Page 1
Vacuum Pump V-100
Operation Manual
11593636E en
Page 2
Imprint
Product Identification:
Operation Manual (Original) Vacuum Pump V-100
11593636
Publication date: 06.2017
BÜCHI Labortechnik AG
Meierseggstrasse 40
Postfach
CH-9230 Flawil 1
E-Mail: quality@buchi.com
BUCHI reserves the right to make changes to the manual as deemed necessary in the light of experience, especially with respect to structure, illustrations and technical detail.
This manual is copyrighted. Information from it may not be reproduced, distributed, or used for competitive purposes, nor made available to third parties. The manufacture of any component with the aid of this
manual without prior written agreement is also prohibited.
Page 3
BÜCHI Labortechnik AG Contents
Operation Manual Vacuum Pump V-100 iii
Contents
1 About this document........................................................................................................... 5
1.1 Warning notices in this document........................................................................................................ 5
1.2 Symbols............................................................................................................................................... 5
1.2.1 Warning symbols .....................................................................................................................5
1.2.2 Mandatory directive symbols ...................................................................................................6
1.2.3 Other symbols..........................................................................................................................6
1.3 Available languages............................................................................................................................. 6
1.4 Trademarks.......................................................................................................................................... 6
2 Safety....................................................................................................................................7
2.1 Intended use........................................................................................................................................ 7
2.2 Use other than that intended ............................................................................................................... 7
2.3 Staff qualification ................................................................................................................................. 7
2.4 Residual risks ...................................................................................................................................... 8
2.4.1 Dangerous vapors.................................................................................................................... 8
2.4.2 Faults during operation ............................................................................................................ 8
2.5 Personal protective equipment ............................................................................................................ 8
2.6 Modifications........................................................................................................................................ 8
3 Product description........................................................................................................... 10
3.1 Description of function ....................................................................................................................... 10
3.2 Configuration ..................................................................................................................................... 10
3.2.1 Front view ..............................................................................................................................10
3.2.2 Rear view ............................................................................................................................... 11
3.2.3 Internal view...........................................................................................................................12
3.2.4 Typical application .................................................................................................................13
3.2.5 Type plate .............................................................................................................................. 14
3.3 Specifications supplied ...................................................................................................................... 14
3.4 Technical data ................................................................................................................................... 15
3.4.1 Vacuum Pump V-100.............................................................................................................15
3.4.2 Ambient conditions.................................................................................................................15
3.4.3 Materials ................................................................................................................................15
4 Transport and storage ......................................................................................................16
4.1 Transport ........................................................................................................................................... 16
4.2 Storage .............................................................................................................................................. 16
4.3 Removing transit fixings..................................................................................................................... 17
5 Installation.......................................................................................................................... 18
5.1 Important considerations prior to commissioning .............................................................................. 18
5.2 Installation site................................................................................................................................... 19
5.3 Connecting laboratory equipment...................................................................................................... 19
5.4 Connecting the silencer ..................................................................................................................... 21
5.5 Connecting a Woulff bottle................................................................................................................. 23
5.6 Connecting a secondary condenser .................................................................................................. 24
5.7 Connecting a secondary cooling cold trap......................................................................................... 26
5.8 Electrical connections........................................................................................................................ 27
5.9 Fitting and connecting the Interface I-100 ......................................................................................... 28
5.9.1 Fitting an interface unit to the Vacuum Pump V-100 .............................................................28
5.9.2 Connecting interface unit to Vacuum Pump V-100................................................................ 29
Page 4
Contents BÜCHI Labortechnik AG
iv Operation Manual Vacuum Pump V-100
6 Operation............................................................................................................................ 30
6.1 Operating V-100 with Interface I-100................................................................................................. 30
6.2 Operating V-100 without Interface I-100............................................................................................ 30
7 Cleaning and servicing .....................................................................................................31
7.1 Cleaning............................................................................................................................................. 31
7.1.1 Important considerations when cleaning................................................................................ 31
7.1.2 Cleaning the pump.................................................................................................................31
7.1.3 After working with strong acids .............................................................................................. 31
7.1.4 Cleaning the housing ............................................................................................................. 32
7.1.5 Cleaning glass components...................................................................................................32
7.1.6 Cleaning tubing...................................................................................................................... 32
7.1.7 Cleaning valve heads.............................................................................................................32
7.1.8 Cleaning non-return valve......................................................................................................33
7.1.9 Cleaning the membrane......................................................................................................... 33
7.2 Servicing............................................................................................................................................ 33
7.2.1 Notes on servicing .................................................................................................................33
7.2.2 Dismantling and reassembling pump head............................................................................35
7.2.3 Replacing the membrane.......................................................................................................38
7.2.4 Replacing valve......................................................................................................................39
7.2.5 Replacing tubing .................................................................................................................... 40
8 Help with faults ..................................................................................................................41
8.1 Faults, possible causes and remedies............................................................................................... 41
8.2 Customer service............................................................................................................................... 42
9 Taking out of service and disposal.................................................................................. 43
9.1 Taking out of service.......................................................................................................................... 43
9.2 Disposal............................................................................................................................................. 43
10 Appendix ............................................................................................................................44
10.1 Solvent table...................................................................................................................................... 44
10.2 Spare parts and accessories ............................................................................................................. 46
10.2.1 Accessories............................................................................................................................46
10.2.2 Wear parts .............................................................................................................................47
10.2.3 Spare parts ............................................................................................................................48
10.3 List of abbreviations........................................................................................................................... 49
10.4 Health and safety approval................................................................................................................ 49
10.5 Health and safety............................................................................................................................... 50
Page 5
BÜCHI Labortechnik AG About this document | 1
Operation Manual Vacuum Pump V-100 5/52
1 About this document
These operating instructions describe the Vacuum Pump V-100 at the time supplied.
