BUCHI K-436 User Manual

0 (0)

Operation Manual

SpeedDigester

K 425/K 436

11593346 en

Table of contents

Table of contents

1

About this manual . . . . . . . . . . . . . . . . . . . . . . . .

. . .

. . . . . .

. . .

. .

. 5

2

Safety . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

. . .

. . . . . .

. . .

. .

. 6

 

2.1

User qualification . . . . . . . . . . . . . .

. .

. . . .

. .

. .

6

 

2.2

Proper use . . . . . . . . . . . . . . . .

. .

. . . .

. .

. .

6

 

2.3

Improper use . . . . . . . . . . . . . . . .

. .

. . . .

. .

.

6

 

2.4

Safety warnings and safety signs used in this manual . .

. .

. . . .

. .

. .

7

 

2.5

Product safety

 

 

 

 

9

 

2.5.1

General hazards

 

 

 

 

9

 

2.5.2

Warning labels on housing and assemblies . . . . . .

. .

. . . .

. .

.

10

 

2.5.3

Personal protective equipment . . . . . . . . . .

. .

. . . .

. .

.

11

 

2.5.4

Built-in safety elements and measures . . . . . . .

. .

. . . .

. .

.

11

 

2.6

General safety rules . . . . . . . . . . . . . .

. .

. . . .

. .

.

12

3

Technical data . . . . . . . . . . . . . . . . . . . . . . . . . .

. . .

. . . . . .

. . .

. .

13

 

3.1

Scope of application and delivery . . . . . . . . .

. .

. . . .

. .

.

13

 

3.1.1

Available system configurations . . . . . . . . . .

. .

. . . .

. .

.

13

3.1.2Accessories for 300 ml sample tubes (for standard applications) . . . . . . . . 14

3.1.3Accessories for 500 ml sample tubes (for large sample volumes / at low nitrogen level) 15

 

3.1.4

Accessories for 3rd party production, 250 ml sample tubes . . . . . . . . .

 

. 15

 

3.2

Technical data

 

16

 

3.2.1

SpeedDigester K-425 / 110 – 120 V version . . . . . . . . . . . . . .

.

16

 

3.2.2

SpeedDigester K-425 / 220 – 240 V version . . . . . . . . . . . . . .

.

17

 

3.2.3

SpeedDigester K-436 / 220 – 240 V version . . . . . . . . . . . . . .

.

18

 

3.3

Materials used

 

19

4

Description of function . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

.

20

 

4.1

Functional principle . . . . . . . . . . . . . . . . . . . . . .

.

20

5

Putting into operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

.

21

 

5.1

Installation site

 

21

 

5.2

System fixation . . . . . . . . . . . . . . . . . . . . . . . .

 

22

 

5.3

Electrical connections

 

23

6

Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

.

24

6.1Operating controls and housing . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24

6.1.1

SpeedDigester K-425

— front side . . . . . . . . . . . .

. . . .

.

. 24

6.1.2

SpeedDigester K-425

— rear side

 

 

25

6.1.3

SpeedDigester K-436

— front side . . . . . . . . . . . .

. . . .

.

. 26

6.1.4

SpeedDigester K-436

— rear side

 

 

27

6.2

Preparing of SpeedDigester, suction module(s) and sample tubes

 

 

27

6.2.1

Kjeldahl digestion —preparing sample tubes

 

 

28

6.2.2

Peroxide digestion —preparing sample tubes . . . . . . . . .

. . . .

.

29

6.2.3

Installing a suction module and sample tubes (300 ml)

 

 

29

6.2.4

Installing 500 ml sample tubes

 

 

32

6.2.5

Starting up the SpeedDigester . . . . . . . . . . . . . .

. . . .

.

34

6.3

Performing a Kjeldahl digestion process

 

 

34

6.3.1

Preparational steps . . . . . . . . . . . . . . . . . .

. . . .

.

34

3

K-425 / K-436 Operation Manual, Version A

Table of contents

 

6.3.2 Starting a digestion process

 

34

 

6.4

Performing a peroxide digestion process . . . . . . . . . . . . . .

.

. 35

 

6.4.1

Preparational steps . . . . . . . . . . . . . . . . . . . . . .

.

35

 

6.4.2 Starting a digestion process

 

35

 

6.5

Finishing a digestion process . . . . . . . . . . . . . . . . . .

.

