WarrantyWe guarantee the instrument described for 3 years from the date of
The use of advanced technology and the high quality standard of our
instruments are the result of continuous development. This may result
in differences between this operating manual and your instrument.
Also, we cannot guarantee that there are absolutely no errors in this
manual. Therefore, we are sure you will understand that we cannot
accept any legal claims resulting from the data, figures or descriptions.
purchase.
The instrument warranty covers manufacturing faults that are discovered within the warranty period. The warranty does not cover components that are replaced during maintenance work, e.g. batteries.
The warranty claim extends to restoring the instrument to readiness for
use but not, however, to any further claim for damages. Improper
handling or unauthorized opening of the instrument invalidates any
warranty claim.
This compact precision handheld meter enables you to carry out pH / ORP
measurements and conductivity measurements rapidly and reliably.
The handheld meter provides the maximum degree of operating comfort, reliability and measuring certainty for all applications.
The proven MultiCal
®
calibration procedures or the proven procedure for adjusting or setting the cell constant and the special AutoRead function support
you in your work with the handheld meter.
ba75370e0311/2009
1Keypad
2Sample display
3Jack field
5
Overviewhandylab pH/LF 12
M
CAL
STO
RUN/ENTER
AR
RCL
M
STO
CAL
RCL
AR
RUN/ENTER
1.2Keypad
Key functions
Select the measured variable <M>:
– pH value / ORP voltage
– Conductivity / salinity
Save a measured value
<STO>
Switch measuring instrument on/off
<ON/OFF>
Calibrate the currently set measured variable
<CAL>
Display/transmit measured values
<RCL>
Activate/deactivate the AutoRead function
<AR>
Select the measuring mode, increase values,
scroll <▲ >
6
Select the measuring mode, decrease values,
scroll <▼ >
Confirm entries, start AutoRead
<RUN/ENTER>
ba75370e0311/2009
handylab pH/LF 12Overview
Sal
S
mg/l
M
cm
%
mbar
O
°
F
TDS
Time
Baud
Day.Month No.
Ident
Year
8
8.
8
8
8
8
°
C
LoBat
1
UpH
RCL
Auto
Store
ARng
AR
S/
m
AutoCal DIN
AutoCal TEC
cm
Lin
Tref25
Tref20
nLF
Cal
mV/pH
Sal
1/
cm
/
K
%
TP
Status display
Meas. value display
Function and
temperature display
Probe symbol
5
13
4
2
1.3Display
1.4Jack field
ba75370e0311/2009
1Conductivity measuring cell
2pH electrode
3pH temperature probe
4Plug-in power supply (optional)
5Serial interface RS 232
7
Overviewhandylab pH/LF 12
1.5 Operating structure
The following overview diagram shows which keys you have to press to select between the different measuring modes:
Note
When connecting a conductivity measuring cell with temperature probe, the
measuring instrument recognizes the probe and automatically switches to
the last selected conductivity measuring mode. As soon as the probe is disconnected, the instrument switches to the pH or ORP measuring mode.
8
ba75370e0311/2009
handylab pH/LF 12Overview
1.6Technical data
Dimensions
and weight
Mechanical
structure
Electrical
safety
Test certificates
Ambient
conditions
Length [mm]172
Width [mm]80
Height [mm]37
Weight [kg]approx. 0.3
Type of protectionIP 66
Protective classIII
cETLus, CE
Storage- 25 °C ... + 65 °C
Operation-10 °C ... + 55 °C
Relative atmospheric
annual average < 90 %
humidity
pH/ORP measur-
ing ranges
Precision of
pH/ORP
(± 1 digit)
pH correction
function
Measuring rangeResolution
pH- 2.00 ... + 19.990.01
U [mV]- 1999 ... + 19991
T [°C]- 5.0 ... + 105.00.1
pH (after calibration)± 0.01
U [mV]± 1
T [°C]± 0.1
Temperature input
Manually [°C]- 20 ... + 130
ba75370e0311/2009
9
Overviewhandylab pH/LF 12
Measuring ranges
of conductivity
ӕ [µS/cm]0 ... 19991
Measuring rangeResolution
Precision of
conductivity (± 1
digit)
ӕ [mS/cm]0.00 ... 19.99
0.0 ... 199.9
0 ... 500
SAL0.0 ... 70.0 accord-
0.01
0.1
1
0.1
ing to the IOT table
T [°C]− 5.0 ... + 105.00.1
ӕNonlinear compensation:
Precision Sample temperature
± 0.5 %0 °C ... 35 °C
according to EN 27 888;
± 0.5 % 35 °C ... 50 °C
extended nLF function
Linear compensation
Accuracy Sample temperature
± 0.5 % 10 °C ... 75 °C
(The accuracy percentage always refers to
the measured value.)
