3
Fasten the reactors
Fasten each reactor on both sides to the reactor below using the
included clips.
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4
Mount the Y connector
6.2744.330 Y connectors are used to add the reagent. These are supplied with each 6.2845.200 reactor. You can attach several Y connectors to the reactor block.
Attach the Y connectors to the reactors using the included
screws.

3.8.2 2.886.0210 Professional Thermostat

Equipped with the 6.2845.600 column holder, the 886 Professional Ther­mostat / Reactor provides the functionality of a column thermostat.
The easiest way to connect capillaries is outside the oven.
All capillaries must be fed into or out of the oven through the capillary feed-throughs at the right and left side of the oven door.
If you have placed the 886 Professional Thermostat / Reactor under or next to the IC instrument, proceed as follows:
3 Installation
1. Feeding capillaries into the oven
2. Connect the capillaries with the columns
3. Insert column holder
Start with "Feeding capillaries into the oven", page 24.
If you have placed the 886 Professional Thermostat / Reactor on top of the IC instrument, proceed as follows:
1. Connect the capillaries with the columns
2. Insert column plate
3. Guide capillaries out of the oven
Start with "Connect the capillaries", page .24
Note
In order to keep the dead volume as low as possible, make sure that capillary connections are as short as possible.
Always shorten capillaries with the 6.2621.080 capillary cutter to obtain flawless level cut capillary ends.
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3.8 Installing accessories
1
2
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Feeding capillaries into the oven
Figure 14 Feeding capillaries into the oven – thermostat
Column inlet capillary
1
Column outlet capillary
2
1
Feed capillaries into the oven
Guide the column inlet capillary and the column outlet capillary
through the two capillary feed-throughs at the left and right side of the oven door.
The column holder can hold two columns with a maximum length of 150 mm. If one of the columns is an iColumn, the system ensures that the oven is not heated up higher than the standard operating temperature of the column. You can also use columns without chip, in this case you have to set the maximum oven temperature manually.
The second bore hole of the column block can also hold additional col­umns and/or guard columns with a total length of 150 mm. For applica­tions requiring a 250 mm column, you can combine a 150 mm iColumn with a second 100 mm column and an on column guard column. The fol­lowing figure illustrates how the preheating capillary and the columns are connected.
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1
2
3
4
5
3 Installation
Figure 15 Connecting the columns
Main column
1
iColumn clicked into the column holder. Maximum length: 150 mm.
Preheating capillary
3
Part of accessories set 6.2845.600.
Capillary
5
Connection between main column and detector.
Connecting and inserting columns
To install the columns, you need:
main column: an intelligent separation column (iColumn) of maximum
150 mm length (e.g. Metrosep A Supp 15 -150/4.0)
auxiliary column: a guard column compatible with the main column
(e.g. Metrosep A Supp 15 S-Guard/4.0) or a second column compatible with the main column (e.g. Metrosep A Supp 15 - 100/4.0) with an on column guard column (Metrosep A Supp 15 Guard/4.0)
sections of the included capillary 6.1831.100 the capillary cutter (6.2621.080)
Auxiliary column
2
Either a second column (of 100 mm length) with on column guard system or guard col­umn only.
Capillary
4
Connection between main column and aux­iliary column.
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3.8 Installing accessories
1
2
3
4
5 6
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1
Insert main column
Slide the main column into the rear bore hole of the column
block.
Click the head of the column into the column holder at the con-
tact block.
2
Connect auxiliary column
Connect the input of the main column with the output of the
guard column. Use the connection capillary included with the guard column.
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3 Installation
If you want to use a second column with on column guard col-
umn, use a section of the 6.1831.100 capillary to connect the two columns.
3
Insert additional column
Slide the auxiliary column into the upper bore hole of the column
block.
4
Connect preheating capillary
The preheating capillary (15-3) is inserted in the lower bore hole of the column block and secured from sliding out with two knurled screws situated at the front of the column block.
Before connecting the preheating capillary, loosen these knurled
screws and pull the preheating capillary out of the bore hole.
Connect the preheating capillary and the input of the auxiliary col-
umn.
5
Insert preheating capillary
Slide the preheating capillary back into its bore hole. Secure it from sliding out by fastening the two knurled screws.
6
Connect column outlet capillary
Attach a section of the 6.1831.100 capillary (15-5) to the outlet
of the column.
Inserting the column plate
To insert the column plate, you need the 6.2621.140 hexagon key 2.5 mm.
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3.8 Installing accessories
1
2
3
4
■■■■■■■■■■■■■■■■■■■■■■
1
Lower the latches
Loosen the outer screws of both latches with the 6.2621.140 hexa­gon key 2.5 mm turning them counterclockwise.
The latches open and unlock the insertion rails of the heating plate.
2
Insert the column plate
Insert the column plate into the oven by fitting the two bolts at
the sides of the column plate into the insertion rails of the heating plate.
Slide the column plate into the oven as far as it will go. Take care
not to jam or pinch the capillaries.
3
Lift the latches
Tighten the outer screws of both latches with the 6.2621.140 hexa­gon key 2.5 mm turning them clockwise.
The latches lift and fix the column holder on the heating plate.
4
Connect the capillaries to the system
In case the free capillary ends are not yet guided through the capil­lary feed-throughs, guide them out of the oven.
Connect the free end of the preheating capillary with the injection
valve.
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Connect the free end of the column outlet capillary with the
detector.

