BÜCHI Labortechnik AG
Meierseggstrasse 40
Postfach
CH-9230 Flawil 1
E-Mail: quality@buchi.com
BUCHI reserves the right to make changes to the manual as deemed necessary in the light of experience, especially with respect to structure, illustrations and technical details.
This manual is copyrighted. Information from it may neither be reproduced, distributed, or used for competitive purposes, nor made available to third parties. The manufacture of any component with the aid of
this manual without prior written agreement is also prohibited.
Page 3
BÜCHI Labortechnik AGTable of contents
Table of contents
1About this document........................................................................................................... 7
1.1Warning notices in this document........................................................................................................ 7
2.1Proper use ........................................................................................................................................... 9
2.2Use other than intended ...................................................................................................................... 9
3.4.4Location of the type plate.......................................................................................................16
3.5Scope of delivery ............................................................................................................................... 17
3.7Technical data ................................................................................................................................... 17
4.3Lifting the instrument ......................................................................................................................... 20
6.3.3Application menu ...................................................................................................................35
6.3.4Tools menu ............................................................................................................................ 36
6.4Status bar .......................................................................................................................................... 38
6.5Log in administrator mode ................................................................................................................. 39
6.6Editing an application......................................................................................................................... 40
6.6.1Creating a new application.....................................................................................................40
6.6.2Changing the name of an application ....................................................................................41
6.6.3Changing the alias of an application......................................................................................41
6.6.4Changing the Measurement view of an application ............................................................... 42
6.6.5Changing the Measurement mode of an application .............................................................43
6.6.6Changing the Sample presentation of an application ............................................................43
6.6.7Enter a description for an application.....................................................................................44
6.6.8Changing the Rotation of an application................................................................................44
6.6.9Changing the Measurement duration of an application .........................................................45
6.6.10 Enter a Standard Operating Procedure (SOP) for an application..........................................45
6.6.11 Changing the selection ability of an application.....................................................................46
6.7Deleting an application ...................................................................................................................... 47
6.8Editing a property............................................................................................................................... 47
6.8.1Creating a new Property ........................................................................................................ 47
6.8.2Changing the name of a property ..........................................................................................48
6.8.3Changing the alias of a property............................................................................................48
6.8.4Changing the Sort order of a property ...................................................................................49
6.8.5Changing the Prediction type of a property............................................................................49
6.8.6Changing the Initial Wavelength Range (Calibration model only).......................................... 53
6.8.7Changing the Postpredicted Value (Calibration model only) .................................................54
6.8.8Changing the Calibration Base (Calibration model only) ....................................................... 55
6.8.9Changing the Display Basis (Calibration model only)............................................................55
6.8.10 Changing the Formula (Calculated Property only).................................................................56
6.8.11 Changing the Observer (Color only) ...................................................................................... 57
6.8.12 Changing the Illuminant (Color only)......................................................................................57
6.8.13 Changing the Metric (Color only) ........................................................................................... 58
6.8.14 Changing the Metric Element (Color only).............................................................................59
6.8.15 Changing the Decimal places of a property...........................................................................59
6.8.16 Changing the Unit of a property.............................................................................................60
6.8.17 Changing the Bias of a property ............................................................................................60
6.8.18 Changing the Slope of a property .......................................................................................... 61
6.8.19 Changing the Mahalanobis of a property (Calibration model only)........................................61
6.8.20 Changing the Target of a property.........................................................................................62
6.8.21 Changing the Limit maximum of a property ........................................................................... 62
6.8.22 Changing the Limit minimum of a property ............................................................................ 63
6.8.23 Changing the Tolerance maximum of a property...................................................................63
6.8.24 Changing the Tolerance minimum of a property....................................................................64
6.9Deleting a property ............................................................................................................................ 65
6.10Adding measurement data to a calibration ........................................................................................ 65
6.10.1 Performing a calibration update with AutoCal........................................................................65
6.10.2 Setting a reference value to a property..................................................................................66
6.10.3 Activating a measurement for AutoCal ..................................................................................66
6.11Exporting application data ................................................................................................................. 67
6.13Creating a report................................................................................................................................ 68
10.4.2 Spare parts ............................................................................................................................92
viOperation Manual ProxiMate™
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BÜCHI Labortechnik AGAbout this document | 1
1About this document
This operation manual is applicable for all variants of the instrument.
Read this operation manual before operating the instrument and follow the instructions to ensure safe and trouble-free operation.
Keep this operation manual for later use and pass it on to any subsequent user or
owner.
BÜCHI Labortechnik AG accepts no liability for damage, faults and malfunctions resulting from not following this operation manual.
If you have any questions after reading this operation manual:
u Contact BÜCHI Labortechnik AG Customer Service.
https://www.buchi.com/contact
1.1Warning notices in this document
Warning notices warn you of dangers that can occur when handling the device. There
are four danger levels, each identifiable by the signal word used.
Signal wordMeaning
DANGERIndicates a danger with a high level of risk which could result in
death or serious injury if not prevented.
WARNINGIndicates a danger with a medium level of risk which could result in
CAUTIONIndicates a danger with a low level of risk which could result in mi-
NOTICEIndicates a danger that could result in damage to property.
1.2Symbols
The following symbols are displayed in this operation manual or on the device:
1.2.1Warning symbols
SymbolMeaning
death or serious injury if not prevented.
nor or medium-severity injury if not prevented.
General warning
Breakable items
Hot surface
Dangerous electrical voltage
Device damage
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1.2.2Mark-ups and symbols
NOTE
This symbol draws attention to useful and important information.
R This character draws attention to a requirement that must be met before the in-
structions below are carried out.
u This character indicates an instruction that must be carried out by the user.
ð This character indicates the result of a correctly carried out instruction.
Mark-upExplanation
Win dowSoftware Windows are marked-up like this.
TabTabs are marked-up like this.
Dia logDialogs are marked-up like this.
[Button]Buttons are marked-up like this.
[Field names]Field names are marked-up like this.
[Menu / Menu item]Menus or menu items are marked-up like this.
StatusStatus is marked-up like this.
SignalSignals are marked-up like this.
1.3Trademarks
Product names and registered or unregistered trademarks that are used in this document are used only for identification and remain the property of the owner in each
case.
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BÜCHI Labortechnik AGSafety | 2
2Safety
2.1Proper use
The instrument is designed and built for laboratories and production environments (atline). It serves to determine the concentration of selected constituents contained
within a substance.
The instrument can be used for the following tasks:
Determination of quantifiable product properties.
2.2Use other than intended
Use of any kind other than that described in Chapter2.1 "Proper use", page9 and
any application that does not comply with the technical specifications (see Chapter3.7 "Technical data", page17) constitutes use other than that intended.
In particular, the following applications are not permissible:
Use of the instrument in rooms which require Ex-protected instruments.
Use of samples, which can explode or inflame (example: explosives, etc.) due to
shock, friction, heat or spark formation.
2.3Staff qualification
Unqualified persons are unable to identify risks and are therefore exposed to greater
dangers.
The device may only be operated by suitably qualified laboratory staff.
These operating instructions are aimed at the following target groups:
Users
Users are persons that meet the following criteria:
They have been instructed in the use of the device.
They are familiar with the contents of these operating instructions and the applica-
ble safety regulations and apply them.
They are able on the basis of their training or professional experience to assess
the risks associated with the use of the device.
Operator
The operator (generally the laboratory manager) is responsible for the following aspects:
The device must be correctly installed, commissioned, operated and serviced.
Only suitably qualified staff may be assigned the task of performing the operations
described in these operating instructions.
The staff must comply with the local applicable requirements and regulations for
safe and hazard-conscious working practices.
Safety-related incidents that occur while using the device should be reported to the
manufacturer (quality@buchi.com).
BUCHI service technicians
Service technicians authorized by BUCHI have attended special training courses and
are authorized by BÜCHI Labortechnik AG to carry out special servicing and repair
measures.
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2 | SafetyBÜCHI Labortechnik AG
2.4Residual risks
The device has been developed and manufactured using the latest technological advances. Nevertheless, risks to persons, property or the environment can arise if the
device is used incorrectly.
Appropriate warnings in this manual serve to alert the user to these residual dangers.
2.4.1Glass and acrylic breakage
Broken glass and acrylic can cause severe cuts.
