Xylem Oxi 1970i User Manual
Oxi 1970i
ON / OFF
CAL
O
7
92
1 7 6
°
C
R
A
R
n
g
RCL
M
AUTO READ
RUN / ENTER
E
STO
Operating manual
m
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l
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Oxi 1970i
ba75691e01 01/2007
Portable oxygen measuring instrument
Oxi 1970i
Accuracy when
going to press
The use of advanced technology and the high quality standard of our
instruments are the result of a continuous development. This may result in differences between this operating manual and your instrument.
Also, we cannot guarantee that there are absolutely no errors in this
manual. Therefore, we are sure you will understand that we cannot accept any legal claims resulting from the data, figures or descriptions.
Copyright
© Weilheim 2007, WTW GmbH
Reproduction in whole - or even in part - is prohibited without the express written permission of WTW GmbH, Weilheim.
Printed in Germany.
2
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Oxi 1970i Contents
Oxi 1970i - Contents
1 Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
1.1 Display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
1.2 Keypad . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
1.3 Socket field . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
2 Safety . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.1 Authorized use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.2 General safety instructions . . . . . . . . . . . . . . . . . . . . . . . 10
3 Commissioning. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
3.1 Scope of delivery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
3.2 Power supply . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
3.3 Initial commissioning . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
3.4 Sensor quiver . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
4 Operation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
4.1 Switching on the measuring instrument . . . . . . . . . . . . . 15
4.2 Measuring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
4.2.1 General information . . . . . . . . . . . . . . . . . . . . . . 16
4.2.2 Measuring the D. O. concentration . . . . . . . . . . 17
4.2.3 Measuring the D. O. saturation . . . . . . . . . . . . . 18
4.2.4 Automatic selection of the measuring range,
AutoRange . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
4.2.5 AutoRead AR (drift control) and hold function . . 19
4.2.6 Sensor with stirrer (StirrOx G) . . . . . . . . . . . . . . 20
4.3 Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
4.3.1 Calibrating with the air calibration vessel . . . . . 23
4.3.2 Calibrating via a comparison measurement . . . 25
4.3.3 Entering the salt content (salinity) . . . . . . . . . . . 27
4.4 Saving . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
4.4.1 Saving manually . . . . . . . . . . . . . . . . . . . . . . . . 28
4.4.2 Saving automatically . . . . . . . . . . . . . . . . . . . . . 30
4.4.3 Outputting the data storage . . . . . . . . . . . . . . . . 32
4.4.4 Clearing the memory . . . . . . . . . . . . . . . . . . . . . 36
4.5 Transmitting data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
4.5.1 Data transmission interval (Int 2) . . . . . . . . . . . 37
4.5.2 Recorder (analog output) . . . . . . . . . . . . . . . . . 39
4.5.3 PC/external printer (RS232 interface) . . . . . . . . 40
4.5.4 Remote control . . . . . . . . . . . . . . . . . . . . . . . . . 40
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Contents Oxi 1970i
4.6 Configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41
4.7 Reset . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
5 Maintenance, cleaning, disposal . . . . . . . . . . . . . . . . . 47
5.1 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
5.2 Cleaning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
5.3 Disposal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
6 What to do if... . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49
7 Technical data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
7.1 General data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
7.2 Measuring ranges, resolutions, accuracies . . . . . . . . . . 56
8 Lists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
4
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Oxi 1970i Overview
RUN / ENTER
1Overview
The portable Oxi 1970i measuring instrument enables you to carry out
oxygen measurements rapidly and reliably.
The Oxi 1970i provides the maximum degree of operating comfort, reliability and measuring certainty for all applications.
The proven OxiCal
®
calibration procedure supports you in your work
with the measuring instrument. The special AutoRead function enables
precise measurements.
1
ON / OFF
M
AUTO READ
RUN / ENTER
CAL
2
O
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°
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Oxi 1970i
3
4
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5
1 Keypad
2 Display
3 Integrated, exchangeable sensor quiver
4 Socket field
5 Carrying and positioning handle
5
Overview Oxi 1970i
Note
If you need further information or application notes, you can obtain the
following material from WTW:
z Application reports
z Primers
z Safety datasheets.
