Xylem OxiTop Control OC 100 Operating Manual

OPERATING MANUAL
ON/OFF
GLP
RUN/ENTER
OC 1x0
®
ba31114e07 08/2014

OxiTop® Control OC 100

®
OxiTop

BOD/OXYGEN CONSUMPTION: BOD, RESPIRATION, BIOGAS DETERMINATION

C or OxiTop® C/B
Copyright © 2016 Xylem Analytics Germany GmbH
Printed in Germany.
OxiTop® Control OC 100 Contents
OxiTop® Control OC 100 - Contents
1 Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
1.1 The system OxiTop® Control. . . . . . . . . . . . . . . . . . . . . . . . . . . 7
1.2 The measurement principle. . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
1.3 Data management. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
1.4 Literature . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
2 Safety. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.1 Safety information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.1.1 Safety information in the operating manual . . . . . . . . . . . 9
2.1.2 Safety signs on the meter. . . . . . . . . . . . . . . . . . . . . . . . . 9
2.2 Safe operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.2.1 Authorized use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.2.2 Requirements for safe operation . . . . . . . . . . . . . . . . . . . 9
2.2.3 Unauthorized use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
3 Commissioning. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
3.1 Scope of delivery. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
3.2 Power supply. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
3.2.1 Batteries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
3.2.2 Battery status signals . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
3.2.3 Energy saving feature (automatic switch-off) . . . . . . . . . 12
3.3 Initial commissioning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
3.3.1 Inserting the supply battery holder - controller . . . . . . . . 12
4 Operation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
4.1 General operating principles . . . . . . . . . . . . . . . . . . . . . . . . . . 15
4.1.1 Keys - controller . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
4.1.2 Socket field - controller. . . . . . . . . . . . . . . . . . . . . . . . . . 16
4.2 Switching on . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
4.2.1 Switching on the controller . . . . . . . . . . . . . . . . . . . . . . . 16
4.2.2 Switching on the measuring heads. . . . . . . . . . . . . . . . . 16
4.3 Navigation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
4.3.1 Operating modes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
4.3.2 Menus, functions and dialogs. . . . . . . . . . . . . . . . . . . . . 18
4.3.3 The course of the measurement. . . . . . . . . . . . . . . . . . . 19
5 Operating mode: BOD Standard / BOD Routine . . . . . . . . . 21
5.1 Sample preparation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
5.2 Starting the measurement . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
5.3 Calling up all data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
5.4 SAMPLE STATUS TYPE list (sample management) . . . . . . . 26
5.4.1 Showing a sample . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
5.4.2 Erasing data of finished samples . . . . . . . . . . . . . . . . . . 28
5.4.3 Showing the measuring head list . . . . . . . . . . . . . . . . . . 29
ba31114e07 08/2014 3
Contents OxiTop® Control OC 100
5.4.4 Calling up data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
5.4.5 Calling up data - Stop. . . . . . . . . . . . . . . . . . . . . . . . . . . 31
5.5 Evaluation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
5.5.1 Sample statistics (BOD Standard operating mode) . . . . 34
5.5.2 Excluding a curve (BOD Standard operating mode) . . . 35
5.5.3 Cursor interrogation . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
5.5.4 Curves display for cold samples. . . . . . . . . . . . . . . . . . . 37
5.5.5 Measured values outside the measuring range . . . . . . . 37
6 Printing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
7 GLP/TOOLS. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41
7.1 GLP/TOOLS main menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41
7.2 Show free measuring heads . . . . . . . . . . . . . . . . . . . . . . . . . . 42
7.3 Show settings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
7.4 Settings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43
7.4.1 Operating mode . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43
7.4.2 Operational life . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
7.4.3 Date/time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
7.4.4 GLP (Operating mode BOD Standard ) . . . . . . . . . . . . . 45
7.4.5 GLP - calibration interval (- Calinterval) . . . . . . . . . . . . . 46
7.4.6 Data storage. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
7.4.7 AutoTemp. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
7.4.8 Switch-off interval. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49
7.4.9 Language . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50
7.5 Check. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51
7.5.1 Showing the measuring heads. . . . . . . . . . . . . . . . . . . . 51
7.5.2 Measuring head information. . . . . . . . . . . . . . . . . . . . . . 51
7.5.3 Controller information. . . . . . . . . . . . . . . . . . . . . . . . . . . 53
7.5.4 cal-test . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
7.5.5 Pneumatic test . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55
7.6 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56
7.6.1 Erasing finished samples . . . . . . . . . . . . . . . . . . . . . . . . 57
7.6.2 Reset/release . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
7.6.3 Reading out data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60
8 Transmitting data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
8.1 Achat OC software. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
9 Maintenance, cleaning, disposal. . . . . . . . . . . . . . . . . . . . . . 63
9.1 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 63
9.1.1 General maintenance activities . . . . . . . . . . . . . . . . . . . 63
9.1.2 Replacing the supply batteries (controller). . . . . . . . . . . 63
9.1.3 Replacing the data backup battery (controller). . . . . . . . 65
9.1.4 Changing the supply battery (measuring head) . . . . . . . 67
9.2 Cleaning. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
9.2.1 Cleaning of the sample bottles. . . . . . . . . . . . . . . . . . . . 68
9.2.2 Cleaning of the controller and measuring heads . . . . . . 68
9.3 Disposal. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
4 ba31114e07 08/2014
OxiTop® Control OC 100 Contents
10 What to do if.... . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69
10.1 Display messages . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69
10.2 Display messages on the charging status of the batteries . . . 74
10.2.1 Batteries in the controller . . . . . . . . . . . . . . . . . . . . . . . . 74
10.2.2 Battery in the measuring head . . . . . . . . . . . . . . . . . . . . 74
10.3 General information. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75
11 Technical data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 79
11.1 Controller OxiTop® OC 100. . . . . . . . . . . . . . . . . . . . . . . . . . . 79
11.2 Measuring head OxiTop
®
-C or OxiTop®-C/B . . . . . . . . . . . . . 80
ba31114e07 08/2014 5
Contents OxiTop® Control OC 100
6 ba31114e07 08/2014
OxiTop® Control OC 100 Overview


