Xylem pH-ION 3400i User Manual

pH/ION 3400i
Operating manual
6
M
C
AL
S
T
O
R
C
L
AR
pH
9
2
29
4
8
°C
O
pH/Ion meter
ba75685e01 01/2007
Accuracy when
going to press
Warranty We guarantee the instrument described for 3 years from the date of
The use of advanced technology and the high quality standard of our instruments are the result of continuous development. This may result in differences between this operating manual and your instrument. Also, we cannot guarantee that there are absolutely no errors in this manual. Therefore, we are sure you will understand that we cannot accept any legal claims resulting from the data, figures or descriptions.
purchase. The instrument warranty covers manufacturing faults that are discov­ered within the warranty period. The warranty does not cover compo­nents that are replaced during maintenance work, e.g. batteries.
The warranty claim extends to restoring the instrument to readiness for use but not, however, to any further claim for damages. Improper handling or unauthorized opening of the instrument invalidates any warranty claim.
To ascertain the warranty liability, return the instrument and proof of purchase together with the date of purchase freight paid or prepaid.
Copyright
© Weilheim 2007, WTW GmbH
Reproduction in whole - or even in part - is prohibited without the express written permission of WTW GmbH, Weilheim. Printed in Germany.
pH/ION 3400i Contents
1 Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
1.1 General features . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
1.2 SETs of equipment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
1.3 Keypad . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
1.4 Display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
1.5 Jack field . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
1.6 Operating structure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
2 Safety . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
2.1 Authorized use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
2.2 General safety instructions . . . . . . . . . . . . . . . . . . . . . . . 12
3 Commissioning. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
3.1 Scope of delivery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
3.2 Initial commissioning . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
4 Operation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
4.1 Switching on the measuring instrument . . . . . . . . . . . . . 15
4.2 pH value / ORP voltage . . . . . . . . . . . . . . . . . . . . . . . . . 16
4.2.1 General information . . . . . . . . . . . . . . . . . . . . . . 16
4.2.2 Measuring the pH value . . . . . . . . . . . . . . . . . . 17
4.2.3 Measuring the ORP voltage . . . . . . . . . . . . . . . 19
4.3 pH calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
4.3.1 AutoCal TEC . . . . . . . . . . . . . . . . . . . . . . . . . . . 22
4.3.2 AutoCal DIN . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
4.3.3 ConCal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
4.4 Ion concentration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32
4.4.1 General information . . . . . . . . . . . . . . . . . . . . . . 32
4.4.2 Measuring the ion concentration . . . . . . . . . . . . 33
4.4.3 Calibration for ion selective measurements . . . 34
4.5 Calibration interval (Int 3) . . . . . . . . . . . . . . . . . . . . . . . 41
4.6 Saving . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
4.6.1 Saving manually . . . . . . . . . . . . . . . . . . . . . . . . 42
4.6.2 Switching on AutoStore (Int 1) . . . . . . . . . . . . . 44
4.6.3 Outputting the data storage . . . . . . . . . . . . . . . . 46
4.6.4 Clearing the memory . . . . . . . . . . . . . . . . . . . . . 52
4.7 Transmitting data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
4.7.1 Data transmission interval (Int 2) . . . . . . . . . . . 53
4.7.2 PC/external printer (RS232 interface) . . . . . . . . 54
4.7.3 Remote control . . . . . . . . . . . . . . . . . . . . . . . . . 55
4.8 Configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56
4.9 Reset . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
5 Maintenance, cleaning, disposal. . . . . . . . . . . . . . . . . 63
5.1 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 63
3
Contents pH/ION 3400i
5.2 Cleaning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 64
5.3 Disposal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 64
6 What to do if... . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65
6.1 pH system messages . . . . . . . . . . . . . . . . . . . . . . . . . . . 65
6.2 ISE system messages . . . . . . . . . . . . . . . . . . . . . . . . . . 67
6.3 General errors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
7 Technical data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71
8 Lists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75
4
pH/ION 3400i Overview