3.9 Connecting the instrument

3.9.1 Connecting the instrument to the PC

Note
The instrument must be switched off when connecting the PC.
1
Connecting the USB cable
Connect the PC connection socket of the instrument to a USB con­nector of the computer via the 6.2151.020 USB cable.

3.9.2 Connecting the instrument to mains supply

3 Installation
Warning
The power supply unit must not get wet. Protect it against the direct effect of liquids.
Mains cable
Which mains cable is supplied depends on the location:
6.2122.020 with plug SEV 12 (Switzerland, …) 6.2122.040 with plug CEE(7), VII (Germany, …) 6.2122.070 with plug NEMA 5-15 (USA, …)
The mains cable is three-core and provided with a plug with grounding. If another plug has to be mounted, the yellow/green conductor (IEC stand­ard) must be connected to the protective ground (protection class I).
1
Connecting the mains cable
Plug the mains cable into the mains connection socket . Connect the mains cable to the mains supply.
2
Switching the instrument on and off
Switch the instrument on and off with the mains switch .
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4 Start-up

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The 886 Professional Thermostat / Reactor is set up together wit other instruments, e.g. an 850 Professional IC and the 887 Professional UV/VIS Detector.
Putting the 886 Professional Thermostat / Reactor into operation
Start MagIC Net.
1
Connect the 886 Professional Thermostat / Reactor to PC and switch
2
on.
The 886 Professional Thermostat / Reactor is recognized automati­cally by MagIC Net.
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5 Operation

5 Operation

The instrument is operated via MagIC Net software only. Additional infor­mation on operating MagIC Net can be found in the document "Tutorial for MagIC Net" or in the online help.
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6.1 General notes

6 Handling and maintenance

6.1 General notes

6.1.1 Care

Warning
The instrument housing must not be opened by untrained personnel.
The instrument requires appropriate care. Excess contamination of the instrument may result in functional disruptions and a reduction in the serv­ice life of the sturdy mechanics and electronics.
Caution
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Although this is prevented to a great extent by design measures, the mains plug should be unplugged immediately if aggressive media has penetrated the inside of the instrument, so as to avoid serious damage to the instrument electronics. In such cases, the Metrohm Service must be informed.
Spillages of chemicals and solvents should be cleaned up immediately. In particular, the plug connections on the rear panel of the instrument (espe­cially the mains plug) should be protected from contamination.

6.1.2 Maintenance by Metrohm Service

Maintenance of the instrument is best carried out as part of an annual service, which is performed by specialist personnel from Metrohm. If working frequently with caustic and corrosive chemicals, a shorter mainte­nance interval is recommended. The Metrohm service department offers every form of technical advice for maintenance and service of all Metrohm instruments.

6.1.3 Operation

Caution
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38
In order to avoid disturbing temperature influences, the entire system including the eluent bottle must be protected against direct sunlight.
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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6.1.4 Shutting down

If the instrument is not used for a longer period, the whole IC system (except the columns) must be rinsed salt free with methanol/ultrapure water (1:4), in order to prevent eluent salts and reagents from forming crystals which may cause subsequent damage.
Rinsing salt free the IC system
To rinse the system, proceed as follows:
Remove the separation column from the eluent path. Connect the
1
connection capillaries directly with each other using a coupling (6.2744.040).
Rinse the IC system with methanol/ultrapure water (1:4) for 15
2
minutes.
Rinse with eluent for at least 15 minutes at starting up again and before connecting the guard column and separation column.
6 Handling and maintenance

