The trademarks of the products mentioned in this manual are held by the companies that
produce them.
LabVIEW™ is a trademark of National Instruments.
Z-Match® and SQM-242™ are trademarks of INFICON GmbH.
Windows®, Microsoft®, Visual Basic® and ActiveX® are registered trademarks of Microsoft Corporation.
All other brand and product names are trademarks or registered trademarks of their respective companies.
Disclaimer
The information contained in this manual is believed to be accurate and reliable. However, INFICON assumes
no responsibility for its use and shall not be liable for any special, incidental, or consequential damages related
to the use of this product.
Due to our continuing program of product improvements, specifications are subject to change without notice.
This is to certify that this equipment, designed and manufactured by:
INFICON Inc.
Two Technology Place
East Syracuse, NY 13057
USA
meets the essential safety requirements of the European Union and is placed on the market
accordingly. It has been constructed in accordance with good engineering practice in safety
matters in force in the Community and does not endanger the safety of persons, domestic
animals or property when properly installed and maintained and used in applications for
which it was made.
Equipment Description:
Applicable Directives: 2006/95/EC (LVD)
SQM-242 (including all options)
2004/108/EC (General EMC)
2002/95/EC (RoHS)
Applicable Standards:
Safety: EN 61010-1:2001
Emissions: EN 61326-1:1997/A1: 1998/A2: 2001 (Radiated & Conducted Emissions)
Class A: Emissions per Table 3
(EMC – Measurement, Control & Laboratory Equipment)
Immunity: EN 61326-1:1997/A1: 1998/A2: 2001 (General EMC)
Class A: Immunity per Table A1
(EMC – Measurement, Control & Laboratory Equipment)
RoHS: Fully compliant
CE Implementation Date:
July 2003 (Updated February 2011)
Authorized Representative:
Steve Schill
Thin Film Business Line Manager
INFICON Inc.
ANY QUESTIONS RELATIVE TO THIS DECLARATION OR TO THE SAFETY OF INFICON'S PRODUCTS SHOULD BE DIRECTED, IN
WRITING, TO THE AUTHORIZED REPRESENTATIVE AT THE ABOVE ADDRESS.
Warranty
WARRANTY AND LIABILITY - LIMITATION: Seller warrants the products
manufactured by it, or by an affiliated company and sold by it, and described on
the reverse hereof, to be, for the period of warranty coverage specified below, free
from defects of materials or workmanship under normal proper use and service.
The period of warranty coverage is specified for the respective products in the
respective Seller instruction manuals for those products but shall not be less than
two (2) years from the date of shipment thereof by Seller. Seller's liability under
this warranty is limited to such of the above products or parts thereof as are
returned, transportation prepaid, to Seller's plant, not later than thirty (30) days
after the expiration of the period of warranty coverage in respect thereof and are
found by Seller's examination to have failed to function properly because of
defective workmanship or materials and not because of improper installation or
misuse and is limited to, at Seller's election, either (a) repairing and returning the
product or part thereof, or (b) furnishing a replacement product or part thereof,
transportation prepaid by Seller in either case. In the event Buyer discovers or
learns that a product does not conform to warranty, Buyer shall immediately notify
Seller in writing of such non-conformity, specifying in reasonable detail the nature
of such non-conformity. If Seller is not provided with such written notification,
Seller shall not be liable for any further damages which could have been avoided if
Seller had been provided with immediate written notification.
THIS WARRANTY IS MADE AND ACCEPTED IN LIEU OF ALL OTHER
WARRANTIES, EXPRESS OR IMPLIED, WHETHER OF MERCHANTABILITY OR
OF FITNESS FOR A PARTICULAR PURPOSE OR OTHERWISE, AS BUYER'S
EXCLUSIVE REMEDY FOR ANY DEFECTS IN THE PRODUCTS TO BE SOLD
HEREUNDER. All other obligations and liabilities of Seller, whether in contract or
tort (including negligence) or otherwise, are expressly EXCLUDED. In no event
shall Seller be liable for any costs, expenses or damages, whether direct or
indirect, special, incidental, consequential, or other, on any claim of any defective
product, in excess of the price paid by Buyer for the product plus return
transportation charges prepaid.
No warranty is made by Seller of any Seller product which has been installed,
used or operated contrary to Seller's written instruction manual or which has been
subjected to misuse, negligence or accident or has been repaired or altered by
anyone other than Seller or which has been used in a manner or for a purpose for
which the Seller product was not designed nor against any defects due to plans or
instructions supplied to Seller by or for Buyer.
