Xylem HandyLab 100 User Manual

OPERATING MANUAL
HandyLab 100
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HandyLab 100
PH METER
HandyLab 100
Reprinting - even as excerpts - is only allowed with the explicit written authorization of SI Analytics GmbH, Mainz. Printed in Germany.
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HandyLab 100 Contents
HandyLab 100 - Contents
1 Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
1.1 Keypad . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
1.2 Display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
1.3 Connectors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
2 Safety . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.1 Authorized use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
2.2 General safety instructions . . . . . . . . . . . . . . . . . . . . . . . 10
3 Commissioning. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
3.1 Scope of delivery. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
3.2 Initial commissioning . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
3.2.1 Inserting the batteries. . . . . . . . . . . . . . . . . . . . . 13
3.2.2 Switching on the meter. . . . . . . . . . . . . . . . . . . . 14
3.2.3 Setting the date and time . . . . . . . . . . . . . . . . . . 14
4 Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
4.1 Switching on the meter . . . . . . . . . . . . . . . . . . . . . . . . . . 15
4.2 General operating principles . . . . . . . . . . . . . . . . . . . . . . 16
4.2.1 Operating modes . . . . . . . . . . . . . . . . . . . . . . . . 16
4.2.2 Navigation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
4.2.3 Navigation example 1:Setting the language. . . . 19
4.2.4 Example 2 on navigation: Setting the date and
time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
4.3 Sensor-independent settings . . . . . . . . . . . . . . . . . . . . . 23
4.3.1 System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
4.3.2 Data storage. . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
4.3.3 Automatic Stability control . . . . . . . . . . . . . . . . . 24
4.4 pH value / ORP voltage. . . . . . . . . . . . . . . . . . . . . . . . . . 24
4.4.1 General information . . . . . . . . . . . . . . . . . . . . . . 24
4.4.2 Measuring the pH value . . . . . . . . . . . . . . . . . . . 26
4.4.3 Measuring the ORP . . . . . . . . . . . . . . . . . . . . . . 28
4.4.4 Settings for pH and ORP measurements. . . . . . 30
4.4.5 pH calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . 32
4.4.6 Calibration interval . . . . . . . . . . . . . . . . . . . . . . . 36
4.4.7 Carrying out automatic calibration (AutoCal) . . . 37
4.4.8 Carrying out a manual calibration (VariCal) . . . . 41
4.4.9 Displaying calibration records . . . . . . . . . . . . . . 44
4.4.10 Continuous measurement control (CMC
function) . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
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Contents HandyLab 100
4.5 Data memory . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
4.5.1 Manual storage . . . . . . . . . . . . . . . . . . . . . . . . . . 46
4.5.2 Editing the measurement data memory . . . . . . . 47
4.5.3 Erasing the measurement data memory. . . . . . . 48
4.6 Reset . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49
4.6.1 Resetting the measurement settings . . . . . . . . . 49
4.6.2 Resetting the system settings. . . . . . . . . . . . . . . 50
5 Maintenance, cleaning, disposal . . . . . . . . . . . . . . . . . 51
5.1 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51
5.1.1 Replacing the batteries . . . . . . . . . . . . . . . . . . . . 51
5.2 Cleaning. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
5.3 Packing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
5.4 Disposal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
6 What to do if... . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55
7 Technical data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
7.1 General data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
7.2 Measuring ranges, resolution, accuracy . . . . . . . . . . . . . 60
8 Lists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
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HandyLab 100 Overview
1
2
3
HandyLab 100

1Overview

The compact HandyLab 100 precision pH meter enables you to per­form pH measurements rapidly and reliably. The HandyLab 100 pro­vides the maximum degree of operating comfort, reliability and measuring certainty for all applications. The proven calibration procedures and automatic stability control func­tion (AR) support your work with the pH meter.
1 Keypad
2Display
3 Connectors
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Overview HandyLab 100
F1
CAL
STO
RCL
ENTER
AR

1.1 Keypad

In this operating manual, keys are indicated by brackets <..> . The key symbol (e.g. <ENTER>) generally indicates a short keystroke (under 2 sec) in this operating manual. A long keystroke (approx. 2 sec) is indicated by the underscore behind the key symbol (e.g.
<ENTER
_>).
<F1>:
_>:
<F1
<ON/OFF>: Switches the meter on or off
<M>: Selects the measured parameter
<CAL>:
_>:
<CAL
<STO>: Saves a measured value manually
<RCL>: Displays the manually stored measured values
<>: Increments values, scrolls
<>: Decrements values, scrolls
Softkey providing situation dependent functions, e.g.:
<F1>/[Menu]: Opens the menu for measurement settings
_>/[Menu]: Opens the menu for system settings
<F1
Calls up the calibration procedure Displays the calibration data
<ENTER>: <ENTER
<AR> Freezes the measured value (HOLD function)
6
_>:
Opens the menu for measurement settings / confirms entries Opens the menu for system settings
Switches the AutoRead measurement on or off
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HandyLab 100 Overview
HOLD AR
25.0
6.093
pH
°C
4
3
2
5 6 7 8
1
0
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Menu