SALRange 0.0 ... 42.0
Accuracy Sample temperature
± 0.1 5 °C ... 25 °C
± 0.2 25 °C ... 30 °C
Cell constant,
calibrating
Reference
temperature of
conductivity
T [°C] ± 0.1
C [cm-1]0.450 ... 0.500
TrefCan be set to 20 °C or 25 °C
10
ba75370e0311/2009
handylab pH/LF 12Overview
Serial
interface
Power
supply
Automatic switchover if a PC or printer is connected.
TypeRS232, data output
Baud rateSelectable 1200, 2400, 4800, 9600 baud
Data bits8
Stop bit2
ParityNone
HandshakeRTS/CTS + Xon/Xoff
Cable length Max. 15 m
Batteries4 x 1.5 V alkali-manganese batteries, Type
AA
Operational lifeapprox. 3000 operating hours
MainsFRIWO FW7555M/09, 15.1432.500-00
Friwo Part. No. 1883259
Input: 100 ... 240 V ~ / 50 ... 60 Hz / 400 mA
Output: 9 V = / 1.5 A
Connection max. overvoltage category II
Primary plugs contained in the scope of
delivery: Euro, US, UK and Australian.
ba75370e0311/2009
11
Overviewhandylab pH/LF 12
FCC Class A Equipment Statement
Note: This equipment has been tested and found to comply with
the limits for a Class A digital device, pursuant to Part 15 of the
FCC Rules. These limits are designed to provide reasonable
protection against harmful interference when the equipment is
operated in a commercial environment. This equipment
generates, uses, and can radiate radio frequency energy and, if
not installed and used in accordance with the instruction manual,
may cause harmful interference to radio communications.
Operation of this equipment in a residential area is likely to cause
harmful interference in which case the user will be required to
correct the interference at his own expense.
Applicable
guidelines and
norms
EMCEC guideline 2004/108/EC
EN 61326-1
EN 61000-3-2
EN 61000-3-3
FCC Class A
Instrument safetyEC guideline 2006/95/EC
EN 61010-1
ANSI/UL 61010-1
CAN/CSA-C22.2 No. 61010-1
Climatic classVDI/VDE 3540
Type of protectionEN 60529
12
ba75370e0311/2009
handylab pH/LF 12Safety
2Safety
This operating manual contains basic instructions that you must follow during
the commissioning, operation and maintenance of the measuring instrument.
Consequently, all responsible personnel must read this operating manual before working with the measuring system. The operating manual must always
be available within the vicinity of the measuring system.
Target groupThe measuring instrument was developed for work in the field and in the lab-
oratory.
We assume that, as a result of their professional training and experience, the
operators will know the necessary safety precautions to take when handling
chemicals.
Safety instructionsThe individual chapters of this operating manual use the following safety la-
bels to indicate various types of danger:
Warning
indicates instructions that must be followed precisely in order to avoid the
possibility of slight injuries or damage to the instrument or the environment.
Further notes
Note
indicates notes that draw your attention to special features.
Note
indicates cross-references to other documents, e.g. operating manuals.
2.1Authorized use
The authorized use of the measuring instrument consists exclusively of the
pH and ORP measurement or the measurement of the conductivity and salinity in the field and laboratory.
The technical specifications as given in section 1.6 T
observed. Only the operation and running of the measuring instrument according to the instructions given in this operating manual is authorized.
Any other use is considered to be unauthorized.
