BUCHI K-449 User Manual

KjelDigester K-446/K-449
Operation Manual
11593546 en
Imprint
Product Identification: Operation Manual, KjelDigester K-446/K-449 115 9354 6 en
Publication date:
BÜCHI Labortechnik AG Meierseggstrasse 40 Postfach CH-9230 Flawil 1
E-Mail: quality@buchi.com
BUCHI reserves the right to make changes to the manual as deemed necessary in the light of experience; espe­cially in respect to structure, illustrations and technical detail.
This manual is copyright. Information from it may not be reproduced, distributed, or used for competitive purpos­es, nor made available to third parties. The manufacture of any component with the aid of this manual without prior written agreement is also prohibited.
Table of contents
1 General 7
1.1 About this manual ...................................................................................... 7
1.1.1 Structure of the manual .................................................................... 7
1.1.2 Additional user information ............................................................... 8
1.1.3 Available languages .......................................................................... 8
1.1.4 Reference documents ...................................................................... 8
1.1.5 Abbreviations ................................................................................... 8
1.2 About the KjelDigester K-446/K-449 .......................................................... 9
1.2.1 General information .......................................................................... 9
1.2.2 Type plate ........................................................................................ 9
1.3 Scope of delivery ...................................................................................... 10
2 Safety 11
2.1 User qualifications .................................................................................... 11
2.2 Proper use ............................................................................................... 11
2.3 Safety warnings ....................................................................................... 11
2.3.1 Warning explanation ....................................................................... 11
2.3.2 Symbols ......................................................................................... 12
2.4 General safety rules .................................................................................. 13
2.4.1 Responsibility of the operator ......................................................... 13
2.4.2 Duty of maintenance and care........................................................ 13
2.4.3 Spare parts to be used .................................................................. 13
2.4.4 Modifications ................................................................................. 13
2.5 Product safety .......................................................................................... 14
2.5.1 General hazards ............................................................................. 14
2.5.2 Specific hazard .............................................................................. 15
2.5.3 Personal protective equipment ....................................................... 16
2.5.4 Built-in safety elements and measures ........................................... 16
3 Technical data 17
3.1 Device dimensions ................................................................................... 17
3.1.1 K-446 ............................................................................................ 17
3.1.2 K-449 ............................................................................................ 17
3.2 General technical data .............................................................................. 17
3.2.1 Electrical system ............................................................................ 18
3.2.2 Environmental conditions ............................................................... 18
4 Description of function 19
4.1 Purpose and design ................................................................................. 19
4.2 KjelDigester overview ............................................................................... 19
4.2.1 Front and side view ........................................................................ 19
4.2.2 Rear view ....................................................................................... 20
4.2.3 Top-side view ................................................................................. 20
3Operation Manual KjelDigester K-446/K-449
4.3 Function ................................................................................................... 21
4.3.1 Digestion process .......................................................................... 21
4.4 Control panel ........................................................................................... 22
4.4.1 Control panel display ...................................................................... 22
4.4.2 Control panel buttons..................................................................... 22
4.4.3 Scrubber control (K-449 only) ........................................................ 23
4.5 Rack, cooling and heating position ........................................................... 24
4.6 Functionality comparison K-446/K-449 .................................................... 24
5 Installation 25
5.1 Unpacking ................................................................................................ 25
5.2 Preparation for assembly .......................................................................... 25
5.3 Transport lock, removal ............................................................................ 26
5.4 Device assembly ...................................................................................... 26
5.4.1 Drip tray, installation ....................................................................... 26
5.4.2 Suction module, installation ............................................................ 27
5.4.3 Scrubber/water jet pump, connection ............................................ 27
5.4.4 Device fixation (earthquake) ............................................................ 29
5.4.5 Electrical connection ...................................................................... 29
5.5 Settings .................................................................................................... 29