This manual is intended for private use by INFICON® Inc. and its customers.
Contact INFICON before reproducing its contents.
NOTE: These instructions do not provide for every contingency that may arise in
connection with the installation, operation or maintenance of this equipment.
Should you require further assistance, please contact INFICON.
The SQM-242 Card is a powerful thin film deposition controller on a PCI card.
Significant features include:
Measure four 1 MHz to 10 MHz quartz crystal sensors simultaneously.
Controls two deposition source supplies simultaneously (co-deposition).
Install multiple cards for up to 24 sensors and 12 control outputs.
Measure four +/- 10 V analog inputs with optional (SAM-242) piggyback card.
Installs in any PC running Windows
PCI slot.
Interfaces to your program with Windows DLL and ActiveX
Sample Visual Basic
Figure 1-1 SQM-242 Deposition Control Card
SQM-242 Operating Manual
Chapter 1
Introduction
®
98/2000/ME/XP/7-32-bit with a vacant
®
interfaces.
®
and LabVIEW™ programs with source code are included.
IPN 074-549-P1A
The sample software included with SQM-242 card allows you to:
Co-deposit up to six materials, using up to eight sensors.
Use analog inputs to control heaters, gas flow, and other process variables.
Use outputs for recording rate, thickness, power, or voltage.
Save film setup parameters and deposition data to disk.
Simulate deposition for developing and testing film setups.
1 - 1
SQM-242 Operating Manual
The optional SQS-242 software allows multi-layer deposition recipes, graphics,
flexible PLC-based digital I/O and RS-232/Ethernet external control.
The SQM-242 card is a PID loop process controller designed for use primarily in
physical vapor deposition. The SQM-242 card monitors and/or controls the rate
and thickness of thin film depositions. The SQM-242 reads frequency from an
in-vacuum 1 to 10 MHz quartz crystal driven by a small external oscillator module.
The oscillator module uses the in-vacuum crystal as the feedback element of an IC
oscillator circuit to amplify the crystal signal to about 0.75 volts peak to peak. The
SQM-242 card supplies 5 V (dc) to the oscillator module, and reads the module's
frequency output signal on a single BNC cable. On the SQM-242, a 200 MHz
reference oscillator sets a known measurement period. By counting the input
transitions during the measurement period, a frequency is calculated.
Deposition rate and thickness are inferred from the frequency change induced by
mass added to a quartz crystal. This technique positions sensors in the path
between, or to the side of, the target substrate and the source of vaporized
material. The sensor incorporates an exposed oscillating quartz crystal whose
frequency decreases as material accumulates. The change in frequency provides
information to determine rate and thickness and to continually control the
evaporation power source. With user supplied time, thickness and power limits and
with desired rates and material characteristics, the SQM-242 card is capable of
automatically controlling the process in a precise and repeatable manner. User
interaction is accomplished via the front panel or serial communications and
consists of selection or entry of parameters to define the process.
When reading this SQM-242 Manual, please pay particular attention to the
NOTES, CAUTIONS, and WARNINGS found throughout the text. The Notes,
Cautions, and Warnings are defined in section 1.2.1 on page 1-3.
1.1.1 Related Manuals
Sensors are covered in separate manuals. PDF files of these manuals are
contained in the 074-5000-G1 CD, part of the Ship Kit.
074-154 - Bakeable Sensor
074-156 - Front Load Sensor, Single/Dual
074-157 - Sputtering Sensor
147-800 - Cool Drawer Sensor, Single/Dual
IPN 074-549-P1A
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SQM-242 Operating Manual
CAUTION
WARNING
WARNING - Risk Of Electric Shock
1.2 Instrument Safety
1.2.1 Definition of Notes, Cautions and Warnings
When using this manual, please pay attention to the NOTES, CAUTIONS and
WARNINGS found throughout. For the purposes of this manual they are defined as
follows:
NOTE: Pertinent information that is useful in achieving maximum instrument
efficiency when followed.
Failure to heed these messages could result in damage
to the instrument.
Failure to heed these messages could result in personal
injury.
Dangerous voltages are present which could result in
personal injury.
IPN 074-549-P1A
1 - 3
SQM-242 Operating Manual
WARNING - Risk Of Electric Shock
WARNING - Risk Of Electric Shock
WARNING
1.2.2 General Safety Information
The SQM-242/SAM-242 card(s) do not have any user
serviceable components.