1Overview

1.1 General features

This compact precision handheld meter enables you to carry out pH / ORP measurements and concentration measurements using ion selec­tive electrodes rapidly and reliably. The handheld meter provides the maximum degree of operating com­fort, reliability and measuring certainty for all applications.
The proven MultiCal
®
calibration procedures and the special AutoRead
function support you in your work with the handheld meter.
6
M
C
AL
S
T
O
R
C
L
AR
pH
9
2
29
4
8
°C
O
3
2
1
1 Keypad
2 Sample display
3 Jack field
Note
If you need further information or application notes, you can obtain the following material from WTW:
z Application reports
z Primers
z Safety datasheets.
You will find information on available literature in the WTW catalog or via the Internet.
5
Overview pH/ION 3400i

1.2 SETs of equipment

The measuring instrument is also available as part of individual SETs of equipment. You will find additional information on this and other accessories in the WTW catalog or via the Internet.
6
pH/ION 3400i Overview
Set (sample configuration):
1 pH/ION 3400i measuring instrument
2 Stand
3 Measuring beaker,50 ml
4 50 ml pH buffer solution, STP 4
5 50 ml pH buffer solution, STP 7
6 Storing solution for pH electrodes
7 pH combination electrode
8 Plug-in power supply (optional)
7
Overview pH/ION 3400i

1.3 Keypad

STOM
ARRCLCAL
RUN/ENTER
Key functions
M
STO
CAL
RCL
AR
Select the measured variable <M>:
pH value / ORP voltage
Ion concentration
Save a measured value
<STO>
Switch measuring instrument on/off
<ON/OFF>
Calibrate the currently set measured variable
<CAL>
Display/transmit measured values
<RCL>
Activate/deactivate the AutoRead function
<AR>
Select the measuring mode, increase values, scroll < >
Select the measuring mode, decrease values, scroll <>
RUN/ENTER
Confirm entries, start AutoRead
<RUN/ENTER>
8
pH/ION 3400i Overview

1.4 Display

Status display
ISE
UpH
S
8
1
Baud
Time
Day.Month No.
Year
Ident
AutoCal DIN
LoBat
AutoCal TEC

1.5 Jack field

8
8.
Auto
ConCal
8
Store
88
8
°F °C
CalError
ARng
mol/L mV/pH % ppm
mg/l
%
Tem pEr ro r
AR
TP
RCL
Probe symbol
Meas. value display
Function and temperature display
5 4
f
e
R
123
1 pH electrode or ISE (combination) electrode
2 Reference electrode
3 Plug-in power supply (optional)
4 pH temperature sensor
5 Serial interface RS 232 / analog output (recorder)
9
Overview pH/ION 3400i

1.6 Operating structure

The following overview diagram shows which keys you have to press to select between the different measuring modes:
10
pH/ 3400i Safety

2 Safety

This operating manual contains basic instructions that you must follow during the commissioning, operation and maintenance of the measur­ing instrument. Consequently, all responsible personnel must read this operating manual before working with the measuring system. The op­erating manual must always be available within the vicinity of the mea­suring system.
Target group The measuring instrument was developed for work in the field and in
the laboratory. We assume that, as a result of their professional training and experi­ence, the operators will know the necessary safety precautions to take when handling chemicals.
Safety instructions The individual chapters of this operating manual use the following safe-
ty labels to indicate various types of danger:
Warning
indicates instructions that must be followed precisely in order to avoid the possibility of slight injuries or damage to the instrument or the envi­ronment.
Further notes
Note
indicates notes that draw your attention to special features.
Note
indicates cross-references to other documents, e.g. operating manu­als.

2.1 Authorized use

The authorized use of the measuring instrument consists exclusively of the pH and ORP measurement or the measurement of the ion concen­tration in the field and laboratory.
The technical specifications as given in chapter 7 T must be observed. Only the operation and running of the measuring instrument according to the instructions given in this operating manual is authorized. Any other use is considered to be unauthorized.
ECHNICAL DATA
11
Safety pH/ 3400i