You will find information on available literature in the WTW catalog or
via the Internet.
1.1 Display
Status display indicator
pH
O
Sal
Time
Day.Month
Year
LoBat
S
1
Baud
No.
Ident
Tref25 Tref20
nLF
Lin
8
88
8 8 8 8
Store
Auto
Cal
TEC
Oxi
ARng
%
m
1/
°
S/
C
pHmV/
mg/l
cm
cm
K
%
/
AR
Sal
TP
REL2REL1
RCL
Sensor symbol
Measured value
display
Function and
Temperature display
6
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Oxi 1970i Overview
RCL
STO
1.2 Keypad
Key functions
ON / OFF
M
CAL
AUTO READ
RUN / ENTER
Calibrate
Switch measuring instrument on/off
<ON/OFF>
Select the measuring mode <M>:
– D. O. concentration
– Oxygen saturation
<CAL>
Activate/deactivate the AutoRead function
<AUTO READ>
Confirm entries, start AutoRead,
output measured values
<RUN/ENTER>
Select the measuring mode, increase values,
scroll
<▲ >
Select the measuring mode, decrease values,
scroll
<▼ >
RCL
STO
Display/transmit measured values
<RCL>
Save a measured value
<STO>
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7
Overview Oxi 1970i
1.3 Socket field
Sensors You can use the following sensors with the Oxi 1970i:
z Oxygen depth armature
z D. O. sensor CellOx 325, or
z D. O. sensor DurOx 325, or
z Self-stirring D. O. sensor StirrOx G
Connectors
2
3
4
1
5
Sensor / Instrument Socket
Oxygen sensor 1
Integrated stirrer StirrOx G 2
Printer or PC (serial interface, RS232) 3
Plug-in power supply unit 4
Watertight valve for internal pressure equalization 5
Warning
Only connect sensors to the measuring instrument that cannot return
any voltages or currents that are not allowed (> SELV and > current circuit with current limiting). Nearly all sensors - especially WTW sensors
- fulfill these conditions.
8
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Oxi 1970i Safety
2 Safety
This operating manual contains basic instructions that you must follow
during the commissioning, operation and maintenance of the measuring instrument . Consequently, all responsible personnel must read this
operating manual before working with the measuring system. The operating manual must always be available within the vicinity of the measuring system.
Target group The measuring instrument was developed for work in the field and in
the laboratory.
We assume that, as a result of their professional training and experience, the operators will know the necessary safety precautions to take
when handling chemicals.
Safety
instructions
Further notes
The individual chapters of this operating manual use safety instructions
such as the label shown below to indicate various hazards or dangers:
Warning
indicates instructions that must be followed precisely in order to avoid
the possibility of slight injuries or damage to the instrument or the environment.
Note
indicates notes that draw your attention to special features.
Note
indicates cross-references to other documents, e.g. operating manuals.
2.1 Authorized use
The authorized use of the measuring instrument consists exclusively of
the measurement of the dissolved oxygen (D. O.) content of liquid media in the field and laboratory.
The technical specifications as given in chapter 7 T
be observed. Only the operation and running of the measuring instrument according to the instructions given in this operating manual is authorized.
Any other use is considered to be unauthorized.
ECHNICAL DATA must
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9
Safety Oxi 1970i
2.2 General safety instructions
This instrument is built and inspected according to the relevant guidelines and norms for electronic measuring instruments (see chapter
7T
ECHNICAL DATA).
It left the factory in a safe and secure technical condition.
Function and operating
safety
Safe operation If safe operation is no longer possible, the instrument must be taken out
The smooth functioning and operational safety of the measuring instrument can only be guaranteed if the generally applicable safety measures and the specific safety instructions in this operating manual are
followed during operation.
The smooth functioning and operational safety of the measuring instrument can only be guaranteed under the environmental conditions that
are specified in chapter 7 T
ECHNICAL DATA.
If the instrument was transported from a cold environment to a warm
environment, the formation of condensate can lead to the faulty functioning of the instrument. In this event, wait until the temperature of the
instrument reaches room temperature before putting the instrument
back into operation.
of service and secured against inadvertent operation!