ECHNICALDATA must be
ba75370e0311/2009
13
Safetyhandylab pH/LF 12
2.2General safety instructions
This instrument is built and inspected according to the relevant guidelines
and norms for electronic measuring instruments (see section 1.6 T
DATA).
It left the factory in a safe and secure technical condition.
ECHNICAL
Function and oper-
ating safety
The smooth functioning and operational safety of the measuring instrument
can only be guaranteed if the generally applicable safety measures and the
specific safety instructions in this operating manual are followed during operation.
The smooth functioning and operational safety of the measuring instrument
can only be guaranteed under the environmental conditions that are specified
in chapter 6 W
HATTODOIF....
If the instrument was transported from a cold environment to a warm environment, the formation of condensate can lead to the faulty functioning of the instrument. In this event, wait until the temperature of the instrument reaches
room temperature before putting the instrument back into operation.
Safe operationIf safe operation is no longer possible, the instrument must be taken out of
service and secured against inadvertent operation!
Safe operation is no longer possible if the measuring instrument:
z has been damaged in transport
z has been stored under adverse conditions for a lengthy period of time
z is visibly damaged
Obligations of the
purchaser
z no longer operates as described in this manual.
If you are in any doubt, please contact the supplier of the instrument.
The purchaser of the measuring instrument must ensure that the following
laws and guidelines are observed when using dangerous substances:
z EEC directives for protective labor legislation
z National protective labor legislation
z Safety regulations
z Safety datasheets of the chemical manufacturers.
14
ba75370e0311/2009
handylab pH/LF 12Commissioning
3Commissioning
3.1Scope of delivery
z handylab pH/LF 12LF 12 handheld meter
z Operating manual and short operating manual
z 4 batteries, 1.5 V Mignon type AA (in the instrument)
3.2Initial commissioning
Perform the following activities:
z Set the date and time
z Connect the plug-in power supply (optional)
Setting the date
and time
1Press the <M> key and hold it down.
2Press the <ON/OFF> key.
The display test appears briefly on the display.
3Press the <RUN/ENTER> key repeatedly until the date ap-
pears on the display.
4Set the date of the current day with <▲> <▼>.
5Confirm with <RUN/ENTER>.
The date (month) flashes in the display.
6Set the current month with <▲> <▼>.
7Confirm with <RUN/ENTER>.
The year appears on the display.
8Set the current year with <▲> <▼>.
9Confirm with <RUN/ENTER>.
The hours flash on the display.
10Set the current time with <▲> <▼>.
11Confirm with <RUN/ENTER>.
The minutes flash on the display.
ba75370e0311/2009
12Set the current time with <▲> <▼>.
13Confirm with <RUN/ENTER>.
The instrument switches to a measuring mode.
15
Commissioninghandylab pH/LF 12
2
1
3
Connecting the
original
plug-in power sup-
ply unit
You can either operate the measuring instrument with batteries or with the
plug-in power supply. The plug-in power supply supplies the measuring instrument with low voltage (12 VDC). This saves the batteries.
Warning
The line voltage at the operating site must lie within the input voltage range
of the original plug-in power supply (see section 1.6 T
ECHNICALDATA).
Warning
Use original plug-in power supplies only (see
section 1.6 T
ECHNICALDATA).
1Plug the jack (1) into the socket (2) of the measuring instru-
ment.
2Connect the original SI Analytics plug-in power supply (3) to an
easily accessible mains socket.
16
ba75370e0311/2009
handylab pH/LF 12Operation
4Operation
4.1Switching on the measuring instrument
1Press the <ON/OFF> key.
The display test appears briefly on the display.
After this, the measuring instrument automatically switches to
the measuring mode.
Measuring mode
when switching on
Connected sensorMeasuring mode
No sensor or pH/ORP electrodepH or ORP measurement (de-
The measuring instrument has an energy saving feature to avoid unnecessary battery depletion. The energy saving feature switches the measuring instrument off if no key has been pressed for an hour.