6.2 Door

Caution
The door is made of PMMA (polymethylmetacrylate). It must never be cleaned with abrasive media or solvents.
Caution
Never hold the instrument at the door when lifting or moving.
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7 Quality Management and validation with
Metrohm
Quality Management
Metrohm offers you comprehensive support in implementing quality man­agement measures for instruments and software. Further information on this can be found in the brochure «Quality Management with Metrohm» available from your local Metrohm agent.
Validation
Please contact your local Metrohm agent for support in validating instru­ments and software. Here you can also obtain validation documentation to provide help for carrying out the Installation Qualification (IQ) and the Operational Qualification (OQ). IQ and OQ are also offered as a service by the Metrohm agents. In addition, various application bulletins are also available on the subject, which also contain Standard Operat- ing Procedures (SOP) for testing analytical measuring instruments for reproducibility and correctness.
Maintenance
Electronic and mechanical functional groups in Metrohm instruments can and should be checked as part of regular maintenance by specialist per­sonnel from Metrohm. Please ask your local Metrohm agent regarding the precise terms and conditions involved in concluding a corresponding maintenance agreement.
Note
You can find information on the subjects of quality management, vali­dation and maintenance as well as an overview of the documents cur­rently available at www.metrohm.com/com/ under Support.
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8 Troubleshooting

8.1 Problems and their solutions

Problem Cause Remedy

8 Troubleshooting

Marked drop in pressure
Drift of the baseline
Extreme spread of the peaks in the chromatogram. Splitting (dual peaks)
Leak in the system.
Thermal equilibrium not yet attained.
Leak in the system.
Capillary connections – dead volume in the system.
Check all capillary connections and seal leaks, if necessary (see Chapter 3.4, page 17).
Condition instrument with the column heater switched on.
Check all capillary connections and seal leaks, if necessary (see Chapter 3.4, page 17).
Check connections (see Chapter 3.4, page 17) (use PEEK capillaries with an internal diameter of 0.25 mm between the injection valve and detector).
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9.1 Reference conditions

9 Technical specifications

9.1 Reference conditions
The technical specifications listed in this chapter refer to the following ref­erence conditions:
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Ambient tempera­ture
Instrument status
+25 °C (±3 °C)
> 40 min in operation

9.2 Instrument

IC system
Intelligent compo­nents
Connections for external compo­nents
Metal free system for heating intelligent reactors and columns.
iColumns, iReactors, Dosinos
up to three extension modules for reagent delivery etc. up to two Dosinos Analog data output (optional)

9.3 Leak sensor

Type
Electronic, no calibration necessary

9.4 Ambient conditions

Operation
Storage
Transport
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42
Ambient tem­perature
Humidity
Ambient tem­perature
Ambient tem­perature
+5…+45 °C
20…80 % relative humidity
–20…+70 °C
–40…+70 °C
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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9.5 Housing

Dimensions
Width
Height
Depth
9 Technical specifications
365 mm
131 mm
380 mm
Material of base tray, housing and covering plate
Operating ele­ments
Indicators
On/Off switch
Polyurethane hard foam (PUR) with flame retardation
LED for power display
On the rear of the instrument

9.6 Reactor / Column thermostat

Number of reac­tors
Number of col­umns
Adjustable tem­perature range
Stability
Reproducibility
up to 4
up to 2
0 °C…+150 °C, adjustable in steps of 0.1 °C
less than 0.05 °C deviation
better than ± 0.2 °C
Temperature accuracy
Heating up time
Maximum pres­sure
Reactor
Heating type
safety shutdown
Function
Maximum tem­perature
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
< 1 °C (typical)
< 10 Min. from 20 °C to 40 °C
2 MPa
Resistor type thermostat for intelligent reactors and intelligent separa­tion columns
Automatic switch off when maximum temperature is exceeded
nominal 169 °C, response time: immediately
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43

9.7 Mains connection

9.7 Mains connection
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Required voltage
Required fre-
100…240 V ± 10 % (auto-sensing)
50…60 Hz ± 3 (auto-sensing)
quency
Power consump­tion
Power supply unit
40 W input power (typical anion analysis) 15 W input power at standby (idle)
Up to 300 W maximum, electronically monitored internal fuse 3.15 A