. 37

 

6.6

Optional 'Stand with drip tray'

 

40

7

Maintenance and repairs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

. .

41

 

7.1

Customer service . . . . . . . . . . . . . . . . . . . . . .

.

. 42

 

7.2

General condition and cleaning instructions . . . . . . . . . . . . . .

.

42

 

7.2.1

Breakage of glassware inside a housing chamber

 

43

 

7.2.2

Liquid ingress into the instrument . . . . . . . . . . . . . . . . .

.

43

 

7.3

Glass component conditions . . . . . . . . . . . . . . . . . .

.

. 44

 

7.3.1

Sample tubes . . . . . . . . . . . . . . . . . . . . . . . .

.

44

 

7.4

Sealing system . . . . . . . . . . . . . . . . . . . . . . .

.

44

 

7.5

Rack system . . . . . . . . . . . . . . . . . . . . . . . .

.

45

 

7.5.1

300 ml sample tube support spring . . . . . . . . . . . . . . . .

.

. 45

 

7.5.2

500 ml sample tube support spring . . . . . . . . . . . . . . . .

.

. 46

8

Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

. .

47

 

8.1

Malfunctions and their remedy

 

47

 

8.2

Device fuses

 

48

9

Shutdown, storage, transport and disposal . . . . . . . . . . . . . . . . . . . . . .

. .

49

 

9.1

Storage and transport

 

49

 

9.2

Disposal

 

50

 

9.2.1

Thermostat(s) . . . . . . . . . . . . . . . . . . . . . . . .

.

50

10

Spare parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

. .

52

 

10.1

Spare parts, optional accessories and consumables . . . . . . . . . .

.

. 52

11 Declarations and requirements . . . . . . . . . . . . . . .

. .

. . . . . .

. . .

. . .

. .

55

11.1

FCC requirements (for USA and Canada) . . . .

.

.

. . . .

. .

. .

.

. 55

11.2

Declaration of conformity . . . . . . . . . .

 

. .

. . . .

. .

. .

.

56

4

K-425 / K-436 Operation Manual, Version A

1  About this manual

1 About this manual

This manual describes the SpeedDigester K-425 / K-436 and provides all information required for its safe operation and to maintain it in good working order.

It is addressed to laboratory personnel and operators in particular.

Read this manual carefully before installing and running your system and note the safety precautions in chapter 2 in particular. Store the manual in the immediate vicinity of the instrument, so that it can be consulted at any time.

No technical modifications may be made to the instrument without the prior written agreement of Buchi. Unauthorized modifications may affect the system safety or result in accidents. Technical data are subject to change without notice.

Note

The symbols pertaining to safety (WARNINGS and ATTENTIONS) are explained in chapter 2.

This manual is copyright. Information from it may not be reproduced, distributed or used for competitive purposes, nor made available to third parties. The manufacture of any component with the aid of this manual without prior written agreement is also prohibited.

The English manual is the original language version and serves as basis for all translations into other languages. If you need another language version of this manual, you can download available versions at www.buchi.com.

5

K-425 / K-436 Operation Manual, Version A

2  Safety

2 Safety

This chapter introduces the safety concept of the instrument and contains general rules of behavior and warnings from direct and indirect hazards concerning the use of the product.

For the users safety, all safety instructions and safety messages in the individual chapters shall be strictly observed and followed. Therefore, the manual must always be available to all persons performing any tasks described herein.

2..1 User qualification

The instrument may only be used by laboratory personnel and other persons who on account of training and professional experience know the potential dangers that can develop when operating the instrument.

Untrained personnel, or persons who are currently being trained, require careful supervision by a qualified person. This Operation Manual serves as a basis for training.

2..2 Proper use

The SpeedDigester K-425 / K-436 has been designed and built for laboratory use only. Its intended use is to allow digestion of samples with concentrated acids or peroxides by heating up the probe.

A suction unit (e.g. Scrubber or water jet pump) has to be connected to the suction module to safely withdraw fumes which will emerge during digestion. In any case, all exhausts and fumes leaving the system or assemblies such as Scrubber or water jet pump have to be removed instantly inside a fume hood. This is mandatory to remove all possibly hazardous substances (e.g. acid fumes) from the working area. The ventilation system of the fume hood has to be equipped with safety measures such as outlet filters to avoid contamination of the environment.

When the SpeedDigester K-425 / K-436 is used in combination with other instruments (e.g. Scrubber and fume hood) all related manuals are to be fully observed.