2.2 General safety instructions

This instrument is built and inspected according to the relevant guide­lines and norms for electronic measuring instruments (see chapter 7T
ECHNICAL DATA).
It left the factory in a safe and secure technical condition.
Function and operating
safety
Safe operation If safe operation is no longer possible, the instrument must be taken out
The smooth functioning and operational safety of the measuring instru­ment can only be guaranteed if the generally applicable safety mea­sures and the specific safety instructions in this operating manual are followed during operation.
The smooth functioning and operational safety of the measuring instru­ment can only be guaranteed under the environmental conditions that are specified in chapter 6 W
HAT TO DO IF....
If the instrument was transported from a cold environment to a warm environment, the formation of condensate can lead to the faulty func­tioning of the instrument. In this event, wait until the temperature of the instrument reaches room temperature before putting the instrument back into operation.
of service and secured against inadvertent operation! Safe operation is no longer possible if the measuring instrument:
z has been damaged in transport
z has been stored under adverse conditions for a lengthy period of
time
Obligations of the pur-
chaser
12
z is visibly damaged
z no longer operates as described in this manual.
If you are in any doubt, please contact the supplier of the instrument.
The purchaser of the measuring instrument must ensure that the fol­lowing laws and guidelines are observed when using dangerous sub­stances:
z EEC directives for protective labor legislation
z National protective labor legislation
z Safety regulations
z Safety datasheets of the chemical manufacturers.
pH/ 3400i Commissioning

3 Commissioning

3.1 Scope of delivery

z 3400i handheld meter
z Plug-in power supply (optional)
z Operating manual and short operating manual
z 4 batteries, 1.5 V Mignon type AA (in the instrument)
Setting the date and
time
For details of scope of delivery of SETs, see chapter 1.2 SET
EQUIPMENT and WTW catalog.

3.2 Initial commissioning

Perform the following activities:
z Set the date and time
z Connect the plug-in power supply (optional)
1 Press the <M> key and hold it down.
2 Press the <ON/OFF> key.
The display test appears briefly on the display.
3 Press the <RUN/ENTER> key repeatedly until the date ap-
pears on the display.
4 Set the date of the current day with <> <>.
5 Confirm with <RUN/ENTER>.
The date (month) flashes in the display.
S OF
6 Set the current month with <> <>.
7 Confirm with <RUN/ENTER>.
The year appears on the display.
8 Set the current year with <> <>.
9 Confirm with <RUN/ENTER>.
The hours flash on the display.
10 Set the current time with <> <>.
11 Confirm with <RUN/ENTER>.
The minutes flash on the display.
12 Set the current time with <> <>.
13
Commissioning pH/ 3400i
13 Confirm with <RUN/ENTER>.
The instrument switches to a measuring mode.
14 Switch the instrument off using <ON/OFF>.
Connecting the original
plug-in power supply
unit
You can either operate the measuring instrument with batteries or with the plug-in power supply. The plug-in power supply supplies the mea­suring instrument with low voltage (12 VDC). This saves the batteries.
Warning
The line voltage at the operating site must lie within the input voltage range of the original plug-in power supply (see chapter 7 T
TA).
ECHNICAL DA-
Warning
Use original plug-in power supplies only (see chapter 7 T
ECHNICAL DATA).
2
f
e
R
1
3
14
1 Plug the jack (1) into the socket (2) of the measuring instru-
ment.
2 Connect the original WTW plug-in power supply (3) to an easily
accessible mains socket.
pH/ 3400i Operation

4 Operation

4.1 Switching on the measuring instrument

1 Press the <ON/OFF> key.
The display test appears briefly on the display. After this, the measuring instrument automatically switches to the measuring mode.
Note
The measuring instrument has an energy saving feature to avoid un­necessary battery depletion. The energy saving feature switches the measuring instrument off if no key has been pressed for an hour.
The energy saving feature is not active
z if the power is supplied by the plug-in power supply,
z if the AutoStore function is active,
z if the communication cable and a PC with a running communication
program are connected,
z if the printer cable is connected (for external printers).
15
Operation pH/ 3400i