They are an integral part of the product and contain important information that is necessary for safe operation and maintenance.
These operating instructions apply to all variants of the Vacuum Pump V-100 and are
intended primarily for laboratory staff.
u To ensure safe and trouble-free operation, read these operating instructions be-
fore starting up the device and follow the guidance they contain.
u Keep the operating instructions somewhere near to the device.
u Pass on the operating instructions to any subsequent owner or user.
BÜCHI Labortechnik AG accepts no liability whatsoever for any faults or damage that
result from the failure to follow these operating instructions.
u If you still have any questions after reading these operating instructions, please
contact BÜCHI Labortechnik AG Customer Service. Contact details for your local
agents can be found on the back cover of these operating instructions or on the Internet at http://www.buchi.com.
1.1 Warning notices in this document
Warning notices warn you of dangers that can occur when handling the device. There
are four danger levels, each identifiable by the signal word used.
Signal word Meaning
DANGER Indicates a danger with a high level of risk which could result in
death or serious injury if not prevented.
WARNING Indicates a danger with a medium level of risk which could result in
death or serious injury if not prevented.
CAUTION Indicates a danger with a low level of risk which could result in mi-
nor or medium-severity injury if not prevented.
IMPORTANT Indicates a danger that could result in damage to property.
1.2 Symbols
The following symbols may be displayed in this instruction manual or on the device:
1.2.1 Warning symbols
Symbol Meaning Symbol Meaning
General warning Corrosive substance
Dangerous electrical voltage Flammable substance
Biological hazard Potentially explosive atmos-
phere
Breakable items Dangerous gases
Page 6
1 | About this document BÜCHI Labortechnik AG
6/52 Operation Manual Vacuum Pump V-100
Symbol Meaning Symbol Meaning
Hot surface Health-harming or irritant
substances
Risk of hand injury Strong magnetism
1.2.2 Mandatory directive symbols
Symbol Meaning Symbol Meaning
Wear safety goggles Wear protective clothing
Wear protective gloves Heavy load, do not lift with-
out assistance
1.2.3 Other symbols
NOTE
This symbol draws attention to useful and important information.
R This character draws attention to a requirement that must be met before the in-
structions below are carried out.
u This character indicates an instruction that must be carried out by the user.
5 This character indicates the result of a correctly carried out instruction.
1.3 Available languages
These operating instructions were originally produced in German and have been
translated into several other languages. The translations are available on the enclosed CD or can be obtained as a PDF file via http://www.buchi.com.
1.4 Trademarks
Product names and registered or unregistered trademarks that are used in this instruction manual are used only for identification and remain the property of the owner
in each case.
For example, Rotavapor® is a registered trademark of BÜCHI Labortechnik AG.
Page 7
BÜCHI Labortechnik AG Safety | 2
Operation Manual Vacuum Pump V-100 7/52
2 Safety
2.1 Intended use
The Vacuum Pump V-100 has been designed and built as an item of laboratory
equipment. Its intended use is the evacuation of laboratory apparatus. This is done by
means of a PTFE-membrane pump – with or without regulation by a vacuum controller.
PTFE-membrane pumps are used primarily for the following applications:
Evacuating distillation apparatus, in particular rotary evaporators (Rotavapor®)
Vacuum filtration
Vacuum-drying cabinets
Drying kilns
2.2 Use other than that intended
Use of any kind other than that referred to and any application that does not comply
with the technical specifications constitutes use other than that intended. The operator alone is liable for any damage brought about by use of the device in a manner
other than that intended.
In particular, the following applications are not permissible:
Use in areas which require explosion-safe apparatus.
Pumping of liquids and solid particles.
Processing samples which could be caused to explode or ignite by impact, friction,
heat or sparks (e.g. explosives).
Use for analysis (e.g. Kjeldahl).
Generation of positive pressure (pressurizing a system).
Operation at ambient temperatures >40 °C.
2.3 Staff qualification
Unqualified persons are unable to identify risks and are therefore exposed to greater
dangers.
The device may only be operated by suitably qualified laboratory staff.
These operating instructions are aimed at the following target groups:
Users
Users are persons that meet the following criteria:
They have been instructed in the use of the device.