9.8 Interfaces

USB
Input
Output
MSB
Number
column recogni­tion
1 USB Upstream, type B (connection to PC).
2 USB Downstream, type A
2 MSB MiniDin 8-pol female for iDosino, Stirrers, Remote, etc.
for an intelligent reactor or an intelligent column
Leak sensor
Further connec­tions
Extension mod­ule
Analog Output (optional)
Service
1 jack plug
1 DSUB 15-pin (female)
1 DSUB 15-pin (female)
1 DSUB 15-pin high density (female)
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44
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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9.9 Safety specification

9 Technical specifications
Design / Test
EN/IEC 61010-1 UL 61010-1 CSA-C22.2 No. 61010-1 Protection class I

9.10 Electromagnetic compatibility (EMC)

Emission
Immunity
EN/IEC 61326-1 EN/IEC 61000-6-3 EN 55011 / CISPR 11 EN/IEC 61000-3-2 EN/IEC 61000-3-3
EN/IEC 61326-1 EN/IEC 61000-6-2 EN/IEC 61000-4-2 EN/IEC 61000-4-3 EN/IEC 61000-4-4 EN/IEC 61000-4-5 EN/IEC 61000-4-6 EN/IEC 61000-4-8 EN/IEC 61000-4-11 EN/IEC 61000-4-14 NAMUR

9.11 Weight

1.886.0010
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
7.7 kg (without accessories)
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45

10 Warranty (guarantee)

Metrohm guarantees that the deliveries and services it provides are free from material, design or manufacturing errors. The warranty period is 36 months from the day of delivery; for day and night operation it is 18 months. The warranty remains valid on condition that the service is provi­ded by an authorized Metrohm service organization.
Glass breakage is excluded from the warranty for electrodes and other glassware. The warranty for the accuracy corresponds to the technical specifications given in this manual. For components from third parties that make up a considerable part of our instrument, the manufacturer's war­ranty provisions apply. Warranty claims cannot be pursued if the Customer has not complied with the obligations to make payment on time.
During the warranty period Metrohm undertakes, at its own choice, to either repair at its own premises, free of charge, any instruments that can be shown to be faulty or to replace them. Transport costs are to the Cus­tomer's account.
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Faults arising from circumstances that are not the responsibility of Metrohm, such as improper storage or improper use, etc. are expressly excluded from the warranty.
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46
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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11 Accessories

Note
Subject to change without notice.

11.1 Scope of delivery

11.1.1 2.886.0110 Professional Reactor

2.886.0110 886 Professional Reactor
Qty. Order no. Description
1 1.886.0010 886 Professional Thermostat / Reactor
11 Accessories
1 6.2122.0x0 Mains cable with C13 line socket
IEC-60320-C13
Cable plug according to customer requirements.
Switzerland: Type SEV 12
6.2122.020
Germany, …: Type CEE(7), VII
6.2122.040
USA, …: Type NEMA/ASA
6.2122.070
1 6.1015.100 Metrosep BP 1 Guard/2.0
Backpressure column for the Professional Reactor
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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47
11.1 Scope of delivery
Qty. Order no. Description
1 6.1803.150 PTFE capillary i.d. 0.25 mm / 1 m
2 6.1831.100 PEEK capillary 0.25 mm i.d. / 1 m
Material: PEEK Outer diameter (inches): 1/16 Inner diameter (mm): 0.25 Length (m): 1
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1 6.2151.020 Cable USB A - USB B / 1.8 m
USB connecting cable
Length (m): 1.8
1 6.2621.100 Hexagon key 3 mm
Hexagon key 3 mm. For IC sample changer
Length (mm): 73
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48
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
■■■■■■■■■■■■■■■■■■■■■■
Qty. Order no. Description
1 6.2621.140 Hexagon key 2.5 mm
1 6.2744.010 Pressure screw 5x
With UNF 10/32 connector. For connecting PEEK capillaries
Material: PEEK Length (mm): 26
11 Accessories
1 6.2744.014 Pressure screw 2x
With UNF 10/32 connector. For connecting PEEK capillaries
Material: PEEK Length (mm): 26
1 6.2845.100 Reactor plate complete to Professional
Reactor
Intelligent reactor plate with reactor for PCR applications.
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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49
11.1 Scope of delivery

