MEASURING INSTRUMENT WITH AUTOMATIC SENSOR RECOGNITION
AND ELECTRONIC ACCESS CONTROL
ProLab 1000
CE conformity
Radio data transmission
SI Analytics GmbH hereby declares that the ProLab 1000 meter is in
compliance with the basic requirements and the other relevant
regulations of the directive 1999/5/EC.
The EC declaration of conformity can be requested from SI Analytics
GmbH.
The ProLab 1000 precision pH meter enables you to perform pH, ORP
and ion-selective measurements rapidly and reliably.
The ProLab 1000 provides the maximum degree of ease of use,
reliability and, above all, measuring certainty for all applications.
The proven calibration procedures, and stability control function (SC)
and the sensor recognition function support your work with the meter.
In addition, the ProLab 1000 provides an electronic access control.
Documented measurement data is thus automatically assigned to a
user.
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1Keypad
2Display
3Reader field for electronic access control
4Socket field
7
OverviewProLab 1000
MENU
OK
SCMODE
STO
ESC
PRINT
CAL
RCL
MODE
CAL
SC
STO
RCL
PRINT
1.2Keypad
In this operating manual, keys are indicated by brackets <..> .
The key symbol (e.g. <MENU/OK>) generally indicates a short
keystroke (under 2 sec) in this operating manual. A long keystroke
(approx. 2 sec) is indicated by the underscore behind the key symbol
(e.g. <MENU/OK
_>).
Key functions
<On/Off>Switch the meter on/off
<MODE>
<MODE
<CAL>
<CAL
<SC>Switch on or off the stability control
<STO>
<STO
<RCL>
<RCL
<PRINT>
<PRT
_>
_>
_>
_>
_>
Select measured parameter
Activate operation lock
Call up calibration procedure
Open menu for calibration data storage
function manually.
Store measured value
Open menu for automatic storing
function
Open menu for manually stored
measured values
Open menu for automatically stored
measured values
Print
Open menu for automatic printing
<▲>Increment values, scroll
8
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ProLab 1000Overview
MENU
OK
ESC
Measured value (with unit)
Temperature display
ID sensor symbol
CalClock
Status line
pH
7.000
25.0°C
26.04.06 10:37
<▼>Decrement values, scroll
<MENU/OK>
<MENU/OK
<ESC>Return to higher menu level /
_>
Confirm entries
Open setting menu for system settings
Cancel inputs
1.3Display
The graphic display displays the measurement data. The illumination
enables to read the display even in the darkness.
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9
OverviewProLab 1000
1
2
3
6
7
8
4
5
1.4Socket field
Connections:
1pH electrode
2 + 4Reference electrode
3Temperature sensor
5Dead stop connection
(e.g. for double platinum electrodes)
6USB interface
7Power pack
8RS232 interface/analog output
CAUTION
Only connect sensors to the meter that cannot return any voltages
or currents that are not allowed (> SELV and > current circuit with
current limiting).
Nearly all commercial sensors - especially SI Analytics sensors fulfill these requirements.
10
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ProLab 1000Overview
DIN
BNC
1.5Automatic sensor recognition
The automatic sensor recognition function enables
to operate a sensor with different meters without recalibrating
to operate different sensors with one meter without recalibrating
to assign measurement data to a sensor
– measurement datasets are always downloaded to the interface
with the sensor type and sensor series number.
– measurement datasets are always stored together with the
sensor type and sensor series number.
to assign calibration data to a sensor
– calibration data is always downloaded to the interface with the
sensor type and sensor series number.
To be able to use the automatic sensor recognition function a meter is
required that supports the automatic sensor recognition (e.g.
ProLab 1000), and a sensor (ID sensor) that is suitable for sensor
recognition.
In every ID sensor, sensor data is stored that clearly identifies the
sensor.
The sensor data is sent to the meter automatically via radio
communication and used for sensor identification there.
Note
With the ProLab 1000 meter, you can also operate non-ID sensors.
