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P-12
User Manual
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BUCHI P-12 User Manual

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MultivaporTM P-6/P-12
Operation Manual
093156 en
Table of contents
Table of contents
1.1 Reference documents. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
1.2 Trademarks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
1.3 Abbreviations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
2.1 User qualification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
2.2 Proper use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
2.3 Improper use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
2.4 Safety warnings and safety signals used in this manual . . . . . . . . . . . . . . . . . 9
2.5 Product safety. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
2.5.1 Instrument-related hazards . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
2.5.2 Other hazards . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
2.5.3 Personal protective equipment . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
2.5.4 Safety elements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
2.6 General safety rules . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
3.1 Scope of delivery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
3.1.1 Instrument configurations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
3.1.2 Ordering matrix . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
3.1.3 Standard accessories . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
3.1.4 Standard accessory glassware . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22
3.1.5 Optional accessories . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
3.2 Materials used. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
3.3 Technical data overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
3.4 Solvent table . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
Read this manual carefully before installing and running your system and note the safety precautions in chapter 2 in particular. Store the manual in the immediate vicinity of the instrument, so that it can be consulted at any time. No technical modifications may be made to the instrument without the prior written agreement of BUCHI. Unauthorized modifications may affect the system safety or result in accidents. This manual is copyright. Information from it may not be reproduced, distributed, or used for competi­tive purposes, nor made available to third parties. The manufacture of any component with the aid of this manual without prior written agreement is also prohibited.
The English manual is the original language version and serves as basis for all translations into other languages. Other language versions can be downloaded at www.buchi.com.
3 Multivapor™ Operation Manual, Version E
Table of contents
4.1 Functional principle of the Multivapor . . . . . . . . . . . . . . . . . . . . . . . . . 28
4.1.1 Functional principle of the stand-alone unit . . . . . . . . . . . . . . . . . . . . . . 28
4.1.2 Functional principle of the Multivapor-Rotavapor edition. . . . . . . . . . . . . . . . 29
4.1.3 Controls of the Multivapor (stand-alone) . . . . . . . . . . . . . . . . . . . . . . . . 30
4.1.4 Display of the Multivapor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
4.1.5 Rear connections of the Multivapor . . . . . . . . . . . . . . . . . . . . . . . . . . 31
4.2 Multivapor platform . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
4.3 Crystal rack . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32
4.4 Sample preparation rack . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32
4.5 Blank adapters (optional) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
4.6 PE frits . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
4.7 Adapter spring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
4.8 Sample transfer plate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34
4.9 Vacuum cover. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34
4.10 Protective shield (optional). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
4.11 Condensation (optional) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
4.12 High-boiling solvents - Woulff bottle (optional) . . . . . . . . . . . . . . . . . . . . . 36
4.13 Vacuum solution (optional). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
4.14 Connection to a rotary evaporator (optional). . . . . . . . . . . . . . . . . . . . . . 37
4.15 Refrigerated receiver (optional) . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
5.1 Installation site. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38
5.2 Electrical connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38
5.3 Commissioning the Multivapor basic instrument. . . . . . . . . . . . . . . . . . . . 39
5.3.1 Commissioning the crystal rack . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
5.3.2 Assembling the Woulff bottle (optional) . . . . . . . . . . . . . . . . . . . . . . . . 40
5.3.3 Anti-seismic tie-down . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40
5.4 Glass assembly . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41
5.4.1 Type S and type C condenser . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41
5.4.2 Condenser assembly with the refrigerated receiver (optional) . . . . . . . . . . . . . 41
5.5 Tube connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
5.5.1 Cooling water . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
5.5.2 Vacuum tubes. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43
5.6 Commissioning the Multivapor-Rotavapor edition . . . . . . . . . . . . . . . . . . . 44
5.7 Functional test. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
5.7.1 Vacuum tightness test. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
4 Multivapor™ Operation Manual, Version E
Table of contents
6.1 Settings at the Multivapor platform . . . . . . . . . . . . . . . . . . . . . . . . . . 46
6.1.1 Selecting a preset temperature . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
6.1.2 Changing/switching off the preset temperature . . . . . . . . . . . . . . . . . . . . 47
6.1.3 Setting the rotational speed . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
6.2 Sample preparation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
6.2.1 Heating up the instrument . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
6.2.2 Sample preparation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
6.3 Selecting the distillation conditions . . . . . . . . . . . . . . . . . . . . . . . . . . 50
6.4 Distillation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51
6.5 Optimizing the vacuum conditions (optional). . . . . . . . . . . . . . . . . . . . . . 51
6.5.1 Manual vacuum control and solvent library (V-850/V-855) . . . . . . . . . . . . . . . 51
6.5.2 Pressure gradients (V-855) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52
6.5.3 Automatic distillation (V-855) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
6.6 Optimizing the distillation conditions. . . . . . . . . . . . . . . . . . . . . . . . . . 53
6.7 When the distillation “dies out” . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54
6.8 At the end of a run . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54
7.1 Housing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55
7.2 Tube connections and joints. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55
7.3 Sealing system . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55
7.3.1 Cleaning the seals. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55
7.3.2 Replacing the tube adapter seals . . . . . . . . . . . . . . . . . . . . . . . . . . . 56
7.3.3 Replacing the conical adapter O-rings. . . . . . . . . . . . . . . . . . . . . . . . . 56
7.3.4 Cleaning the vacuum cover and replacing the corresponding O-rings . . . . . . . . . 57
7.4 Crystal rack . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57
7.5 Glass components . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
7.6 PE frits (optional) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
8.1 Malfunctions and their remedy. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60
8.2 Customer service . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
9.1 Storage and transport . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
9.2 Disposal. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
9.3 Health and safety clearance form . . . . . . . . . . . . . . . . . . . . . . . . . . . 63
10.1 Basic instrument . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 64
10.2 Evaporation unit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65
10.3 Adapter sets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 67
10.4 Condenser assemblies . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
10.5 Various glass parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69
10.6 Miscellaneous . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71
11.1 FCC requirements (for USA and Canada) . . . . . . . . . . . . . . . . . . . . . . . 73
11.2 Declaration of conformity . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74
5 Multivapor™ Operation Manual, Version E
1 About this manual
This manual describes the Multivapor P-6 and P-12 and provides all information required for its safe operation and to maintain it in good working order. It is addressed in particular to laboratory personnel and operators.
NOTE
The symbols pertaining to safety (WARNINGS and ATTENTIONS) are explained in chapter 2.

