Metrohm 752 User Manual

CH-9101 Herisau/Switzerland Tel. ++41 71 353 85 85 Fax ++41 71 353 89 01 Internet www.metrohm.ch E-Mail info@metrohm.ch
752 Pump Unit
Pump Unit752
POWER
REMOTE PUMP
OFFOFF
MetrohmMetrohm
8.752.1013 Instructions for Use
1.10.1998 / dö

Table of contents

Table of contents
1 Introduction............................................................................................1
1.1 Instrument description.............................................................................1
1.2 Parts and controls..................................................................................... 2
1.3 Information about the Instructions for Use..........................................4
1.3.1 Organization ..................................................................................4
1.3.2 Notation and pictograms............................................................... 5
1.4 Safety notes ...............................................................................................6
1.4.1 Electrical safety..............................................................................6
1.4.2 General precautionary rules.......................................................... 6
2 Installation..............................................................................................7
2.1 Setting up the instrument........................................................................ 7
2.1.1 Packaging......................................................................................7
2.1.2 Check ............................................................................................7
2.1.3 Location......................................................................................... 7
2.1.4 Arrangement of the instruments....................................................7
2.2 Mains connection......................................................................................8
2.2.1 Setting the mains voltage..............................................................8
2.2.2 Fuses.............................................................................................9
2.2.3 Mains cable and mains connection ..............................................9
2.2.4 Switching the instrument on/off..................................................... 9
2.3 Connection to the IC System ................................................................10
2.3.1 Electrical connection to the 732 IC Detector............................... 10
2.3.2 Connection of the suppressor module .......................................10
3 Operation................................................................................................15
3.1 Manual Operation....................................................................................15
3.2 Operation via 732 IC Detector...............................................................15
4 Troubleshooting.............................................................................17
4.1 Insufficient or non-existing flow rate...................................................17
4.2 Leaking of tubing nipples......................................................................17
4.3 Air bubbles in pump circuit...................................................................18
4.4 Exchanging the pump tubing................................................................18
5 Appendix..................................................................................................19
5.1 Technical data..........................................................................................19
5.2 Standard equipment ...............................................................................21
5.3 Optional accessories..............................................................................21
5.4 Warranty and conformity.......................................................................22
5.4.1 Warranty ......................................................................................22
5.4.2 EU Declaration of conformity ......................................................23
5.4.3 Certificate of conformity and system validation .......................... 24
5.5 Index..........................................................................................................25
752 Pump Unit I
Table of contents
List of figures
Fig. 1: Front of the 752 Pump Unit ............................................................................... 2
Fig. 2: Rear of the 752 Pump Unit................................................................................ 3
Fig. 3: Setting the mains voltage.................................................................................. 9
Fig. 4: Connection 752 Pump Unit – 732 IC Detector................................................ 10
Fig. 5: Connections at suppressor module................................................................ 11
Fig. 6: Installing pump tubings................................................................................... 12
752 Pump UnitII

1 Introduction

1.1 Instrument description
The 752 Pump Unit is a 2-channel peristaltic pump which can be used to pump two solutions simultaneously. It is particularly suitable for op­erating the suppressor module in the 2.733.0X30 IC Separation Center by supplying regeneration and rinsing solutions. This application is de­scribed in detail in these Instructions for Use.
The 752 Pump Unit can either be operated manually by means of the on/off switch for the pump or remotely controlled via the remote inter­face.