Then, however, you cannot use the advantages of the sensor
recognition function.
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11
OverviewProLab 1000
pH
7.000
25.0°C
26.04.06 10:37
ID sensor symbol
ID sensorsSI Analytics ID sensors support the automatic sensor recognition
function. Their sensor designation has the addition "ID", e.g.
A 161 1M DIN-ID electrode.
Note
Information on available ID sensors is given on the Internet or directly
by SI Analytics.
ID sensors connected to the ProLab 1000 meter can be recognized by
the ID sensor symbol on the display of the meter.
Sensor data from ID
sensors
ID sensors transmit the following sensor data to the meter:
SENSOR ID
– Sensor type
– Sensor series number
Calibration data
– Calibration date
– Calibration characteristics
– Calibration interval
– Selected buffer set (pH electrodes only)
The calibration data is updated in the ID sensor after each calibration
procedure. The ID sensor symbol flashes while this is done.
Note
While the ID sensor symbol is flashing, the sensor must not be
disconnected because otherwise the calibration data will not be
completely transmitted. The sensor will then have no valid calibration.
Note
If non-ID sensors are used, the calibration data from the meter is used
and also stored in the meter.
12
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ProLab 1000Overview
MENU
OK
Reader unit for
access control
1.6Electronic access control
The ProLab 1000 always documents measurement data and
calibration data with an ID number (USER ID).
If the USER ID is assigned to a certain user, all measurement data is
also assigned to the user in compliance with GLP.
The USER ID is easily and safely transmitted to the ProLab 1000 via
an electronic key. Each electronic key in the form of a keyring pendant
contains a key number. The key number is read by the meter via a
contactless radio data connection and used as the USER ID.
The meter checks the access authorization for the USER ID.
Measurements with an electronic key are only possible if the USER ID
is registered in the meter.
The measuring data is then documented along with the registered
USER ID.
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If the USER ID of the electronic key is not registered in the meter,
access to the meter with this electronic key is denied.
Anonymous access is always possible. For anonymous access, the
USER ID 0 is used automatically.
By labeling measurement data without electronic key with USER ID 0,
this data can be separated from the GLP-compliant documentation of
measurements.
13
OverviewProLab 1000
14
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ProLab 1000Safety
2Safety
This operating manual contains basic instructions that you must follow
during the commissioning, operation and maintenance of the meter.
Consequently, all responsible personnel must read this operating
manual before working with the measuring system. The operating
manual must always be available within the vicinity of the meter.
Target groupThe meter was developed for work in the laboratory.
Thus, we assume that, as a result of their professional training and
experience, the operators will know the necessary safety precautions
to take when handling chemicals.
Safety instructionsThe individual chapters of this operating manual use the following
safety instruction to indicate various types of danger:
CAUTION
indicates instructions that must be followed precisely in order to
avoid the possibility of slight injuries or damage to the meter or
the environment.
Further notes
Note
indicates notes that draw your attention to special features.
Note
indicates cross-references to other documents, e.g. operating
manuals.
2.1Authorized use
This meter is authorized exclusively for pH, ORP and ion-selective
measurements in the laboratory.
The technical specifications as given in chapter 7 T
(page 83) must be observed. Only the operation and running of the
meter according to the instructions given in this operating manual is
authorized. Any other use is considered unauthorized.
ECHNICALDATA
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15
SafetyProLab 1000
2.2General safety instructions
This instrument is built and inspected according to the relevant
guidelines and norms for electronic measuring instruments (see
page 83).
It left the factory in a safe and secure technical condition.
Function and
operational safety
The smooth functioning and operational safety of the meter can only be
guaranteed if the generally applicable safety measures and the specific
safety instructions in this operating manual are followed during
operation.
The smooth functioning and operational safety of the meter can only be
guaranteed under the environmental conditions that are specified in
chapter 7 T
ECHNICALDATA (page 83).