5.5.1 Accessing the settings menu ......................................................... 29
5.5.2 Adjust the contrast ......................................................................... 30
5.5.3 Adjust the maximum temperature .................................................. 30
5.5.4 Adjust the temperature offset ......................................................... 31
5.5.5 Set the clock (K-449 only) .............................................................. 31
5.5.6 Adjust the Scrubber control (K-449 only) ........................................ 31
5.6 User protection shield, installation ............................................................ 32
5.7 Condensate bottle, installation ................................................................. 33
5.8 Air supply hose, installation ...................................................................... 34
6 Operation 35
6.1 General application information ................................................................ 35
6.2 Start a digestion ....................................................................................... 36
6.3 Set parameters for manual digestion ........................................................ 36
6.3.1 K-446 ............................................................................................ 36
6.3.2 K-449 ............................................................................................ 37
6.4 Editing parameters during a digestion ...................................................... 37
6.5 Abort a digestion ...................................................................................... 38
6.6 Switch off the KjelDigester ........................................................................ 38
6.7 KjelDigester K-446 ................................................................................... 39
6.7.1 Digestion process .......................................................................... 39
6.8 KjelDigester K-449 ................................................................................... 40
6.8.1 Digestion process, manual mode ................................................... 40
4 KjelDigester K-446/K-449 Operation Manual
6.8.2 Digestion process, automatic mode ............................................... 41
6.8.3 Digestion process, delayed start .................................................... 42
6.8.4 Set parameters for an automatic digestion ..................................... 43
6.8.5 Edit a method ................................................................................ 44
6.8.6 Select a method ............................................................................. 44
6.8.7 Set up a delayed start time ............................................................ 44
6.8.8 Moving the lift up or down .............................................................. 45
7 Maintenance 47
7.1 Maintenance plan ..................................................................................... 47
7.1.1 Maintenance as required/after use ................................................. 47
7.1.2 Daily maintenance .......................................................................... 47
7.1.3 Maintenance every week ................................................................ 47
7.1.4 Maintenance every year or after every 1000 digestion cycles.......... 48
7.1.5 Maintenance every 3 years ............................................................. 48
7.2 Cleaning ................................................................................................... 48
7.2.1 KjelDigester, cleaning ..................................................................... 48
7.2.2 Scrubber hose, cleaning ................................................................ 49
7.2.3 Suction module sealing and spring, cleaning .................................. 49
7.2.4 Sample tube, cleaning ................................................................... 49
7.3 Suction module sealing and spring ,replacement ...................................... 50
7.4 Fuse power supply, replacement .............................................................. 51
7.5 Rechargeable battery (K-449 only), replacement ...................................... 52
7.6 Suction module, removal .......................................................................... 54
8 Troubleshooting 55
8.1 Customer service ..................................................................................... 55
8.2 Error messages on the display ................................................................. 55
8.3 Faults ....................................................................................................... 56
8.3.1 Broken sample tube during digestion ............................................. 56
8.3.2 Power supply failure [ERR1] during a digestion .............................. 57
8.3.3 Sample tubes jam in the heating block (K-449 only) ....................... 57
8.4 Checks .................................................................................................... 57
8.4.1 Suction module sealing and spring, check ..................................... 57
8.4.2 Glass parts, check ......................................................................... 58
8.4.3 Rechargeable battery (K-449 only), check ...................................... 58
9 Taking out of operation 61
9.1 Transport .................................................................................................. 61
9.2 Taking out of operation ............................................................................. 61
9.3 Materials used .......................................................................................... 62
5Operation Manual KjelDigester K-446/K-449
10 Spare parts 63
10.1 General information .................................................................................. 63
10.2 Spare parts KjelDigester K-446/K-449 ..................................................... 64
10.3 Optional accessories ................................................................................ 67
10.3.1 Kjeldahl Tablets .............................................................................. 68
11 Appendix 69
11.1 FCC requirements (for USA and Canada) ................................................. 69
11.2 Declaration of conformity .......................................................................... 70
Index .................................................................................. 71
6 KjelDigester K-446/K-449 Operation Manual

