The Rotavapor® R-300 meets the highest expectations in convenience and versatility for rotary
evaporation. Its modular design allows for easy extension of the R-300 to a fully integrated system where a central interface regulates each component.
Overview of Rotavapor® R-300 stand-alone and systems
System
Rotavapor® R-300
Rotavapor® R-300 / R-300 Hand Lift**11
Heating Bath B-301 / B-305***1
Interface I-300 / I-300 Pro (incl. VacuBox)***1
Vacuum Pump V-300-1
Recirculating Chiller F-305 / F-308**-*
* optional, according to order code
** according to order code
“Rotavapor® Dynamic”
Rotavapor® R-300
The Rotavapor® R-300 represents high reliability and convenience in laboratory rotary evaporation applications.
The Rotavapor® R-300 is available with either an electronic or manual lift, and can optionally include the Heating Bath B-301 or B-305 and, a glass assembly of your choice and the Interface I-300 or I-300 Pro.
All accessories and connections are included for out of the box usage.
2
Order code
Choose the configuration according to your needs:
Rotavapor® R-300
1301R0
Lift System
1 Manual lift
2 Electronic lift
Heating Bath
0 Without
1 B-301: 20 – 95 °C (water),
max. flask size: 1 L
5 B-305: 20 – 220 °C, max. flask size: 5 L
V Vertical (incl. receiving flask)
A Diagonal (incl. receiving flask)
C Cold trap (incl. receiving flask)
S Vertical reflux (incl. receiving flask)
Protective Coating
0 Without
1 Safety coating (P+G)
1)
2)
Interface
0 Without
1 Without, with Woulff bottle
2 I-300, with Woulff bottle (incl. VacuBox)
3 I-300 Pro, with Woulff bottle (incl. VacuBox)
4 I-300, with valve unit (incl. VacuBox)
5 I-300 Pro, with valve unit (incl. VacuBox)
Voltage
1 220 – 240 V
2 100 – 120 V
1)
If glass assembly E, CR or BY is required, for Glass Assembly select “N”, for Standard Joint select either “1” or “2” and for Protective
Coating select “0” (vapor duct and evaporating flask are included). Glass assembly E, CR or BY need to be ordered separately.
2)
”Safety coating (P+G)” applies to condenser and receiving flask
3
Scope of delivery of Rotavapor® R-300
All configurations are delivered ready to use and are complete of:
ComponentsRotavapor® R-300
Rotavapor® R-300 / R-300 Hand Lift**1
Heating Bath B-301 / B-305***
Glass assembly***
Vapor duct (with Combi-Clip)**
Vacuum seal (WD26)1
Evaporating flask (1 liter)**
Receiving flask (1 liter)**
Flyer “List of solvents”1
Set of required cooling hoses**
Power cable (1 for heating bath, 1 for Rotavapor®)**
Interface I-300 / I-300 Pro***
VacuBox*
* optional, according to order code
** according to order code
4
System “Rotavapor® Dynamic”
The rotary evaporator R-300 system meets the highest expectations in convenience and versatility. It is
bundled with the Vacuum Pump V-300, controlled by the Interface I-300 / I-300 Pro and can include the
Recirculating Chiller F-305 / F-308. The interface is the central control unit for all process parameters. Rotation
speed, heating-, cooling-, vapor-temperature and pressure are perfectly synchronized to optimize the
distillation process while increasing efficiency and convenience. All the “Rotavapor® Dynamic” systems are P+G
coated. All accessories and connections are included for out of the box usage.
Choose the configuration according to your needs:
11S
30R0
Lift System
1 Manual lift
2 Electronic
Heating Bath
1 B-301: 20 – 95 °C (water),
max. flask size: 1 L
5 B-305: 20 – 220 °C, max. flask size: 5 L
*To connect a Vacuum Pump V-300 and a Recirculating Chiller F-305 or F-308 to an Interface I-300 or Interface I-300 Pro a VacuBox is needed. A VacuBox is included when ordering a Rotavapor® R-300 with an
Interface I-300 or Interface I-300 compatibility pack.
R-300 with I-100regulatedregulatedregulatedautonomousregulated
Chiller
F-105 /
F-108
controlled
10
Pump
V-300
Pump
V-700 /
V-710
Pump
V-10 0
Chiller
F-100
Chiller
F-105 /
F-108
R-300 with V-850 /
V-850
To connect the Vacuum Pump V-100 or V-710 and the Recirculating Chiller F-100 or F-105 to the Interface
I-300 or Interface I-300 Pro a Vacubox and a LegacyBox is needed. A VacuBox is included when ordering a
Rotavapor R-300 with Interface I-300 or an Interface I-300 compatibility pack.
