Parr Instrument 4857 User Manual

No. 519M
r
Parr Instrument Company
4857
Process Controlle
4857 Reactor Controllers

TABLE OF CONTENTS

Related Instructions .............................2
Customer Service.................................2
Preface 3
Scope...................................................3
Applications..........................................3
Explanation of Symbols........................4
Safety Information................................4
Intended Usage....................................4
General Specifications.........................5
Environmental Conditions....................5
User’s Responsibility............................6
Unpack Carefully..................................6
Installation 7
General Instructions.............................7
Connections.........................................7
Switches and Indicators 8
4857 Switches and Indicators..............8
Protective Fuses 8
4857 Fuses ..........................................8
Model 4857 Process Controller Specifications 9
Temperature Control Parameters.......9
Software Installation 10
Before Software Installation.................10
Minimum PC Requirements.................10
CalGrafix Installation Instructions.........10
Install USB Drivers...............................10
Single Reactor......................................11
Two Reactors.......................................12
Operation of the 4857 Controller 13
Running CalGrafix................................13
Restoring Factory Defaults...................15
Finding the Active COM Port................16
Setting the Active COM Port................16
Changing the Name of a Module .........17
Autotuning............................................18
Module 1: Temperature Control Module
Setpoint Adjustment.............................19
High Temperature Alarm Adjustment...20
Changing PID Settings.........................21
Temperature Programmer....................22
Module 2: Pressure Display and High Pressure Alarm
Alarm Adjustment.................................25
Module 3: Tachometer
Stirring Speed Adjustment...................26
Module 4: Optional Module
Optional Module...................................27
Data Logging 28
Creating a Chart ..................................28
Exporting Data from a Chart................30
Solenoid Valve Module 30 Cleaning and Maintenance 31
Fuses...................................................31
Access to Controller Cabinet...............31
Controller and Circuit Diagrams 32 Parts for the 4857 Controller 35 Related Instructions
The following Parr publications are also included to further your understanding of this instrument and its component parts:
No. Description
201M Limited Warranty 521M 4857 Process Controller CD 547M 4857 CalGrafix CD 567M 4875 Power Controller Operating
Instructions
Customer Service
Questions concerning the installation or operation of this instrument can be answered by the Parr Customer Service Department: 309-762-7716 800-872-7720 Fax: 309-762-9453 www.parrinst.com parr@parrinst.com
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4857 Reactor Controllers