Broken glass or acrylic can enter production.
u Handle the Petri Dishes and other glass and acrylic components carefully and do
not drop them.
u Always visually inspect glass and acrylic components for damage every time they
are to be used.
u Do not continue to use glass and acrylic components that are damaged.
u Always wear protective gloves when disposing of broken glass and acrylic.
2.4.2Faults during operation
If a device is damaged, sharp edges or exposed electrical wires can cause injuries.
u Regularly check device for visible damage.
u If faults occur, switch off the device immediately and inform the operator.
u Do not continue to use devices that are damaged.
2.4.3Instrument damage due to an incorrectly installed IP module
An incorrectly installed IP module can cause material and moisture to enter the instrument.
u Do not open the IP module.
u Make sure that the USB sockets are covered when not in use.
2.4.4Malware infection due to connections with other devices or network
Connections with other devices or a network can cause a malware infection to the instrument.
u Install antivirus software and firewall on the instrument before connecting it to
other devices or network.
2.4.5Data loss
In the event of a power failure, e.g. due to lightning or interruption of power supply,
measurement data may be lost.
u Carry out regular data backup.
2.4.6Damage to the internal memory due to incorrect shutting down of the
instrument
Incorrect shutting down of the instrument can cause damage to the internal memory.
u Shut down the instrument as described. See Chapter6 "Operation", page27
2.5Personal protective equipment
Depending on the application, hazards due to heat and/or corrosive chemicals may
arise.
u Always wear appropriate personal protective equipment such as safety goggles,
protective clothing and gloves.
u Make sure that the personal protective equipment meets the requirements of the
safety data sheets for all chemicals used.
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BÜCHI Labortechnik AGSafety | 2
2.6Modifications
Unauthorized modifications may impair safety and lead to accidents.
u Use only genuine BUCHI accessories, spare parts and consumables.
u Technical modifications to the device or accessories should only be carried out
with the prior written approval of BÜCHI Labortechnik AG and only by authorized
BUCHI technicians.
BUCHI accepts no liability whatsoever for damage arising as a result of unauthorized
modifications.
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3 | Product descriptionBÜCHI Labortechnik AG
3Product description
3.1Description of function
ProxiMate™ is a NIR spectrometer that can be used to determine the concentration
of different parameters in food and feed samples in a nondestructive way.
ProxiMate™ is supplied in different versions. Dependent on the version specified
ProxiMate™ is either an NIR or combined NIR and visible spectrometer.
The instrument generates a beam of NIR and visible light which is focused onto the
sample under investigation. Light reflected from the sample is collected and spatially
separated by a diffraction element. The diffracted light is directed onto a diode array
detector. Signals from the detector are processed and a reflectance spectrum is constructed. This spectrum undergoes further processing to calculate the constituents required.
Data processing
The NIR light interacts with the sample material in different ways, leaving a characteristic fingerprint on the spectrum. Spectra from both liquids and solids can be measured with ProxiMate™. The spectra of solid samples are collected directly, liquid
samples require the use of a transflectance adapter.
Application
The Application defines all of the parameters related to measurement of a particular
sample type.
This includes:
the properties to be measured
the calibrations used
the standard operating procedure
It is possible to Import or Export a file that contains all Application data to allow the
same Application to be used on a second ProxiMate™ (dependent on calibration license requirements).
3.2Sample presentation options
The choice of sample presentation of ProxiMate™ is optimised for the type of sample
under analysis and for the working environment where the instrument is used.
ProxiMate™ can be configured with a choice of sample presentation options: up view
and down view configurations.
3.2.1Up view option
The up view option directs and collects light from the underside of the sample. The
NIR light passes through the base of a glass petri dish before interacting with the
sample under evaluation. Up view measurement has the advantage that a more consistent surface is presented to the ProxiMate™ ensuring accurate measurement output. Glass petri dishes are recommended to enable best performance. Additionally,
when used in conjunction with a transflectance adapter, it is also possible to measure
liquids using the up view option.
3.2.2Down view option
With down view option light is focussed onto and collected from the top surface of the
sample. In areas where glass is prohibited (such as some food production areas), the
down view mode offers the advantage that NIR light does not interact with the sample
container. As plastics have their own NIR spectra, changes in type of dish can influ-
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BÜCHI Labortechnik AGProduct description | 3
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1
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ence the measurement output leading to perceived measurement shifts. Use of the
down view mode prevents this from occurring. Additionally ProxiMate™ down view
also allows the use of large volume sample dishes. These are particularly useful with
samples that are inhomogeneous, as the measurement is averaged over a much
larger sample area.
3.3Measurement modes
3.3.1Diffuse reflection mode
Fig.1: Reflection mode (up view geometry)
1 Sample2 Sensor3 Light
Non-translucent materials can be analyzed via diffuse reflection.
NIR light penetration is limited by the sample material. It interacts with the sample, is
refracted and diffusely reflected into the sensor. The reflected rays contain the spectral information of the sample.
3.3.2Transflectance mode
Fig.2: Transflectance mode (up view mode)
1 Transflectance
2 Petri dish3 Sensor4 Light
cover
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3 | Product descriptionBÜCHI Labortechnik AG
5
4
1
2
3
Translucent and opaque liquids can be analyzed via transflectance mode. The light
penetrates the liquid, is diffusely reflected by the reference plate and passes through
the sample a second time. The transflected rays contain the spectral information of
the sample.
Type: xxx
SN: 10xxxxxxxx
Volt: xxx-xxx VAC
Frequ.: xx Hz
Power: xxxx W
Built: 20xx
Made in Switzerland
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5
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3
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7
8
9
10
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3.5Scope of delivery
NOTE
The scope of delivery depends of the configuration of the purchase order.
Accessories are delivered as per the purchase order, order confirmation, and delivery note.
3.6Type plate
The type plate identifies the instrument. The type plate is located at the side of the instrument. See Chapter3.4.4 "Location of the type plate", page16
Fig.7: Type Plate
1Company name and address2Instrument name
3Serial number4Input voltage range
5Frequency6Power consumption maximum
7Year of manufacture8Product code
9Approvals10 Symbol for "Do not dispose of as
3.7Technical data
3.7.1ProxiMate™
SpecificationProxiMate™
Dimensions (W x D x H)260 x 435 x 500 mm
Weight23 kg
Power consumption60 W
Frequency50 / 60 Hz
Connection voltage100 - 240 VAC ± 10 %
Max. power for all USB-Ports5 W
IP CodeIP69
Overvoltage categoryII
household waste"
Pollution degree2
Appliance classesI
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3 | Product descriptionBÜCHI Labortechnik AG
SpecificationProxiMate™
Detector NIRThermoelectrically cooled In-
GaAs
Detector VISSi
Wavelength range NIR900 - 1700 nm
Resolution NIR7.0 nm
NIR Data Resolution3.1 nm
Wavelength range VIS400 - 900 nm
Resolution VIS10 nm
VIS Data Resolution2 nm
Up view illumination spot size8 mm
Down view illumination spot size30 mm
ApprovalCE / CSA
Lamp typeTungsten-halogen
Average life
(lamp)
Display10.4 in
3.7.2Ambient conditions
For indoor use only.
Max. altitude above sea level2000 m
Ambient temperature5 - 40 °C (25 °C)
Maximum relative humidity80% for temperatures up to 31
Storage temperaturemax. 45 °C
3.7.3Materials
ComponentMaterial of construction
HousingSteel 1.4301
Seals housingEPDM 50
HousingAluminum with coating
9000 h
°C
decreasing linearly to 50 % rela-
tive humidity at 40 °C
Seals housingEPDM 70
Glass up viewSapphire Al2O3
Glass down viewBorofloat
Seals glassesEPDM A 75
CoolerAluminum with coating
EPOFLON 526/4562
Sealing frame coolerHD-PE
Seals coolerEPDM
DisplayGlass
Frame displaySteel 1.4301
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BÜCHI Labortechnik AGProduct description | 3
ComponentMaterial of construction
Seal Display1K MS-Polymer Körapop 225
Seals wire moduleFKM
Housing USB/Wi-FiSteel 1.4301
Cover USB/Wi-FiPE-HD
Seals USB/Wi-FiSilicon
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4 | Transport and storageBÜCHI Labortechnik AG
4Transport and storage
4.1Transport
NOTICE
Risk of breakage due to incorrect transportation
Make sure that the instrument is fully dismantled.