They are familiar with the contents of these operating instructions and the applica-
ble safety regulations and apply them.
They are able on the basis of their training or professional experience to assess
the risks associated with the use of the device.
Page 8
2 | Safety BÜCHI Labortechnik AG
8/52 Operation Manual Vacuum Pump V-100
Operator
The operator (generally the laboratory manager) is responsible for the following aspects:
The device must be correctly installed, commissioned, operated and serviced.
Only suitably qualified staff may be assigned the task of performing the operations
described in these operating instructions.
The staff must comply with the locally applicable requirements and regulations for
safe and hazard-conscious working practices.
Safety-related incidents that occur while using the device should be reported to the
manufacturer (quality@buchi.com).
BUCHI service technicians
Service technicians authorized by BUCHI have attended special training courses and
are authorized by BÜCHILabortechnikAG to carry out special servicing and repair
measures.
2.4 Residual risks
The device has been developed and manufactured using the latest technological advances. Nevertheless, risks to persons, property or the environment can arise if the
device is used incorrectly.
Appropriate warnings in this manual serve to alert the user to these residual dangers.
2.4.1 Dangerous vapors
Distillation can produce dangerous vapors that are capable of causing life-threatening
toxic effects.
u Do not inhale any vapors produced during distillation.
u Ensure that vapors are removed immediately by a suitable fume hood.
u Only use the device in well ventilated areas.
u If vapors escape from joints or connections, check the seals concerned and re-
place them if necessary.
u Do not distill any unknown fluids.
u Observe the safety data sheets for all fluids used.
2.4.2 Faults during operation
If a device is damaged, sharp edges or exposed electrical wires can cause injuries.
u Regularly check device for visible damage.
u If faults occur, switch off the device immediately, unplug the power cord and in-
form the operator.
u Do not continue to use devices that are damaged.
2.5 Personal protective equipment
Depending on the application, hazards due to heat and/or corrosive chemicals may
arise.
u Always wear appropriate personal protective equipment such as safety goggles,
protective clothing and gloves.
u Make sure that the personal protective equipment meets the requirements of the
safety data sheets for all chemicals used.
2.6 Modifications
Unauthorized modifications may impair safety and lead to accidents.
Page 9
BÜCHI Labortechnik AG Safety | 2
Operation Manual Vacuum Pump V-100 9/52
u Use only genuine BUCHI accessories, spare parts and consumables.
u Technical modifications to the device or accessories should only be carried out
with the prior written approval of BÜCHILabortechnikAG and only by authorized
BUCHI technicians.
BUCHI accepts no liability whatsoever for damage arising as a result of unauthorized
modifications.
Page 10
3 | Product description BÜCHI Labortechnik AG
10/52 Operation Manual Vacuum Pump V-100
3 Product description
3.1 Description of function
The Vacuum Pump V-100 is intended for evacuating laboratory apparatus to a terminal vacuum of 10mbar (±2mbar).
Once switched on, the V-100 runs in continuous mode unless it is connected to the
Interface I-100 unit. In unregulated continuous mode, the pump runs at a maximum
speed of 1280 rpm and generates a terminal vacuum of 10mbar (±2mbar). The time
required for evacuation depends on the size (volume) of the vessel.
After 1 hour of operation, the V-100 switches automatically to ECO mode. In ECO
mode, the V-100 runs at 70% capacity but still generates the same terminal vacuum
of 10mbar (±2mbar).
The pump can be operated either as a standalone device or combined with optional
accessories (see Chapter3.3 "Specifications supplied", page14).
3.2 Configuration
3.2.1 Front view
Fig.1: Design of V-100
1 Carrying handle
2 Pump top cover
3 On/Off master switch
Page 11
BÜCHI Labortechnik AG Product description | 3
Operation Manual Vacuum Pump V-100 11/52
3.2.2 Rear view
1
1
1
2
1
4
1
5
1
6
1
7
1
3
1
1
Fig.2: Rear view of V-100
1 Knurled-head screws 4 Pump intake (vacuum)
2 Pump outlet 5 Mini-DIN connection
3 Type plate 6 Power supply connection
7 Lashing eye (for securing against
earthquakes)
Page 12
3 | Product description BÜCHI Labortechnik AG
12/52 Operation Manual Vacuum Pump V-100
3.2.3 Internal view
3
4
5
6
7
1
2
Fig.3: Internal view of V-100 showing pump head and pump-head connection piece
1 Torx key (TX10) 3 Torx key (TX25)
2 Pump top cover 4 Pump outlet
5 Pump-head metal cover
6 GL14 cap nut
7 Pump-head connection piece
Page 13
BÜCHI Labortechnik AG Product description | 3
Operation Manual Vacuum Pump V-100 13/52
3.2.4 Typical application
The V-100 is used for evacuating laboratory apparatus such as tubes, flasks and
other apparatus.