2
0
m
l
lt
m
2
Op
T
T
V
VV
TR
OM
BOD
 
 
M(O2) Molecular weight (32000 mg/mol) R Gas constant (83.144 lmbar/molK) T
0
Reference temperature (273.15 K)
T
m
Measuring temperature
V
t
Bottle volume (nominal volume in ml)
V
l
Sample volume in ml a Bunsen absorption coefficient (0.03103) p(O
2
) Difference of the D. O. partial pressure (mbar)

1 Overview

1.1 The system OxiTop
®
Control
The classical application field for the OxiTop® measuring heads and controller is the BODx determination (BODx = Biochemical Oxygen Demand for the time x). The evaluation of biological degradability (e.g. test according to OECD 301F) is also part of this field.
With different sample vessels, the OxiTop
®
measuring heads and the OxiTop®
Controller 110 can also be used for other applications such as: Evaluation of respiration and toxicity in earth, sludge, waste and sediment
(e.g. extraction of contaminated earth according to recovery concepts)
Evaluation of the respiration rate of cell culturesMicrobiological growth and stress examinationsMeasurement of anaerobic degradation processes (e.g. biogas determina-
tion with the measuring head OxiTop
®
-C/B)
Accessories: see WTW catalog and price list

1.2 The measurement principle

The respirometric measurement is a pressure measurement. If oxygen is consumed in a closed vessel at a constant temperature, a negative pressure develops. If a gas is released, an overpressure develops. The OxiTop measuring head measures and stores this pressure for the whole duration of a measurement once started.
®
The OxiTop
OC 100 controller collects the pressure values from the
measuring heads and processes them. The formula shown below is the basis for all calculations for the BOD using the
®
values from the OxiTop
measuring head.
®
ba31114e07 08/2014 7
Overview OxiTop® Control OC 100
The interpretation of the pressure differences in the temporal course depends on the measured material and its preparation and on the sample manipulation (e. g. intermediate aerations) during the measuring period.

1.3 Data management

The measuring head records the measured values and stores the measuring data. Using the controller, the collected and stored data are read out from the measuring head and stored in the “sample management“. Starting at the OxiTop
®
sample management, it is possible to make the graphical and statis-
tical evaluation of the sample data. The data can be transferred from the controller to a computer via the RS232
interface. The read-out software Achat OC facilitates to process the stored data further.
Additionally, the data can be transferred to an IR printer via the IR interface.