11.1.2 2.886.0210 Professional Thermostat

2.886.0210 886 Professional Thermostat
Qty. Order no. Description
1 1.886.0010 886 Professional Thermostat / Reactor
1 6.2122.0x0 Mains cable with C13 line socket
IEC-60320-C13
Cable plug according to customer requirements.
Switzerland: Type SEV 12
6.2122.020
Germany, …: Type CEE(7), VII
6.2122.040
USA, …: Type NEMA/ASA
6.2122.070
1 6.1831.100 PEEK capillary 0.25 mm i.d. / 1 m
Material: PEEK Outer diameter (inches): 1/16 Inner diameter (mm): 0.25 Length (m): 1
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50
1 6.2151.020 Cable USB A - USB B / 1.8 m
USB connecting cable
Length (m): 1.8
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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Qty. Order no. Description
1 6.2621.100 Hexagon key 3 mm
Hexagon key 3 mm. For IC sample changer
Length (mm): 73
1 6.2621.140 Hexagon key 2.5 mm
11 Accessories
1 6.2744.040 2 x UNF 10/32 coupling
For connecting 1/16 in. capillaries. For IC instruments
Material: PEEK Length (mm): 24
1 6.2744.070 Pressure screw short
Short version. With UNF 10/32 connector. 5 pieces. For connecting PEEK capillaries
Material: PEEK Length (mm): 21
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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51

11.2 Optional accessories

Qty. Order no. Description
1 6.2845.600 Column holder complete to Professional
Thermostat
Intelligent column holder for the Professional Thermostat
11.2 Optional accessories

11.2.1 2.886.0110 Professional Reactor

2.886.0110 886 Professional Reactor
Order no. Description
6.1602.200 Bottle attachment 2 x M6, 1 x M8 to 6.1608.120
Bottle attachment for PP eluent bottle.
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6.1608.120 PP eluent bottle, 2 L
Eluent bottle for applications where glass should be avoided.
6.1836.020 Preheating capillary with core, 1.44 m
Preheating capillary to Professional Reactor / Thermostat
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52
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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Order no. Description
6.2061.100 Bottle holder (ProfIC)
Bottle holder for Professional IC instruments
6.2061.110 Base tray with sensor for Professional IC systems
6.2061.120 System Connector
Connects an IC module with the footprint of a Professional IC with a Compact IC
11 Accessories
6.2744.330 Y-Connector 3 x UNF 10/32
6.2845.110 Reactor plate HT complete to Professional Reactor
Reactor plate with reactor for PCR applications at high temperatures (> 120 °C).
6.2845.200 Reactor complete to 6.2845.100
Spare reactor for the reactor plate
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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53
11.2 Optional accessories
Order no. Description
6.2845.600 Column holder complete to Professional Thermostat
Intelligent column holder for the Professional Thermostat
6.5333.000 IQ/OQ Kit for IC
The IQ/OQ Kit for IC contains all parts and standard solutions required for IQ/OQ in ion chromatography.
6.6059.021 MagIC Net™ 2.x Multi: 1 additional license
1 additional license
6.6059.022 MagIC Net™ 2.x Multi: 5 additional licenses
5 additional licenses
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6.6059.023 MagIC Net™ 2.x Multi: 10 additional licenses
10 additional licenses
6.6059.232 MagIC Net™ 2.3 Professional CD 1 license
Professional PC program for controlling intelligent Professional IC systems, Com­pact IC instruments and their peripherals such as various Autosamplers, 800 Dosino, 771 Compact Interface, etc. The software permits control, data acquisi­tion, evaluation and monitoring as well as report generation of ion chromato­graphic analyses. Graphical user interface for routine operations, extensive data­base programs, method development, configuration and manual system con­trol; very flexible user administration, efficient database operations, extensive data export functions, individually configurable report generator, control and monitoring of all system components and the chromatography results. MagIC Net™ Professional complies fully with FDA Regulation 21 CFR Part 11 as well as GLP. Dialog languages: German, English, French, Spanish, Chinese, Korean, Japanese, et. al. 1 license.
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54
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
■■■■■■■■■■■■■■■■■■■■■■