1 General

This manual describes the KjelDigester K-446 and K-449 and provides all information required for its safe operation and to maintain it in good working order.
It is addressed to laboratory personnel in particular.

1.1 About this manual

Read this manual carefully before installing and running the device. Note the safety precautions in chapter 2 in particular. Store the manual in the immediate vicinity of the device, so that it can be consulted at any time.

1.1.1 Structure of the manual

The operation manual consists of 11 chapters which cover all information relevant to the opera­tor of the device.
1 General
Chapter Meaning
1 General Gives a general overview about the manual and device. It also
gives a brief information on how to use this manual and other general information.
2 Safety Describes the safety concept of the device and contains gen-
eral rules of behavior and warnings from hazards concerning the use of the product.
3 Technical data Introduces the reader to the device specifications. It contains
technical data, requirements and performance data.
4 Description of function Explains the basic principle of the device, shows how it is
structured and gives a functional description of the assem­blies.
5 Installation Describes how the device is installed and gives instructions on
initial startup.
6 Operation Gives examples of typical device applications and instructions
on how to operate the device properly and safely.
7 Maintenance Gives instructions on all maintenance work to be performed in
order to keep the device in good working condition.
8 Troubleshooting Helps to resume operation after a minor problem has oc-
curred. It lists possible occurrences, their probable cause and suggests how to remedy the problem. Explains checks for troubleshooting and maintenance.
9 Taking out of operation Instructs how to store and dispose the device. It also instructs
users for the reuse after a storage period.
10 Spare parts Lists spare parts, accessories, and options including their
ordering information.
11 Appendix Additional documents regarding requirements.
1 – 7Operation Manual KjelDigester K-446/K-449
1 General

1.1.2 Additional user information

Page number
The page number in the footer contains the current chapter (e.g. 1 – 12) and the page number (e.g. 1 – 12).
Cross-references
Cross-References consist at least the chapter and the page number (1 – 12).
NOTE
Paragraphs starting with NOTE transport helpful information for working with the device/software. NOTE’s are not related to any kind of hazard or damage.

1.1.3 Available languages

This operation manual is available in the following languages:
Language Order number
English 115 93 54 6 German 115 93 547 French 11593548 Italian 115 93 54 9 Spanish 1159 35 50 Chinese 115 93 5 51 Japanese 115 93 55 2

1.1.4 Reference documents

Scrubber K-415
Language Order number
English 115 93 50 5 German 115 93 50 6 French 1159 35 07 Italian 1159 3 50 8 Spanish 1159 35 09 Chinese 115 93 510 Japanese 115 93 511

1.1.5 Abbreviations

EPDM Ethylene propylene diene monomer
FCC Federal Communications Commission
TKN Total Kjeldahl nitrogen
METH Method
1 – 8
KjelDigester K-446/K-449 Operation Manual
MSDS Material safety data sheets
No Number
Pcs Pieces
PTFE Polytetrafluoroethylene
Qty Quantity

1.2 About the KjelDigester K-446/K-449

1.2.1 General information

No technical modifications may be made to the device without the prior written agreement of BUCHI. Unauthorized modifications may affect the system safety or result in accidents.

1.2.2 Type plate

Type plate is located on the right side of the KjelDigester.
1 General
Fig. 1.1 Key of type plate (example)
a Device name e Maximum power rating b Serial number f Year of manufacture c Input voltage range g Country of manufacture d Frequency of input voltage
1 – 9Operation Manual KjelDigester K-446/K-449
1 General

1.3 Scope of delivery

Description Qty Order number
KjelDigester
∙ K-446 with standard suction module ∙ K-446 suction module with condensate trap ∙ K-449 with standard suction module ∙ K-449 suction module with condensate trap
1 – – – –
1154461000
1154462000
1154491000
1154492000 Drip tray holder 1 110 59 8 04 Drip tray 1 110 59 031 Sample tube, 300 mL (4 pcs.) 5 037377 Rack 1 110 59 831 Hose 1.5m, 8mm 1 11056005 Hose connector S19 1 110 57159 Clamp S19 1 110 57149 Power supply cable
∙ Type C H ∙ Type Schuko ∙ Type GB ∙ Type U SA ∙ Type AUS
1 – – – – –
010010 010016 0178 35
033763
0178 36
1 – 10
KjelDigester K-446/K-449 Operation Manual

2 Safety

The safety of the user and personnel can only be ensured if the safety instructions and the safety related warnings in the individual chapters are strictly observed and followed. Therefore, the manual must always be available to all persons performing tasks described herein.
2.1 User qualifications
Before using the KjelDigester the operation manual must be read and understood.
The device may only be used by laboratory personnel and other persons who on account of training or professional experience have an overview of the dangers which can develop when operating the device.