Dangerous voltages may be present whenever the PC is
on or external input/relay connectors are present.
Refer all maintenance to technically qualified personnel.
This instrument contains delicate circuitry which is
susceptible to transient voltages/static.
Refer all maintenance to technically qualified personnel
Failure to operate the SQM-242 card(s) in the manner
intended by INFICON can circumvent the safety
protection provided by the instrument and may result in
personal injury.
IPN 074-549-P1A
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SQM-242 Operating Manual
1.3 How To Contact Customer Support
Worldwide support information regarding:
Technical Support, to contact an applications engineer with questions
regarding INFICON products and applications, or
Sales and Customer Service, to contact the INFICON Sales office nearest you,
or
Repair Service, to contact the INFICON Service Center nearest you,
is available at www.inficon.com.
When you contact Customer Support, please have the following information readily
available:
The firmware version displayed at power-up for your instrument and software
version if you are calling about the optional applications software.
A description of your problem.
An explanation of any corrective action that you may have already attempted.
The exact wording of any error messages that you have received.
To contact Customer Support, see Support at www.inficon.com.
1.3.1 Returning Your Instrument to INFICON
Do not return any component of your instrument to INFICON without first speaking
with a Customer Support Representative. You must obtain a Return Material
Authorization (RMA) number from the Customer Support Representative.
If you deliver a package to INFICON without an RMA number, your package will be
held and you will be contacted. This will result in delays in servicing your
instrument.
Prior to being given an RMA number, you may be required to complete a
Declaration Of Contamination (DOC) form. DOC forms must be approved by
IPN 074-549-P1A
INFICON before an RMA number is issued. INFICON may require that the
instrument be sent to a designated decontamination facility, not to the factory.
Before returning your instrument, create a record of all user-entered parameters so
they may be re-entered, if required.
1If the SQM-242 card has not been removed from its packaging, do so now.
2Carefully examine the card for damage that may have occurred during
shipping. This is especially important if you notice obvious rough handling on
the outside of the container. Immediately report any damage to the carrier and
to INFICON.
3Do not discard the packing materials until you have taken inventory and have
at least performed successful installation.
4Take an inventory of your order by referring to your order invoice and the
information contained in section 1.6.
5To install the card, see Chapter 2, Installation.
6For additional information or technical assistance, contact INFICON, refer to
Above kits consist of oscillator 782-900-010, 6 inch BNC oscillator to feedthrough
cable 782-902-011 and BNC controller to oscillator cable 782-902-012-10,
782-902-012-25, 782-902-012-50 or 782-902-012-99. These kits are designed for
use with the standard in-vacuum cables ranging in length from 6 inches (15.2 cm)
to 36 inches (91.4 cm). The 007-044 standard in-vacuum cable supplied with the
front load style sensors are 30.75 inches (78.1 cm) long.
NOTE: Multi-crystal (rotary) sensors should not be used with the SQM-242
NOTE: Consult individual sensor manuals for part muber configurations.
pneumatic shutter actuator control valve.
1 - 10
IPN 074-549-P1A
2.1 SQM-242 Card Installation
Card 1Card 2Card 3Card 4Card 5Card 6
JP5JP5JP5JP5JP5JP5
JP5
Card 1 Jumper
with SAM-242 Card installed
Card 1 with SAM-242
Ribbon Cable installed
The SAM-242 card can go on
either side of SQM-242 Card 1,
as long as
the ribbon cable is
not twisted (red stripe on one
side of both cards).
Jumper each SQM-242 card before installation as shown in Figure 2-1.
Figure 2-1 Jumper Configurations
If you are installing a SAM-242 analog piggyback card, it must be connected to
Card 1. Set the Card 1 jumper as shown in Figure 2-2 when the optional SAM-242
card is used.
SQM-242 Operating Manual
Chapter 2
Installation
IPN 074-549-P1A
Figure 2-2 SAM-242 Card Installation
Once each card is jumpered:
1Turn off the computer, unplug the power cord, and remove the computer cover.
2Locate an empty PCI slot and remove the screw holding the blank bracket for
the slot. Remove the blank bracket.
3With the card’s gold contacts down, place it above the PCI slot with the BNC
connectors on the card extending through the back of the computer. Press
down on the card to seat it into the connector. Repeat with each card.
4Replace the screw at the top of the card bracket to secure the card. Replace
the cover on the computer and plug in the power cord.