Pack every instrument components properly to prevent breakage. Use the original
packaging whenever possible.
Avoid sharp movements during transit.
u After transporting, check the instrument and all glass components for damage.
u Damage that has occurred in transit should be reported to the carrier.
u Keep packaging for future transportation.
4.2Storage
u Make sure that the ambient conditions are complied with (see Chapter3.7 "Tech-
nical data", page17).
u Wherever possible, store the device in its original packaging.
u After storage, check the device for damage and replace if necessary.
4.3Lifting the instrument
WARNING
Danger due to incorrect transportation
The possible consequences are crushing injuries, cuts and breakages.
u The instrument should be transported by two persons at the same time.
u Lift the instrument at the points indicated.
Fig.8: Lifting the instrument
u Lift the instrument – this requires two persons lifting at the points indicated on the
bottom of the instrument.
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BÜCHI Labortechnik AGInstallation | 5
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5Installation
5.1Before installation
NOTICE
Instrument damage due to switching it on too early.
Switching on the instrument too early after transportation can cause damage.
u Climatize the instrument after transportation.
5.2Installation site
The installation site must meet the following requirements:
Firm, level and vibration-free surface.
Minimum space requirement: 260 mm x 435 mm x 500 mm (W x D x H).
Take into account the maximum product dimensions and weight.
Do not expose the instrument to any external thermal loads, such as direct solar
radiation.
NOTE
Make sure that the power supply can be disconnected at any time in an emergency.
5.3Securing against earthquakes
Fig.9: Securing against earthquakes
1Cooler2Cord
u Loop a cord around the cooler and attach it to a fixed point.
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5.4Establishing electrical connections
The instrument is design for stationary installation and therefore not equipped with a
mains plug. The electrical installation must be performed by an electrician or equivalent specialist in any case.
WARNING
Death or serious burns by electric current.
u Have the installation carried out by an electrician or a person with similar expert
knowledge.
u After installation, check electrical safety.
An emergency power-off device must be installed in the vicinity of the instrument with
free access granted.
For details about the installation requirements, see "Electric Installation Instruction"
document.
NOTE
Observe the regulatory provisions when connecting the instrument to power supply.
4 Use external main switches (e.g., emergency off) in accordance with the stan-
dards IEC 60947-1 and IEC 60947-3.
4 Use additional electrical safety features (e.g., residual-current circuit breakers) to
comply with local laws and regulations.
The power supply must fulfill the following conditions:
1. Provide the mains voltage and frequency specified on the type plate of the instru-
ment.
2. Be designed for the load imposed by the instruments connected.
3. Be equipped with suitable fuses and electrical safety features.
4. Be equipped with a proper grounding.
NOTICE
Risk of property damage and diminished performance due to use of unsuitable power cables.
The power supply cables supplied with the product by BUCHI precisely match the requirements of the device. If other power cables that do not meet those requirements
are used, the device may be damaged and/or its performance diminished.
u Use only the power supply cables supplied with the product or ordered separately
from BUCHI.
u If using any other power supply cables, make sure that they match the specifica-
tions on the type plate.
5.5Installing a USB device
NOTE
Make sure that the USB socket is covered either with the cover lid or the protection
cover.
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BÜCHI Labortechnik AGInstallation | 5
u Open one of the cover lids for the USB socket.
u Plug USB device in the USB socket.
u Attach the protection cover.
5.6Software settings
5.6.1Apply for a licence
NOTE
The location of the destination folder is fixed. See Chapter10.2 "Folder locations",
page89
The following data is necessary for the licence request:
Article Name
Software licence serial number (sticker on the cover page of the Quick Guide)
Company Name
First Name
Last Name
Serial Number
Country
E-Mail address
Navigation path
➔➔[Licence Request]
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u Navigate to the action [Licence Request] action via the navigation path.
ð The display shows a dialog with the mandatory information needed for appli-
cation.
u Tap the button
ð The display shows a dialog with an alphanumeric input box.
u Enter your data.
u Tap the button [OK].
ð The dialog box closes.
u After entering all mandatory data tap the button [Create].
u Confirm the secure question by tapping the button [OK].
ð The application file is created.
u Send the file to Buchi to apply for a licence.
E-Mail: registration@buchi.com
5.6.2Import Licence
NOTE
Installed demo license
Delete installed demo license before importing the permanent license.
4 Start the software [Windows Explorer] on the instrument.
4 Navigate to folder options via the following navigation path: View ➔ Folder Op-
tions ➔ View
4 Activate the function [Show hidden files, folders and drives].
4 Delete the demo license file from the following location: c:\ProgramData\BUCHI
\LicenseManager\Licences.
next to the information.
Navigation path
➔➔[Licence Import]
Precondition:
R The licence file is saved on the instrument.
u Navigate to the action [Licence Import] via the navigation path.
ð The display shows a dialog for choosing the folders on the instrument.
u Navigate to the saving folder of the licence you wish to import.
u Select the application.
u Tap the button [OK].
ð The instrument imports the licence.
5.6.3Calibrating a Baseline Correction Vector (BCV)
The Baseline Correction Vector reduces the influence of the sample container or presentation method during measurement.
For routine sample presentation a BCV is calculated with the correct (matching) white
reference standard mounted on the correct spacer. For measurements of liquids the
BCV is calculated using an empty glass petri-dish and transflectance adapter.
NOTE
To ensure that the BCV is calculated correctly the white reference or sample presentation should be rotated 5 times during the operation.
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Navigation path
➔➔[Calibrate BCV]
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
R A sample presentation is defined.
R The instrument is stabilized with at least 2 hours continuous running.
u Navigate to the action [Calibrate BCV] via the navigation path.
ð The instrument shows a dialog box with mandatory settings.
Fig.10: Dialog box Cal ibr ate BCV
1Measurement view2External Reference
3Progress (view)4Measurement mode
5Sample presentation ID
u Select the name of the sample presentation you wish to calibrate.
u Enter the corresponding values.
u Place the white reference or empty sample presentation method in the correct po-
sition.
u Tap the button [Start].
u Follow instructions on the display during the calibration.
u Confirm the instructions by tapping the [OK] button.
5.6.4Import external reference data
NOTE
The location of the destination folder is fixed. See Chapter10.2 "Folder locations",
page89
Navigation path
➔➔ [Import External Refer-
ence Data]
Precondition:
R The reference data file is saved on the instrument.
u Navigate to the action [Import External Reference Data] via the navigation path.
ð The display shows the dialog box Imp ort Ex ter nal Ref ere nce Da ta.
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u Tap the button next to the input box file.
ð The display shows a dialog box with the selectable reference data.
u Select the import file.
u Tap the button [OK].
ð The dialog box closes.
u Tap the button [Import].
ð The external reference is imported.
5.6.5Changing the language of the instrument
Navigation path
➔➔[General]
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the view Gen era l via the navigation path.
u Tap the function [Edit] on the function bar.
u Tap the action [Selected Language].
ð The control panel shows a dialog box with selectable languages.
u Select a language.
u Tap the button [OK].
ð The dialog box closes.
ð The control panel shows a dialog box.
u Tap the button [OK] to confirm the dialog box.
u Restart the software.
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6Operation
CAUTION
Risk of injury from glass splinters
Sharp objects can damage the display.
u Keep sharp objects away from the display.
6.1Layout of the control panel
Fig.11: Control panel
No.DescriptionFunction
1Status barShows the current status of the instru-
ment.
See Chapter6.4 "Status bar", page38
2Menu barShows symbols representing the menus.
3Content areaShows current settings, submenus or ac-
4Function barShows functions that can be performed
See Chapter6.3 "Menu bar", page28
tions depending on the current operation.
according to current operation.
See Chapter6.2 "Function bar",
page27
6.2Function bar
The function bar shows available functions according to the current operation.
The functions on the function bar are executed by tapping the relevant function buttons.
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6 | OperationBÜCHI Labortechnik AG
SymbolDescriptionMeaning
[Back]The display reverts to the previous
view.
[Confirm]Confirm a measurement result.
[Switch off]The instrument shuts down.
[Select]Selects the marked application.
[Login]The display shows the dialog L ogi n.
[Multiple selection]Activates multiple selection of mea-
surements.