1.2 Display

1 Status information
2 Measured value (with unit)
3 Measured parameter
Function display
indicators
4 Continuous measurement control (CMC function)
5 Sensor symbol (calibration evaluation, calibration interval)
6 Measured temperature (with unit)
7 Status line
8 Softkeys and date + time
AutoCal e.g. TEC
VariCal
Error An error occurred during calibration
LoBat Batteries are almost empty
AR Stability control (AutoRead) is active
HOLD Measured value is frozen (<AR> key)
Calibration with automatic buffer recognition, e.g. with the buffer set: Technical buffers
Calibration with any buffers
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Overview HandyLab 100
4
1
2
3

1.3 Connectors

1 pH electrode
2 Reference electrode / temperature sensor
3 Reference electrode / temperature sensor
4 Service interface
Caution
Only connect sensors to the meter that cannot return any voltages or currents that are not allowed (> SELV and > current circuit with current limiting). Almost all customary sensors fulfill these conditions.
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HandyLab 100 Safety

2 Safety

This operating manual contains basic instructions that you must follow during the commissioning, operation and maintenance of the meter. Consequently, all responsible personnel must read this operating man­ual before working with the meter. The operating manual must always be available within the vicinity of the meter.
Target group The meter was developed for work in the field and in the laboratory.
Thus, we assume that, as a result of their professional training and experience, the operators will know the necessary safety precautions to take when handling chemicals.
Safety instructions Safety instructions in this operating manual are indicated by the warn-
ing symbol (triangle) in the left column. The signal word (e.g. "Caution") indicates the level of danger:
Further notes
Warning
indicates instructions that must be followed precisely in order to avoid possibly great dangers to personnel.
Caution
indicates instructions that must be followed precisely in order to avoid the possibility of slight injuries or damage to the instrument or the environment.
Note
indicates notes that draw your attention to special features.
Note
indicates cross-references to other documents, e.g. operating manu­als.
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Safety HandyLab 100

2.1 Authorized use

This meter is authorized exclusively for pH and ORP measurements in a laboratory or field environment. The technical specifications as given in chapter 7 T
ECHNICAL DATA must
be observed. Only the operation and running of the meter according to the instructions given in this operating manual is authorized. Any other use is considered unauthorized.

2.2 General safety instructions

This meter is constructed and tested in compliance with the IEC 1010 safety regulations for electronic measuring instruments. It left the factory in a safe and secure technical condition.
Function and
operational safety
The smooth functioning and operational safety of the meter can only be guaranteed if the generally applicable safety measures and the specific safety instructions in this operating manual are followed during opera­tion.
The smooth functioning and operational safety of the meter can only be guaranteed under the environmental conditions that are specified in chapter 7 T
ECHNICAL DATA.
If the meter was transported from a cold environment to a warm envi­ronment, the formation of condensate can lead to the faulty functioning of the meter. In this event, wait until the temperature of the meter reaches room temperature before putting the meter back into opera­tion.
Caution
The meter is only allowed to be opened by authorized personnel.
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HandyLab 100 Safety
Safe operation If safe operation is no longer possible, the meter must be taken out of
service and secured against inadvertent operation! Safe operation is no longer possible if the meter:
has been damaged in transport
has been stored under adverse conditions for a lengthy period of
time
is visibly damaged
no longer operates as described in this manual.
If you are in any doubt, please contact the supplier of the meter.
Obligations of the
purchaser
The purchaser of this meter must ensure that the following laws and guidelines are observed when using dangerous substances:
EEC directives for protective labor legislation
National protective labor legislation
Safety regulations
Safety datasheets of the chemical manufacturers.
Caution
In addition to the safety instructions mentioned here, also follow the safety instructions of the sensors used.
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Safety HandyLab 100
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HandyLab 100 Commissioning
2
1

3 Commissioning

3.1 Scope of delivery

pH meter HandyLab 100
4 batteries 1.5 V Mignon type AA
Short instructions
CD-ROM with
– detailed operating manual

3.2 Initial commissioning

Perform the following activities:
Insert the supplied batteries
For line-powered operation: Connect the power pack Switch on the
meter
Set the date and time

3.2.1 Inserting the batteries

1 Unscrew the four screws (1) on the underside of the meter.
2 Open the battery compartment (2) on the underside of the
meter.
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Commissioning HandyLab 100
3 Place four batteries (type Mignon AA) in the battery compart-
ment.
4 Close the battery compartment.
Caution
Make sure that the poles of the batteries are positioned correctly. The ± signs on the batteries must correspond to the battery compartment.
Note
Alternatively, you can also use Ni-MH rechargeable batteries (type Mignon AA). In order to charge the batteries, an external charging device is required.