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SQM-242 Operating Manual
2.2 SQM-242 Driver Installation
1Turn on the computer and start Windows. Windows will find new hardware and
prompt to Install Device Drivers.
2If you are prompted for the location of the Device Drivers, insert the INFICON
CD-ROM and direct Windows to D:\SQM242 Card\SQM242_V100_DRIVERS
(assuming D is your CD drive).
3When driver installation is complete, you may be prompted to restart your
computer.
4Check the README.txt file in the \SQM242 Card\SQM242_V100_DRIVERS
folder of the INFICON CD-ROM for additional steps that are specific to your
version of Windows.
5Verify that the card was installed properly in Device Manager. Right-click on My
Computer, then left-clicking on Properties. Click on the Device Manager tab
(Hardware tab in Windows 2000 or XP, then Device Manager). You should see
Sigma Instruments listed, with the SQM-242 cards in the sub folder.
If the card is not listed (or has a red x or yellow exclamation point), repeat the
installation procedures above carefully.
NOTE: Occasionally it may be necessary to completely uninstall and reinstall a
card. Highlight the improperly installed card in Device Manager and press
<Delete>. Next, run the "clean" program in the \SQM242
Card\SQM242_V100_DRIVERS folder of the INFICON CD-ROM. Reboot
the computer, then follow the steps above carefully.
2.3 Software Installation
SQM-242 Card programs are also on the INFICON CD-ROM. Insert the CD-ROM,
click the Windows Start button, and then select Run. Type D:\SQM242
Card\Setup.exe and click OK.
Accept the default installation prompts. When installation completes, you may be
prompted to restart your computer. This installer will install three programs:
SQM-242 CoDep, SQM-242 Monitor, and SQM-242 Multi.
To run the any software program, click Start, then Program, then Sigma
Instruments and select the program.
To verify the SQM-242 cards are properly installed, start SQM-242 CoDep. Select
the View menu, then Card Setup. If the card revision for each installed card is
greater than 0.00, then it is installed properly.
IPN 074-549-P1A
2 - 2
NOTE: If the version is shown as 0.00, then reinstall the Windows drivers as
explained in section 2.2. Pay particular attention to any Windows version
specific instructions in the README file.
2.4 SQM-242 Card Connections
Sensor 1
Sensor 2
Sensor 3
Sensor 4
Power Supply
Control Outputs
The control output and sensor input connectors to the SQM-242 card are shown
below. Refer to this drawing in the subsequent hookup instructions.
Figure 2-3 SQM-242 Setup
SQM-242 Operating Manual
IPN 074-549-P1A
Sensor Connections
A BNC cable connects the SQM-242 sensor input to the
"instrument" connector on the remote oscillator. The
maximum length is 50 feet (15 meters).
To ensure proper operation of the SQM-242, use oscillators
manufactured by INFICON [PN 782-900-010].
The connection from the remote oscillator "feedthru"
connector to the vacuum chamber feedthrough is made using
a short 6 inch (15 cm) cable with BNC male to female
connectors [PN 782-902-011]. Inside the vacuum chamber, your in-vac cable must
be no longer than 36 inches (91.4 cm). It connects from the feed-through to the
crystal sensor.
NOTE: The SQM-242 will not work with INFICON ModeLock oscillators.
2 - 3
SQM-242 Operating Manual
CAUTION
SLEEVE
Chan. 1 (Ring)
Chan. 2 (Tip)
Ground
(Sleeve)
Output Connections
The SQM-242 output connection is via a 1/4" Stereo Phone Jack. A standard 1/4"
Stereo Phone Plug is shown below (with outer collar removed to show the
contacts). Output 1 is on the ring, Output 2 is on the tip, and a common ground is
on the sleeve.
Figure 2-4 1/4" Stereo Phone Jack
Connect the SQM-242 output to your evaporation power supply, recorder, or other
equipment as described in the equipment’s operating manual.
Special care must be taken in connecting the SQM-242
card output to the input connector of your equipment.
Failure to understand and follow the equipment
manufacturer’s instructions can result in damage to the
equipment and/or SQM-242 card.
The SQM-242 output is 0 to +/- 10 V (dc). See section 3.3 of this manual for
instructions on setting the SQM-242 output Full Scale level to match your power
supply. If your equipment needs a 4-20 mA control signal, you must obtain a
voltage-to-current converter.
NOTE: If you are using the SQM-242 as a monitor only, no output connection is
needed.
Ground Connection
The chassis of all control components should be tied to a common earth ground
using a low resistance cable. This is particularly important in high noise E-Beam
systems.