2.2 Proper use

The KjelDigester has been designed and built for laboratories. It serves for the heating of con­centrated H2SO4 for the oxidation of organic sample components.
2 Safety

2.3 Safety warnings

2.3.1 Warning explanation

DANGER, WARNING, CAUTION and NOTICE are standardized signal words for identifying levels of hazard seriousness of risks related to personal injury and property damage. All signal words, which are related to personal injury are accompanied by the general safety sign.
For the safety it is important to read and fully understand the table with the different signal words and their definitions.
Sign Signal word Definition Risk level
DANGER
WARNING
CAUTION
NOTICE
Indicates a hazardous situation which, if not avoided, will result in death or serious injury.
Indicates a hazardous situation which, if not avoided, may result in serious injury or death.
Indicates a hazardous situation which, if not avoided, may result in minor or moderate injury.
Indicates possible material damage, but no prac­tices related to personal injury.
★★★★
★★★☆
★★☆☆
☆☆☆☆
Supplementary safety information symbols may be placed in a rectangular panel on the left to the signal word and the supplementary text.
2 – 11Operation Manual KjelDigester K-446/K-449
2 Safety
Fig. 2.1 Example of warning
a Safety symbol d Result of danger if not avoided b Source of danger e Warning title c Instruction to avoid danger

2.3.2 Symbols

The reference list incorporates safety symbols and their meaning. The symbols can occur in this operation manual or on the device.
Warning safety symbols
Symbol Meaning Symbol Meaning
General warning Corrosive hazard
Electrical hazard Flammable
Biohazard Explosive environment
Broken glass Inhalation harmful
Device damage Hot surface
Hand bruising Magnet
2 – 12
KjelDigester K-446/K-449 Operation Manual
Mandatory safety symbols
Symbol Meaning Symbol Meaning
Wear protective goggles Wear protective clothes
Wear protective gloves Heavy load, lift with assistance

2.4 General safety rules

2.4 .1 Responsibility of the operator

The head of the laboratory is responsible for training his personnel.
The operator shall inform the manufacturer without delay of any safety-related incidents which might occur during operation of the device or its accessories.
2 Safety
Issues can be reported to the e-mail address: quality@buchi.com.
Legal regulations, such as local, state and federal laws applying to the device or its accessories must be strictly followed.

2.4.2 Duty of maintenance and care

The operator is responsible for the proper condition of the device. This includes maintenance, service and repair jobs that are performed on schedule by authorized personnel only.

2.4.3 Spare parts to be used

Use only genuine BUCHIconsumables and spare parts for maintenance to assure good system performance, reliability and safety. Any modifications of spare parts or assemblies are only al­lowed with the prior written permission of BUCHI.
2.4.4 Modifications
Modifications to the device are only permitted after prior consultation and with the written ap­proval of BUCHI. Modifications and upgrades shall only be carried out by an authorized BUCHI technical engineer. BUCHI will decline any claim resulting from unauthorized modifications.
2 – 13Operation Manual KjelDigester K-446/K-449
2 Safety

2.5 Product safety

The device is designed and built in accordance with current state-of-the-art technology. Never­theless, risks to users, property, and the environment can arise when the device is used care­lessly or improperly.
BUCHI has identified the following residual dangers emanating from the device:
∙ The device is operated by insufficiently trained personnel. ∙ The device is not operated according to its proper use. ∙ Appropriate warnings in this manual serve to make the user alert to these residual dangers.