1.4 Literature

Further information and application reports on the subject of measuring with the system OxiTop
CD-ROM Applications for OxiTop
®
Control can be obtained at no cost from WTW:
®
Control
CD-ROM Principles of measuring technique
8 ba31114e07 08/2014
OxiTop® Control OC 100 Safety

2 Safety

2.1 Safety information

2.1.1 Safety information in the operating manual

This operating manual provides important information on the safe oper­ation of the instrument. Read this operating manual thoroughly and make yourself familiar with the instrument before putting it into opera­tion or working with it. The operating manual must b e kept in the vicinity of the instrument so you can always find the information you need.
Important safety instructions are highlighted in this operating manual. They are indicated by the warning symbol (triangle) in the left column. The signal word (e.g. "CAUTION") indicates the danger level:
WARNING
indicates a possibly dangerous situation that can lead to seri­ous (irreversible) injury or death if the safety instruction is not followed.
CAUTION
indicates a possibly dangerous situation that can lead to slight (reversible) injury if the safety instruction is not followed.
NOTE
indicates a possibly dangerous situation where goods might be damaged if the actions mentioned are not taken.

2.1.2 Safety signs on the meter

Note all labels, information signs and safety symbols on the instrument. A warning symbol (triangle) without text refers to safety information in this operating manual.

2.2 Safe operation

2.2.1 Authorized use

Only the operation and running of the instrument according to the instructions and technical specifications given in this operating manual is authorized (see section 11 T
ECHNICAL DATA, page 79).
Any other use is considered unauthorized.

2.2.2 Requirements for safe operation

Note the following points for safe operation:
The instrument may only be operated according to the authorized
ba31114e07 08/2014 9
Safety OxiTop® Control OC 100
use specified above.
The instrument may only be supplied with power by the energy sources mentioned in this operating manual.
The instrument may only be operated under the environmental conditions mentioned in this operating manual.
The instrument may only be opened if this is explicitly described in this operating manual (example: Changing the batteries).

2.2.3 Unauthorized use

The instrument must not be put into operation if:
it is visibly damaged (e.g. after being transported)
it was stored under adverse conditions for a lengthy period of time (storing conditions, see section 11 T
ECHNICAL DATA, page 79).
10 ba31114e07 08/2014
OxiTop® Control OC 100 Commissioning

3 Commissioning

3.1 Scope of delivery

Controller OxiTop® OC 100  Battery holder with batteries (3 x Mignon, AA, AM3, LR6)Operating manualAdditional scope of delivery: depending on set composition

3.2 Power supply

The controller OxiTop® OC 100 and measuring head OxiTop®-C or OxiTop®­C/B are both battery-powered.
Additionally, the controller has a data backup battery. This battery ensures that your measuring data and instrument settings are stored in the controller OxiTop
®
OC 100.

3.2.1 Batteries

Controller Power supply 3 alkaline batteries (alkali manganese),
Size: Mignon, AA, AM3, LR6 Runtime: > 100 h (approx. 1000 start-ups in normal use)
Data backup 1 x lithium battery CR2430 (accessory).
Runtime: typically 4 years
Measuring head
Power supply Batteries: 2 x lithium battery CR2430 (accessory).
Runtime: typically 2 years

3.2.2 Battery status signals

®
The OxiTop
-OC 100 controller and the OxiTop® measuring heads are pow­ered by batteries. A low battery status of the controller or measuring head is automatically indicated by a display message and a signal tone after the instru­ment is switched on (see section 10.2 D
STATUS OF THE BATTERIES, page 74).
ISPLAY MESSAGES ON THE CHARGING
1st level (warning level) Battery LoBat ! 2nd level (error level) Battery empty !
The current battery status can also be queried in the menu:
 Controller: Menu GLP/TOOLS - Check - Controller Info  Measuring head: Menu GLP/TOOLS -Check - info
ba31114e07 08/2014 11
Commissioning OxiTop® Control OC 100
LISTED 8F93 LaboratoryEquipment E163694
This device complies with Part 15 of the FCC Rules. Operation is subject to the following conditions: (1)This devise may not cause harmful interference, and (2) this devise must accept any interference received, including interference that may cause undesired operation.
Ser.-Nr.:05150013
OxiTop OC 1x0
WTW 82362 Weilheim
Made in Germany
1x CR 2430 Lithium
3xAlkaline, AA size, 1,5V
1
1
1
1

3.2.3 Energy saving feature (automatic switch-off)

The instrument switches off automatically following the last key actuation after expiry of the specified switch-off interval.
To specify the switch-off interval: see section 7.4.8 S
WITCH-OFF INTERVAL, page
49.