4.2 pH value / ORP voltage

4.2.1 General information

Preparatory activities Perform the following preparatory activities when you want to measure:
1 Connect the pH electrode to the measuring instrument.
If necessary, press the <M> key repeatedly until the status dis- play pH (pH measurement) or U (measurement of the ORP voltage) appears.
2 Adjust the temperature of the buffer solutions or test solutions,
or measure the current temperature, if you measure without a temperature sensor.
3 Calibrate or check the measuring instrument with the elec-
trode.
4Using <> <>, toggle between the pH or mV measuring
modes.
Note
Incorrect calibration of pH electrodes leads to incorrect measured val­ues. Calibrate regularly before measuring.
Warning
When connecting an earthed PC/printer, measurements cannot be per­formed in earthed media as incorrect values would result. The RS232 interface is not galvanically isolated.
Temperature sensor You can measure with or without a temperature sensor. If a tempera-
ture sensor is connected, it is indicated on the display by TP.
Note
The measuring instrument automatically recognizes the type of the temperature sensor used. Therefore, you can connect temperature sensors of the NTC30 or Pt1000 type.
The temperature measurement is absolutely essential for a reproduc­ible pH measurement. If the measurement is made without a tempera­ture sensor, proceed as follows:
16
1 Measure the current temperature of the test sample using a
thermometer.
2 Enter the temperature on the instrument: While pressing the
<RUN/ENTER> key, enter the temperature value of the test sample with <> <>.
pH/ 3400i Operation

4.2.2 Measuring the pH value

1 Perform the preparatory activities according to section 4.2.1.
2 Immerse the pH electrode in the test sample.
3 If required, enter the temperature of the test sample with <>
<> while keeping the <RUN/ENTER> key depressed.
4 Press the <> <> keys until pH appears in the status display.
The pH value appears on the display.
ISE
U
pH
29
8
°F °C
CalError
ARng
mol/L mV/pH % ppm
mg/L
TP
%
TempError
RCL
AR
S
6
1
Time
Day.Month No.
Year
AutoCal DIN
LoBat
AutoCal TEC
Baud
Ident
8
9
2
Auto
ConCal
4
Store
Setting the resolution
AutoRead AR
(drift control)
1 Press the <RUN/ENTER> key and hold it down.
2 Press the <M> key. The measured values are displayed with a
high resolution, e.g. pH = 4.012.
3 Press the <RUN/ENTER> and <M> key once more.
The measured values are displayed with a low resolution, e.g. pH = 4.01.
The AutoRead function (drift control) checks the stability of the mea­surement signal. The stability has a considerable impact on the repro­ducibility of the measured values.
For identical measurement conditions, the following criteria apply:
Reproducibility Response time
Better than 0.02 > 30 seconds
1 Call up the pH measuring mode with <M> and <> <> .
2 Activate the AutoRead function with <AR>.
The current measured value is frozen (hold function).
17
Operation pH/ 3400i
3 Start AutoRead with <RUN/ENTER>.
AR flashes until a stable measured value is reached. This measured value is transmitted to the interface.
4 If necessary, start the next AutoRead measurement with
<RUN/ENTER>.
5 To terminate the AutoRead function: Press the <AR> key.
Note
The current AutoRead measurement can be terminated at any time (accepting the current value) by pressing <RUN/ENTER>.
18
pH/ 3400i Operation

4.2.3 Measuring the ORP voltage

In conjunction with an ORP electrode, e.g. SenTix ORP, the measuring instrument can measure the ORP voltage (mV) of a solution.
1 Perform the preparatory activities according to section 4.2.1.
2 Submerse the ORP electrode in the sample.
3 Press the <> <> keys until the U status display appears.
The ORP voltage (mV) of the test sample appears on the dis­play.
4 Wait for a stable measured value.
ISE
S
6
1
Baud
Time
Day.Month No.
Year
Ident
AutoCal DIN
LoBat
AutoCal TEC
Note
ORP electrodes are not calibrated. However, you can check ORP elec­trodes using a test solution.
9
8
pH
U
2
Auto
ConCal
0
4
Store
5
8
CalError
ARng
mol/L mV/pH
mV % ppm
mg/L
°F
%
°C
TempError
AR
TP
RCL
19
Operation pH/ 3400i