2..3 Improper use

Applications not mentioned in section 2.2 are considered to be improper. Applications which do not comply with the technical data (see section 3 of this manual) are also considered to be improper.

The operator bears the sole risk for any damages or hazards caused by improper use!

The following uses are expressly forbidden:

Digestion operations outside an active fume hood.

Digestion of samples (e.g. food and feed) in nitrosulfuric acids which can produce explosive nitro compounds.

Digestion of sample material of unknown composition in nitrosulfuric acids.

Use of samples which can explode or ignite due to shocks, friction, heat or sparks.

Installation or use of the instrument in rooms, which require ex-protected instruments.

Use of glassware which is not specified in section 2.5.4.

6

K-425 / K-436 Operation Manual, Version A

2  Safety

2..4 Safety warnings and safety signs used in this manual

DANGER, WARNING, CAUTION and NOTICE are standardized signal words for identifying levels of hazard seriousness of risks related to personal injury and property damage. All signal words, which are related to personal injury are accompanied by the general safety sign.

For your safety it is important to read and fully understand the table below with the different signal words and their definitions!

Sign

Signal word

Definition

Risk level

 

DANGER

Indicates a hazardous situation which, if not avoided, will result in

 

 

death or serious injury.

 

 

 

 

 

 

 

 

WARNING

Indicates a hazardous situation which, if not avoided, could result

 

 

in death or serious injury.

 

 

 

 

 

 

 

 

CAUTION

Indicates a hazardous situation which, if not avoided, may result

 

 

in minor or moderate injury.

 

 

 

 

 

 

 

no

NOTICE

Indicates possible property damage, but no

 

 

practices related to personal injury.

(property damage only)

 

 

 

 

 

 

 

 

 

Supplementary safety information symbols may be placed in a rectangular panel on the left to the signal word and the supplementary text (see below example).

Space for

!

SIGNAL WORD

 

 

Supplementary text, describing the kind and level of hazard / risk seriousness.

supplementary

safety

• List of measures to avoid the herein described, hazard or hazardous situation.

information

• ...

 

symbols.

• ...

 

 

 

 

Table of supplementary safety information symbols

The reference list below incorporates all safety information symbols used in this manual and their meaning.

Symbol Meaning

General warning

Electrical hazard

Heavy weight, avoid overexertion

Explosive gases, explosive environment

7

K-425 / K-436 Operation Manual, Version A

BUCHI K-436 User Manual

2  Safety

Symbol Meaning

Explosive material

Fire hazard

Harmful to life-forms

Hot item, hot surface

Device damage

Inhalation of substances

Chemical burns by corrosives

Fragile components

Wear laboratory coat

Wear protective goggles

Wear protective gloves

Heavy weight, lifting requires more than one person

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K-425 / K-436 Operation Manual, Version A

2  Safety

Additional user information

Paragraphs starting with Note transport helpful information for working with the device / software or its supplementaries. Notes are not related to any kind of hazard or damage (see following example).

Note

Useful tips for the easy operation of the instrument / software.

2..5 Product safety

The SpeedDigester K-425 / K-436 has been designed and built in accordance with current state-of- the-art technology. Safety warnings in this manual (as described in section 2.4) serve to make the user alert to and avoid hazardous situations emanating from residual dangers by giving appropriate counter measures.

However, risks to users, property and the environment can arise when the instrument is damaged, used carelessly or improperly.

2..5..1 General hazards

The following safety messages show hazards of general kind which may occur when handling the instrument. The user shall observe all listed counter measures in order to achieve and maintain the lowest possible level of hazard.

Additional warning messages can be found whenever actions and situations described in this manual are related to situational hazards.

!DANGER

Death or serious injuries by use in explosive environments.

Do not store or operate the instrument in explosive environments

Do not store chemicals in the vicinity of the device

Operate the device in a fume hood with sufficient ventilation to directly withdraw fumes

!WARNING

Death or serious burns by flammable vapors.

Remove all sources of flammable vapors

Do not store flammable chemicals in the vicinity of the device

9

K-425 / K-436 Operation Manual, Version A

2  Safety

!WARNING

Risk of death or serious chemical burns by hot acid or peroxide fumes.

Do not operate the system with faulty parts

Check instrument setup for proper sealing before use

Do not inhale process fumes

Operate the instrument inside an active fume hood

• Do not move the instrument or parts of it during digestion

!CAUTION

Risk of minor or moderate cuts by sharp edges.