1.1 Reference documents

For information on the Rotavapor, the vacuum controller and the vacuum pump, please refer to the corresponding manuals available in English, German, French, Spanish and Italian:
• Rotavapor R-210/215, Operation Manual numbers 93076–93080
• Vacuum Controller, Operating Manual numbers 93081–93085
• Vacuum Pump, Operating Manual numbers 93090–93094

1 About this manual

1.2 Trademarks

The following product names and any registered and unregistered trademarks mentioned in this manual are used for identification purposes only and remain the exclusive property of their respective owners:
®
is a registered trademark of Dionex Corporation
ASE
• Multivapor™ is a trademark of BÜCHI Labortechnik AG
• Rotavapor
®
is a registered trademark of BÜCHI Labortechnik AG
6 Multivapor™ Operation Manual, Version E

1.3 Abbreviations

Chemicals:
EPDM: Ethylenepropylenedimonomer FEP: Combination of tetrafluoroethylene and hexafluoropropylene FFKM: Perfluoro caoutchouc FKM: Fluoric caoutchouc PBT: Polybutyleneterephthalate PE: Polyethylene PEEK: Polyetheretherketone PET(P): Polyethyletherphtalate PETP: Polyethylterephthalate PFA: Perfluoroalkoxy PTFE: Polytetrafluoroethylene PUT: Polyurethane
Miscellaneous:
rpm: revolutions per minute P+G: PLASTIC+GLAS is a unique protective layer for glass components. It offers improved mechan-
ical rupture resistance and increases protection against broken glass whilst ensuring no sample is lost in the event of the receiving flask being damaged.
1 About this manual
7 Multivapor™ Operation Manual, Version E
2 Safety
This chapter highlights the safety concept of the Multivapor and contains general rules of behavior and warnings from hazards concerning the use of the product. The safety of users and personnel can only be ensured if these safety instructions and the safety­related warnings in the individual chapters are strictly observed and followed, therefore, the manual must always be available to all persons performing the tasks described herein.
2.1 User qualification
The instrument may only be used by laboratory personnel or other persons who on account of training or professional experience have an overview of the dangers which can develop when operating the instrument. Personnel without this training or persons who are currently being trained require careful supervision. The present Operation Manual serves as a basis for training.