If the meter was transported from a cold environment to a warm
environment, the formation of condensate can lead to the faulty
functioning of the meter. In this event, wait until the temperature of the
meter reaches room temperature before putting the meter back into
operation.
Safe operationIf safe operation is no longer possible, the meter must be taken out of
service and secured against inadvertent operation!
Safe operation is no longer possible if the meter:
has been damaged in transport
has been stored under adverse conditions for a lengthy period of
time
16
Obligations of the
purchaser
is visibly damaged
no longer operates as described in this manual.
If you are in any doubt, please contact the supplier of the meter.
The purchaser of this meter must ensure that the following laws and
guidelines are observed when using dangerous substances:
EEC directives for protective labor legislation
National protective labor legislation
Safety regulations
Safety datasheets of the chemical manufacturers.
The power pack supplies the meter with low voltage (9 V DC).
The batteries are only used to buffer the system time if the power
supply is interrupted.
CAUTION
The line voltage at the operating site must lie within the input
voltage range of the original power pack (see page 83).
CAUTION
Use original power packs only (see page 83).
1Insert the plug into the socket of the meter.
2Connect the original power pack to an easily accessible power
outlet.
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17
CommissioningProLab 1000
3.3Initial commissioning
Perform the following activities:
Insert the batteries (see page 77)
Connect the power pack (see page 17).
Switch on the meter (see page 19)
Set the language (see page 23)
Set the date and time (see page 25)
Set up the access authorization for electronic keys (see page 27)
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ProLab 1000Operation
[i] Apply electronic key
or
Press OK (anonym. access).
Anonymous access
User
[i] Identification successfull
[i]USER ID = 9876543210
Register USER ID
USER ID:1234567890
Erase
Output to RS232/USB
Continue
User
only with administrator login
4Operation
4.1Switch the meter on and off
Switching on
1Press the <On/Off> key.
The display shows the meter designation and software version.
Subsequently, the access control display appears.
2Start anonymous access with <MENU/OK>.
The meter switches to the measuring mode.
or
Place the electronic key on the read field and leave it there for
approx. 2 seconds until the key has been recognized.
The display shows the USER ID that was read.
Switching off
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3Confirm the displayed data with <MENU/OK>.
The meter switches to the measuring mode.
1Press the <On/Off> key.
The meter is switched off.
19
OperationProLab 1000
4.2General operating principles
This section contains basic information on the operation of the
ProLab 1000.
Operating elements,
display
Operating modes,
navigation
An overview of the operating elements and the display is given on
page 8 and page 9.
An overview of the operating modes and navigation of the ProLab 1000
is given on page 20 and page 21.
4.2.1Operating modes
The meter has the following operating modes:
Measuring
Measurement data of the connected sensor appears in the
measured value display
Calibration
The course of a calibration with calibration information, functions
and settings is displayed
Storage in memory
The meter stores measuring data automatically or manually
Transmitting data
The meter transmits measuring data and calibration records to the
serial interface automatically or manually.
Setting
The system menu or a sensor menu with submenus, settings and
functions is displayed
20
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ProLab 1000Operation
General
Measurement
Interface
Clock function
Service information
Reset
System
Language:English
Beep
:On
Illumination
:On
Contrast
:48 %
System
4.2.2Navigation
Measured value displayIn the measured value display, you can
open the relevant measuring menu with <MENU/OK>.
open the system menu with the sensor-independent settings with
<MENU/OK
_>.
change the display in the selected measuring window (e. g. pH <−>
mV) by pressing <MODE>.
Menus and dialogsThe menus for settings and dialogs contain further submenus. The
selection is made with the <▲><▼> keys. The current selection is
displayed in a frame.
Submenus
The name of the submenu is displayed at the upper edge of the
frame. Submenus are opened by confirming with <MENU/OK>.
Example:
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Settings
Settings are indicated by a colon. The current setting is displayed on
the right-hand side. The setting mode is opened with <MENU/OK>.