Recirculating
Chiller F-100
Fig.4: Typical application for the V-100 in a laboratory
1 Recirculating Chiller F-100
2 Rotavapor R-100
3 Vacuum Pump V-100 with Interface I-100
Evacuation changes the physical and chemical properties of materials. The V-100 is
ideally suited to connection to a Rotavapor R-100 in combination with a Recirculating
Chiller F-1xx. With that combination of apparatus controlled by a controller such as
the Interface I-100, ideal distillation configurations for all commonly used solvents can
be created.
Page 14
3 | Product description BÜCHI Labortechnik AG
14/52 Operation Manual Vacuum Pump V-100
3.2.5 Type plate
The type plate is on the rear of the Vacuum Pump V-100.
BUCHI Operations India Pvt Ltd
394230 Surat / India
Type: V-100
SN: 1000000000
Volt: 100 – 240 VAC
Frequ.: 50/60 Hz
Power: 150 W
Built: 2014
Designed by BUCHI in Switzerland,
Made in India
3
7
2
1
5
4
6
8
9
1011
Fig.5: Type plate (example)
1 Company name and address 7 Year of manufacture
2 Device name 8 Country of manufacture
3 Serial number 9 Approvals
4 Input voltage 10 Symbol for "Do not dispose of as
household waste"
5 Frequency 11 Product code
6 Maximum power rating
3.3 Specifications supplied
V-100
Vacuum Pump V-100 1
Vacuum tubing (2 m) 1
Power supply cable 1
Silencer 1
Tubing connections (set) 1
Interface I-100 *
Woulff bottle *
Condensation unit *
Communication cables *
* As per order code
Page 15
BÜCHI Labortechnik AG Product description | 3
Operation Manual Vacuum Pump V-100 15/52
3.4 Technical data
3.4.1 Vacuum Pump V-100
Dimensions (W x H x D) 180 x 275 x 210 mm
Weight 5.6 kg
Power supply voltage 100 – 240 V, 50/60 Hz
Power consumption 150 W
Power consumption in ECO mode 70 W
Terminal vacuum (absolute) 10 mbar (± 2 mbar)
Pump capacity 1.5 m3/h
Vacuum connection GL-14
Motor Brushless DC motor
Rotation speed 1280 rpm max.
Rotation speed in ECO mode 70% of max. capacity
Noise level 32 to 57 dBA
57 dBA: with 100% load
Overvoltage category II
Pollution degree 2
Enclosure rating IP20
Certificates CE
3.4.2 Ambient conditions
Max. altitude above sea level 2000 m
Ambient temperature 5 - 40 °C
Maximum relative humidity 80 % for temperatures up to 31 °C
decreasing linearly to 50 % at 40 °C
The Vacuum Pump V-100 may only be used in indoor areas.
3.4.3 Materials
Component Material
Pump heads PPS
Drive unit body Aluminium
Housing PBT
Membranes PTFE/rubber
Valve plate PEEK
Valve head PEEK
Pump-head connection piece FEP
Vacuum tubing Silicone/natural rubber
Non-return valve O-rings FFKM
Page 16
4 | Transport and storage BÜCHI Labortechnik AG
16/52 Operation Manual Vacuum Pump V-100
4 Transport and storage
4.1 Transport
IMPORTANT
Risk of breakage due to incorrect transportation
u Make sure that all parts of the device are safely packed in such a way as to pre-
vent breakage, ideally in the original box.
u Avoid sharp movements during transit.
u After transportation, check the device for damage.
u Damage that has occurred in transit should be reported to the carrier.
u Keep packing for future transportation.
4.2 Storage
u Make sure that the ambient conditions are complied with (see Chapter3.4 "Tech-
nical data", page15).
u Wherever possible, store the device in its original packaging.
u After storage, check the device, all seals and tubing for damage and replace if
necessary.
Page 17
BÜCHI Labortechnik AG Transport and storage | 4
Operation Manual Vacuum Pump V-100 17/52
4.3 Removing transit fixings
Fig.6: Transit fixings on the rear of the Vacuum Pump V-100
1 Transit fixings 2 GL14 cap nuts
Before the V-100 is set up and put into service, the transit fixings (red) have to be removed.
u On the rear of the V-100, unscrew the GL14 cap nuts (2) from the pump intake
and pump outlet.
u Pull off the red transit fixings (1).
u Screw the cap nuts back on.
Page 18
5 | Installation BÜCHI Labortechnik AG
18/52 Operation Manual Vacuum Pump V-100
5 Installation
5.1 Important considerations prior to commissioning
WARNING
Risk of irritation of mucous membranes and poisoning from inhalation
of hazardous gases and vapors.
In the process of evacuation it is possible that hazardous substances may be pumped
out at the same time and released into the atmosphere. In addition, it is possible for
such substances to collect as condensation at leaking connections.
u Operate the pump inside a fume hood.
u Direct vapors from the pump outlet into the fume hood.
u If necessary, wear a face mask and safety goggles.
u If necessary, only handle pump and accessories with protective gloves.
WARNING
Risk of fire or explosion from flammable solvent vapors.