2 Safety

2.2 Proper use

The instrument has been designed and built for laboratory use only. It serves for activities associated with the parallel evaporation of multiple samples by means of heating under vacuum, with or without regulation by a vacuum controller. The vacuum is typically applied by a PTFE diaphragm vacuum pump. Alternatively, the instrument can be used in combination with a rotary evaporator. In this case the Multivapor serves as an accessory and is connected via an interface to the condenser of the Rotavapor.

2.3 Improper use

Applications beyond those described above are improper. Furthermore, applications which do not comply with the technical data are also considered improper. The operator bears the sole risk for any damages caused by such improper use.
The following applications are expressly forbidden:
• Use of the instrument in rooms which require ex-protected instruments.
• Use as a calibrating instrument for other instruments.
• Preparation of samples which can explode or inflame due to shock, friction, heat or spark forma­tion.
• Use in high pressure situations.
• Processing of hard, brittle and abrasive materials (e.g. stones, sherds, soil samples, etc.) which may destruct the sample tubes.
• Use of the instrument for digestions (e.g. Kjeldahl).
8 Multivapor™ Operation Manual, Version E

2.4 Safety warnings and safety signals used in this manual

DANGER, WARNING, CAUTION and NOTICE are standardized signal words for identifying levels of hazard seriousness of risks related to personal injury and property damage. All signal words, which are related to personal injury are accompanied by the general safety sign.
For your safety it is important to read and fully understand the below table with the different signal words and their definitions!
Sign Signal word Definition Risk level
DANGER
Indicates a hazardous situation which, if not avoided, will result in death or serious injury.
2 Safety
★★★★
WARNING
CAUTION
NOTICE
no
Supplementary safety information symbols may be placed in a rectangular panel on the left to the signal word and the supplementary text (see below example).
Space for
supplementary
safety
information
symbols.
Indicates a hazardous situation which, if not avoided, could result in death or serious injury.
Indicates a hazardous situation which, if not avoided, may result in minor or moderate injury.
Indicates possible property damage, but no practices related to personal injury.
!
SIGNAL WORD
Supplementary text, describing the kind and level of hazard / risk seriousness.
• List of measures to avoid the herein described hazard or hazardous situation.
• ...
• ...
(property damage only)
★★★☆
★★☆☆
★☆☆☆
Table of supplementary safety information symbols The below reference list incorporates all safety information symbols used in this manual and their
meaning.
Symbol Meaning
General warning
Electrical hazard
9 Multivapor™ Operation Manual, Version E
Symbol Meaning
Explosive gases, explosive environment
Harmful to life-forms
Hot item, hot surface
Explosive substance
2 Safety
Device damage
Inhalation of substances
Flammable substances
Fragile items / content
Do not dispose of in household trash
Wear protective mask
Wear laboratory coat
10 Multivapor™ Operation Manual, Version E
2 Safety
Symbol Meaning
Wear protective goggles
Wear protective gloves
Additional user information Paragraphs starting with NOTE transport helpful information for working with the device / software or
its supplementaries. NOTEs are not related to any kind of hazard or damage (see example below).
NOTE
Useful tips for the easy operation of the instrument / software.

2.5 Product safety

The Multivapor is designed and built in accordance with current state-of-the-art technology, however, risks to users, property, and the environment can arise when the instrument is used carelessly or improperly. The manufacturer has determined residual dangers emanating from the instrument
• if the instrument is operated by insufficiently trained personnel.
• if the instrument is not operated according to its proper use.
Appropriate warnings in this manual serve to make the user alert to these residual dangers.