4.3 pH calibration

Why calibrate? pH electrodes age. This changes the asymmetry (zero point) and slope
of the pH electrode. As a result, an inexact measured value is dis­played. Calibration determines the current values of the asymmetry and slope of the electrode and stores them in the measuring instru­ment. Thus, you should calibrate at regular intervals.
When to calibrate? z After connecting another electrode
z When the sensor symbol flashes
(after the calibration interval has expired)
after a voltage interruption, e. g. after changing the batteries
You can select one of 3 calibration procedures:
AutoCal TEC is specially matched to the WTW technical buffer solutions as a fully au-
tomatic two-point calibration. The buffer solutions are automatically recognized by the measuring instrument. Depending on the instrument setting (see section 4.8 C relevant buffer nominal value or the current electrode voltage in mV. The calibration can be terminated after the first buffer solution. This cor­responds to a single-point calibration. When doing so, the instrument uses the Nernst slope (-59,16 mV/pH at 25 °C) and determines the asymmetry of the electrode.
ONFIGURATION), the instrument displays the
AutoCal DIN is specially adapted to the permanently programmed buffer solutions in
ConCal This function is a conventional two-point calibration using two buffer
AutoRead When calibrating with AutoCal TEC and AutoCal DIN, the AutoRead
Displaying the calibra-
tion data
Printing the calibration
record
accordance with DIN 19266 as a fully automatic two-point calibration. The operating sequence of the AutoCal DIN calibration corresponds to that of the AutoCal TEC calibration. The calibration can only be termi­nated after the first buffer solution (single point calibration).
solutions (pH 7.0 ± 0.5 and any other buffer solution) or a single-point calibration using any buffer solution, which is used as a high-speed method.
function is automatically activated. The current AutoRead measurement can be terminated at any time (accepting the current value) by pressing <RUN/ENTER>.
You can view the data of the last calibration on the display. The pro­ceeding is described on page 48.
The calibration protocol contains the calibration data of the current cal­ibration. You can transmit the calibration protocol to a printer via the se­rial interface (see page 51).
20
pH/ 3400i Operation
Note
You can automatically print a calibration protocol after the calibration. To do so, connect a printer to the interface according to section 4.7.2 before calibrating. After a valid calibration, the record is printed.
Sample printout:
CALIBRATION PROTOCOL
02.03.01 14:19 Device No.: 12345678 Calibration pH Cal time: 01.03.01 / 15:20 Cal interval: 7d AutoCal TEC Tauto Buffer 1 2.00 Buffer 2 4.01 Buffer 3 7.00 * Buffer 4 10.00 C1 184.1 mV 25.0°C C2 3.0 mV 25.0°C S1 -59.4 mV/pH ASY1 - 4 mV Probe: +++
Calibration evaluation After the calibration, the measuring instrument automatically evaluates
the calibration. The asymmetry and slope are evaluated separately. The worst evaluation appears on the display.
Display Asymmetry
[mV]
Slope [mV/pH]
-15 ... + 15 -60.5 ... -58
-20 ... +20 -58 ... -57
-25 ... +25 -61 ... -60.5 or
-57 ... -56
-30 ... +30 -62 ... -61 or
-56 ... -50
Clean the electrode according to the electrode operating manual
E3
Eliminate the error according to chap­ter 6 W
HAT TO DO IF...
< -30 or > 30
... -62 or ... -50
21
Operation pH/ 3400i
Preparatory activities
1 Connect the pH electrode to the measuring instrument.
If necessary, press the <M> key repeatedly until the status dis- play pH (pH measurement) or U (measurement of the ORP voltage) appears.
2 Keep the buffer solutions ready.
3 Adjust the temperature of the solution and measure the current
temperature if the measurement is made without the use of a temperature sensor (the TP display indicator is missing from the display).