In the process of evacuation, it is possible for solvent vapors to get into the inside of
the pump and catch fire or explode due to the electric current.
u Follow the guidance notes for the solvents used.
u Connect a Woulff bottle upstream of the pump intake.
u Operate the pump inside a fume hood.
CAUTION
Health risks when handling corrosive substances.
u When working with strong acids or caustic solutions, always wear personal protec-
tive equipment (safety goggles, protective clothing, protective gloves).
Page 19
BÜCHI Labortechnik AG Installation | 5
Operation Manual Vacuum Pump V-100 19/52
5.2 Installation site
u Before setting up the V-100 and putting it into service, remove the transit fixings
(red) on the rear of the device (see Chapter4.3 "Removing transit fixings",
page17).
IMPORTANT
Risk of property damage from falling equipment (e.g. in an earthquake)
u Secure the Vacuum Pump against falling by means of the lashing eye on the rear
of the device (see Chapter3.2.2 "Rear view", page11).
The installation site must meet the following requirements:
Firm and level surface: at least 200 mm x 300 mm (W x D)
Height: at least 300 mm
Set up inside a fume hood or
feed the pump outlet into the fume hood
Sufficient air supply to the pump cooler
The V-100 is intended for use in laboratory environments (see Chapter3.4.2 "Ambient conditions", page15).
5.3 Connecting laboratory equipment
1
2
Fig.7: Vacuum Pump (V-100) with transit fixings
1 Pump outlet 2 Pump intake (vacuum)
Page 20
5 | Installation BÜCHI Labortechnik AG
20/52 Operation Manual Vacuum Pump V-100
The V-100 is connected by a vacuum tubing to the laboratory apparatus to be evacuated. The vacuum tubing leads via a GL14 connection from the pump intake (2) to the
outlet of the laboratory device concerned.
Precondition:
R Transit fixings have been removed (see Chapter4.3 "Removing transit fixings",
page17).
u Fit tubing to pump intake (2) using the GL14 cap nut.
If vapors are to be expected during evacuation, we recommend the following:
u Connect a Woulff bottle upstream of the pump intake (see Chapter5.5 "Connect-
ing a Woulff bottle", page23).
u Connect the tubing to the Woulff bottle intake using a GL14 cap nut.
For details of connecting the V-100 to a rotary evaporator (e.g. Rotavapor® R-100)
see the relevant section of the device's operating instructions.
For more information on the use of the V-100, see Chapter3.2.4 "Typical application",
page13.
Page 21
BÜCHI Labortechnik AG Installation | 5
Operation Manual Vacuum Pump V-100 21/52
5.4 Connecting the silencer
1
1
2
3
4
Fig.8: Silencer on pump outlet of V-100
1 GL14 cap nut 3 Silencer
2 Flow direction marker 4 Silencer outlet
The silencer can be connected directly to the pump or to the outlet of the secondary
condenser.
Connecting silencer directly to V-100
u Fit the silencer (3) onto the pump outlet so that the flow direction marker (2) on the
silencer points away from the pump.
u Slide forwards the GL14 cap nut (1) on the top connection of the silencer and
screw it onto the GL14 thread of the pump outlet.
Connecting the silencer to the outlet of the secondary condenser
1
Fig.9: Connection for the silencer
1 Secondary condenser outlet
u Position the silencer inlet on the secondary condenser outlet (1).
Page 22
5 | Installation BÜCHI Labortechnik AG
22/52 Operation Manual Vacuum Pump V-100
u Slide forwards the GL14 cap nut on the silencer inlet and screw it onto the thread
of the condenser outlet.
Page 23
BÜCHI Labortechnik AG Installation | 5
Operation Manual Vacuum Pump V-100 23/52
5.5 Connecting a Woulff bottle
1
5
2
4
6
8
9
10
3
7
Fig.10: Connecting a Woulff bottle to the V-100
1 GL14 cap nut 6 Pump intake
2 Woulff bottle outlet 7 Connection piece
3 Top outlet for connecting Interface
I-100
8 Screw
4 Woulff bottle inlet 9 Mounting rail for holder
5 Woulff bottle glass component 10 Woulff bottle holder
The Woulff bottle is connected to the pump intake on the rear of the V-100.
Tools required: Torx key (fitted in pump top cover)
u Fix the mounting rail (9) for the holder below the pump intake (6) using the screw
(8).
u Fit the holder (10) onto the mounting rail.
u Unscrew the GL14 screw-cap from the pump intake (6).
u Fit the connection piece (7) from the outlet of the Woulff bottle onto the pump in-
take. Screw the GL14 cap nut (1) on the end of the tubing onto the pump intake
thread.
u Press the Woulff bottle into the holder.
Connecting an Interface I-100 via a Woulff bottle
u If necessary connect the Woulff bottle to the Interface I-100 as follows: Fit the con-
nection piece to the top outlet (3) of the Woulff bottle.
u For details of connecting the connection piece to the interface unit and the setup,
also refer to the operating instructions for the I-100.