Safe operation is no longer possible if the measuring instrument:
z has been damaged in transport
z has been stored under adverse conditions for a lengthy period of
time
10
Obligations
of the purchaser
z is visibly damaged
z no longer operates as described in this manual.
If you are in any doubt, please contact the supplier of the instrument.
The purchaser of the measuring instrument must ensure that the following laws and guidelines are observed when using dangerous substances:
z EEC directives for protective labor legislation
z National protective labor legislation
z Safety regulations
z Safety datasheets of the chemical manufacturers.
ba75691e01 01/2007
Oxi 1970i Commissioning
3 Commissioning
3.1 Scope of delivery
z Portable measuring instrument, Oxi 1970i with integrated recharge-
able battery
z Carrying and positioning handle
z Carrying strap
z Sensor quiver
z Plug-in power supply unit
z Operating manual
3.2 Power supply
Mains operation and
charging the battery
Charging time of the
battery
You can either operate the measuring instrument with the integrated rechargeable battery or with the plug-in power supply. The plug-in power
supply supplies the measuring instrument with low voltage (12 V DC).
At the same time, the rechargeable battery is charged.
Note
The automatic stirring function of the self-stirring D. O. sensor
StirrOx G can only be used when the plug-in power supply is connected.
approx. 16 hours. The battery is charged even when the instrument is
switched off. The LoBat display indicator appears when the battery is
nearly empty and has to be charged as soon as possible.
Warning
The line voltage at the operating site must lie within the input voltage
range of the original plug-in power supply (see chapter 7 T
TA).
ECHNICAL DA-
Warning
Use original plug-in power supplies only (see
chapter 7 T
ECHNICAL DATA).
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11
Commissioning Oxi 1970i
Connecting the plug-in
power supply unit
2
1
3
Setting the date and
time
1 Connect the plug (1) to the socket (2) of the measuring instru-
ment.
2 Connect the original WTW plug-in power supply (3) to an easily
accessible mains socket.
3.3 Initial commissioning
Perform the following activities:
z For mains operation and charging the battery: Connect the plug-in
power supply (see section 3.2 P
z Set the date and time.
1 Press the <M> key and hold it down.
2 Press the <ON/OFF> key.
The display test appears briefly on the display.
3 Press the <RUN/ENTER> key repeatedly until the date flashes
on the display (Day.Month display indicator).
OWER SUPPLY).
12
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Oxi 1970i Commissioning
m
%
1/
°
mg/l
S/
cm
%
C
REL1
AR
pH/mV
cm
K
/
Sal
TP
REL2
RCL
pH
O
Sal
Time
Day.Month
Year
LoBat
S
I
Baud
No.
Ident
0 9 0 4
Tref25
Tref20
nLF
Lin
5t2
Auto
Store
Cal
Oxi
TEC
ARng
4 Set the date of the current day with <▲> <▼>.
5 Confirm with <RUN/ENTER>.
The date (month) flashes in the display.
6 Set the current month with <▲> <▼>.
7 Confirm with <RUN/ENTER>.
The year appears on the display.
8 Set the current year with <▲> <▼>.
9 Confirm with <RUN/ENTER>.
The hours flash on the display.
10 Set the current time with <▲> <▼>.
11 Confirm with <RUN/ENTER>.
The minutes flash on the display.
12 Set the current time with <▲> <▼>.
13 Confirm with <RUN/ENTER>.
The instrument switches to the measuring mode.
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Commissioning Oxi 1970i
3.4 Sensor quiver
To store the sensors during field operation and to keep the sensor element moist, the quiver tip contains a sponge rubber insert that can be
moistened with deionized water.
Note
For further details on proper storage, refer to the operating manual of
the sensor.
Moistening the
quiver insert
1 Press the quiver out of the holder from the back side of the in-
strument and pull it out completely.
2 Pull off the quiver tip and moisten the sponge rubber with
deionized water.
14
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Oxi 1970i Operation
4 Operation
4.1 Switching on the measuring instrument
1 Connect the D. O. sensor to the measuring instrument.
2 Press the <ON/OFF> key.
The display test appears briefly on the display.
The relative slope for the sensor type that was just connected
subsequently appears for approx. one second.