3.3 Initial commissioning

Perform the following activities: Insert the supply battery holder in the controller (see section 3 .3.1 I
THE SUPPLY BATTERY HOLDER - CONTROLLER, page 12)
Switch on the instrumentSet the date and time (see section 7.4 S
ETTINGS, page 43)

3.3.1 Inserting the supply battery holder - controller

Loosen the 4 screws underneath the housing using a Phillips screwdriver.
NSERTING
1Screws
Place the controller on the lower case.Remove the upper case and put it down to the right next to the lower case
with the display downwards.
Connect the supply battery holder with the power supply contacts of the
upper case.
Insert the supply battery holder in the lower case with the open side down.
12 ba31114e07 08/2014
OxiTop® Control OC 100 Commissioning
1
2
1 Supply batteries in the battery holder (lower case) 2 Data backup battery (upper case)
Set the upper case on top of the lower case, turn the controller and tighten
the housing screws using the screwdriver.
Switch on the controller. The battery insertion was successful if no error
message appears concerning the supply batteries.
ba31114e07 08/2014 13
Commissioning OxiTop® Control OC 100
14 ba31114e07 08/2014
OxiTop® Control OC 100 Operation
ON/OFF
GLP
RUN/ENTER
1
2
5
34
7
8
6
The function keys are used to start a function or to change to another function. Confirmed data and settings are preserved.
1 <On/Off> Switching on/off
2 <PRINT> Printing of measurement data and set-
tings via IR interface
3 <RUN/
ENTER>
Confirmation of entries
4<><> Select and change settings
Function keys: 5 <ORG> Sample management: List of samples,
reading/calling up/deleting the data of indi­vidual measuring heads or samples, shows measuring heads or samples
6 <COMM> Communication with measuring heads:
Start measuring, change or show settings, call up data
7 <GRAPH> Evaluation: Graphic and numerical dis-
play of measuring data
8 <GLP> GLP/Tools: Change or display settings,
display free measuring heads, display or change settings, perform checks or main­tenance
ON/OFF
RUN/ENTER
GLP

4Operation

4.1 General operating principles

4.1.1 Keys - controller

ba31114e07 08/2014 15
Operation OxiTop® Control OC 100
1

4.1.2 Socket field - controller

1 RS232 interface
The RS232 interface is used for communication with the PC. Usage of the RS232 interface is exclusively intended with the WTW software "Achat OC“ (see section 8.1 A
CHAT OC SOFTWARE, page 62).

4.2 Switching on

4.2.1 Switching on the controller

The current date and time appear for approx. 2 seconds (important for the allocation of sample numbers). If the date or time is wrong, correct them under GLP/TOOLS.
The instrument is in the sample management mode (operating mode BOD Routine , in the default condition).

4.2.2 Switching on the measuring heads

The measuring heads are immediately ready for operation. The controller switches the measuring heads on and off during communication.
To avoid malfunctions:
If you use two or more controllers simultaneously make sure that the distance between the controllers is at least 3 meters!
16 ba31114e07 08/2014
OxiTop® Control OC 100 Operation

4.3 Navigation

4.3.1 Operating modes

BOD Routine:
(preselected)
Measurement of single samples for a BOD
(x = 0.5h ... 99d) at 20 °C
x
The measuring range and filling volume can be selected out of seven per-
manent ranges and the corresponding filling volumes.
The function is permanently switched on
BOD Standard:  Measurement of up to 12 parallel sample processes per overall sample for
a BOD
(x = 0.5h ... 99d) at 20 °C
x
The measuring range and filling volume can be selected out of seven per-
manent ranges and the corresponding filling volumes.
Automatic sample statistics with averagingThe AutoTemp function and the GLP mode can be switched on
ba31114e07 08/2014 17
Operation OxiTop® Control OC 100