Page 24
5 | Installation BÜCHI Labortechnik AG
24/52 Operation Manual Vacuum Pump V-100
5.6 Connecting a secondary condenser
1
1
4
1
2
1
3
Fig.11: Connecting secondary condenser to V-100
1 Secondary condenser 3 Holder
2 Pump outlet 4 Screw
NOTE
Connecting a secondary condenser is advised particularly in cases where the pump
outlet cannot be connected to a fume hood or the solvent concentration in the vapor
is too high. The secondary condenser reduces the amount of vapor emitted.
The secondary condenser is connected directly to the pump outlet (2) on the rear of
the V-100.
Fitting holder for secondary condenser
Tools required: Torx key (fitted in pump top cover – see Chapter3.2.3 "Internal view",
page12).
u Position the holder (3) below the pump outlet (2) and fix to the pump housing by
means of two screws (4).
Page 25
BÜCHI Labortechnik AG Installation | 5
Operation Manual Vacuum Pump V-100 25/52
Fitting secondary condenser into the holder and connecting up
5
4
6
3
2
1
Fig.12: V-100 with secondary condenser connected
1 Connection piece 4 Secondary condenser outlet
2 GL14 cap nut 5 Ball joint clamp
3 Pump outlet 6 Receiving flask
u Push secondary condenser together with connection piece (1) and GL14 cap nut
(2) fully home into holder from above.
u Fit the unattached end of the connection piece into the pump outlet (3).
u Screw the GL14 cap nut (2) on the connection piece onto the thread on the pump
outlet.
u Fit receiving flask (6) underneath the secondary cooling cold trap and fix with ball
joint clamp (5).
Page 26
5 | Installation BÜCHI Labortechnik AG
26/52 Operation Manual Vacuum Pump V-100
5.7 Connecting a secondary cooling cold trap
1
3
1
2
6
5
1
1
1
4
7
Fig.13: Cold trap for V-100
1 Cover 5 Secondary cooling cold trap outlet
2 Secondary cooling cold trap 6 Ball joint clamp
3 Secondary cooling cold trap inlet with
connecting tubing
7 Receiving flask
4 Holder for secondary cooling cold
trap
Connecting a secondary cooling cold trap upstream of the pump outlet reduces the
amount of residual vapor released into the atmosphere.
Fitting to pump outlet
Tools required: Torx key (fitted in pump top cover – see Chapter3.2.3 "Internal view",
page12).
u Position the holder (4) for the secondary cooling cold trap below the pump outlet
and fix it to the housing using two screws.
u Unscrew the GL14 cap nut from the pump outlet and slide it narrow-end first over
the connecting tubing on the inlet (3) of the secondary cooling cold trap.
u Fit the unattached end of the connecting tubing (3) into the pump outlet.
u Screw the GL14 cap nut on the connecting tubing back onto the thread on the
pump outlet.
u Push secondary cooling cold trap (2) fully home into holder.
u Fit receiving flask (7) into the bottom outlet of the secondary cooling cold trap and
fix with the aid of a ball joint clamp (6).
u From the outlet (5) of the secondary cooling cold trap, feed another connecting
tubing directly into a waste drum.
Page 27
BÜCHI Labortechnik AG Installation | 5
Operation Manual Vacuum Pump V-100 27/52
5.8 Electrical connections
1
1
4
1
2
1
3
Fig.14: Electrical connections on the V-100 (left) and the Interface I-100 (right)
1 Mini-DIN connection (Interface I-100) 3 Mini-DIN connection (vacuum pump)
2 Power supply for Interface I-100 4 Power supply for vacuum pump
u Make sure that the available power supply matches the rating indicated on the
type plate.
u Join the mini-DIN socket (1) of the V-100 to the mini-DIN socket (3) of the Inter-
face I-100 with a communication cable.
u Plug the mains power cord supplied into the power supply socket (4) on the V-100.
u Plug the mains power cord into a grounded mains power socket.
u Connect the power adapter for the Interface I-100 to the socket (2) for the power
supply.
Page 28
5 | Installation BÜCHI Labortechnik AG
28/52 Operation Manual Vacuum Pump V-100
5.9 Fitting and connecting the Interface I-100
5.9.1 Fitting an interface unit to the Vacuum Pump V-100
Fitting the holder
1
1
2
3
4
Fig.15: Fitting the holder for the Interface I-100
1 Screw 3 Rubber plug (in thread for screw)
2 Holder for Interface I-100 4 Lower hinge of holder
The Torx key required for fitting the holder is included in the specifications supplied.
u Remove rubber plug (3).
u Fit the holder (2) onto the pump top cover from behind and secure it with the
screw (1).
u Make sure that the hinge (4) of the holder is engaged in the slot on the rear of the
V-100.
Page 29
BÜCHI Labortechnik AG Installation | 5
Operation Manual Vacuum Pump V-100 29/52
Fitting the interface unit
1
1
2
3
Fig.16: Fitting the Interface I-100
1 Interface I-100 3 T-screw
2 Holder
u Fit the interface unit (1) onto the holder (2).
u Tighten the T-screw (3) on the back of the interface unit by turning it clockwise.