2.5.1 Instrument-related hazards

Pay attention to the following safety notices:
!
Risk of minor or moderate burns when handling hot parts.
• Do not touch hot parts or surfaces (especially the heating plate with up to 95 °C)
!
Death or serious injuries by formation of explosive atmospheres (peroxides) inside the instrument.
• Directly withdraw released fumes and gaseous substances by sufficient ventilation at filling
• Before operation, check all gas connections for correct installation
• Establish inert system atmosphere before processing substances that can form explosive or reactive gases or powders
• Check for proper earth connection to lead off electrostatic charges
CAUTION
WARNING
11 Multivapor™ Operation Manual, Version E
2 Safety

2.5.2 Other hazards

Risk of glass breakage by excessive strains.
• Mount all glassware parts without strains
• Check glassware for proper fixing regularly and readjust fixing points if necessary
• Do not use defective glassware
• Use the protective shield (optional)
Risk of instrument damage by wrong mains supply.
• External mains supply must meet the voltage given on the type plate
• Check for sufficient grounding
Death or serious burns by flammable vapors.
• Remove all sources of flammable vapors
• Do not store flammable chemicals in the vicinity of the device
!
NOTICE
NOTICE
WARNING

2.5.3 Personal protective equipment

Always wear personal protective equipment such as protective eye goggles, protective clothing and gloves. The personal protective equipment must meet all requirements of the supplementary data sheets for the chemicals used.
!
WARNING
Death or serious poisoning by contact or incorporation of harmful substances.
• Wear safety goggles
• Wear safety gloves
• Wear a laboratory coat
12 Multivapor™ Operation Manual, Version E

2.5.4 Safety elements

Electronics
• The heating plate is equipped with an electronic over-temperature protection. It controls the temperature limit (the actual heating plate temperature may not exceed the set temperature by 2 °C for more than 2 minutes) and the function of the temperature sensor.
• The heating plate is equipped with safety fuses.
Parts in direct contact with the instrument
• Combi clip for fixing the vacuum joint.
• Ball joint clip for safe fixing of the receiving flask.
• Rods and holder for attaching the condensation assemblies.
Glass
• Use of high quality, inert 3.3 borosilicate glass.
• Use of tube clips GL-14 for preventing glass breakage.
• PLASTIC+GLAS (P+G) is a unique protective layer for glass components. It offers improved mechanical damage resistance and increases protection against broken glass. It also makes sure that the solvent in the receiving flask is not spilled, if the flask is damage. All glass parts of the condenser assembly are P+G coated.
2 Safety
Anti-seismic tie-down
• The instrument is equipped with a tie-down to fix it in the event of an earthquake.
• Optional
• The protective shield (optional but recommended accessory) protects operators in case of acci­dents from broken glass, solvent splashes, hot water, explosion or implosion.

2.6 General safety rules

Responsibility of the operator The head of laboratory is responsible for training his personnel.
The operator shall inform the manufacturer without delay of any safety-related incidents which might occur during the operation of the instrument. Legal regulations, such as local, state and federal laws applying to the instrument must be strictly followed.
Duty of maintenance and care The operator is responsible for ensuring that the instrument is only operated in proper manner and
that maintenance, service, and repairs are performed with care, on schedule and by authorized personnel only.
Spare parts to be used Use only recommended consumables and spare parts for maintenance to ensure continued optimum
system performance and reliability. Any modifications to the spare parts used are only allowed with the prior written permission of the manufacturer.
Modifications Modifications to the instrument are only permitted after prior consultation with and written approval
obtained from the manufacturer. Modifications and upgrades should only be carried out by an autho­rized BUCHI technical engineer. The manufacturer reserves the right to decline any claim resulting from unauthorized modifications.
13 Multivapor™ Operation Manual, Version E
3 Technical data
This chapter introduces the reader to the Multivapor and its main components. It contains technical data, requirements and performance data.