[Select all]Selects all measurements in the list.
NOTICE!only available if multiple
selection is activated
[Report]Generates on-screen report
[Save Excel]Saves the report as Excel file.
[Save PDF]Saves the report as PDF file.
[Edit]Allows the selected item to be
edited.
[New]Creates a new application or prop-
erty.
[Delete]Deletes the selected value.
[Copy]Copies the marked application.
[Autocal]Starts the auto calibration function.
[Import]Imports an application.
[Export]Exports the marked application.
[Export measurement
data]
Export the marked measurement
data.
[Information]Shows information about the instru-
ment and the installed Licenses.
[Full page ]The report fits on full page.
[Width scrolling]The report fits to width scrolling.
6.3Menu bar
The menus are represented by symbols on the menu bar. Menus are navigated via
the touchscreen.
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The following menus are available:
Menu symbolMeaningActions
[Start] menu Carrying out a measurement.
See Chapter6.3.1 "Start menu",
page30
[History] menu Shows the results of completed
measurements.
Creating reports.
Adding sample reference values.
Adding samples to calibration set.
Updating calibrations using the
AutoCal function.
Exporting Measurement Data.
See Chapter6.3.2 "History menu",
page32
[Application] menu Creating, editing or selecting an
application.
See Chapter6.3.3 "Application
menu", page35
[Tools] menu Setting up configurations, mainte-
nance and system tests.
Viewing instrument log and other
instrument counters.
Licence requests and import func-
tions.
Setting up remote sessions.
Changing Login credentials.
5Timestamp (automatically)6Shows the properties of the selected
application
7Shows the Standard Operation Pro-
cedure for the selected application
8Note
See Chapter "Insert note", page32
9Barcode
See Chapter "Insert barcode",
page31
Control button
The [control] button can show the following symbols:
SymbolMeaning
The measurement is finished.
The tested sample is in the specifications.
By tapping the symbol the instrument carries out a measure-
ment.
Target value is the expected parameter for the product.
The target value is defined in the Application.
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SymbolMeaning
No application available.
Measurement not possible.
The measurement is finished.
The predicted value is outside the tolerance.
Tolerance is a difference from the target value.
Tolerances are defined in the Application.
The measurement is finished.
A calibration model is missing.
Mahalanobis outlier
The predicted value is outside calibration range.
The predicted value is outside of the set limit.
Limit is an absolute value.
Limits are defined in the Application.
The measurement is in progress.
Cancel measurement.
Insert sample ID
The Sample ID is a label to identify the sample under analysis.
Navigation path
➔
u Tap the button next to [Sample ID].
ð The display shows a dialog with an alphanumeric input box.
u Enter a sample number, name or code.
u Tap the button [OK].
ð The sample ID is saved.
ð The dialog box closes.
Insert barcode
The bar code is a label to identify the sample under analysis.
A barcode reader can be connected to the instrument. When the barcode reader is
configured the user can use this label to identify the sample under analysis.
As an alternative insert a barcode manually
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Navigation path
➔
u Tap the button next to the [Barcode].
ð The display shows a dialog with an alphanumeric input box.
u Enter the Barcode for the sample.
u Tap the button [OK].
ð The barcode is saved.
ð The dialog box closes.
Insert note
The Note is a label to identify the sample under analysis. With default settings the
Note is not a mandatory field.
Navigation path
➔
u Tap the button next to the [Note].
ð The display shows a dialog with an alphanumeric input box.
u Enter a note.
u Tap the button [OK].
ð The note is saved.
ð The dialog box closes.
Insert order
The Order is a label to identify the sample under analysis. With default settings the
Order is not a mandatory field.
Navigation path
➔
u Tap the button next to the [Order].
ð The display shows a dialog with an alphanumeric input box.
u Enter an order number or code.
u Tap the button [OK].
ð The order is saved.
ð The dialog box closes.
6.3.2History menu
The [History] menu lists past measurement data.
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9
8
7
6
12
13
5
42
1
3
11
10
Fig.13: Data menu
1Shows selected filter options
2Timestamp
See Chapter "Select filter", page33
Chapter "Deselect filter", page34
3Filter button4Sample ID
5Sample properties6Displays spectra
7Displays properties / spectra8Enlarge Note Area
9Barcode10 Note
11 Add to calibration dataset button12 Application name
13 Order number
[Cleaning Mode]ProcedureSee Chapter7.7 "Cleaning the dis-
play", page85
(all users)
[Operational Counters]
View / ProcedureThe data is displayed depends on
the system configuration:
Total Operation time / NIR Operation
Time / Lamp UP View / Reference
Up View / System Temperature / Rotation Time / VIS Operation Time /
Lamp Down View / References
Down View / System Humidity
(administrator only)
[Extended System
Test History]
ViewShows a dialog with a further infor-
mation about the tests carried out.
(administrator only)
[Calibrate BCV]ProcedureSee Chapter5.6.3 "Calibrating a
The status bar shows the status of the instrument.
The following statuses are possible:
Indications on the status bar
ViewStatus
Stabilizing SpectrometerShows the remaining time.
Ready to MeasureThe instruments is ready to measure.
Tempering toThe instrument is warming up.
The Status bar shows the target and current instrument temperature.
Configuring…The instrument is starting up.
The instrument is loading an application.
Measuring...The instrument is carrying out a measurement.
Adjusting Exposure Time…Instrument initialization
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ViewStatus
Calibrating BCV…The instrument calibrates the Baseline Correction
Vector.
Initializing…Instrument initialization
Measuring Dark Reference…The instrument measures the internal dark refer-
ence.
ErrorAn error occurred.
See Chapter8 "Help with faults", page86
Extended System TestsThe action Extended System Test is activated. In-
strument waits for action.
Preconditioning…Instrument initialization
Standard System Test Running…
The instrument carries out a Standard System
Test.
System Testing…Instrument running internal tests
Ready for Configuration No application selected.
No Baseline Correction for Sample Presenta-
tion of current application defined.
Measuring White Reference...Instrument initialization
Lamp Pre-HeatingThe instrument is heating the lamp. The Status
bar shows the remaining time.
Symbols on the status bar
SymbolStatus
The current user is logged on as administrator
The instrument is in administrator mode.
The current user is logged on as operator.
The instrument is in operator mode.
A warning has occurred check the [NIRWise log].
See Chapter6.3.4 "Tools menu", page36
6.5Log in administrator mode
Navigation path
➔
Precondition:
R The instrument is in operator mode.
u Navigate to the [Tools] menu via the navigation path.
u Tap the function [Login] in the function bar.
ð The display shows a dialog box with the available Users.
u Tap [Administrator].
ð The display shows a dialog with an alphanumeric input box.
u Enter the password.
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u Tap the button [OK].
ð The dialog box closes.
ð The instrument is in administrator mode.
ð The status bar shows the icon administrator.
6.6Editing an application
NOTE
Applications can only be edited in Administrator mode.
6.6.1Creating a new application
There are two ways to create an application:
by copying an existing application
See Chapter "Creating a new application by copying an existing application",
page40
by creating a new application
See Chapter "Creating a new application", page40
Creating a new application
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the function [Add] on the function bar.
ð The display shows a dialog with an alphanumeric input box.
u Enter a name for the application.
u Tap the button [OK].
ð The dialog box closes.
ð The new application is created.
Creating a new application by copying an existing application
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
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u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the application you wish to copy.
ð The display highlights the application in green.
u Tap the function [Copy] on the function bar.
ð The display shows a dialog with an alphanumeric input box.
u Enter a name for the application.
u Tap the button [OK].
ð The display shows a dialog with the properties of the copied application high-
lighted in green.
u Tap the properties you do not want to copy.
ð The disabled properties are highlighted in white.
u Tap the button [OK].
ð The dialog box closes.
ð The new application is created.
6.6.2Changing the name of an application
NOTE
It is not possible to rename an application after it has been used once.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the action [Name].
ð The display shows a dialog with an alphanumeric input box.
u Enter a name for the new application.
u Tap the button [OK].
ð The dialog box closes.
ð The new name is saved.
6.6.3Changing the alias of an application
The alias function allows to give a previously defined application a local name.
Proceedings:
Navigation path
➔
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Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the action [Alias].
ð The display shows a dialog with an alphanumeric input box.
u Enter an alias for the application.
u Tap the button [OK].