5.9.2 Connecting interface unit to Vacuum Pump V-100
The V-100 is connected to the Interface I-100 by means of a communication cable
(mini-DIN socket on rear of vacuum pump – see illustration in Chapter5.8 "Electrical
connections", page27) and a tubing (from top outlet of Woulff bottle – see illustration
in Chapter5.5 "Connecting a Woulff bottle", page23). For more information on connecting the tubing and communication cable, refer to the section "Commissioning" in
the operating instructions for the Interface I-100.
Page 30
6 | Operation BÜCHI Labortechnik AG
30/52 Operation Manual Vacuum Pump V-100
6 Operation
6.1 Operating V-100 with Interface I-100
The Vacuum Pump V-100 can be controlled by an Interface I-100. Control encompasses the following parameters and functions:
Setting the required vacuum
Timer
Details of controlling the V-100 and the other laboratory equipment involved in evacuation can be found in the operating instructions for the Interface I-100.
6.2 Operating V-100 without Interface I-100
1
2
Fig.17: V-100
1 Pump outlet 2 Pump intake (vacuum)
If not controlled by an Interface I-100, the vacuum pump runs in continuous mode and
switches to ECO mode after one hour, see Chapter3.1 "Description of function",
page10.
Page 31
BÜCHI Labortechnik AG Cleaning and servicing | 7
Operation Manual Vacuum Pump V-100 31/52
7 Cleaning and servicing
NOTE
Users may only carry out the servicing and cleaning operations described in this section.
Any servicing and repair work which involves opening up more than the pump top
cover may only be carried out by authorized service technicians.
u Use only genuine BUCHI consumables and spare parts in order to ensure correct
operation of the device and preserve the warranty.
u Before carrying out any servicing work, switch off the device and disconnect it
from the power cable.
7.1 Cleaning
7.1.1 Important considerations when cleaning
WARNING
Risk of fatal injury from electric shock.
If the pump is opened up while it is running there is a risk of dangerous electric
shocks.
u Before carrying out any cleaning or servicing work, always shut down the device
and disconnect the power cable.
7.1.2 Cleaning the pump
u Disconnect all connections to the device.
u Place a collecting vessel under the pump outlet.
u Switch on the Vacuum Pump V-100 and allow it to run.
u Spray ethanol into the pump intake.
u Hold your finger over the pump intake so that a vacuum is created for a short time.
u Remove your finger from the pump intake again.
u Allow the pump to run until there is no more liquid inside the pump heads.
u Repeat the procedure if necessary.
u Switch off the pump and reconnect the apparatus.
7.1.3 After working with strong acids
After distilling strong acids or corrosive solutions the pump should be flushed out in
order to increase its service life.
u Detach tubing connections to other laboratory equipment.
u If present, remove Woulff bottle from pump intake and secondary condenser or
cold trap from pump outlet and clean them.
u Place a bowl or glass collection vessel under the pump outlet.
u Switch on the pump and pour 5 to 10 mL of water into the pump intake.
u Test the pH level of the water collected at the pump outlet.
u Repeat the flushing process until the discharged water has a pH level of between
3 and 9.
u Allow the pump to run for two to three minutes to dry out.
Page 32
7 | Cleaning and servicing BÜCHI Labortechnik AG
32/52 Operation Manual Vacuum Pump V-100
7.1.4 Cleaning the housing
IMPORTANT
Risk of acid damage
The housing of the unit is made of plastic. Escaping acid may damage the material.
u Immediately remove any drops of acid with a damp cloth.
u Only use a damp cloth to clean the device.
u To clean the housing, only use ethanol or soapy water.
7.1.5 Cleaning glass components
The V-100 does not itself contain any glass components but the accessories (Woulff
bottle, secondary cooling cold trap, secondary condenser) consist mainly of glass and
must always be inspected and cleaned before and after use.
As the glass components are under vacuum when in use, they are subjected to high
stress.
u Before use, check all glass components for cracks, chipping and any other dam-
age.
u Replace any damaged glass components.
u Rinse out glass components with water and a conventional cleaning agent (e.g.
mild soap and water solution).
u Wherever possible, clean glass components by hand.
NOTE
Feeding a thin copper wire into the cooling coil of the secondary condenser or cold
trap reduces the amount of dirt deposited.
7.1.6 Cleaning tubing
After evacuation, there may still be residual fluid in the tubing from condensed vapors.
The pump can largely dry itself out when running idle.
u Detach connections to other laboratory equipment and allow the pump to run in
continuous mode.
u Switch off the pump after three to five minutes.
To clean the connecting tubing inside the pump between the two pump heads it is
necessary to open up the pump as follows:
Precondition:
R Pump has been shut down.
u Remove the pump top cover and take out the pump tubing (see Chapter7.2.5
"Replacing tubing", page40).
u Rinse out the tubing with clean water. If necessary, remove residues inside the
tubing with a copper wire.
u Refit the pump tubing (see Chapter7.2.5 "Replacing tubing", page40).
u Switch on the pump and allow it to run in continuous mode until the inside of the
tubing is dried out.
u Refit the pump top cover.