Do not touch defective or broken glassware with bare hands

Do not touch thin metal edges

!CAUTION

Risk of burns by hot machine parts and glassware.

Do not touch hot parts or surfaces

Let the system and inserted glassware cool down safely

Do not move the instrument or parts of it when hot

NOTICE

Risk of instrument damage by liquids or mechanical shocks.

Do not spill liquids over the instrument or its components

Do not move the instrument when it is loaded with sample liquid

Do not drop the instrument or its components

Keep external vibrations away from the instrument

Safely attach the instrument to the bench in earthquake prone regions

Do not operate the instrument without the protection cover installed at the front

2..5..2 Warning labels on housing and assemblies

The following warning sticker(s) can be found on the housing or assemblies of the SpeedDigester:

Symbol

Meaning

Location

 

Hot item, hot surface

Sticker / label, located on top of the housing and

 

at the racks

 

 

Do NOT put rack into side cooling position

Label on 500 ml racks

10

K-425 / K-436 Operation Manual, Version A

2  Safety

2..5..3 Personal protective equipment

Always wear personal protective equipment such as protective eye goggles, protective clothing and gloves. The personal protective equipment must meet all requirements of the supplementary data sheets for the chemicals used.

!WARNING

Serious chemical burns by corrosives.

Observe supplementary data sheets of all used chemicals.

Handle corrosives in well ventilated environments only.

Always wear protective goggles.

Always wear protective gloves.

Always wear protective clothes.

Do not use damaged glassware.

2..5..4 Built-in safety elements and measures

Buchi glassware design

All original Buchi digestion glassparts are made of high temperature and chemical resistant borosilicate glass.

Acid fumes generated during digestion accumulate in the suction module

The fumes must be safely withdrawn from the suction module via one or more hoses to a Scrubber (e.g. Scrubber B-414) or via water jet pump into a sink or sufficient suction flow.

3rd party glassware

The quality of the material is an essential part of the safety concept of the SpeedDigester K-425 / K-436. For the special rack (order no. 11055440), the following qualified vendors offer sample tubes of sufficient quality grade to withstand the temperatures and the aggressive chemical digestion agents:

 

Qualified vendor

 

 

Tested sample tube(s)

 

 

Gerhardt

 

250 ml / 6100

 

 

 

 

 

 

 

Velp

 

ø 42×300 mm / A00000144

 

Foss

 

250 ml / 10014278

 

 

 

 

 

 

Heater

Each heating chamber is equipped with a safety overtemperature switch. In case of an emergency the switch cuts off the power of the corresponding chamber and the 'Heating indicator' light.

11

K-425 / K-436 Operation Manual, Version A

2  Safety

2..6 General safety rules

Responsibility of the operator

The head of the laboratory is responsible for training his/her personnel.

The operator shall inform the manufacturer without delay of any safety-related incidents which might occur during operation of the instrument or its accessories. Legal regulations, such as local, state and federal laws applying to the instrument or its accessories must be strictly followed.

Duty of maintenance and care

The operator is responsible for the proper condition of instrument. This includes maintenance, service and repair jobs that are performed and on schedule by authorized personnel only.

Spare parts to be used

Use only genuine consumables and spare parts for maintenance to assure good system performance, reliability and safety. Any modifications of spare parts or assemblies are only allowed with the prior written permission of the manufacturer.

Modifications

Modifications to the instrument are only permitted after prior consultation and with the written approval of the manufacturer. Modifications and upgrades shall only be carried out by an authorized Buchi technical engineer. The manufacturer will decline any claim resulting from unauthorized modifications.

12

K-425 / K-436 Operation Manual, Version A

3  Technical data

3 Technical data

This chapter introduces the reader to the SpeedDigester K-425 / K-436 and its specifications. It contains the scope of delivery, technical data, requirements and performance data.

3..1 Scope of application and delivery

All system configurations come with a limited set of accessories as a starter kit. Within a system family, additionally available accessories (see section 3.1.2 and the following) can be used to easily reconfigure your system to every configuration listed in section 3.1.1.

Parts that are required to change a system configuration:

Rack

Suction module

Insulation plate (fireclay insert)

Sample tubes

The scope of delivery depends on the ordered system configuration and can be checked according to the individual delivery note and the listed order numbers.