ð The dialog box closes.
ð The alias is saved.
6.6.4Changing the Measurement view of an application
Depending on instrument configuration the following measurement views are available:
ViewExplanation
UpThe application uses the up view lamp.
Radiation is directed and collected from the underside of the
sample through the sample cup.
DownThe application uses the down view lamp.
Radiation is directed onto and collected from the upper surface of the sample. The radiation does not interact with the
sample cup.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the action [Measurement view].
ð The display shows a dialog box with the selectable values.
u Select a value.
u Tap the button [OK].
ð The dialog box closes.
ð The setting is saved.
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6.6.5Changing the Measurement mode of an application
Choose the measurement mode according to the setting for the sample presentation.
See Chapter6.6.6 "Changing the Sample presentation of an application", page43
The following measurement modes are available:
ModeExplanation
Diffuse reflectionThe application runs the measurement in the reflection mode.
Diffuse reflectance measurement mode is used to measure
solid and powdered samples.
Transflection
(up-view instru-
ments only)
The application runs the measurement in the transflection
mode.
Transflectance mode is used to measure liquids and gels.
Transflectance mode require the use of a transflection cover.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the action [Measurement mode].
ð The display shows a dialog box with the selectable values.
u Select a value.
u Tap the button [OK].
ð The dialog box closes.
ð The setting is saved.
6.6.6Changing the Sample presentation of an application
With Baseline Correction Vector (BCV) Different Sample Presentation modes can be
defined to correct, for example, the effect of sample container on the spectral measurement.
The following presentation modes are available:
ModesExplanation
DefaultApply the default settings for baseline correction.
NewCalibrate an individual Baseline correction. See Chapter5.6.3
"Calibrating a Baseline Correction Vector (BCV)", page24
Individual Baseline
Individual calibrated Baseline corrections.
correction
Proceedings:
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Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the action [Sample presentation].
ð The display shows a dialog box with the selectable values.
u Select a value.
u Tap the button [OK].
ð The dialog box closes.
ð The setting is saved.
6.6.7Enter a description for an application
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the action [Description].
ð The display shows a dialog with an alphanumeric input box.
u Enter a description for the application.
u Tap the button [OK].
ð The dialog box closes.
ð The description is saved.
6.6.8Changing the Rotation of an application
The Application has the option to select whether the sample is rotated during measurement.
The following settings are available:
ModeExplanation
YesThe sample carrier rotates during the measurement.
NoThe sample carrier does not rotate during the measurement.
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Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the action [Rotation].
ð The display shows a dialog box with the selectable values.
u Select a value.
u Tap the button [OK].
ð The dialog box closes.
ð The setting is saved.
6.6.9Changing the Measurement duration of an application
The default measurement time (15 seconds) allows the sample to complete one rotation. Shorter measurement time does not allow a complete rotation of the sample.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the action [Measurement duration].
ð The display shows a dialog box with a numeric input box.
u Enter the value in the numeric input box.
u Tap the button [OK].
ð The dialog box closes.
ð The value for the duration is saved.
6.6.10Enter a Standard Operating Procedure (SOP) for an application
Each Application has an optional Standard Operating Procedure (SOP) associated
with it. A Standard Operating Procedure SOP shows instructions for the user to follow
during measurement.
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Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the action [SOP].
ð The display shows a dialog with an alphanumeric input box.
u Enter the steps which the operator has to carry for the application.
u Tap the button [OK].
ð The dialog box closes.
ð The description is saved.
6.6.11Changing the selection ability of an application
Change whether an Application can be selected by the user during operation.
The following modes are available:
ModeExplanation
YesThe application is selectable.
NoThe application is not selectable.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the action [Selectable].
ð The display shows a dialog box with the selectable values.
u Select a value.
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u Tap the button [OK].
ð The dialog box closes.
ð The setting is saved.
6.7Deleting an application
NOTE
It is not possible to delete an application after it has been used for measurement.
NOTE
The following procedure fully deletes the Application. It is not possible to restore the
Application after it has been deleted.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application you wish to remove.
ð The display highlights the application in green.
u Tap the function [Remove] on the function bar.
u Select [Yes] to confirm the action in response to the confirmation question.
ð The application is deleted.
6.8Editing a property
NOTE
Properties can only be edited in Administrator mode.
6.8.1Creating a new Property
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
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u Tap one of the available properties.
ð The display shows the view Pro per ty.
u Tap the function [Add] on the function bar.
ð The display shows a dialog with an alphanumeric input box.
u Enter a name for the property.
u Tap the button [OK].
ð The dialog box closes.
ð The new property is created.
6.8.2Changing the name of a property
NOTE
It is not possible to rename a property after it was used once.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Name].
ð The display shows a dialog with an alphanumeric input box.
u Enter a name for the property.
u Tap the button [OK].
ð The dialog box closes.
ð The new name is saved.
6.8.3Changing the alias of a property
The alias function allows to give a previously defined property a local name.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
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u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Alias].
ð The display shows a dialog with an alphanumeric input box.
u Enter an alias for the property.
u Tap the button [OK].
ð The dialog box closes.
ð The alias is saved.
6.8.4Changing the Sort order of a property
The sort order defines the position in which the property will be displayed within an
Application when there are multiple properties.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Sort order].
ð The display shows a dialog box with a numeric input box.
u Enter the value in the numeric input box.
u Tap the button [OK].
ð The dialog box closes.
ð The value for the Sort order is saved.
6.8.5Changing the Prediction type of a property
The setting of the prediction type influences the further setting possibilities of the
property.
The following settings are available:
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Prediction type ExplanationAvailable predictions settings
[Calibration
model]
Uses assigned calibration model
to predict parameter value from
spectrum.
The calibration model uses a
chemometric model.
Decimal Places see Chapter6.8.15 "Changing the Decimal places of a property",
page59
Unit see Chapter6.8.16 "Changing the Unit of a property",
page60
Initial Wavelength Range
seeChapter6.8.6 "Changing the
Initial Wavelength Range (Calibration model only)", page53
Postpredicted Value see Chapter6.8.7 "Changing the Postpredicted Value (Calibration model
only)", page54
Slope see Chapter6.8.18
"Changing the Slope of a property", page61
Bias see Chapter6.8.17
"Changing the Bias of a property", page60
Mahalanobis see Chapter6.8.19
"Changing the Mahalanobis of a
property (Calibration model
only)", page61
Target see Chapter6.8.20
"Changing the Target of a property", page62
Tolerance Min. see Chapter6.8.24 "Changing the Tolerance minimum of a property",
page64
Tolerance Max. see Chapter6.8.23 "Changing the Tolerance maximum of a property",
page63
Limit Min. see Chapter6.8.22
"Changing the Limit minimum of
a property", page63
Limit Max. seeChapter6.8.21
"Changing the Limit maximum of
a property", page62
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Prediction type ExplanationAvailable predictions settings
[Calculated
Property]
Uses define properties that are
mathematical calculated from
other properties. e.g. Dry Matter
= 100 - Moisture
Decimal Places see Chapter6.8.15 "Changing the Decimal places of a property",
page59
Unit see Chapter6.8.16 "Changing the Unit of a property",
page60
Formula see Chapter6.8.10
"Changing the Formula (Calculated Property only)", page56
Slope see Chapter6.8.18
"Changing the Slope of a property", page61
Bias see Chapter6.8.17
"Changing the Bias of a property", page60
Target see Chapter6.8.20
"Changing the Target of a property", page62
Tolerance Min. see Chapter6.8.24 "Changing the Tolerance minimum of a property",
page64
Tolerance Max. see Chapter6.8.23 "Changing the Tolerance maximum of a property",
page63
Limit Min. seeChapter6.8.22
"Changing the Limit minimum of
a property", page63
Limit Max. see Chapter6.8.21
"Changing the Limit maximum of
a property", page62
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Prediction type ExplanationAvailable predictions settings
[Color]Only for models with a visible
detector.
Measures the sample color.