The measuring instrument then automatically switches to the
measuring mode that was last selected. The display shows the
relevant measured value.
Note
The measuring instrument has an energy saving feature to avoid unnecessary battery depletion. The energy saving feature switches the
measuring instrument off if no key has been pressed for an hour. The
energy saving feature is not active when the AutoStore function is active.
The energy saving feature is also not active
z if the power is supplied by the plug-in power supply,
z if the communication cable and a PC with a running communication
program are connected,
z if the recorder cable is connected,
z if the printer cable is connected (for external printers).
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Operation Oxi 1970i
4.2 Measuring
4.2.1 General information
You can measure the following variables:
z D. O. concentration
z D. O. saturation
The measuring instrument is supplied with the following functions:
z AutoRange (automatic switchover of the measurement range). If a
measuring range is exceeded, AutoRange causes the measuring instrument to change automatically to the next higher measuring
range and back again. Therefore, the instrument always measures
in the measuring range with the highest possible resolution. The
function can be switched off.
z The AutoRead function (drift control) for checking the stability of the
measurement signal. This ensures the reproducibility of the measuring signal. For details of how to switch the AutoRead function on/off,
see page 19.
Preparatory activities Perform the following preparatory activities when you want to measure:
1 Connect the D. O. sensor to the measuring instrument (see
section 1.3 S
OCKET FIELD).
2 Calibrate or check the measuring instrument with the D. O.
sensor. How to calibrate is described in section 4.3.
3 Select the measuring mode with <M>.
Note
Incorrect calibration of D. O. sensors will result in incorrect measured
values. Calibrate at regular intervals.
Note
The measuring instrument automatically recognizes the type of the D.
O. sensor (CellOx 325 or DurOx 325).
Temperature sensor The D. O. sensor has an integrated temperature sensor that always
measures the current temperature of the test sample.
16
Warning
When connecting an earthed PC/printer, measurements cannot be performed in earthed media as incorrect values would result. The RS232
interface is not galvanically isolated.
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Oxi 1970i Operation
4.2.2 Measuring the D. O. concentration
Note
When measuring the concentration of test samples with a salt content
of more than 1 g/l, a salinity correction is required. For this, you have to
measure and input the salinity of the measured medium first. This is described in section 4.3.3 on page 27.
Switching the salt content correction on or off, see below.
To measure the D. O. concentration with and without salt content correction, proceed as follows:
1 Perform the preparatory activities according to section 4.2.1.
2 Immerse the D. O. sensor in the test sample.
3 Press the <M> key repeatedly until the D. O. concentration in
mg/l appears on the display.
Switching on/off the salt
content correction
m
m
%
1/
°
%
1/
°
mg/l
S/
cm
%
C
REL1
AR
mg/l
S/
cm
%
C
REL1
AR
pH/mV
cm
K
/
REL2
pH/mV
cm
K
/
REL2
Sal
TP
RCL
Sal
TP
RCL
pH
S
O
Sal
Time
Day.Month
Year
LoBat nLF
Proceed as follows to switch on the salt content correction:
1 In the D. O. concentration measuring mode, switch on the salt
pH
7
Lin
8
Oxi
92
1 7 6
Auto
Store
Cal
TEC
ARng
1
Baud
No.
Ident
Tref25 Tref20
content correction with <▲ > . The SAL display indicator appears on the display. The value that was entered is taken into
consideration during the measurement (see section 4.3.3).
S
O
Sal
Time
Day.Month
Year
LoBat nLF
1
Baud
No.
Ident
Tref25 Tref20
Lin
5
8
1 7 6
Oxi
42
Auto
Store
Cal
TEC
ARng
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2 Switch the salt content correction off with <▼ >. The SAL dis-
play indicator is no longer displayed.
17
Operation Oxi 1970i
4.2.3 Measuring the D. O. saturation
You can measure the D. O. saturation as follows:
1 Perform the preparatory activities according to section 4.2.1
2 Immerse the D. O. sensor in the test sample.
3 Press the <M> key repeatedly until the saturation in % appears
on the display.
/mV
%
m
1/
°
S/
C
pH
mg/l
cm
cm
%
/
REL1
AR
K
Sal
TP
REL2
RCL
pH
S
O
Sal
1
Time
Day.Month
Year
LoBat nLF
8
Baud
No.