3.1 Scope of delivery

Check the scope of delivery according to the order number.
NOTE
For detailed information on the listed products, see www.buchi.com or contact your local dealer.
3.1.1 Instrument configurations
The Multivapor is a compact parallel evaporation system with either 6 or 12 position, referred to as Multivapor P-6 or Multivapor P-12, respectively. Both setups are availble in different configurations implying peripherals such as condenser units, vacuum pumps/controllers and a rotary evaporator interface.

3 Technical data

Multivapor Basic Multivapor platform with the crystal rack, vacuum cover, tube adapters, transfer and sample prepara-
tion rack, P+G coated condenser and receiving flask.
14 Multivapor™ Operation Manual, Version E
3 Technical data
Table 3-1: Items included in the Basic configuration
Product Order number
Multivapor platform 220–240 V 100–120 V
Crystal rack P-6 P-12
Vacuum cover P-6 P-12
Tube adapters BUCHI Standard P-6 (6 pieces) BUCHI Standard P-12 (12 pieces)
Glassware BUCHI Standard vessel P-6 (6 pieces) BUCHI Standard vessel P-12 (25 pieces)
Transfer rack P-6 P-12
Sample preparation rack P-6 P-12
Condenser unit, P+G coated type S, 1 l type S, 2 l type C, 1 l type C, 2 l
– –
11057500 11057505
49773 49615
11056598 11057082
49774 49662
49250 49251
49783 49755
48889 48890 48887 48888
Multivapor Professional The difference between the EasyVac and the Professional configuration is that the latter comprises an
additional secondary condenser for the vacuum pump and the vacuum controller V-855.
Table 3-3: Items included in the Professional
configuration
Product Order number
Multivapor P-6/P-12 Basic –
V-700/V-855, Woulff bottle and secondary post pump condenser (type according to
71311 or
71312
the primary condenser)
15 Multivapor™ Operation Manual, Version E
3 Technical data
Multivapor Rotavapor In contrast to the stand-alone configurations described before, this setup is connected to an already
installed rotary evaporator. Delivery therefore includes the Multivapor with a Rotavapor set to combine it with the condenser of the rotary evaporator.
Table 3-4: Items included in the Rotavapor
configuration
Product Order number
Multivapor platform 220–240 V 100–120 V
Crystal rack P-6 P-12
Vacuum cover P-6 P-12
Tube adapters BUCHI Standard P-6 (6 pieces) BUCHI Standard P-12 (12 pieces)
Glassware BUCHI Standard vessel P-6 (6 pieces) BUCHI Standard vessel P-12 (25 pieces)
Transfer rack P-6 P-12
Sample preparation rack P-6 P-12
– –
11057500 11057505
49773 49615
11056598 11057082
49774 49662
49250 49251
49783 49755
Rotavapor adapter set 48740
NOTE
The Rotavapor is not included in the Rotavapor configuration.
16 Multivapor™ Operation Manual, Version E

3.1.2 Ordering matrix

In this section the items accessible by the ordering matrix are listed.
NOTE
The standard plastic material is PETP, however, for very harsh conditions such as trifluoric acid (TFA) PEEK is available as a highly resistant alternative. In this case configure the system without evapo­ration unit and tube adapters (position „00“ in the matrix section „evaporation unit“) and order the corresponding items separately as accessory.
Order number:
MP
x x x x x x x
3 Technical data
Number of sample positions
Product
1: Multivapor P-12
2: Multivapor P-6
Order number:
x x x x x x x
MP
Voltage
Product
1: 220–240 V
2: 100–120 V
17 Multivapor™ Operation Manual, Version E
Order number:
MP
x x
x x x x x
1
Order number:
x x x x x x
MP
3 Technical data
Protective shield
Product Order number
Protective shield P-6, P-12 48784
Evaporation unit, tube adapter, glassware
Product
01: Configuration with evaporation unit (i.e. crystal rack
and vacuum cover), set of tube adapters for BUCHI’s standard sample tubes, preparation/transfer rack, set of BUCHI’s standard sample tubes (ø 60 mm for P-6, ø 25 mm for P-12).
99: Configuration with evaporation unit but without
tube adapters and glassware. The corresponding adapters have to be ordered separately according to the Multivapor Adapter Guide.
00: Configuration without evaporation unit, without
preparation/transfer rack and without adapters and glassware. This is the recommended choice to set up a PEEK system instead of a PETP system. The corresponding items have to be ordered separately as accessory (not via the ordering matrix).
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Order number:
x x x x x x
MP
3 Technical data
Condenser assembly, P+G coated
Product Order number
Type S condenser for tap water or a recirculating chiller.
S1: Condenser with 1 l receiving flask 48889
S2: Condenser with 2 l receiving flask 48890
Type C condenser (cold trap) for dry-ice cooling:
C1: Cold trap with 1 l receiving flask
48887
C2: Cold trap with 2 l receiving flask 48888
R0: Rotavapor adapter set 48740
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Order number:
x x x x x x x
MP
3 Technical data
Vacuum solution
Product Order number
Comprises a Woulff bottle to trap particles and droplets before the vacuum inlet.
V-700, V-855 with secondary condenser according to the type of the primary
71311 or 71312
condenser