PREFACE

Scope
These instructions cover the installation and operation of Parr Model 4857 Process Controller as used with Parr Laboratory Reactors and Pressure Vessels. They cover the basic functions provided in each of these controllers. The users should study the instructions carefully before using any of these controllers so that they will fully understand the capabilities of this equipment and the safety precautions to be observed in its operation.
Applications
Each Series 4857 Process Controller consists of a packaged temperature control unit completely wired and assembled with appropriate power and safety relays, switches and pilot lights.
These units are designed specifically for use with Parr reactors and pressure vessels and are to be used only with Parr equipment.
Controllers furnished with Parr reactors equipped with variable speed DC motors have a motor switch and a speed control knob on the front panel of the power controller. Controllers to be used with AC equipment or an air motor do not have a speed control knob.
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Explanation of Symbols
4857 Reactor Controllers
I
O
This CAUTION symbol may be present on the Product Instrumentation
Safety Information
To avoid electrical shock, always:
1. Use a properly grounded electrical outlet of correct voltage and current handling capacity.
2. Ensure that the equipment is connected to electrical service according to local national electrical codes. Failure to properly connect may create a fire or shock hazard.
3. For continued protection against possible hazard, replace fuses with same type and rating of fuse.
4. Disconnect from the power supply before maintenance or servicing. The power supply cord of the equipment is the main disconnect device.
To avoid personal injury:
1. Do not use in the presence of flammable or combustible materials where fire or explosion may result. This device contains components which may ignite such materials.
2. Refer servicing to qualified personnel.
On position Off position
and literature. If present on the product, the user must consult the appropriate part of the accompanying product literature for more information.
Protective Earth (PE) terminal. Provided for connection of the Protective Earth (green or green/yellow) supply system conductor.
Intended Usage
This controller has been designed for use with Parr Pressure Vessels, Reactors and Power Controllers. It has been designed, built, and tested to strict physical and electrical standards. However, it is the user's responsibility to install and operate it in conformance with local pressure and electrical codes.
If the instrument is used in a manner not specified by Parr Instrument Company, the protection provided by the equipment may be impaired.
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4857 Reactor Controllers
General Specifications
Electrical Ratings:
115VAC 50/60 Hz 3.0 Amps
230VAC 50/60 Hz 3.0 Amps
Before connecting to a reactor or heating device, the user must be sure that the line, load and other characteristics of the installation do not exceed the following limits:
Voltage: Fluctuations in the line voltage should not exceed 10% of the rated nominal supply voltage shown on the data plate.
Frequency: Controllers can be operated from either a 50 or 60 Hertz power supply without affecting their operation or calibration.
Current: The total current drawn should not exceed the rating shown on the data plate on the controller by more than 10 percent.
Thermocouple. Unless otherwise specified, all Series 4857 Process Controllers operate with a Type J (iron-constantan) thermocouple. The total resistance of the thermocouple and the lead wires should not exceed 100 ohms. If the resistance of the thermocouple circuit is higher, it will not function properly.
Environmental Conditions
This instrument is to be used indoors and requires 3 square feet of space below the controller in a well-ventilated area with convenient access to an electric outlet.
Operating: 15°C to 30°C; maximum relative
humidity of 80% non-condensing. Installation Category II (overvoltage) in accordance with IEC 664. Pollution degree 2 in accordance with IEC 664. Altitude Limit: 2,000 meters.
Storage: -25°C and 65°C; 10% to 85%
relative humidity.
Provisions for Lifting and Carrying Before moving the instrument, disconnect all connections from the rear of the apparatus. Lift the instrument by grabbing underneath each corner.
Caution
Do not use in hazardous atmospheres.
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4857 Reactor Controllers
User’s Responsibility
All Parr Reactors and Pressure Vessels are designed and manufactured with great care to assure safe operation when used within their prescribed temperature and pressure limits.
But…the basic responsibility for safety when using this equipment rests entirely with the user; who must:
1. Select a reactor or pressure vessel that has
the capability, pressure rating, corrosion resistance, and design features that are suitable for its intended use. Parr engineers will be glad to discuss available equipment and material options with prospective users, but the final responsibility for selecting a reactor or pressure vessel that will perform to the user's satisfaction in any particular reaction or test must rest with the user - not with Parr.
In exercising the responsibility for the selection of pressure equipment, the prospective user is often faced with the choice between over- or under-designed equipment. The hazards introduced by under-designed pressure vessels are readily apparent, but the penalties that must be paid for over-designed apparatus are often overlooked. Recognizing these criteria, Parr reactors and pressure vessels are offered in several different styles, each designed for convenient use in daily operation within certain temperature and pressure limits, using gaskets, closures, and other elements carefully selected for safe operation within the limits specified for that design. But in order to preserve the validity of these designs, all temperature and pressure limits must be observed, and no attempt should be made to increase these limits by making alterations or by substituting components which are not recommended by Parr Instrument Company.
2. Install and operate the equipment within a
suitable barricade, if required, with appropriate safety accessories and in full compliance with local safety codes and rules.
All standard Parr pressure vessels are provided with either a suitable relief device or a means to attach one (typically in the form of a plugged opening). When a pressure vessel is delivered without a pressure venting device, it is the customer’s responsibility to provide pressure relief in order to protect the operator and the equipment from destructive high pressures. If you need more information or need help in selecting a proper relief device, please contact Parr Instrument Company.
3. Establish training procedures to ensure that any person handling the equipment knows how to use it properly.
4. Maintain the equipment in good condition and establish procedures for periodic testing to be sure the vessel remains structurally sound.
Unpack Carefully
Unpack the equipment carefully and check all the parts against the packing list. If shipping damage is discovered, report it immediately to the delivering carriers. Examine the components closely for any loose parts or shipping damage and be sure to check all layers of packing materials thoroughly so as not to overlook any parts which might otherwise be discarded.
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4857 Reactor Controllers