Subsequently, the setting can be changed with <▲><▼> and
<MENU/OK>.
Example:
21
OperationProLab 1000
Calibration record
Buffer
:NIST/DIN
Calibration interval:7 d
Unit for zero pointpH
Unit for slope
:mV/pH
[i] 2.00 4.01 7.00 10.01
pH
[i] Buffer seriesNIST/DIN
[i] Immerse sensor in buffer 1
Set temperature:25 °C
Continue
pH
Functions
Functions are indicated by the name of the function. They are
immediately carried out by confirming with <MENU/OK>.
Example: Display the Calibration record function.
MessagesInformation or operating instructions are designated by the [i] symbol.
They cannot be selected.
Example:
22
Note
The principles of navigation are explained in the two following sections
by reference of examples:
Setting the language (see page 23)
Setting the date and time (see page 25)
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ProLab 1000Operation
pH
7.000
25.0°C
26.04.06 10:37
Data storage
Display
System
Storage & config
General
Measurement
Interface
Clock function
Service information
Reset
System
4.2.3Navigation example 1: Setting the language
1Switch on the meter (see page 19)
2In the measured value display:
Open the system menu with <MENU/OK
(press for approx. 2 s).
The meter is in the setting mode.
_>
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3Select the System submenu with <▲><▼>.
The current selection is displayed in a frame.
4Open the System submenu with <MENU/OK>.
23
OperationProLab 1000
Language:English
Beep
:Off
Illumination:On
Contrast
:48 %
System
Language:English
Beep
:Off
Illumination:On
Contrast
:48 %
System
5Select the General submenu with <▲><▼>.
The current selection is displayed in a frame.
6Open the General
submenu with <MENU/OK>.
7Open the setting mode for the Language with <MENU/OK>.
24
8Select the required language with <▲><▼>.
9Confirm the setting with <MENU/OK>.
The setting becomes active the next time the system menu is
called up.
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ProLab 1000Operation
Time:14:53:40
Date
:26.04.06
Date format:dd.mm.yy
System
4.2.4Navigation example 2: Setting the date and time
The meter has a clock with a date function. The date and time are
indicated in the status line of the measured value display. This
indication can be switched off. When storing measured values and
calibrating, the current date and time are automatically stored as well.
The correct setting of the date, time and date format is important for the
following functions and displays:
Current date and time
Calibration date
Identification of stored measured values.
Therefore, check the time at regular intervals.
Note
After a drop of the voltage of the buffer batteries (empty batteries), the
date and time are reset and have to be adjusted again.
Setting the date, time
and date format
The data format can be switched from the display of day, month, year
(dd.mm.yy) to the display of month, day, year (mm/dd/yy or mm.dd.yy).
1In the measured value display:
Open the system menu with <MENU/OK
(press for approx. 2 s).
The meter is in the setting mode.
2Using <▲><▼> and <MENU/OK>, select and confirm the
System / Clock function menu.
The setting menu for the date and time appears.
3Using <▲><▼> and <MENU/OK>, select and confirm the Time
menu.
The seconds are highlighted.
_>
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4Change and confirm the setting with <▲><▼> and <MENU/
OK>.
The minutes are highlighted.
25
OperationProLab 1000
5Change and confirm the setting with <▲><▼> and <MENU/
OK>.
The hours are highlighted.
6Change and confirm the setting with <▲><▼> and <MENU/
OK>.
The time is set.
7If necessary, set the Date and Date format. The setting is made
similarly to that of the time.
8If necessary, select and set the Date with <▲><▼> and
<MENU/OK>.
9To make further settings, switch to the next higher menu level
with <ESC>.
or
Switch to the measured value display with <MODE>.
The meter is in the measuring mode.
26
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ProLab 1000Operation
[i] Apply electronic key
or
Press OK (anonym. access).
Anonymous access
User
4.3Access control
When the meter is delivered, only the enclosed electronic administrator
key has an access authorization for the meter.