Note

For additional information about the listed products, see www.buchi.com or contact your local dealer.

3..1..1 Available system configurations

SpeedDigester K- 425

 

 

 

 

 

 

 

 

 

 

 

Configuration

 

Sample

 

Sample tube sizes

 

Suction modules

 

 

 

 

 

order number

 

positions

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Condensate

 

Module for

 

 

 

 

 

 

 

 

 

 

 

110 – 120 V

220 – 240 V

 

5

6

 

250 ml

300 ml

500 ml

Standard

H2O2

3rd party

 

 

trap

 

 

 

 

 

 

 

 

 

 

 

tubes

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

1154251500

1154252500

 

 

 

 

 

 

 

 

1154251100

1154252100

 

 

 

 

 

 

 

 

1154251200

1154252200

 

 

 

 

 

 

 

 

1154251300

1154252300

 

 

 

 

 

 

 

 

1154251400

1154252400

 

 

 

*

 

 

 

 

 

*

*Third party sample tubes require special accessories such as the BUCHI “Module for 3rd party tubes” and the matching rack / insulation plate. Tubes are not included in the set!

Note

The SpeedDigester K-425 is available in different versions for 110 – 120 V or 220 – 240 V mains supply. Check your local voltage requirements and order accordingly!

13

K-425 / K-436 Operation Manual, Version A

 

 

 

 

 

 

 

 

 

 

 

3  Technical data

SpeedDigester K- 436

 

 

 

 

 

 

 

 

 

 

 

 

Configuration

 

Sample

 

Sample tube sizes

 

Suction modules

 

 

 

 

 

order number

 

positions

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Condensate

 

 

Module for

 

 

 

 

 

 

 

 

 

 

 

 

110 – 120 V

220 – 240 V

 

10

12

 

250 ml

300 ml

500 ml

Standard

H O

 

3rd party

 

 

 

 

 

 

 

 

 

 

trap

2

2

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

tubes

 

 

 

 

 

 

 

 

 

 

 

 

 

 

n.a.

1154362500

 

 

 

 

 

 

 

 

 

n.a.

1154362100

 

 

 

 

 

 

 

 

 

n.a.

1154362200

 

 

 

 

 

 

 

 

 

n.a.

1154362300

 

 

 

 

 

 

 

 

 

n.a.

1154362400

 

 

 

*

 

 

 

 

 

 

*

*Third party sample tubes require special accessories such as the BUCHI “Module for 3rd party tubes” and the matching rack / insulation plate. Tubes are not included in the set!

Note

The SpeedDigester K-436 is only available for 220 – 240 Vmains supply. Check if a voltage converter is necessary to adapt your local mains level before connecting the instrument!

3..1..2 Accessories for 300 ml sample tubes (for standard applications)

 

Item

Additional info

Order number

Recommended quantity

 

 

to order

 

 

 

 

 

 

 

 

 

K-425

 

K-436

 

Set of sample tubes

300 ml, 4 tubes

037377

 

 

 

 

 

 

 

 

 

Suction module standard

6 place

11055849

 

 

 

 

 

 

 

 

 

Suction module condensate trap

6 place

11055865

 

 

 

 

 

 

 

 

 

Suction module H2O2

6 place, cpl.

11055853

 

 

 

 

 

 

 

 

 

Connectors to suction module

Adapter and plug

11055367

 

 

 

 

 

 

 

 

 

EPDM hose

Set for K-425

11056005

 

 

 

 

 

 

 

 

 

EPDM hose set

Set for K-436

11056219

 

 

 

 

 

 

 

 

 

Insulation plate (fireclay)

Insertion, for 300 ml tubes

11055142

 

 

 

 

 

 

 

 

 

Rack

6 place, for 300 ml tubes

11055248

 

 

 

 

 

 

 

 

 

Glass caps (set of 4)

OPTIONAL

040049

 

 

 

 

 

 

 

 

 

Insulation cap

OPTIONAL

11056024

 

 

 

 

 

 

 

 

 

Sealing FKM (set of 6)

Spare part

038122

 

 

 

 

 

 

 

 

 

Sealing PTFE (1 pcs)

OPTIONAL

022442

 

 

 

 

 

 

 

 

 

Rubber GUKOs for H2O2 suc. mod.

Spare part set of 6

044495

 

 

 

 

 

 

 

 

 

Filter funnel for H2O2 suc. mod.