The energy saving feature is not active
z if the power is supplied by the plug-in power supply,
z if the AutoStore function is active,
z if the communication cable and a PC with a running communication pro-
gram are connected,
z if the printer cable is connected (for external printers).
ba75370e0311/2009
17
Operationhandylab pH/LF 12
4.2pH value / ORP voltage
4.2.1General information
Preparatory
activities
Perform the following preparatory activities when you want to measure:
1Connect the pH electrode to the measuring instrument.
If necessary, press the <M> key repeatedly until the status dis-
play pH (pH measurement) or U (measurement of the ORP
voltage) appears.
2Adjust the temperature of the buffer solutions or test solutions,
or measure the current temperature, if you measure without a
temperature probe.
3Calibrate or check the measuring instrument with the elec-
trode.
4Using <▲ > <▼>, toggle between the pH or mV measuring
modes.
Note
Incorrect calibration of pH electrodes leads to incorrect measured values.
Calibrate regularly before measuring. You can only connect electrodes of the
NTC30 type or without temperature probe.
Warning
When connecting an earthed PC/printer, measurements cannot be performed in earthed media as incorrect values would result. The RS232 interface is not galvanically isolated.
18
ba75370e0311/2009
handylab pH/LF 12Operation
Temperature
measurement in
pH measurements
You can perform pH measurements with or without a temperature probe as
well as with the temperature probe of a conductivity measuring cell. The measuring instrument recognizes which sensors are connected and automatically
switches to the correct mode for the temperature measurement.
The following cases are distinguishable.
Temperature probeDisplayMode
pHCond
yes-TPAutomatic with
pH temperature probe
yesyesTP
--Manual
-yesTP
flashes
The temperature value of the
2nd sensor (Cond) in the
same test sample is used for
the pH measurement*
* If you do not wish that, you can:
– either disconnect the 2nd sensor and use the manual temperature input
or
– use an electrode with a temperature probe.
If a temperature probe is connected, it is indicated on the display by TP.
Note
When calibrating without a temperature probe (no TP display indicator displayed), enter the current temperature of the respective buffer solution manually using the <▲> <▼> keys while keeping the
<RUN/ENTER> key depressed.
ba75370e0311/2009
19
Operationhandylab pH/LF 12
Tref20
Lin
Cal
8
1
S
SalOU
%
mg/l
mV/pH
1/
cm
Sal
AutoCal DIN
Tref25nLF
AutoCalTEC
RCL
Auto
Store
LoBat
ARng
AR
Time
Baud
Day.MonthNo.
Ident
Year
mbar
TDS
cm
M
°
F
/
K
%
S/
m
cm
8
4
2
9
9
6
°
C
TP
pH
4.2.2Measuring the pH value
1Perform the preparatory activities according to section 4.2.1.
2Immerse the pH electrode in the test sample.
3Press the <▲> <▼> keys until pH appears in the status display.
The pH value appears on the display.
AutoRead AR
(drift control)
4When measuring without a connected temperature probe:
Options:
z Determine the current temperature using a thermometer
and, while keeping the <RUN/ENTER> key depressed, enter this temperature value with <▲> <▼>.
z TP display indicator not displayed, socket for the second
probe is free:
Connect the second probe (Cond) and immerse it in the
same test sample. TP flashes, the temperature is automatically measured using the second probe.
The AutoRead function (drift control) checks the stability of the measurement
signal. The stability has a considerable impact on the reproducibility of the
measured values.
For identical measurement conditions, the following criteria apply:
ReproducibilityResponse time
Better than 0.02> 30 seconds
20
1Call up the pH measuring mode with <M> and <▲> <▼> .
2Activate the AutoRead function with <AR>.
The current measured value is frozen (hold function).
ba75370e0311/2009
handylab pH/LF 12Operation
3Start AutoRead with <RUN/ENTER>.
AR flashes until a stable measured value is reached.
This measured value is transmitted to the interface.
4If necessary, start the next AutoRead measurement with
<RUN/ENTER>.
5To terminate the AutoRead function: Press the <AR> key.