11.2.2 2.886.0210 Professional Thermostat

2.886.0210 886 Professional Thermostat
Order no. Description
6.1015.100 Metrosep BP 1 Guard/2.0
Backpressure column for the Professional Reactor
6.1602.200 Bottle attachment 2 x M6, 1 x M8 to 6.1608.120
Bottle attachment for PP eluent bottle.
11 Accessories
6.1608.120 PP eluent bottle, 2 L
Eluent bottle for applications where glass should be avoided.
6.2061.100 Bottle holder (ProfIC)
Bottle holder for Professional IC instruments
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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55
11.2 Optional accessories
Order no. Description
6.2061.110 Base tray with sensor for Professional IC systems
6.2061.120 System Connector
Connects an IC module with the footprint of a Professional IC with a Compact IC
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6.2744.330 Y-Connector 3 x UNF 10/32
6.2845.100 Reactor plate complete to Professional Reactor
Intelligent reactor plate with reactor for PCR applications.
6.2845.110 Reactor plate HT complete to Professional Reactor
Reactor plate with reactor for PCR applications at high temperatures (> 120 °C).
6.2845.200 Reactor complete to 6.2845.100
Spare reactor for the reactor plate
6.5333.000 IQ/OQ Kit for IC
The IQ/OQ Kit contains all parts and standard solutions required for IQ/OQ in ion chromatography.
■■■■■■■■
56
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
■■■■■■■■■■■■■■■■■■■■■■
Order no. Description
6.6059.021 MagIC Net™ 2.x Multi: 1 additional license
1 additional license
6.6059.022 MagIC Net™ 2.x Multi: 5 additional licenses
5 additional licenses
6.6059.023 MagIC Net™ 2.x Multi: 10 additional licenses
10 additional licenses
6.6059.232 MagIC Net™ 2.3 Professional CD : 1 license
Professional PC program for controlling intelligent Professional IC systems, Com­pact IC systems and their peripherals such as various Autosamplers, 800 Dosino, 771 Compact Interface, etc. The software permits control, data acquisition, eval­uation and monitoring as well as report generation of ion chromatographic analyses. Graphics user interface for routine operations, extensive database pro­grams, method development, configuration and manual system control; very flexible user administration, efficient database operations, extensive data export functions, individually configurable report generator, control and monitoring of all system components and the chromatography results. MagIC Net™ Professio­nal complies fully with FDA Regulation 21 CFR Part 11 as well as GLP. Dialog languages: German, English, French, Spanish, Chinese, Korean, Japanese, et. al. 1 license.
11 Accessories
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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57

Index

Index
■■■■■■■■■■■■■■■■■■■■■■
A
Ambient conditions .................. 42
B
Base tray
Mounting ........................... 13
Removing ........................... 12
Bottle holder
Mounting ........................... 15
Removing ........................... 14
C
Cable feed-throughs ................. 20
Capillaries
Installation ......................... 17
Capillary feed-throughs ............ 20
Connections
Installation ......................... 17
Connector
Mains ................................. 44
D
Design
Safety specification ............. 45
Dimensions .............................. 43
Door ........................................ 39
E
Electromagnetic compatibility ... 45
Electrostatic charge .................... 5
EMC ......................................... 45
Emission ................................... 45
F
Feed-throughs
Capillaries ........................... 20
Frequency ................................ 44
G
GLP .......................................... 40
Guarantee ................................ 46
H
Housing ................................... 43
Humidity .................................. 42
I
Immunity .................................. 45
Installation
Connections ....................... 17
Leak sensor ........................ 19
Instrument
Connecting ........................ 35
Interface
MSB ................................... 44
USB .................................... 44
Interfaces ................................. 44
Further connections ............ 44
L
Leak sensor
Installation ......................... 19
Technical specifications ....... 42
M
Mains cable .............................. 35
Mains connection ............... 35, 44
Mains voltage ............................. 4
Material ................................... 43
MSB ......................................... 44
P
PC connector ............................ 35
Power consumption ................. 44
Power supply unit ..................... 44
Pressure screws
Connection ........................ 17
Protection class ........................ 45
Q
Quality Management ................ 40
R
Reference conditions ................ 42
Regeneration ............................ 38
S
Safety instructions ...................... 4
Safety specification ................... 45
Screws
Connection ........................ 17
Service ................................. 4, 38
Service Agreement ................... 40
Shutting down ......................... 39
Standards ................................. 45
Storage .................................... 42
Switching on ............................ 35
T
Technical specifications
Interfaces ........................... 44
Leak sensor ........................ 42
Reference conditions .......... 42
Temperature ............................. 42
Test
Safety specification ............. 45
Transport ................................. 42
Tubings
Installation ......................... 17
U
USB .......................................... 44
V
Validation ................................. 40
Voltage .................................... 44
W
Warranty .................................. 46
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58
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210)
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