Decimal Places see Chapter6.8.15 "Changing the Decimal places of a property",
page59
Observer see Chapter6.8.11
"Changing the Observer (Color
only)", page57
Illuminate see Chapter6.8.12
"Changing the Illuminant (Color
only)", page57
Metric see Chapter6.8.13
"Changing the Metric (Color
only)", page58
Metric Element see Chapter6.8.14 "Changing the Metric
Element (Color only)", page59
Slope see Chapter6.8.18
"Changing the Slope of a property", page61
Bias see Chapter6.8.17
"Changing the Bias of a property", page60
Target see Chapter6.8.20
"Changing the Target of a property", page62
Tolerance Min. see Chapter6.8.24 "Changing the Tolerance minimum of a property",
page64
Tolerance Max. see Chapter6.8.23 "Changing the Tolerance maximum of a property",
page63
Limit Min. see Chapter6.8.22
"Changing the Limit minimum of
a property", page63
Limit Max. see Chapter6.8.21
"Changing the Limit maximum of
a property", page62
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
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u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Prediction type].
ð The display shows a dialog box with the selectable values.
u Select a value.
u Tap the button [OK].
ð The dialog box closes.
ð The setting is saved.
u Editing the available prediction settings according to your needs.
6.8.6Changing the Initial Wavelength Range (Calibration model only)
Select the wavelength range for initial calibration.
NOTE
Changes in the project file replace the selection made here.
The following settings are available:
Wavelength typeExplanation
[NIR only]NIR wavelength range only (900 - 1700 nm)
[VIS only]VIS wavelength range only (400 - 900 nm)
[VIS NIR]NIR and VIS wavelength range (400 - 1700 nm)
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Initial Wavelength Range].
ð The display shows a dialog box with the selectable values.
u Select a value.
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u Tap the button [OK].
ð The dialog box closes.
ð The setting is saved.
ð The value for the Initial Wavelength Range is saved.
6.8.7Changing the Postpredicted Value (Calibration model only)
The following settings are available:
Postprediction typeExplanation
[Predicted Value]Calculates the values as predicted by the chemometric
model.
[Residuum]Is an indication of the applicability of the model.
The Residuum is the RMS value of the difference between
pre-treated sample and model reconstructed spectra.
[Mahalanobis Distance] Calculates the value on basis of a mahalanobis calcula-
tion
[Calibration Base Standard]
Converts the parameter value of the calibration to the
value obtained at a different moisture content.
A property moisture is necessary for carrying out this postprediction type.
See:
Chapter6.8.8 "Changing the Calibration Base (Calibration
model only)", page55
Chapter6.8.9 "Changing the Display Basis (Calibration
model only)", page55
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Postpredicted Value].
ð The display shows a dialog box with the selectable values.
u Select a value.
u Tap the button [OK].
ð The dialog box closes.
ð The setting is saved.
ð The value is saved.
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6.8.8Changing the Calibration Base (Calibration model only)
The following settings are available:
TypeExplanation
[Dry Basis]The property value is expressed neglecting the presence
of water in the sample.
The water contribution is subtracted from the calculation.
[Moisture xx %]The property value is expressed assuming xx % water
content.
The amount of water is expressed as a percentage of the
total weight.
[As Is]The property value is expressed including the presence of
water in the sample.
The water contribution is included in the calculation.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
R The post prediction type [Calibration Base Standard] is selected.
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Calibration Base].
ð The display shows a dialog box with the selectable values.
u Select a value.
u Tap the button [OK].
ð The dialog box closes.
ð The setting is saved.
ð The value for the calibration base is saved.
6.8.9Changing the Display Basis (Calibration model only)
The following settings are available:
TypeExplanation
[Dry Basis]The property value is expressed neglecting the presence
of water in the sample.
The water contribution is subtracted from the calculation.
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TypeExplanation
[Moisture xx %]The property value is expressed assuming xx % water
content.
The amount of water is expressed as a percentage of the
total weight.
[As Is]The property value is expressed including the presence of
water in the sample.
The water contribution is included in the calculation.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
R The post prediction type [Calibration Base Standard] is selected.
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Display basis].
ð The display shows a dialog box with the selectable values.
u Select a value.
u Tap the button [OK].
ð The dialog box closes.
ð The setting is saved.
ð The value for the Display basis is saved.
6.8.10Changing the Formula (Calculated Property only)
Calculation formula for the prediction.
Rules how to enter a formula see Chapter10.3 "Rules entering a formula", page90
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
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u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Formula].
ð The display shows a dialog with an alphanumeric input box.
u Enter the formula.
u Tap the button [OK].
ð The dialog box closes.
ð The formula is saved.
6.8.11Changing the Observer (Color only)
The settings available corresponding to the international standard CIE 1931 / CIE
1964.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Observer].
ð The display shows a dialog box with the selectable values.
u Select a value.
u Tap the button [OK].
ð The dialog box closes.
ð The setting is saved.
ð The value for the Observer type is saved.
6.8.12Changing the Illuminant (Color only)
The settings available corresponding to the international standard ISO 11664-2:2007 /
CIE S 014-2:2006.
Proceedings:
Navigation path
➔
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Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Illuminant].
ð The display shows a dialog box with a numeric input box.
u Enter the value in the numeric input box.
u Tap the button [OK].
ð The dialog box closes.
ð The value for the Illuminant is saved.
6.8.13Changing the Metric (Color only)
The following settings are available:
TypeExplanation
[Lab]Calculates the metrics in the L*a*b color space.
[LCh]Calculates the metrics in the L*C*h color space.
[XYZ]Calculates the values in XYZ color space.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Metric].
ð The display shows a dialog box with a numeric input box.
u Enter the value in the numeric input box.
u Tap the button [OK].
ð The dialog box closes.
ð The value for the Metric is saved.
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6.8.14Changing the Metric Element (Color only)
Available options depend on the metric selected in Chapter6.8.13 "Changing the
Metric (Color only)", page58
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Metric Element].
ð The display shows a dialog box with the selectable values.
u Select a value.
u Tap the button [OK].
ð The dialog box closes.
ð The setting is saved.
ð The value for the Metric Element is saved.
6.8.15Changing the Decimal places of a property
Number of decimal places displayed by a property.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Decimal places].
ð The display shows a dialog box with a numeric input box.
u Enter the value in the numeric input box.
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u Tap the button [OK].
ð The dialog box closes.
ð The value for the Decimal places is saved.
6.8.16Changing the Unit of a property
NOTE
Special characters
4 Tab the button [Shift] on the alphanumeric input box.
ð The alphanumeric input box shows the available special characters.
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Unit].
ð The display shows a dialog with an alphanumeric input box.
u Enter a unit for the property.
u Tap the button [OK].
ð The dialog box closes.
ð The Unit is saved.
6.8.17Changing the Bias of a property
A bias is a constant value.
This value is added to the result of a prediction to correct a constant deviation between predicted values and reference values.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
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u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Bias].
ð The control panel shows a dialog box with a numeric input box.
u Enter the value in the numeric input box.
u Tap the button [OK].
ð The dialog box closes.
ð The value for the Bias is saved.
6.8.18Changing the Slope of a property
The slope is a factor that is used to correct proportional systematic differences between the result of a measurement and the reference value.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Slope].
ð The control panel shows a dialog box with a numeric input box.
u Enter the value in the numeric input box.
u Tap the button [OK].
ð The dialog box closes.
ð The value for the Slope is saved.
6.8.19Changing the Mahalanobis of a property (Calibration model only)
The Mahalanobis distance is a measure of spectral similarity between the measured
spectrum and the Dataset used in the calibration.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
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u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Mahalanobis].
ð The control panel shows a dialog box with a numeric input box.
u Enter the value in the numeric input box.
u Tap the button [OK].
ð The dialog box closes.
ð The value for the Mahalanobis is saved.
6.8.20Changing the Target of a property
Sets the target value, relative to which the tolerances are considered.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Target].
ð The control panel shows a dialog box with a numeric input box.
u Enter the value in the numeric input box.
u Tap the button [OK].
ð The dialog box closes.
ð The value for the Target is saved.
6.8.21Changing the Limit maximum of a property
Sets the upper limit for the property.
Proceedings:
Navigation path
➔
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Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Limit Max.].
ð The control panel shows a dialog box with a numeric input box.
u Enter the value in the numeric input box.
u Tap the button [OK].
ð The dialog box closes.
ð The value for the Limit is saved.
6.8.22Changing the Limit minimum of a property
Sets the lower limit for the property.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Limit Min.].
ð The control panel shows a dialog box with a numeric input box.
u Enter the value in the numeric input box.
u Tap the button [OK].