Ident
8
Tref25 Tref20
Lin
Oxi
92
1 7 6
Auto
Store
Cal
TEC
ARng
4.2.4 Automatic selection of the measuring range, AutoRange
Sensors You can use the sensors listed in section 1.3 on page 8. The sensor
type is automatically recognized and the resolution is adjusted if necessary (see chapter 7 T
AutoRange Two measuring ranges are available for each measuring mode. If a
measuring range is exceeded, AutoRange causes the measuring instrument to change automatically to the next higher measuring range
and back again. Therefore, the instrument always measures in the
measuring range with the highest possible resolution.
To switch the automatic measurement range selection on/off, see
section 4.6 C
on, ARng appears on the display.
pH
S
ONFIGURATION. When the AutoRange function is switched
O
Sal
Time
Day.Month
Year
LoBat nLF
1
Baud
No.
Ident
Tref25 Tref20
7
8
Lin
Oxi
08
1 7 6
Auto
Cal
ECHNICAL DATA).
mg/l
%
m
S/
1/
cm
%
°
ARng
C
REL1
AR
Store
TEC
pH/mV
cm
K
/
REL2
Sal
TP
RCL
18
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Oxi 1970i Operation
4.2.5 AutoRead AR (drift control) and hold function
The AutoRead function (drift control) checks the stability of the measurement signal. The stability has a considerable impact on the reproducibility of the measured values. With the aid of the hold function the
measured value display is frozen.
Criteria With identical measurement conditions, the following criteria are valid
for the AutoRead function:
Measuring mode Reproducibility Response time
D. O. concentration
D. O. saturation
index
Use the AutoRead function and hold function like this with the sensors
z Oxygen depth armature
z CellOx 325
z DurOx 325
Note
The special features of the self-stirring D. O. sensor StirrOx G can be
found in section 4.2.6 on page 20.
1 Select the measuring mode with <M>.
2 Activate the AutoRead function with <AR>. The current mea-
sured value is frozen (hold function).
3 Start AutoRead with <RUN/ENTER>.
AR flashes until a stable measured value is reached.
better than 0.05 mg/l > 10 seconds
better than 0.6 % > 10 seconds
ba75691e01 01/2007
m
%
1/
°
mg/l
S/
cm
%
C
REL1
AR
pH/mV
cm
K
/
Sal
TP
REL2
RCL
pH
S
O
Sal
Time
Day.Month
Year
LoBat nLF
4 If necessary, start the next AutoRead measurement with
7
Lin
8
Oxi
08
1 7 6
Auto
Cal
1
Baud
No.
Ident
Tref25 Tref20
<RUN/ENTER>.
Store
TEC
ARng
19
Operation Oxi 1970i
5 To terminate the AutoRead function: Press the <AR> key.
4.2.6 Sensor with stirrer (StirrOx G)
Connection Connect the 2-pole stirrer plug to the stirrer output of the measuring in-
strument (designation REL1).
Note
The automatic stirring function of the self-stirring D. O. sensor
StirrOx G can only be used when the plug-in power supply is connected.
Stirrer function The D. O. sensor, StirrOx G, has a temperature sensor and stirrer inte-
grated. Using the key on the sensor you switch the stirrer on.
Measuring with
AutoRead
You can switch on the stirrer and start an AutoRead measurement at
the same time. To do so, proceed as follows:
1 Select the measuring mode with <M>.
2 Activate the AutoRead function with <AR>. The current mea-
sured value is frozen (hold function).
3 Submerse the sensor in the test sample and press the stirrer
button. The stirrer is startet. At the same time, the AutoRead
measurement starts. AR flashes until a stable measured value
is achieved. Subsequently, the stirrer switches itself off.
%
m
1/
°
S/
C
pH/mV
mg/l
cm
cm
%
/
REL1
AR
K
Sal
TP
REL2
RCL
pH
S
O
Sal
1
Time
Day.Month
Year
LoBat nLF
7
Baud
No.
Ident
8
Tref25 Tref20
Lin
Oxi
08
1 7 6
Auto
Store
Cal
TEC
ARng
20
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