2.5.1 General hazards

The following safety messages show hazards of general kind which may occur when handling the device. The user shall observe all listed counter measures in order to achieve and maintain the lowest possible level of hazard.
Additional warning messages can be found whenever actions and situations described in this manual are related to situational hazards.
DANGER
Risk of explosion with incorrect use of the device!
Death or serious injuries can result.
1. Do not store or operate the device in explosive environments.
2. Do not store chemicals in the vicinity of the device.
3. Operate the device in a fume hood with sufficient ventilation to directly with­draw fumes.
4. Use the user protection shield when working with H2O2 or larger amounts of water (>10mL).
5. Follow the safety notes in the application notes.
WARNING
Risk of burns from flammable fumes!
Serious injuries or death can result.
1. Remove all sources of flammable fumes.
2. Do not store flammable chemicals in the vicinity of the device.
2 – 14
KjelDigester K-446/K-449 Operation Manual
WARNING
Risk of chemical burns from hot acid or peroxide fumes!
Serious injuries or death can result.
1. Do not operate the system with faulty parts.
2. Check device setup for proper sealing before use.
3. Do not inhale process fumes.
4. Operate the device inside an active fume hood.
5. Use a Scrubber or water jet pump to neutralize exhaust fumes.
6. Do not move the device or parts of it during digestion.
7. Always wear the personnel protective equipment.
CAUTION
Risk of hot machine parts and glassware!
Minor or moderate burns can result.
1. Do not touch hot parts or surfaces.
2. Let the system and inserted glassware cool down safely.
3. Do not move the device or parts of it when hot.
2 Safety
Risk of spilled liquids or mechanical shocks.
Liquids leaking into the housing or mechanical shocks can damage the device.
1. Do not spill liquids over the device or its components
2. Do not move the device when it is loaded with sample liquid
3. Do not drop the device or its components
4. Keep external vibrations away from the device
5. Safely attach the device to the bench in earthquake prone regions
6. For H2O2 or TKN applications, do not operate the device without the user protection shield installed.
2.5.2 Specific hazard
H2O2 or TKN digestion
Using H2O2 or TKN for the digestion makes it mandatory to perform the following steps to keep the work place as safe as possible.
NOTICE
2 – 15Operation Manual KjelDigester K-446/K-449
2 Safety
WARNING
Risk of explosion and chemical burns!
Serious injuries or death can result.
1. Wear the personal protective equipment.
2. Make sure all components are in proper working condition.
3. Operate the device inside an active fume hood.
4. Follow the safety instructions in the application notes.
1. Use the user protection shield at any time during sample preparation and during digestion (both H2O2 and TKN).
∙ User protection shield, installation, (5–32).
2. Use a suitable dosing device with tube to safely dose H2O2.
3. Preparation and digestion needs to be done within an active fume hood.

2.5.3 Personal protective equipment

Always wear personal protective equipment such as protective eye goggles, protective clothing and gloves. The personal protective equipment must meet all requirements of all MSDS for the chemicals used.

2.5.4 Built-in safety elements and measures

Glassware
All original BUCHI glass parts are made of high temperature, chemical resistant borosilicate glass and optimal match the heating block.
Heating block
The heating block is equipped with a safety overtemperature switch. In case of a temperature above 500°C the heating block will be switched off and the KjelDigester starts a continuous beeping sound.
Fume removal
Acid fumes generated during digestion accumulate in the suction module.
The fumes must be safely withdrawn from the suction module via a EPDM hose to a Scrubber (e.g. Scrubber K-415) or via water jet pump into a sink with sufficient suction flow.
Lift (K-449)
The KjelDigester K-449 is equipped with a rechargeable battery. In case of a power failure the lift moves up automatically.
2 – 16
Before the lift starts moving down automatically a beeping sound informs the operator.
KjelDigester K-446/K-449 Operation Manual

3 Technical data

3.1 Device dimensions

3.1.1 K-446

3 Technical data

3.1.2 K-449

3.2 General technical data

Description K-446 K-449
Weight, total 30kg 37.3kg Weight, w/o accessory 18.5kg 25.8kg Approval UL/CSA, CE UL/CSA,CE Pollution degree 2 2 Overvoltage category II II Clearance to wall 5cm 5cm
3 – 17Operation Manual KjelDigester K-446/K-449
3 Technical data
Description K-446 K-449
Display 2 rowLCD display 2 rowLCD display Resolution temperature display 1°C 1°C Temperature range 30 – 450 °C 30 – 450 °C Average temperature stability ±1°C ±1°C Absolute temperature accuracy ±7°C at 420°C ±7°C at 420°C

3.2.1 Electrical system

Description K-446 K-449
Input voltage Frequency 50 – 60 Hz 50 – 60 Hz Power consumption max. 2300W 2300W Output current, Scrubber 0.7A 0.7A Fuse 2× T10A/L250V 2× T10A/L250V

3.2.2 Environmental conditions

Description K-446 K-449
Temperature 5 – 40°C 5 – 40°C Altitude above sea level max. 2000m 2000m Humidity Maximum relative humidity 80% for temperatures
Use For indoor use only
220 – 240V ±10 % 220 – 240V ±10%
up to 31°C, decreasing linearly to 50% relative humidity at 40°C
3 – 18
KjelDigester K-446/K-449 Operation Manual

4 Description of function

4.1 Purpose and design

The KjelDigester is suitable for digestion processes with concentrated boiling H2SO4 and a cata­lyst. The digestion parameters are listed in the BUCHI Application Notes.