3.1.3 Standard accessories

Table 3-5: Standard accessories
Product Order number
Crystal rack P-6 11057500
Crystal rack P-12 11057505
Vacuum cover P-6, PETP* Vacuum cover P-6, PEEK** Vacuum cover P-12, PETP* Vacuum cover P-12, PEEK**
49773 49710 49615
48845 *equipped with EPDM O-rings (FKM enclosed) **equipped with FFKM O-rings
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3 Technical data
Table 3-5: Standard accessories (cont.)
Product Order number
Sample preparation rack P-6 49783
Sample preparation rack P-12 49755
Transfer plate P-6 49251
Transfer plate P-12 49250
Transfer plate P-6 for P-12 adapter 11055146
Table 3-6: Multivapor adapter P-12
Product Order number
Adapter carrier PETP 11057171
Adapter carrier PEEK 11057179
Set of 12 gaskets 11057468
Multivapor and Syncore tool 11057214
Table 3-7: Documentation
Product Order number
Application booklet 48858
Installation/Operation guide 93163
Multivapor IQ/OQ, English 48822
Operation Manual:
English 93156
German 93157
French 93158
Italian 93159
Spanish 93160
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3.1.4 Standard accessory glassware

3 Technical data
1
Fig. 3.1: Overview over the available BUCHI glassware and the corresponding adapters
Sample tubes available from BUCHI
2
3 4
5
6
Adapter set (12) **
PETP PEEK
7
8
Seals **
a BUCHI tube P-12, 60 mL (25 pcs) 49662 11057082 11057178 11057468 (12) b ASE/PSE tube, 60 mL (72 pcs) 49535 11057082 11057178 11057468 (12) c Test tube ø 25 mm (50 pcs) 38469 48873 * 49733 (12)
P-12
d Test tube ø 20 mm (100 pcs) 42845 48778 * 48779 (12)
e Test tube ø 16 mm (100 pcs) 38543 48770 * 48773 (12)
f BUCHI tube P-6, 220 mL (6 pcs) 49774 11056598 11057243 11057469 (6)
g ASE/PSE tube, 240 mL (10 pcs) 52672 11056585 * 48853 (12)
P-6
h ASE/PSE tube, 60 mL (72 pcs) 49535 11056585 * 48853 (12)
*available on request **number of items included in the set given in brackets
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3.1.5 Optional accessories

3 Technical data
Table 3-8: Optional accessories
Product Order number
Protective shield P-6/P-12 48784
Set of 60 PE frits P-6/P-12, ø 10 mm 44856
Blank adapters to close vacant positions
P-6, PETP, 6 pieces P-6, PEEK, 6 pieces P-12, PETP, 12 pieces P-12, PEEK, 12 pieces
Set of Woulff bottle including holder and
49729
49730
48791
48796
11057282 tube
Spare glass for Woulff bottle 11056926
Spare tube 11057283
Set of 1 gasket and 1 O-ring for Woulff
11057990 bottle
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