Spare part set of 6

044494

 

 

 

 

 

 

 

 

 

 

 

Set circular spring and holder

Spare part set of 6

11055984

 

 

 

 

 

 

 

 

 

Bed-plate for 300ml racks

OPTIONAL

11055943

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

14

K-425 / K-436 Operation Manual, Version A

3  Technical data

3..1..3 Accessories for 500 ml sample tubes (for large sample volumes / at low nitrogen level)

Standard items

Additional info

Order number

Recommended quantity

 

to order

 

 

 

 

 

 

 

K-425

 

K-436

 

 

 

 

 

 

 

 

 

 

Sample tubes

500 ml, single tube

026128

 

10×

 

 

 

 

 

 

Set of sample tubes

500 ml, 4 tubes

043982

 

 

 

 

 

 

 

Suction module condensate trap

5 place

11055851

 

 

 

 

 

 

 

Connectors to suction module

Adapter and plug

11055367

 

 

 

 

 

 

 

EPDM hose

Set for K-425

11056005

 

 

 

 

 

 

 

EPDM hose set

Set for K-436

11056219

 

 

 

 

 

 

 

Insulation plate (fireclay)

Insertion, for 500 ml tubes

11055143

 

 

 

 

 

 

 

Rack

5 place, for 500 ml tubes

11055327

 

 

 

 

 

 

 

Base for rack

For 500 ml tubes rack

11055612

 

 

 

 

 

 

 

Glass caps (set of 4)

OPTIONAL

040049

 

 

 

 

 

 

 

Insulation cap

OPTIONAL

11056024

 

 

 

 

 

 

 

Sealing FKM (set of 6)

Spare part

038122

 

 

 

 

 

 

 

Sealing PTFE (1 pcs)

OPTIONAL

022442

 

 

 

 

 

 

 

Interlock spring for 500 ml rack

Spare part

11055385

 

 

 

 

 

 

 

3..1..4 Accessories for 3rd party production, 250 ml sample tubes

Item

Additional info

Order number

Recommended quantity

 

to order

 

 

 

 

 

 

 

K-425

 

K-436

 

 

 

 

 

 

 

 

 

 

3rd party sample tubes

250 ml

n.a.

 

12×

 

 

 

 

 

 

Suction module for 3rd party tubes

6 place

11055850

 

 

 

 

 

 

 

Connectors to suction module

Adapter and plug

11055367

 

 

 

 

 

 

 

EPDM hose

Set for K-425

11056005

 

 

 

 

 

 

 

EPDM hose set

Set for K-436

11056219

 

 

 

 

 

 

 

Insulation plate (fireclay)

Insertion, for 250 ml tubes

11055877

 

 

 

 

 

 

 

Rack

6 place, for 250 ml tubes

11055440

 

 

 

 

 

 

 

Sealing FKM (set of 6)

Spare part

038125

 

 

 

 

 

 

 

Set circular spring and holder 6×

Spare part

11055985

 

 

 

 

 

 

 

Note

3rd party sample tubes are not available at Buchi. Please contact your local OEM vendor for these type of tubes.

15

K-425 / K-436 Operation Manual, Version A

3  Technical data

3..2

Technical data

 

3..2..1

SpeedDigester K-425 / 110 – 120 V version

 

 

 

 

 

 

 

 

Technical data

 

 

 

Power consumption

max. 1280 W

 

 

 

 

 

 

 

Temperature control range

level 1 to 10 (70 – 580°C typically)

 

 

 

 

 

 

 

Connection voltage

110 – 120 VAC

 

 

 

 

 

 

 

Input fuse

T 10A L 250 V

 

 

 

 

 

 

 

Frequency

50 / 60 Hz

 

 

 

 

 

 

 

IP degree of protection (two digits)

IP 20

 

 

 

 

Explanation of protection level:

 

 

 

 

2  Protection provided by the enclosure against access

 

 

 

 

to hazardous parts (e.g., electrical conductors,

 

 

 

 

moving parts) and the ingress of solid foreign objects

 

 

 

 

with a diameter of > 12,5 mm.

 

 

 

 

0  No protection of the equipment inside the enclosure

 

 

 

 

against harmful ingress of water.