4.3.2 Menus, functions and dialogs Example: Pressing the <COMM> button causes the controller to change to the

SELECT ACTION menu (communication with the measuring heads).
Signal tone
Action: Press button. The instrument displays:
This symbol in the operating manual means: A signal tone sounds.
Description of what the action caused and possible further request:
SELECT ACTION menu (communication with the mea­suring heads): Preselected: - Start sample.
Select a menu item with <><>. The selected function or line is displayed in inverse video. Confirm the menu item with <RUN/ENTER>. The submenu is opened or the function is carried out.
Measuring head Each measuring head that receives a command from the controller indicates
this by a short flashing signal.
®
The OxiTop
measuring head is indicated by the symbol
18 ba31114e07 08/2014
OxiTop® Control OC 100 Operation
GLP
Time
End of measurement
Start of measurement
AutoTemp
Measurement
Data transfer
Starting the measuring heads
Sample management
Evaluation
Print
Print

4.3.3 The course of the measurement

Preparation before
starting the mea-
surement
Measuring
Select operating modeSelect settings
Operating mode and settings cannot be changed for a measure­ment once it is started!
ba31114e07 08/2014 19
Operation OxiTop® Control OC 100
20 ba31114e07 08/2014

OxiTop® Control OC 100 Operating mode: BOD Standard / BOD Routine

RUN/ENTER
5 Operating mode: BOD Standard / BOD Rou-
tine
The BOD Standard mode (parallel sample process for up to 12 measuring heads per overall sample) is preset in the delivery condition of the controller.
To change to the BOD Routine operating mode (single samples): see section
7.4.1 O The handling of controller and measuring heads is basically the same in both
operating modes. Where there are differences for the BOD Routine operating mode they are described.

5.1 Sample preparation

See application reports.
Screw the OxiTop close them tightly.
PERATING MODE, page 43.
®
measuring heads onto the measuring vessels and
NOTE
Never use joint grease or other lubricants for your OxiTop
®
measuring heads. Some of these products contain solvents that can cause severe damage to the plastic housing of the measuring head. The sealing of the measuring vessels is perfectly adequate without grease. However, you should always wipe off heavy contamination and
®
particles on the sealing surfaces of the rubber sleeves and OxiTop measuring heads. WTW accepts no liability for damage due to the use of joint grease.

5.2 Starting the measurement

SELECT ACTION menu (com­munication with the measuring heads): Preselected: - Start sample.
(In BOD Routine mode appears: START).
Select the measuring range with <><>. The filling volume required is given in the right hand column.
The controller stores the setting (memory function: the last selected measurement range is set).
ba31114e07 08/2014 21
Operating mode: BOD Standard / BOD Routine OxiTop® Control OC 100
RUN/ENTER
RUN/ENTER
Confirm the selected measure­ment range for the sample. The automatically assigned sample number (YY/MM/DD and sequential number) is given in the header line.
Additional information: Type of measurement, run duration, measurement range,
final date, ID number.
Temp display => the AutoTemp function (see section 7.1
GLP/TOOLS
MAIN MENU, page 41) is switched on.
GLP display => the GLP function (see section 7 GLP/
TOOLS, page 41) is switched on.
Change the ID number for the additional identification of the sample (e.g. sampling location) as follows:
Select the - I.D. number menu item with <><>Confirm with <RUN/ENTER>.  Set the required Id number (setting range 001 ... 255) with
<><>.
Confirm with <RUN/ENTER>. Use <PRINT>
(in BOD Routine mode only), see section 6 P
to print out the entire sample information
RINTING, page
39). Confirm the start of measure-
ment. Contact selection:
The controller repeatedly sends the start information in the scanner mode until feedback is successfully received from the OxiTop
®
measuring head. After the successful start message
from the measuring head:
Displays ! started ! From this
point in time, the sample exists within the SAMPLE STATUS TYPE list (sample manage- ment).
Subsequently, the request to start the next measuring head is made automatically.
In BOD Routine operating mode there is no 1... identifier in the display, and the controller automatically returns to the entry menu after starting the measuring head.
22 ba31114e07 08/2014
OxiTop® Control OC 100 Operating mode: BOD Standard / BOD Routine
Start the next measuring head (2). Contact selection:
The number of the measuring head is automatically incre­mented.
The controller continues to work with the contact selection, i.e. you can now start a sequence of measuring heads (parallel sample process) without having to press any further keys by holding the controller to the next measuring head to be started.
When all the measuring heads provided for this sample have been started: Confirm Stop start with <RUN/ENTER>. The controller returns to the entry menu.
If no measuring head is started (e.g. because the controller was not held to - or not close enough to - a measuring head):
The start was stopped. Use <RUN/ENTER> - Continue
start to confirm “Continue start” and hold the controller to a measuring head (see above).
Return to entry level menu with
-Stop  start
If an attempt is made to start a measuring head that was already started:
Displays already used! Use <RUN/ENTER> to confirm -
New  and hold the controller to a free measuring head (see above).
Return to entry level menu with
-Stop  start
In the delivery state, the controller automatically makes space when Start is selected if the measured value memory is full. To do this, it deletes the oldest finished sample (if a finished sample is available). You can change this setting to “manual erase” (see section 7.4.6 D
ATA STORAGE, page 47).
ba31114e07 08/2014 23
Operating mode: BOD Standard / BOD Routine OxiTop® Control OC 100
40 cm to 1 m
RUN/ENTER