INSTALLATION

General Instructions
Set the controller near the reactor on a sturdy bench or table where there is convenient access to an electrical outlet capable of carrying up to 20 amperes. Leave a space of at least twelve inches between the controller and the heater of the reactor so that the controller will not be affected by radiant heat.
Connections
Labeled connections are provided on the rear panel of each controller.
The Control Temp connection is for the internal reactor thermocouple or RTD harness.
The Auxiliary Temp connection is for a secondary thermocouple or RTD harness.
The Tachometer connection is for the optical sensor harness.
The Pressure connection is for the reactor pressure sensor harness.
The Auxiliary connection is for an optional input.
The Power Control connection is for connection to the 4875 Power Controller.
The RS-485 PORT connection is for communication to PC.
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4857 Reactor Controllers
SWITCHES AND INDICATORS
4857 Switches and Indicators
The Main Switch is a manual, two-position,
illuminated switch which will cut off power to the controller. The light indicates power the power is on. Take care to position the controller such that the main power switch may be accessed easily when the controller needs to be disconnected.
PROTECTIVE FUSES
4857 Fuses
Two instrument fuses are mounted on the
back panel. These are Fast-acting, 250VAC, 3.0 amp fuses, intended to protect the internal circuitry of the controller.
4857 Process Controller Front Panel
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4857 Reactor Controllers

MODEL 4857 PROCESS CONTROLLER SPECIFICATIONS

Temperature Control Parameters
To facilitate start up with reasonably good PID control parameters for heating and cooling, all 4857 Process Controllers are programmed at the factory with the temperature control settings shown on the right.
Output 1 on these controllers drives the heater. Output 2 can be used to activate a cooling system. Control parameters can be set independently for each of these outputs.
Module 1: Temperature Control
Cycle time 2 seconds Proportional Band Integral Time 5 min Derivative Time 25 sec
Input thermocouple Operating range Display resolution Setpoint resolution System accuracy
Control action Control output 1 Control output 2
Operating voltages Maximum switching load
25 °C
Type J 0 to 800 °C .1 °C .1 °C +/- 0.1% FS
+/- 1°C typical Three term PID control plus limit control 15 amp @ 115V, 15 amp @ 230V
0.25 amp 115 and 230 VAC 15 amp @ 115 VAC 15 amp @ 230 VAC
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4857 Reactor Controllers

SOFTWARE INSTALLATION OF THE 4857 PROCESS CONTROLLER

Before Software Installation
The CalGrafix software should be installed on a PC which has not previously been used to run software for Cal applications. The PC should meet at least the minimum system requirements.
Minimum PC Requirements
As a general requirement, we would recommend a minimum of Pentium 450MHz with 256MB RAM, Windows screen resolution, 1024 x 768. 100MB of free hard drive space is more than sufficient.
TM
2000/XP and
Installation Instructions:
Note: Temperature control modules have been set to park mode as a precaution against heating before connection to a PC. Following these installation instructions will reset the parameters for these modules to allow heating and stirring.
Do not connect the 4857 to the PC until the following installation has been completed.
CalGrafix Installation Instructions:
1. Locate the 547M CalGrafix CD and insert it into the CD drive.
2. From the CD, open the setup.exe file to run the installation program.
3. Follow on screen instructions to complete installation.
Install USB Drivers (for USB cables only)
Note: If using serial port communication, no driver installation is required.
1. Insert the 521M CD.
2. Attach USB Cable to PC. Do not connect cable to 4857 Process Controller yet.
3. The "Add new hardware" wizard should appear. Click "Next."
4. Select "Search for the best driver for your device." Click "Next."
5. The wizard will then ask the location of the driver. With the Parr 521M CD in the CD-
drive, select "CD-ROM drive" and click "Next."
6. The wizard should find the "\FTDIBUS.INF" file. If it does not find the driver, select
“specify driver location” and find the driver at: ”/installation/USB-SerialPortAdapter/BB­Elec/USOTL4/VISTA_XP or WIN98_ME”. Click "Next."
7. The wizard should install the driver. Click "Next."
8. The wizard will also find the USB Serial Port. This should be installed in the same
manner as the previous driver. When it is finished, click "Finish."
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4857 Reactor Controllers
Connections between single Reactor,
4857 Process Controller, and single 4875 Power Controller
Diagram 1: Schematic Diagram of Connections to
4857 Process Controller for control of a single reactor with 4875 Power Controller
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4857 Reactor Controllers
Connections between two Reactors,
4857 Process Controller, and dual 4875 Power Controllers
Diagram 2: Schematic Diagram of Connections to
4857 Process Controller for control of two reactors with two 4875 Power Controllers
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