ð The dialog box closes.
ð The value for the Limit is saved.
6.8.23Changing the Tolerance maximum of a property
Tolerance is a difference from the target value.
Sets the upper tolerance relative to the target.
Proceedings:
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Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Tolerance Max.].
ð The control panel shows a dialog box with a numeric input box.
u Enter the value in the numeric input box.
u Tap the button [OK].
ð The dialog box closes.
ð The value for the Tolerance is saved.
6.8.24Changing the Tolerance minimum of a property
Tolerance is a difference from the target value.
Sets the lower tolerance relative to the target.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property that you wish to edit.
ð The display shows the view Pro per ty.
u Tap the action [Tolerance Min.].
ð The control panel shows a dialog box with a numeric input box.
u Enter the value in the numeric input box.
u Tap the button [OK].
ð The dialog box closes.
ð The value for the Tolerance is saved.
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6.9Deleting a property
NOTE
It is not possible to delete a property after it has been used for measurement.
Proceedings:
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the application that you wish to edit.
ð The display highlights the application in green.
u Tap the name of the property you wish to remove.
ð The display highlights the application in green.
u Tap the function [Remove] on the function bar.
u Select [Yes] to confirm the action in response to the confirmation question.
ð The property is deleted.
6.10Adding measurement data to a calibration
6.10.1Performing a calibration update with AutoCal
For performing the AutoCal function the following measurement data is needed:
minimum three measurements
Two of these three measurements with different reference values
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
R Reference values are set. See Chapter6.10.2 "Setting a reference value to a
property", page66
R The measurement you wish to use is activated for AutoCal. See Chapter6.10.3
"Activating a measurement for AutoCal", page66
u Navigate to the [History] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the measurement that you wish to use.
u Tap the button [ AutoCal] on the function bar.
ð The display shows the dialog Aut oCa l.
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1
25
6
34
7
8
Fig.18: Dialog Aut oCa l
1Name of statistic parameters2Values of statistic parameters of ac-
tual calibration
3Values of statistic parameters of new
calibration
5Parameter values according to actual
calibration
4IDs of last n (default = five) measure-
ments
6Parameter values as predicted by
new calibration
7Button [Accept]8Button [Reject]
u Check the data.
u Press the button [Accept].
6.10.2Setting a reference value to a property
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [History] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the measurement that you wish to edit.
u Tap the property you wish to edit.
u Enter the reference value.
u Tap the button [OK].
ð The display shows a dialog box with a numeric input box.
ð The reference value is set.
6.10.3Activating a measurement for AutoCal
Navigation path
➔
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Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [History] menu via the navigation path.
u Tap the function [Edit] on the function bar.
ð The display highlights the function [Edit] in green.
u Tap the name of the measurement that you wish to use.
u Tap the button [Add to calibration dataset ].
ð The measurement is activated for AutoCal.
6.11Exporting application data
This export function allows the use of (unlicenced) applications onto another instrument.
NOTE
The location of the destination folder is fixed. See Chapter10.2 "Folder locations",
page89
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the application you wish to export.
ð The display highlights the application in green.
u Tap the function [Export] on the function bar.
ð The display shows a dialog with the properties of the application you wish to
export. All properties are highlighted in green.
u Tap the properties you do not want to export.
ð The disabled properties are highlighted in white.
u Tap the button [OK].
ð The dialog box closes.
ð The application is exported.
6.12Importing application data
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [Application] menu via the navigation path.
u Tap the function [Import] on the function bar.
ð The display shows a dialog for choosing the folders on the instrument.
u Navigate to the saving folder of the application you wish to import.
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u Select the application.
ð The display shows a dialog with the properties of the application you wish to
import. All properties are highlighted in green.
u Tap the properties you do not want to import.
ð The disabled properties are highlighted in white.
u Tap the button [OK].
ð The dialog box closes.
ð The application is imported.
6.13Creating a report
NOTE
The location of the destination folder is fixed. See Chapter10.2 "Folder locations",
page89
Navigation path
➔
u Navigate to the [History] menu via the navigation path.
u Tap the name of the measurement you wish to create a report.
ð The display highlights the selected measurement in green.
ð The result display shows the values
u Tap the function [Report] on the function bar.
ð The display shows the report.
u According to the requirements tap [Save Excel] or [Save PDF] on the function bar.
ð The report is saved.
6.14Exporting measurement data
Measurement data can be exported for use with NIRWise PLUS or in general export
format (JCAMP.dx or .csv).
NOTE
The location of the destination folder is fixed. See Chapter10.2 "Folder locations",
page89
Navigation path
➔
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the [History] menu via the navigation path.
u Select the measurements you wish to export.
u Tap the function [Export] on the function bar.
ð The display shows a dialog with selectable values.
u Select the file format in which you wish to export the measurement data.
u Tap the button [OK].
ð The measurement data is exported.
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6.15Carrying out a measurement
NOTE
Barcode / Sample ID / Order / Note
Barcode, Sample ID, Order and Note for a sample can be edited during the measurement process at any time.
4 See Chapter "Insert sample ID", page31
4 See Chapter "Insert barcode", page31
4 See Chapter "Insert note", page32
4 See Chapter "Insert order", page32
NOTE
Returning the test sample in the production can cause contamination.
4 Do not return test sample in the production.
NOTE
Contaminated or defective sample carrier
A contaminated or defective sample carrier causes measuring errors.
4 Do not use defective sample carriers.
4 Make sure that the sample carrier is clean.
NOTE
Wrong measurement results due to overfilled petri dishes.
The sample material can fall out from overfilled Petri dishes. This sample material
can lead to an accumulation of material on the measurement window leading to incorrect measurement results.
4 Do not overfill petri dishes.
6.15.1Preparing the instrument
Time required:
up to 30 min
Precondition:
R All commissioning operations have been completed. See Chapter5 "Installation",
page21
u Tap the On/Off master switch.
ð The system starts up.
ð The display highlights the status bar yellow.
ð Once the startup phase is complete the status bar changes from yellow to
black.
6.15.2Starting measurement
Navigation path
➔
Precondition:
R The instrument is prepared. See Chapter6.15.1 "Preparing the instrument",
page69
u Navigate to the [Application] menu via the navigation path.
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u Tap the application you wish to use.
ð The display highlights the application in green.
u Tap the function [Select] on the function bar.
ð The display changes to the [Start] menu.
u According to the application requirements put the sample in the sample presenta-
tion area.
u Tap the [Control] button.
ð The instrument is carrying out the measurement.
ð The status bar shows the status Measuring.
6.15.3Ending measurement
Precondition:
R The control button shows one of the status measurement finished.
u The symbol of the control button shows in which specifications category the sam-
ple fits.
The following specifications categories are possible:
Specifications categories
Within specificationxx
Tolerencexx
Limitxx
u Continue according to the specification the sample is in.
Within specificationTolerenceLimit
u Tap the function [Con-
firm] on the function
u Tap the control button
u Tap the function [Con-
bar.
ð The measurement
is saved.
6.15.4Shutting down the instrument
Navigation path
➔
Explanation see Chapter "Control button",
page30
firm] on the function
bar.
ð The measurement
saved.
Explanation see Chapter10.1 "Measurement
results", page89
u Tap the control button
u Tap the function [Con-
firm] on the function
bar.
ð The measurement
saved.
u Navigate to the [Start] menu via the navigation path.
u Tap the function [Switch off] on the function bar.
u Answer YES to the confirmation question.
ð The instrument is shutting down.
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7Cleaning and servicing
NOTE
Users may only carry out the servicing and cleaning operations described in this section.
Any servicing and repair work which involves opening up the casing may only be carried out by BUCHI service technicians.
u Use only genuine BUCHI consumables and spare parts in order to ensure correct
operation of the device and preserve the warranty.
7.1Regular maintenance work
NOTE
If special cleaning processes are necessary contact BUCHI Customer Service.
www.buchi.com/contact
ComponentActionFrequency
Sample vesselu Wipe down the sample containers
with a damp cloth.
u If heavily soiled:
use mild detergent
rinse with clean water
wipe dry with a lint free cloth
Daily
Glass up viewu Wipe down the glass window with a
damp cloth.
u If heavily soiled, use ethanol or a mild
detergent.