1.1 Instrument description

752 Pump Unit 1
1 Introduction

1.2 Parts and controls

33 44 55
Pump Unit752
POWER
REMOTE PUMP
ON ON
OFFOFF
22 11 668899 77
Fig. 1: Front of the 752 Pump Unit
MetrohmMetrohm
11 Pump ON/OFF
On/Off switch for the pump (manual operation mode)
22 Remote ON/OFF
On/Off switch for remote control via remote interface
33 Power on lamp
Lights up when instrument is switched on
44 Tubing cartridge
For 6.1826.050 Pump tubing
55 Contact pressure lever
For adjusting the contact pressure
66 Holding clamp
For locking the tubing cartridge into place
77 Snap-action lever
For releasing the tubing cartridge
88 Pump drive
Roller head with contact rollers
99 Mounting pin
For attaching the tubing cartridge
752 Pump Unit2
1.2 Parts and controls
1010
WARNING - Fire Hazard -
For continued protection replace only with the same type and rating of fuse
f=50-60 Hz S=12 VA
115V: 110-120V: 230V: 220-240V:
Type 1.752.0010 Nr.
Fuse 0,2A(T) 0,1A(T)
S
131312121111
Remote
Pump
Made by Metrohm Herisau Switzerland
1515 1414
Fig. 2: Rear of the 752 Pump Unit
1010 Fuse holder
Changing the fuses, see section 2.2
1111 Voltage selection insert with
display of voltage
1212 Mains switch
For switching the instrument on/off:
I = ON 0 = OFF
1313 Serial number
1414 Remote interface
Remote I/O lines for connection of external devices (e.g. 732 IC De­tector)
1515 Mains connection plug
Mains connection, see section 2.2
752 Pump Unit 3
1 Introduction

1.3 Information about the Instructions for Use

Please read through these Instructions for Use carefully before you put the 752 Pump Unit into operation. The Instructions for Use contain information and warnings to which the user must pay attention in order to assure safe operation of the instruments.

1.3.1 Organization

These 8.752.1013 Instructions for Use for the 752 Pump Unit provide a comprehensive overview of the startup procedure, operation, fault rectification and technical specifications of these instruments. The In­structions for Use are organized as follows:
Section 1 Introduction
General description of instruments, parts and controls and safety notes
Section 2 Installation
Attachment of accessories, connection to IC system
Section 3 Operation
Manual operation and operation via 732 IC Detector
Section 4 Maintenance – Faults
Maintenance, fault rectification
Section5 Appendix
Technical data, standard equipment, options, warranty, declarations of conformity, index
To find the required information on the instruments please use either the Table of contents or the Index at the back.
752 Pump Unit4

1.3.2 Notation and pictograms

The following notations and pictograms (symbols) are used in these In­structions for Use:
<PUMP> Switch or key
1515 Part or control of 752
8989 Part or control of 732/733
"range" Parameter or entry value
1.3 Information about the Instructions for Use
at 732 IC Detector
>PARAM/detector range: 1.00 mS/cm
Display
Text in display 11 of the 732 IC Detector
Hazard
This symbol draws attention to a possible danger to life or of injury if the associated directions are not followed correctly.
Warning
This symbol draws attention to possible damage to instruments or instrument parts if the associated directions are not followed cor­rectly.
Caution
This symbol marks important infor­mation. First read the associated directions before you continue.
Comment
This symbol marks additional in­formation and tips.
752 Pump Unit 5
1 Introduction

1.4 Safety notes

1.4.1 Electrical safety

While electrical safety in the handling of the 752 Pump Unit is assured in the context of the specifications IEC 1010-1 (protection class 1, de­gree of protection IP40), the following points should be noted:
Mains connection
Setting the mains voltage, checking the mains fuse and the mains connection must be effected in accordance with the instructions in
section 2.2.
Opening the 752 Pump Unit
When the 752 Pump Unit is connected to the power supply the in­strument must neither be opened nor should parts be removed from it, otherwise there is a danger of coming into contact with compo­nents which are live. Always disconnect the instrument from all voltage sources before you open it and ensure that the mains cable is disconnected from mains connection 1515 !
Protection against static charges
Electronic components are sensitive to static charging and can be destroyed by discharges. Before you touch any of the components inside the 752 Pump Unit, you should earth yourself and any tools you are using by touching an earthed object (e.g. housing of the instru­ment or a radiator) to eliminate any static charges which exist.

1.4.2 General precautionary rules

Handling of solvents
Check all pump tubings and all input and output lines periodically for possible leaks. Follow the relevant instructions regarding the handling of flammable and/or toxic solvents and their disposal.
Regular exchange of pump tubings
Pump tubings are consumable material and must be replaced from time to time (see section 4.4). Suitable measures must be taken so that any leak which might occur in the pump tubing or connections during unattended operation will cause no damage (placing the instrument at the bottom, collection device for any liquid which may leak out).
752 Pump Unit6
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