The administrator can set up access authorizations for electronic keys
(see below).
Anonymous access (USER ID: 0) is always possible.
4.3.1Administrating access authorizations
The ProLab 1000 provides basic functions to administrate access
authorizations. The administrator can set up, erase and display access
authorizations. The administrating functions are available to the
administrator immediately after registration only.
1When the meter is switched on:
Switch off the meter with <On/Off>.
2Press the <On/Off> key.
The display shows the meter designation and software version.
Subsequently, the access control display appears.
3Place the electronic administrator key on the read field and
leave it there for approx. 2 seconds until the key has been
recognized..
The USER ID and the functions for access control are
displayed.
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27
OperationProLab 1000
[i] Identification successfull
[i]USER ID = 9876543210
Register USER ID
USER ID:1234567890
Erase
Output to RS232/USB
Continue
User
Adding new USER IDs
Displaying registered
USER IDs
Erasing a registered
USER ID
4Using <▲><▼> and <MENU/OK>, select and confirm the
menu item, Register USER ID.
An info text for registration is displayed.
5Place the electronic key on the reader field.
The USER ID is displayed and registered.
6Use <MENU/OK> to complete the registration.
7Using <▲><▼> and <MENU/OK>, select and confirm the
USER ID menu item.
8Using <▲><▼>, display the registered USER IDs individually.
9If necessary (e.g. for deleting), confirm a USER ID with
<MENU/OK>.
10Using <▲><▼> and <MENU/OK>, select and confirm the
Erase menu item.
A safety query appears. After confirming the erasure, the access authorization for the currently displayed key number is
erased.
Outputting a list of the
registered USER IDs
28
Switching to the
measuring mode
11Using <▲><▼> and <MENU/OK>, select and confirm the
menu item, Output to RS232/USB.
The list of all key numbers with access authorization is
downloaded to the interface.
12Confirm the data with <MENU/OK>.
The meter switches to the measuring mode.
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ProLab 1000Operation
4.3.2Lost your electronic key?
Without an electronic key with access authorization, anonymous
access is possible only: (USER ID 0).
Electronic keyKeys for additional users are available from SI Analytics GmbH.
The access authorization for new keys is set up by the administrator
(see page 27).
Electronic administrator
key
Activating the lock
If the electronic administrator key is lost, the access authorization for a
new electronic administrator key can be set up in the factory only.
The addresses and telephone numbers of SI Analytics GmbH are given
on the cover of this operating manual.
4.3.3Lock
The activated lock prevents the inadvertent usage of the meter or
registered USER ID during running operation.
The lock can only can only be released with the currently registered
electronic key or the administrator key.
Note
The lock can only be activated in the measuring mode of operation.
With anonymous access (USER ID: 0), the lock function is not
available.
1If necessary, switch to the measuring mode with <MODE>.
2Use <MODE
The registered USER ID is locked against inadvertent use.
_> to activate the lock.
Releasing the lock
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1Press any key.
2Place the registered electronic key or administrator key on the
reader field.
Place the registered electronic user key or administrator key on
the read field and leave it there for approx. 2 seconds until the
key has been recognized.
The lock is released.
29
OperationProLab 1000
4.4System settings (system menu)
The system menu comprises the following settings:
Data storage (see page 30)
Display (see page 30)
System (see page 31).
4.4.1Data storage
This menu contains all functions to display, edit and erase stored
measured values and calibration records.
Note
Detailed information on the data storage functions of the ProLab 1000
is given on page 61.
4.4.2Display
With the aid of the Display submenu, you can modify the measured
value display to meet your requirements. When doing so, you can
display or hide the following elements:
Date indication in the status line
Time indication in the status line
SettingsIn the measured value display, open the system menu with <MENU/
OK
_>. After completing the settings, switch to the measured value
display with <MODE>.
Menu itemSettingDescription
Display / Time:On
Off
Display / Date:On
Off
Display of the time in the system
status line
Display of the date in the system
status line
30
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