∙ Communication cable 11060649 is additionally needed
Explanation of terms
Autonomous:the peripheral (chiller / pump) can be turned On and Off by its own power
Regulated:
Speed controlled:
Manually controlled:the parameters can be adjusted via the peripherals control buttons
regulatedregulatedregulatedautonomousregulated
switch only
the peripheral (pump and chiller) is automatically turned On and Off via interface -> ON/Off communication
the peripheral (pump) is turned On and Off as well as speed controlled via the
inter face
Controlled:the temperature of the chiller can be also set via interface (bi-directional)
Exemplary solutions
The following items are listed on two solutions, shown in the “Laboratory Rotary Evaporation Solutions”
brochure.
The following items have to be purchased in addition to a system that is ordered without glass.
All glass assemblies include a 1 liter receiving flask (corresponding to order code - either without coating, with
P+G or P+G-LT), required hoses and a ball joint clamp. Evaporating flask, vacuum seal, vapor duct (WD26) and
condenser holder are not included. All condensers allow feeding of the evaporating flask via stopcock.
Cooling
Abbr./
NameType / Application
surface
area (max.)Order code
Ver ticalVertical condenser
∙ For standard applications, the most common
condenser
∙ Connection for vapor temperature sensor
∙ Automatic distillation with Interface I-300 / I-300
Pro possible
∙ Use of foam sensor possible
DiagonalDiagonal condenser
∙ For standard applications where height is limited
Cold trapDry ice condenser
∙ For distillation of solvents with low boiling points
∙ Maximum condensation of vapors
∙ No cooling water needed, but i.e. dry ice or ice
∙ Use of foam sensor possible
RefluxVertical reflux condenser with shut-off valve
∙ For combining reflux reaction and distillation
∙ Connection for vapor temperature sensor
∙ Automatic distillation with Interface I-300 / I-300
Pro possible
∙ Use of foam sensor possible
150 0 c m
150 0 c m
500 cm
150 0 c m
2
110 6 2 4 3 2
110 6 2 4 3 3 P+G
2
04 8168
04 8169 P+G
2
040640
04 0 6 42 P+G
2
048290
048291 P+G-LT
Cold trap
reflux
Dry ice condenser with shut-off valve
∙ For combining reflux reaction and distillation
∙ For distillation of solvents with low boiling points
∙ Maximum condensation of vapors
∙ Connection for vapor temperature sensor
∙ No cooling water needed, but i.e. dry ice or ice
∙ Use of foam sensor possible
500 cm
2
048292
048293 P+G-LT
12
Abbr./
NameType / Application
Cooling
surface
area (max.)Order code
ExpansionDescending condenser with expansion vessel
∙ Ideal for distillations exhibiting foaming and
“bumping” tendencies/products
∙ Connection for vapor temperature sensor
∙ Automatic distillation with Interface I-300 / I-300
Pro possible
Double
jacket
Vertical reflux condenser with double jacket for intensive condensation and with shut-off valve
∙ Vertical intensive condenser with double jack-
et and distributor for particularly efficient
condensation
∙ For combining reflux reaction and distillation
∙ For particularly efficient and intensive condensation
∙ Connection for vapor temperature sensor
∙ With an additional SJ 29/32 joint on top for flexible
expansion
∙ Use of foam sensor possible
150 0 c m
1300 cm
2
110 61112
110 61113 P+ G
2
048176
048297 P+G
For more information concerning the glass assemblies please check the “Laboratory Evaporation Glassware”
brochure.
Features of the glass assemblies
Top in l e t
For easy cleaning of the condenser
1
Condenser holder cpl. (048180) is recommended
CharacteristicsVCACRSEBY
Top inlet
Inner glass tube
Inner glass tube
For reduced chimney effect upon vacuum applications
Stopcock (available for R-215, R-210, R-3; see FAQ)
Used for aeration and feeding (by using the feeding hose)
Inner glass plate
Prevention of solvent back flow
Connector for sensor
For measurement of vapor temperature during distillation
•
(SVL22;
extra large)
••••
••
Flask feeding via stopcock possible
Inner glass plate
•••••••
•
13
Connector for vapor
temperature sensor
Condenser holder
••••
11111
•
1
Reflux possibility (part
•••
included)
Condensate trap
•
Rotavapor® accessories
Adapter B-300. For Heating Bath B-305
Required when Heating Bath B-305 is used with a Rotavapor® R-210, R-215 or R II. Heating Bath B-301
does not fit.
Vapor temperature sensor. Incl. cap nut. seal GL14
Measures the vapor temperature inside the system. Meant to be used with the Interface I-300/I-300 Pro.
Lid. For Heating Bath B-305
To safe energy and to minimize loss of water when heating bath is not in use.
Set earthqake fastener. Lug for backside
To fasten Rotavapor® on lab bench.