5.3 Calling up all data

This function is used to call up the data of all measuring heads, no matter in which operating mode they were started.
To call up the data of individual measuring heads: see section 5.4 SAMPLE STATUS TYPE
LIST (SAMPLE MANAGEMENT), page 26.
SELECT ACTION menu (com­munication with the measuring heads): Preselected: - Start sample.
Select the - Call up all data menu item with <><>
Point the controller at the measuring heads:
Queries the data of all active measuring heads in the scanner mode.
The controller stores the data obtained and updates the
SAMPLE STATUS TYPE list (sample management).
Duration of a pass: approx. 3 seconds for 12 measuring heads in a stirring system.
If the measuring heads do not all respond in the 1st pass of the data query, the controller searches for the missing measuring heads in the scanner mode for approximately a further 7 seconds. Without having to press another key, you can continue the data queries at other locations (e.g. other stirring plat­forms or other thermal cabinets). Approximately 7 seconds after the last call up was performed, the scanner mode breaks off automatically and the following display appears:
24 ba31114e07 08/2014
OxiTop® Control OC 100 Operating mode: BOD Standard / BOD Routine
40 cm to 1 m
RUN/ENTER
Preselected:
- Continue transfer: A new pass is made only for measuring heads that have not yet responded.
Return to the entry menu with -
Stop
For information on searching for missing measuring heads, see section 10 W
HAT TO DO IF..., page
69
Point the controller at the measuring heads:
The call up of further measuring heads is performed in the scan­ner mode.
Message that all the data of all the measuring heads has been called up. The instrument then returns to the entry menu.
Immediately after the complete measurement data records of a fin­ished measurement have been called up, the corresponding mea­suring head is given the free status. The measuring head can be used for a new measurement. The relevant sample in the SAMPLE STATUS TYPE list (sample management) is marked as finished (see section 5.4 SAMPLE STATUS TYPE
MANAGEMENT), page 26), as soon as the measurement time has
LIST (SAMPLE
expired and the data of all measuring heads of this sample have been called up.
ba31114e07 08/2014 25
Operating mode: BOD Standard / BOD Routine OxiTop® Control OC 100
3
2
1

5.4 SAMPLE STATUS TYPE list (sample management)

Entry into the sample management. A list of samples appears in the display (if samples are avail­able):
1 Sample number:
Date (JJ/MM/TT) and consecutive number
2 Temporal process of the sample:
– Status bar partly filled:
The sample is not yet ready.
– Status bar filled:
The ready and complete data set of the sample can be called up from the measuring head.
– Status bar filled plus checkmark:
The sample is ready. The complete data set is given in the con­troller for evaluation.
3 BOD type and run duration.
– B20h: BOD with 20 hours run duration – BOD5: BOD with 5 days run duration
The samples started in the BOD Routine operating mode also appear in the SAMPLE STATUS TYPE lists (sample management) of all other modes. Data of samples that have been started in other operating modes do not appear in the sample management of the BOD Routine operating mode.
Reporting order:
At the upper end of the list: finished samples (if available) Under this: current samples
Sorting of the samples: according to date and sequential number 01 ... 99, from the oldest to the newest sample.
26 ba31114e07 08/2014
Loading...
+ 58 hidden pages