Note
The current AutoRead measurement can be terminated at any time (accepting the current value) by pressing <RUN/ENTER>.
ba75370e0311/2009
21
Operationhandylab pH/LF 12
/pH
Tref20
Cal
8
TDS
S
8
1
pH
SalO
%
mg/l
1/
cm
Sal
AutoCal DIN
Lin
Tref25nLF
AutoCalTEC
RCL
Auto
Store
LoBat
ARng
AR
Time
Baud
Day.MonthNo.
Ident
Year
mbar
cm
M
°
F
/
K
%
S/
m
cm
8
4
2
2
3
°
C
TP
U
mV
4.2.3Measuring the ORP voltage
In conjunction with an ORP electrode, e.g. BlueLine 31Rx, the measuring instrument can measure the ORP voltage (mV) of a solution.
1Perform the preparatory activities according to section 4.2.1.
2Submerse the ORP electrode in the sample.
3Press the <▲> <▼> keys until the U status display appears.
The ORP voltage (mV) of the test sample appears on the display.
4Wait for a stable measured value.
Note
ORP electrodes are not calibrated. However, you can check ORP electrodes
using a test solution.
22
ba75370e0311/2009
handylab pH/LF 12Operation
4.3pH calibration
Why calibrate?pH electrodes age. This changes the asymmetry (zero point) and slope of the
pH electrode. As a result, an inexact measured value is displayed. Calibration
determines the current values of the asymmetry and slope of the electrode
and stores them in the measuring instrument. Thus, you should calibrate at
regular intervals.
When to calibrate?z After connecting another electrode
z When the sensor symbol flashes
– (after the calibration interval has expired)
– after a voltage interruption, e. g. after changing the batteries
You can select one of 3 calibration procedures:
AutoCal TECis specially matched to the SI Analytics technical buffer solutions as a fully
automatic two-point calibration. The buffer solutions are automatically rec-
ognized by the measuring instrument. Depending on the instrument setting
(see section 4.8 C
nominal value or the current electrode voltage in mV. The calibration can be
terminated after the first buffer solution. This corresponds to a single-point calibration. When doing so, the instrument uses the Nernst slope (-59,2 mV/
pH at 25 °C) and determines the asymmetry of the electrode.
ONFIGURATION), the instrument displays the relevant buffer
AutoCal DINis specially adapted to the permanently programmed buffer solutions in ac-
cordance with DIN 19266 as a fully automatic two-point calibration. The operating sequence of the AutoCal DIN calibration corresponds to that of the
AutoCal TEC calibration. The calibration can only be terminated after the first
buffer solution (single point calibration).
ConCalThis function is a conventional two-point calibration using two buffer solu-
tions (pH 7.0 ± 0.5 and any other buffer solution) or a single-point calibra-
tion using any buffer solution, which is used as a high-speed method.
AutoReadWhen calibrating with AutoCal TEC and AutoCal DIN, the AutoRead function
is automatically activated.
The current AutoRead measurement can be terminated at any time (accepting the current value) by pressing <RUN/ENTER>.
Displaying the
calibration data
Printing the
calibration
record
You can view the data of the last calibration on the display. The proceeding
is described on page 53.
The calibration protocol contains the calibration data of the current calibration.
You can transmit the calibration protocol to a printer via the serial interface
(see page 55).
You can automatically print a calibration protocol after the calibration. To do
so, connect a printer to the interface according to section 4.7.2 before calibrating. After a valid calibration, the record is printed.
Sample printout:
Calibration
evaluation
After the calibration, the measuring instrument automatically evaluates the
calibration. The asymmetry and slope are evaluated separately. The worst
evaluation appears on the display.
DisplayAsymmetry
[mV]
Slope
[mV/pH]
-15 ... +15-60.5 ... -58
-20 ... +20-58 ... -57
-25 ... +25-61 ... -60.5
or
-57 ... -56
-30 ... +30-62 ... -61
or
-56 ... -50
24
Clean the electrode according to the
electrode operating manual
E3
Eliminate the error according to chapter 6 W
HATTODOIF...
< -30 or
> 30
< -62 or
> -50
ba75370e0311/2009
Loading...
+ 56 hidden pages
You need points to download manuals.
1 point = 1 manual.
You can buy points or you can get point for every manual you upload.