Order number
110 61317
11060707
110 5 9 5 0 0
110 6 2 3 8 6
Extraction unit Soxhlet. 200 mL, incl. extraction part, reduction part
For Soxhlet extraction applications, Meant to be used with glass assembly S.
Extraction unit Soxhlet. 500 mL, incl. extraction part, reduction part
For Soxhlet extraction applications. Meant to be used with glass assembly S.
Flange screwed connection. For glass assembly V/C/A
Content: Flange nut, pressure spring
Level sensor. Incl. O-ring, cable, rubber band
Prevents an overflow in the receiving flask of condenser/secondary condenser. Placed on receiving flask.
Meant to be used with a Interface I-300/I-300 Pro.
01174 4
01174 5
01810 6
048237
11060954
Holder. For extraction unit, steel, 750 mm, Ø12 mm0119 0 4
Communication cable. Mini-DIN to RJ45, 1.5 m
Connection between Vacuum Controller V-850/V-855 and Vacuum Pump V-300 or between Vacuum Controller V-850/V-855 and Recirculating Chiller F-3xx.
Condensate trap. Grey, TPE, for condenser V, hose connector Ø8 mm
Collects and drains condensate which may accumulate at the condenser.
Condensate trap. Green, TPE, for condenser V, hose connector Ø8 mm
Collects and drains condensate which may accumulate at the condenser
11060649
110 6 2 9 5 5
110 619 8 5
Condenser holder. For glass assembly V/C/S/CR/BY
Content: Holding rod, rubber band, cross sleve
048180
14
Order number
Cooling water valve. 24 VAC
Valve opens cooling water feed during distillation. Meant to be used with a vacuum controller/interface.
Stopcock. For condenser C/CR, glass, SJ18.8/38
For aeration of system. Mounted on vacuum connection at cold trap outer part.
Stopcock. Incl. 3-way valve
For feeding for solvents. Content: Introduction hose 300mm, backfeed hose 600mm, cap nut GL10.
Stopcock. Professional, glass, SJ18.8/38
For aeration of system. Less cross-contamination compared to standard-stopcock (040627).
Stopcock. PTFE, SJ18.8/38
For aeration of system. For applications when grease should be avoided. Used instead of standard-stopcock (040627).
Stopcock. Standard, glass, SJ18.8/38
For aeration of system.
Legacybox. Incl. accessory kit
Interface between Interface I-300/I-300 Pro (with VacuBox) to peripherals of older generations (Vacuum
Pump V-7xx, Recirculating Chiller F-1xx).
Flask holder. EPDM, slip free
Holder for round-bottom flasks (50-5000 mL).
031356
040628
110 5 8 814
000637
023896
040627
110 6116 6
048 618
Flask holders. set. EPDM, slip free
Holder for round-bottom flasks (50-5000 mL).
Tubing, FEP. Ø6/8 mm, transparent, per m
Use: Vacuum, cooling media
Tubing. Natural rubber, Ø6/16 mm, red, per m
Use: Vacuum
Tubing. Nyflex, PVC-P, Ø8/14 mm, transparent, per m
Use: To introduce solvent into evaporating flask during distillation.
Tubing. PTFE, Ø4.7/5.5 mm, transparent, 460 mm
Use: To introduce solvent into evaporating flask during distillation.
Tubing. Silicone rubber, Ø6/9 mm, transparent, per m
Use: Cooling media
Protection shield. Operator protection for heating bath
For Heating Bath B-301 and B-305.
Heating bath balls. 450 pcs, PP, Ø10 mm
To reduce energy consumption of heating bath and for less evaporation of the heating medium. For temperatures up to 100 °C.
11059916
027900
01762 2
0 0 4113
000646
000643
00413 3
110 6140 2
036405
Vacuum valve. Magnetic valve, 24V/4W, Mini-DIN, 1.5 m
Flow valve without flask, meant to be used with a centralized vacuum source or an unregulated vacuum
pump. Meant to be used with the Interface I-300/I-300 Pro.
Vacuum connection. Incl. drain valve, hose barb
Connection piece for aeration of the system, placed between condenser and receiving flask.
11060706
001006
15
Order number
Water regulation nozzle. Flow Regulator, incl. hose clamp, sieve
Used when tap water is used to generate vacuum. Reduces water consumption.
Water jet pump. Plastic
Used when tap water is used to generate vacuum.
Rotavapor® accessories – Heating Baths
Heating bath. Heating Bath B-301, not incl. Base B-300, 110V
For up to 1 Liter evaporating flasks. For temperatures up to 95 °C. Meant to be used with water as
heating media.
Heating bath. Heating Bath B-301, not incl. Base B-300, 230V
For up to 1 Liter evaporating flasks. For temperatures up to 95 °C. Meant to be used with water as
heating media.