 

 

 

 

 

 

 

Insulation category

II

 

 

 

 

 

 

 

Environmental conditions:

 

 

 

 

Pollution degree

2  (for indoor use only)

 

 

 

 

 

 

 

 

Temperature

5 – 40 °C

 

 

 

 

 

 

 

 

Altitude (above sea level)

up to 2000 m

 

 

 

 

 

 

 

 

Humidity (curve parameter)

Maximum relative humidity 80% up to 31 °C, then

 

 

 

 

decreasing linearly to 50% relative humidity at 40 °C

 

 

 

 

 

 

Dimensions in mm (W × D × H)

310 × 620 × 540

 

 

 

 

 

 

Net weight

12 kg

 

 

 

 

 

 

Rack (without glassware)

2,5 kg

 

 

 

 

 

16

K-425 / K-436 Operation Manual, Version A

3  Technical data

3..2..2

SpeedDigester K-425 / 220 – 240 V version

 

 

 

 

 

 

 

 

Technical data

 

 

 

Power consumption

max. 1280 W

 

 

 

 

 

 

 

Temperature control range

level 1 to 10 (70 – 580°C typically)

 

 

 

 

 

 

 

Connection voltage

220 – 240 VAC

 

 

 

 

 

 

 

Input fuse

T 10A L 250 V

 

 

 

 

 

 

 

Frequency

50 / 60 Hz

 

 

 

 

 

 

 

IP degree of protection (two digits)

IP 20

 

 

 

 

Explanation of protection level:

 

 

 

 

2  Protection provided by the enclosure against access

 

 

 

 

to hazardous parts (e.g., electrical conductors,

 

 

 

 

moving parts) and the ingress of solid foreign objects

 

 

 

 

with a diameter of > 12,5 mm.

 

 

 

 

0  No protection of the equipment inside the enclosure

 

 

 

 

against harmful ingress of water.

 

 

 

 

 

 

 

Insulation category

II

 

 

 

 

 

 

 

Environmental conditions:

 

 

 

 

Pollution degree

2  (for indoor use only)

 

 

 

 

 

 

 

 

Temperature

5 – 40 °C

 

 

 

 

 

 

 

 

Altitude (above sea level)

up to 2000 m

 

 

 

 

 

 

 

 

Humidity (curve parameter)

Maximum relative humidity 80% up to 31 °C, then

 

 

 

 

decreasing linearly to 50% relative humidity at 40 °C

 

 

 

 

 

 

Dimensions in mm (W × D × H)

310 × 620 × 540

 

 

 

 

 

 

Net weight

12 kg

 

 

 

 

 

 

Rack (without glassware)

2,5 kg

 

 

 

 

 

17

K-425 / K-436 Operation Manual, Version A

3  Technical data

3..2..3

SpeedDigester K-436 / 220 – 240 V version

 

 

 

 

 

 

 

 

Technical data

 

 

 

Power consumption

max. 2550 W

 

 

 

 

 

 

 

Temperature control range

level 1 to 10 (70 – 580°C typically)

 

 

 

 

 

 

 

Connection voltage

220 – 240 VAC

 

 

 

 

 

 

 

Input fuse

T 10A L 250 V

 

 

 

 

 

 

 

Frequency

50 / 60 Hz

 

 

 

 

 

 

 

IP degree of protection (two digits)

IP 20

 

 

 

 

Explanation of protection level:

 

 

 

 

2  Protection provided by the enclosure against access

 

 

 

 

to hazardous parts (e.g., electrical conductors,

 

 

 

 

moving parts) and the ingress of solid foreign objects

 

 

 

 

with a diameter of > 12,5 mm.

 

 

 

 

0  No protection of the equipment inside the enclosure

 

 

 

 

against harmful ingress of water.

 

 

 

 

 

 

 

Insulation category

II

 

 

 

 

 

 

 

Environmental conditions:

 

 

 

 

Pollution degree

2  (for indoor use only)

 

 

 

 

 

 

 

 

Temperature

5 – 40 °C

 

 

 

 

 

 

 

 

Altitude (above sea level)

up to 2000 m

 

 

 

 

 

 

 

 

Humidity (curve parameter)

Maximum relative humidity 80% up to 31 °C, then

 

 

 

 

decreasing linearly to 50% relative humidity at 40 °C

 

 

 

 

 

 

Dimensions in mm (W × D × H)

310 × 620 × 540

 

 

 

 

 

 

Net weight

15,5 kg

 

 

 

 

 

 

Rack (without glassware)

2× 2,5 kg

 

 

 

 

 

18

K-425 / K-436 Operation Manual, Version A

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