4.3.1 AutoCal TEC

For this procedure, use any two WTW technical buffer solutions (pH values at 25 °C: 2.00 / 4.01 / 7.00 / 10.01).
Note
The calibration for pH 10.01 is optimized for the WTW technical buffer solution TEP 10 Trace or TPL 10 Trace. Other buffer solutions can lead to an erroneous calibration. The correct buffer solutions are given in the WTW catalog or in the Internet.
Note
The buffer solutions are automatically recognized by the measuring in­strument. Depending on the instrument setting (see section 4.8 C
ONFIGURATION ), the instrument displays the relevant buff-
er nominal value or the current electrode voltage in mV.
Note
Skip the steps 2 and 7 if you use a pH electrode with a temperature sensor.
1 Press the <CAL> key repeatedly until the Ct1 display indicator
and the function display AutoCal TEC appears. The sensor symbol displays the evaluation of the last calibration (or no sensor symbol in the delivery state or after the measurement parameters have been reset).
22
pH/ 3400i Operation
Lin
8
Tref20
1
8
pH
t
2
Cal
U
pH
2
Auto
ConCal
OU
1
4
AutoCal DIN
AutoCal TEC
3
4
Store
Sal
mV
%
m
mbar
8
Auto
ARng
3
°F °C
8
CalError
ARng
/pH
mg/l
S/
cm
M
cm
1/
°
%
°
C
F
Store
AR
mol/L mV/pH
mV % ppm
mg/L
%
TempError
AR
cm
Sal
K
/
RCL
TP
RCL
TP
S
7
1
Baud
Time
Day.Month No.
Year
Ident
AutoCal DIN
LoBat
AutoCal TEC
ISE
0
8
U
pH
2
Auto
ConCal
0
4
Store
0
8
CalError
ARng
mol/L mV
mV/pH % ppm
mg/L
°F
%
°C
TempError
AR
TDS
S
C
1
Baud
Time
Day.Month No.
Year
Ident
Tref25
LoBat
nLF
2 If required, enter the temperature of the first buffer solution with
<> <> while keeping the <RUN/ENTER> key depressed.
3 Immerse the pH electrode in the first buffer solution.
4 Press the <RUN/ENTER> key.
The AR display indicator flashes. The electrode voltage (mV) or the buffer nominal value ap­pears on the display. Example:
ISE
S
6
1
Baud
Time
Day.Month No.
Year
Ident
AutoCal DIN
LoBat
AutoCal TEC
TP
RCL
5 When the measured value is stable, Ct2 appears.
ISE
U
pH
2C
8
°F °C
CalError
ARng
mol/L mV/pH % ppm
mg/L
TP
%
TempError
RCL
AR
23
S
6
1
Baud
Time
Day.Month No.
Year
Ident
AutoCal DIN
LoBat
AutoCal TEC
Note
At this point, the AutoCal TEC calibration can be terminated with <M>. This corresponds to a single-point calibration. When doing so, the in-
8
t
2
Auto
ConCal
4
Store
Operation pH/ 3400i
strument uses the Nernst slope (-59,16 mV/pH at 25 °C) and deter­mines the asymmetry of the electrode.
6 Thoroughly rinse the electrode with deionized water.
7 If required, enter the temperature of the second buffer solution
with <> <> while keeping the <RUN/ENTER> key de- pressed.
8 Immerse the pH electrode in the second buffer solution.
9 Press the <RUN/ENTER> key.
The AR display indicator flashes. The electrode voltage (mV) or the buffer nominal value ap­pears on the display. Example:
ISE
U
pH
8
45
0
mV/pH
mV % ppm
°F °C
CalError
ARng
°F
°C
CalError
ARng
mol/L
mg/L
TP
%
TempError
RCL
AR
mol/L mV/pH % ppm
mg/L
%
TempError
AR
1
TP
RCL
S
80
1 4
1
Baud
Time
Day.Month No.
Year
Ident
AutoCal DIN AutoCal DIN
LoBat
10 When the measured value is stable, AR disappears. The value
of the slope (mV/pH) appears on the display. The probe symbol shows the evaluation of the current calibration.
ISE
8
2
Auto
ConCal
U
pH
4
4
Store
S
6
1
Time Day.Month No.
Year
AutoCal DIN
LoBat
AutoCal TEC
Baud
Ident
8
9
s
Auto
ConCal
L
Store
ISE
S
Baud
Time
Day.Month No.
Year
Ident
LoBat
AutoCal TECAutoCal TEC
0
8
U
pH
2
Auto
ConCal
0
4
Store
8
8
CalError
ARng
mol/L
mV
mV/pH % ppm
mg/L
°F
%
°C
TempError
AR
TP
RCL
24
11 Press the <RUN/ENTER> key. The value of the asymmetry
(mV) appears on the display.
pH/ 3400i Operation
ISE
U
pH
4
y
CalError
ARng
mol/L mV/pH
mV % ppm
mg/L
°F
%
°C
TempError
AR
TP
RCL
S
5
6
1
Baud
Time
Day.Month No.
Year
Ident
AutoCal DIN
LoBat
AutoCal TEC
12 Switch to the measuring mode with <M>.
8
9
a
Auto
ConCal
s
Store
25
Loading...
+ 58 hidden pages