Glass down viewu Wipe down the glass window with a
damp cloth.
u If heavily soiled, use ethanol or a mild
detergent.
Sample presentation
u Wipe down the sample presentation
area with a damp cloth.
u If heavily soiled, use ethanol or a mild
detergent.
Datau Perform a data backup. See Chap-
ter7.6 "Carrying out a data backup",
page84
Casingu Wipe down the casing with a damp
cloth.
u If heavily soiled, use ethanol or a mild
detergent.
Cooling finsu Remove dust and foreign objects
from the cooling fins using compressed air or a vacuum cleaner.
Daily
Daily
Daily
Weekly
Weekly
Weekly
Control panelu Carry out an Baseline Correction Vec-
Weekly
tor test. See Chapter7.5.1 "Carrying
out a Baseline Correction Vector
test", page83
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7 | Cleaning and servicingBÜCHI Labortechnik AG
ComponentActionFrequency
Displayu Wipe down the display with a damp
Weekly
cloth. See Chapter7.7 "Cleaning the
display", page85
Sample carrier slid-
u Check that the sample carrier sliders
ers
Control panelu Carry out an Advanced System Test.
Desiccant cartridge u Check function of the desiccant car-
u If necessary change the desiccant
Control panelu Carry out a Comprehensive System
7.2Changing the lamps
NOTICE
Risk of broken lamp
Monthly
do not show excessive wear.
Monthly
See Chapter7.5.3 "Carrying out an
Advanced System Test", page84
Yearly
tridge.Chapter7.3 "Checking the desiccant cartridge", page80
cartridge. See Chapter7.4 "Changing
the desiccant cartridge", page82
Yearly
Test. See Chapter7.5.2 "Carrying out
a Comprehensive System Test",
page84
Touching the bulb or the reflector with hands can cause lamp damage.
u Do not touch the bulb with fingers.
u
Touch the lamp on the indicated areas.
7.2.1Changing the down view lamp
u Disconnect the power supply to the
instrument.
u Wait 15 min. for lamp to cool.
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u Open the cover lid on the top of the
instrument.
u Remove the seal and the cover lid.
u Press the ferrule.
u Turn the ferrule 1/4 turn counterclock-
wise.
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u Remove the defective lamp from the
lamp socket.
u Disconnect the defective lamp.
u Connect the new lamp.
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u Put the connected new lamp in the
lamp socket.
u Make sure that the screw indicated is
in the groove of the lamp socket.
u Put ferrule and spring on the lamp
socket.
u Press the ferrule.
u Turn the ferrule 1/4 turn clockwise.
u Put the seal and the cover lid on the
instrument.
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u Attach the cover lid to the instrument.
u Change the desiccant cartridge. See
Chapter7.4 "Changing the desiccant
cartridge", page82
calibration. See Chapter5.6.3 "Calibrating a Baseline Correction Vector
(BCV)", page24
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7.2.3Confirm Lamp Replacement
Navigation path
➔➔ [Confirm Lamp Replace-
ment]
Precondition:
R The lamp has been changed.
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Tap the On/Off master switch.
ð The system starts up.
ð The display highlights the status bar yellow.
ð After completion the startup phase the display highlights the status bar black.
u Navigate to the action [Confirm Lamp Replacement] via the navigation path.
u Select which lamp was replaced (up view lamp or down view lamp).
u Confirm the secure question with OK.
7.3Checking the desiccant cartridge
ColorDescribtion
Pinkused cartridge (replacement required)
Blueunused cartridge
u Open the cover lid for the desiccant
cartridge.
u Remove the cover lid and the seal.
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ColorDescribtion
u Check the color of the window of the
desiccant cartridge.
u If necessary change the desiccant
cartridge. See Chapter7.4 "Changing
the desiccant cartridge", page82
u Put seal and cover lid on the instru-
ment.
u Attach the cover lid.
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7.4Changing the desiccant cartridge
u Open the cover lid for the desiccant
cartridge.
u Remove the cover lid and the seal.
u Remove the used desiccant cartridge.
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u Put a new desiccant cartridge in the
instrument.
u Put seal and cover lid on the instru-
ment.
u Attach the cover lid.
7.5Carrying out system tests
7.5.1Carrying out a Baseline Correction Vector test
Navigation path
➔➔[Test BCV]
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
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u Navigate to the action [Test BCV] via the navigation path.
ð The display shows the dialog Tes t B CV.
u Select the name of the sample presentation you wish to test.
u Tap the button [Start].
u Follow instructions on the display during the test.
u Confirm the instructions by tapping the [OK] button.
u Once the test is complete, the instrument records the results in a report.
ð The display shows Baseline Correction Tests is completed.
7.5.2Carrying out a Comprehensive System Test
Navigation path
➔➔[Extended System Test]
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
R External reference data for all standards are loaded.
R Performance Test Standards Kit is available.
u Navigate to the action [Extended System Test] via the navigation path.
ð The display shows the dialog Ext end ed Sys tem Tes t.
u Select check box [Comprehensive System Test]
u Tap the button [Start].
u Follow instructions on the display during the test.
u Confirm the instructions by tapping the [OK] button.
u Once the test is complete, the instrument records the results in a report.
ð The display shows Comprehensive System Tests is completed.
7.5.3Carrying out an Advanced System Test
Navigation path
➔➔[Extended System Test]
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the action [Extended System Test] via the navigation path.
ð The display shows the dialog Ext end ed Sys tem Tes t.
u Select check box [Advanced System Test]
u Tap the button [Start].
ð The instrument starts the test.
u Once the test is complete, the instrument records the results in a report.
ð The display shows Advanced System Tests is completed.
7.6Carrying out a data backup
NOTE
The location of the destination folder is fixed. See Chapter10.2 "Folder locations",
page89
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Navigation path
➔➔[Backup NIRWise Data]
Precondition:
R The instrument is in administrator mode. See Chapter6.5 "Log in administrator
mode", page39
u Navigate to the action [Backup NIRWise Data] via the navigation path.
ð The display shows a dialog with values that can be saved.
u Select the values according to your needs.
u Tap the button [Start].
ð The instrument creates a .zip file with the selected data.
u Save the data to an external data store.
7.7Cleaning the display
The cleaning mode switches off the touch function of the touchscreen.
Navigation path
➔➔ [Cleaning Mode]
u Navigate to the action [Cleaning Mode] via the navigation path.
ð The touch function of the display is locked.
ð The display shows a dialog box with a numeric input box.
u Wipe down the display with a damp cloth.
u Enter the displayed secure code.
u Tap the button [OK].
ð The dialog box closes.
ð The touch function of the display is unlocked.
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8 | Help with faultsBÜCHI Labortechnik AG
8Help with faults
8.1Troubleshooting
ProblemPossible causeAction
The sample carrier
does not rotate
smoothly
Inaccurate ResultsDirect solar radiationu Make sure, that there is no
Sample presentation area is
dirty
u Wipe down the sample
presentation area with mild
detergent.
u Rinse the sample presen-
tation area with clean water.
u Dry the sample presenta-
tion area with a lint free
cloth.
direct solar radiation.
The display is black The instrument is in standbyTap the display.
8.2Error messages
Error codeError messageSolution
1000Unspecified error.u Restart the instrument.
1001The communication with the in-
strument could not be established. The configured serial
port is {0}.
1003Instrument data is not available
or is not valid. Check if serial
number and instrument options
are set.
Sample cup not correctly positioned in sample carrier
u Check that the sample cup
sits correctly in the sample
carrier.
Sample cup not filledu Fill the sample cup prior to
measurement.
u Contact BUCHI Costumer
Service.
u Restart the instrument.
u Contact BUCHI Costumer
Service.
u Restart the instrument.
u Contact BUCHI Costumer
Service.
1004The '{0}' view dark reference
max value ({1} cnt) is out of the
u Contact BUCHI Costumer
Service.
expected range ({2}..{3} cnt).
1005The '{0}' view white reference
max value ({1} cnt) is outside
u Contact BUCHI Costumer
Service.
the expected range ({2}..{3} cnt).
1006The internal reference '{0}' might
not be moving properly.
1007The current system temperature
({0} °C) is outside the expected
range ({1}..{2} °C).
u Contact BUCHI Costumer
Service.
u Move the Instrument to a lo-
cation where the ambient
temperature meets specification.