IPN 074-549-P1A
2 - 4
2.5 SAM-242 Card Connections
CAUTION
The input and output and connectors on the SAM-242 card are identical to those
on the SQM-242 card.
Figure 2-5 SAM-242 Card
SQM-242 Operating Manual
Input Connections
BNC cables connect the SAM-242 input to the signals to be measured. The
SAM-242 accepts input voltages within +/- 10 V (dc).
NOTE: You can not connect sensors to these inputs.
IPN 074-549-P1A
The BNC connector shield of each SAM-242 input is
connected to a common analog ground. Input signals to
the SAM-242 must be within +/-10 V (dc) and share a
common ground. Failure to observe this constraint can
result in damage to your equipment and/or the SAM-242
card,
Output Connection
The SAM-242 outputs are identical to the SQM-242. See the previous section for
hookup instructions.
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SQM-242 Operating Manual
2.6 Digital I/O
The SQM-242 card and SQM-242 software do not support the digital I/O required
to automatically open and close shutters, rotate source pockets, etc.
The optional SQS-242 Codeposition software adds this capability to the SQM-242
card. Using an inexpensive PLC, the SQS-242 software provides virtually unlimited
digital I/O capabilities.
Contact INFICON for more information on interfacing the SQM-242 card to your
system's digital I/O.
2 - 6
IPN 074-549-P1A
3.1 Introduction
The SQM-242 CoDep program illustrates most of the capabilities of the SQM-242
card. It is intended as a learning tool for new users, and a programming example
for interfacing to user applications.
3.2 Main Dialog Box
With no cards installed (or with two SQM-242 cards and an SAM-242 card
installed) you will see the dialog box shown in Figure 3-1. The number of "output
frames" shown will change depending on the number of cards installed in your
system. For example, with only one SQM-242 card installed, the main dialog box
shows only two output frames.
SQM-242 Operating Manual
Chapter 3
SQM-242 CoDep
Figure 3-1 SQM-242 Codep Main Dialog Box
IPN 074-549-P1A
Each output frame corresponds to a physical output on an SQM-242 card. In Figure
3-1, the first three outputs are each configured to use quartz sensors to measure
rate and thickness.
The frame labeled "Gas Flow" is a little different. This output uses an analog input
on the SAM-242 card to control backfill gas. The SAM-242 card can use any analog
voltage for control. More about this feature later.
3 - 1
SQM-242 Operating Manual
Output A1 above is turned off, while Output A2 is used as a recorder output. The
output labels are easily edited to provide descriptive names. Dialog boxes within
each output frame will change, depending on the function of that output.
Outputs configured for quartz sensor inputs, like the first three in the sample dialog
box, display rate and thickness information. The first display is the Thickness
Measurement for the material (in kÅ). Immediately below the Thickness
Measurement display is the Thickness Setpoint setting. You can edit the Thickness
Setpoint at any time. When the Thickness Reading reaches the Thickness
Setpoint, the deposition will stop.
NOTE: To adjust a Setpoint, click on the setting and type a new setting. Press
<Enter> to send the setting without moving to another field. To move to
another field, use the <Tab> key or your mouse. Each time you move to
another field, the setting is updated.
Below the thickness displays are the Rate Reading and Rate Setpoint displays (in
Å/s). In Auto mode, the SQM-242 control loop continuously adjusts the output
power to maintain the deposition Rate Reading at the desired Rate Setpoint.
Below the rate displays are the output Power Reading and manual Power Setpoint.
The Power Reading displays the current output power (in % Full Scale). In Manual
mode, the Power Setpoint can be edited to manually adjust output power.
The option buttons control the function of each output. As mentioned previously,
Auto mode uses a PID control loop to control rate. Manual mode, allows you to
manually adjust the output power. That can be useful for material preconditioning
or error conditions.
The Record button configures the output as an analog recorder. A recorder output
provides a signal that is proportional to thickness, rate, power, or analog voltage.
Finally, the Off button sets the output to 0 volts and hides the displays.
readings and PID output control. When Stop
is displayed, stops readings and sets the
power outputs to zero. When Stop is
displayed, a Hold button is also visible.
Hold/Resume . . . . . . . . . . . . . . . . . Clicking Hold sets all output power levels to
zero, and changes the button legend to
Resume. Clicking Resume continues
deposition without zeroing thickness.
Zero All . . . . . . . . . . . . . . . . . . . . . . Sets all material (i.e., output) thickness