Heating bath. Heating Bath B-301, incl. Base B-300, 110V
For up to 1 Liter evaporating flasks. For temperatures up to 95 °C. Meant to be used with water as
heating media.
Heating bath. Heating Bath B-301, incl. Base B-300, 230V
For up to 1 Liter evaporating flasks. For temperatures up to 95 °C. Meant to be used with water as
heating media.
0116 0 6
002913
Order number
11B 3 0 1 0 0 2
11B301001
11B 3 0 11 0 2
11B 3 0 11 0 1
Heating bath. Heating Bath B-305, not incl. Base B-300, 110V
For up to 5 Liter evaporating flasks. For temperatures up to 220 °C. Meant to be used with water or oil
as heating media.
Heating bath. Heating Bath B-305, not incl. Base B-300, 230V
For up to 5 Liter evaporating flasks. For temperatures up to 220 °C. Meant to be used with water or oil
as heating media.
Heating bath. Heating Bath B-305, incl. Base B-300, 110V
For up to 5 Liter evaporating flasks. For temperatures up to 220 °C. Meant to be used with water or oil
as heating media.
Heating bath. Heating Bath B-305, incl. Base B-300, 230V
For up to 5 Liter evaporating flasks. For temperatures up to 220 °C. Meant to be used with water or oil
as heating media.
11B 3 0 5 0 0 2
11B 3 0 5 0 0 1
11B 3 0 510 2
11B 3 0 510 1
Rotavapor® wear parts
Order number
Seal. For cap nut GL14 to FEP, EPDM038225
Seals. set. 10 pcs, for hose barbs GL14, EPDM, black040029
Seals. set. 10 pcs, for hose barbs GL14, FPM, green040040
Seals. set. 20 pcs, for hose barbs GL14, silicone, red040023
O-ring. FKM, 40.9/2.6 mm, for reflux insert048078
O-ring. FPM, for screw cap GL10, Ø3.00/2.70mm023900
Hose barb. Bent, GL14, incl. silicone seal018 916
Hose barbs. set. 2 pcs, bent (1), straight (1), GL14, silicone seal
Content: Hose barbs, cap nuts, seals
04193 9
16
Order number
Hose barbs. set. 2 pcs, bent (1), straight (1), GL14 silicone seal
Content: Hose barbs, cap nut, screw caps seals
Hose barbs. set. 3 pcs, bent, GL14, silicone seal
Content: Hose barbs, seals
Hose barbs. set. 4 pcs, bent GL14, silicone seal
Content: Hose barbs, cap nuts, seals
Hose barbs. set. 4 pcs, bent, GL14, EPDM seal
Content: Hose barbs, cap nuts, seals
Hose barbs. set. 4 pcs, bent, GL14, FEP seal
Content: Hose barbs, cap nuts, seals
Hose barbs. set. 4 pcs, straight, GL14, EPDM seal
Content: Hose barbs, cap nuts, seals
Hose barbs. set. 4 pcs, straight, GL14, FPM seal
Content: Hose barbs, cap nuts, seals
Hose barbs. set. 4 pcs, straight, GL14, silicone seal
Content: Hose barbs, cap nuts, seals
Hose barbs. set. 6 pcs, bent (4), straight (2), GL14, silicone seal
Content: Hose barbs, cap nuts, seals
110 619 2 1
0419 87
037287
043129
040295
043128
040296
037642
038000
Screw caps. set. 5 pcs, GL14040624
Cap nut. Screw cap with hole GL10023875
Cap nuts. set. 10 pcs, screw cap with hole GL14, seal EPDM
Content: Hose barbs, cap nuts, seals
041999
Cap nuts. set. 10 pcs, screw cap with hole, GL1404195 6
Vacuum gasket. WD26, PTFE, FDA-compliant048021
Rotavapor® glass accessories – Vapor ducts
Vapor ducts compatible with WD26
SJ29/3224/4029/4224/2934/35
For glass assembly V, C, S, E, CR, BY
For glass assembly A
For glass assembly C, V (analytical)
For glass assembly C and V (KD22)
110 6 2 18 6110 6 2 18 7110 6 2 4 6 411062909–
110 6 2 26 7110 6 22 6 81106 22 6 9–048167
110 6 2 4 6 5110 6 24 6 6110 6 24 67––
11062910––––
Additional glassware
Additional glassware like evaporating flasks, drying flasks, receiving flasks, beaker flasks, Reitmeyer adapters
(bump traps) and distillation spiders can be found in the “Laboratory Evaporation Glassware”-brochure.
www.buchi.com/laboratory-evaporationQuality in your hands
R-300 D ata Sheet en 1506 A/ Techni cal data are subj ect to cha nge wit hout not ice /
Quali ty Systems ISO 9001
Loading...
+ hidden pages
You need points to download manuals.
1 point = 1 manual.
You can buy points or you can get point for every manual you upload.