3.2.2 Switching on the meter

± signs in the
1 Press the <ON/OFF> key.
The meter performs a self-test. The display shows the manufacturer's logo while the self-test is being performed. Subsequently, the meter switches to the measuring mode (measured value display).
Note
The meter has an energy saving feature to avoid unnecessary battery depletion. The energy saving feature switches off the meter if no key is pressed during the adjusted interval. (How to set the switch-off interval, see sec­tion 4.3.1).

3.2.3 Setting the date and time

1 See section 4.2.4
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HandyLab 100 Operation
pH
6.949
25.0
°C
15.03.2014 010:00
Menu

4 Operation

4.1 Switching on the meter

Switching on Press the <ON/OFF> key.
The meter performs a self-test. The display shows the manufacturer's logo while the self-test is being performed. The measured value display appears.
Switching off Press the <ON/OFF> key.
Automatic switch-off
function
Display illumination The meter automatically switches off the display illumination if no key
The instrument has an automatic switch-off function in order to save the batteries (see section 4.3.1). The automatic switch-off function switch­es off the meter if no key is pressed for an adjustable period.
is pressed for 30 seconds. The illumination is switched on with the next keystroke again.
You can also generally switch the display illumination on or off (see section 4.3.1).
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Operation HandyLab 100

4.2 General operating principles

This section contains basic information on the operation of the HandyLab 100.
Operating elements,
display
Operating modes,
navigation
An overview of the operating elements and the display is given in sec­tion 1.1 and section 1.2.
An overview of the operating modes and navigation of the HandyLab 100 is given in section 4.2.1 and section 4.2.2.

4.2.1 Operating modes

The instrument has the following operating modes:
Measuring
The measurement data of the connected sensor are shown in the measured value display
Calibration
The course of a calibration with calibration information, functions and settings is displayed
Storing in memory
The meter stores the measurement data manually
Setting
The system menu or a sensor menu with submenus, settings and functions is displayed
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HandyLab 100 Operation
General Clock Service information Reset
System
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Back
Language: Deutsch Illumination: On Contrast
: 50 %
Switchoff time: 1 h
General
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Back

4.2.2 Navigation

Measured value display In the measured value display, you can
open the menu for calibration and measurement settings with <F1>
(short
keystroke)
open the system menu with the sensor-independent settings by
pressing <F1>Storage & config for a <F1
_>long keystroke,
approx. 2 s).
change the display in the selected measuring screen (e. g. pH <->
mV) by pressing <M>.
Menus and dialogs The menus for settings and dialogs in procedures contain further sub-
elements. The selection is made with the <><> keys. The current selection is displayed with a frame.
Submenus
The name of the submenu is displayed at the upper edge of the frame. Submenus are opened by confirming with <ENTER>. Exam­ple:
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Settings
Settings are indicated by a colon. The current setting is displayed on the right-hand side. The setting mode is opened with <ENTER>. Subsequently, the setting can be changed with <><> and
<ENTER>. Example:
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Operation HandyLab 100
Calibration record Kalibrierspeicher Buffer
: TEC
One point calibration
: Yes
Calibration interval: 7 d Unit for slope
: mV/pH
i
2.00 4.01 7.00 10.01 (25 °C)
pH
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Back
Calibration record Kalibrierspeicher Buffer
: TEC
One point calibration
: Yes
Calibration interval
: 7 d
Unit for slope: mV/pH
i
2.00 4.01 7.00 10.01 (25 °C)
pH
15.03.2014 010:00
Back
Functions
Functions are designated by the name of the function. They are immediately carried out by confirming with <ENTER>. Example: Display the Calibration record function.
i
Messages Information is marked by the
symbol. It cannot be selected. Example:
18
Note
The principles of navigation are explained in the two following sections by reference of examples:
Setting the language (section 4.2.3)
Setting the date and time (see section 4.2.4).
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HandyLab 100 Operation
pH
6.949
25.0
°C
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Menu
System Data storage
Storage & config
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010:00
Back

4.2.3 Navigation example 1:Setting the language

1 Press the <ON/OFF> key.
The measured value display appears. The instrument is in the measuring mode.
2 Using <F1_>/[Menu], open the Storage & config menu.
The instrument is in the setting mode.
3 Select the System submenu with <><>.
The current selection is displayed with a frame.
4 Open the System submenu with <ENTER>.
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Operation HandyLab 100
General Clock Service information Reset
System
15.03.2014 010:00
Back
Language: Deutsch Illumination: On Contrast
: 50 %
Switchoff time
: 1 h
General
15.03.2014 010:00
Back
Language: Deutsch Illumination
: On
Contrast: 50 % Switchoff time
: 1 h
General
15.03.2014 010:00
Back
5 Select the General submenu with <><>.
The current selection is displayed with a frame.
6 Open the General
submenu with <ENTER>.
7 Open the setting mode for the Language with <ENTER>.
20
8 Select the required language with <><>.
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