4.2 KjelDigester overview

4.2.1 Front and side view

4 Description of function
Fig. 4.1 KjelDigester front and side view
a Fume collection tube g Fuse 10A/250V b Suction tube h Type plate c Drip tray i Rack d Suction hose j Lift (K-449 only)/bracket (K-446) e Control panel, (4–22) k Suction module f Cooling fan, electronic
4 – 19Operation Manual KjelDigester K-446/K-449
4 Description of function

4.2.2 Rear view

Fig. 4.2 KjelDigester rear view
a Eye bolt c Interface Scrubber b Power supply KjelDigester

4.2.3 Top-side view

4 – 20
Fig. 4.3 Heating block components
a Magnet e Main switch b Scrubber hose bracket f Measuring point for external temp. sensor c Heating block cover g Rack support d Drip tray holder
KjelDigester K-446/K-449 Operation Manual

4.3 Function

The KjelDigester is used to convert organic bound nitrogen (e.g. in proteins) in a sample into ammonium sulfate. During the digestion process, acid fumes and reaction gases may emerge and are handled by the Scrubber. The Scrubber is connected to the KjelDigester for neutralizing acid fumes and adsorbing unpleasant odors.

4.3.1 Digestion process

The aluminum heating blockd generates high temperatures of up to 450°C in order to heat the samplec up to 370°C (boiling point). The sample is digested in constantly boiling H2SO4. Hot acid fumes rise into the condensation zoneb, condense and rinse back down to the sample creating a constant reflux. Residual fumes which escape the condensation zone via the acid fume outleta are highly corrosive and must be withdrawn and efficiently neutralized (e.g. with the Scrubber K-415).
The condensation should not take place inside the safety zoneX in order to avoid shortening the lifetime of the sealings. In case the condensation is too close to the suction module (e.g. due to very high temperature settings or if too much catalyst was used) losses of nitrogen through creating N2 are possible and the samples can dry out.
4 Description of function
Fig. 4.4 Function of the KjelDigester
X
Safety zone
c Boiling/digestion sample a Acid fume outlet d Heating block b Condensation zone
4 – 21Operation Manual KjelDigester K-446/K-449
4 Description of function

4.4 Control panel

4.4.1 Control panel display

Fig. 4.5 K-449 Display
a Display, (4–22) c LED heating block (flashing), (4–22) b LED heating block (on/off), (4–22)
Display
Shows various informations such as set and actual temperatures, heating and cooling time.
LED heating block (on/off)
On: The heating block is heating.
Off: The heating block is turned off and the temperature is below 60°C.
LED heating block (flashing)
The heating block is not heating but the temperature is above 60°C.

4.4.2 Control panel buttons

Fig. 4.6 KjelDigester K-449 control panel
4 – 22
a Time, (4–23) f Step, (4–23) b Temperature, (4–23) g Increase/decrease value[+/-] c Start, (4–23) h Enter d Stop, (4–23) i Lift up/down, (4–23) e Method, (4–23)
KjelDigester K-446/K-449 Operation Manual
4 Description of function
Time
Range 0 – 999minutes
Activates the heating time value for an adjustment.
Temperature
Range 30 – 450°C
Activates the heating temperature of the heating block for an adjustment.
Start
Starts a digestion process.
Stop
∙ Stops a digestion process. ∙ Enables access to the settings menu. ∙ Stops the Scrubber.
Method (K-449 only)
Range 0 – 9 methods
Up to 9 methods can be programmed. Each method contains 4 adjustable steps. In each step, the temperature and time can be set. Also the cool down time can be adjusted.
NOTE
The first step is also used as the preheat function.
Method number0 is reserved for the manual mode on the K-449. No steps can be programed.
Step (K-449 only)
Allows to navigate forward within a method during editing.
Lift up/down (K-449 only)
Allows to move the rack up and down at any time.

4.4.3 Scrubber control (K-449 only)

5.5.6 Adjust the Scrubber control (K-449 only), (5–31).
Range 0 – 255 minutes
The Scrubber can be controlled via the KjelDigester. E.g. can the Scrubber be controlled inter­mitted for 1minute on, for 1minute off.
NOTE
An altered value will also be active during the cooling time in the automatic mode.
BUCHI recommends to leave this setting by default (on 0min:, off 0min.) unless a adjustment becomes necessary due to a special application.
4 – 23Operation Manual KjelDigester K-446/K-449
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