7.1.7 Cleaning valve heads
Dirt contamination of the valve heads is evidenced by the V-100 failing to achieve the
terminal vacuum of 10mbar (±2mbar) even though components are intact and connections air-tight. To clean them, proceed as follows:
Page 33
BÜCHI Labortechnik AG Cleaning and servicing | 7
Operation Manual Vacuum Pump V-100 33/52
u Detach all connections (tubing and communication cable) from the pump.
u Place a collecting vessel under the pump outlet.
u Switch on the pump.
u Spray a small amount of acetone (approx. 10mL) into the pump intake.
u Wait until the sound of the pump changes back to what it was before the acetone
was injected.
u Repeat this procedure four times.
u Re-attach the connections to the pump and check whether the terminal vacuum is
now achieved.
If the V-100 is still unable to achieve the required performance even after the valve
heads have been cleaned, both pump heads must be dismantled and manually
cleaned (see Chapter7.2.2 "Dismantling and reassembling pump head", page35).
7.1.8 Cleaning non-return valve
The V-100 operates with a total of four non-return valves. There is one valve with an
O-ring in the connection on each of the two ports on each pump head. To clean the
valves, the pump heads have to be dismantled as follows:
u Remove the pump top cover and dismantle the pump heads (see Chapter7.2.2
"Dismantling and reassembling pump head", page35).
7.1.9 Cleaning the membrane
After evacuation, there may still be residual fluid on the membrane from condensed
vapors. The pump can largely dry itself out when running idle.
u Detach connections to other laboratory equipment and allow the pump to run in
continuous mode.
u Switch off the pump after three to five minutes.
If the membrane is contaminated by residues, the pump heads must first be dismantled and the membranes then unscrewed and cleaned.
u Remove the pump top cover and remove the pump heads (see Chapter7.2.2 "Dis-
mantling and reassembling pump head", page35).
u Unscrew the membranes (see Chapter7.2.3 "Replacing the membrane",
page38).
u Wipe down membranes with a damp cloth.
u Refit the membranes (see Chapter7.2.3 "Replacing the membrane", page38).
u Refit the pump heads and pump top cover (see Chapter7.2.2 "Dismantling and re-
assembling pump head", page35).
7.2 Servicing
7.2.1 Notes on servicing
WARNING
Risk of fatal injury from electric shock.
If the pump is opened up while it is running there is a risk of dangerous electric
shocks.
u Before carrying out any cleaning or servicing work, always shut down the device
and disconnect the power cable.
Page 34
7 | Cleaning and servicing BÜCHI Labortechnik AG
34/52 Operation Manual Vacuum Pump V-100
IMPORTANT
Risk of pump damage and loss of warranty entitlement.
Unauthorized opening up of the lower part of the pump may permanently impair the
function of the pump.
u Only allow authorized BUCHI service technicians to open up the lower part of the
pump.
Page 35
BÜCHI Labortechnik AG Cleaning and servicing | 7
Operation Manual Vacuum Pump V-100 35/52
7.2.2 Dismantling and reassembling pump head
Removing pump top cover
Fig.18: V-100 with pump top section opened up
1 Rubber surrounds
Precondition:
R Pump has been shut down.
u Unscrew the two knurled-head screws on the rear of the V-100 and remove the
pump top cover.
u Remove the rubber surrounds (1) from the pump intake and pump outlet.
Removing pump-head connection piece
3
4
1
1
2
Fig.19: Pump-head connection piece with union nuts between the two pump heads
1 Screw (elbow connection) 3 Pump-head connection piece
2 Elbow connection 4 GL14 cap nut
u Unscrew two screws (1) from each of the two pump heads, and remove the elbow
connections (2) together with the pump-head connection piece (3) from the pump
heads.
u Unscrew the GL14 cap nuts (3) from the elbow connections.
u Pull the GL14 cap nuts off the pump-head connection piece (4).
Page 36
7 | Cleaning and servicing BÜCHI Labortechnik AG
36/52 Operation Manual Vacuum Pump V-100
Removing the pump head
Fig.20: Pump head opened up showing membrane underneath
1 Allen-head screws 3 Pump head
2 Metal cover
u Lie the pump on its side.
u Unscrew the four Allen-head screws (1) and remove the metal cover (2).
u Remove the pump head (3).
Dismantling the pump head
2
3
4
2
6
5
1
6
Fig.21: View of completely dismantled pump head
1 Membrane 4 Elbow connection
2 O-rings 5 Straight connection
3 GL14 cap nut 6 Non-return valves
Page 37
BÜCHI Labortechnik AG Cleaning and servicing | 7
Operation Manual Vacuum Pump V-100 37/52
The pump head has two ports, attached to each of which is a connection (4, 5) with a
non-return valve (6) and an O-ring (2). The straight connection (5) leads to the pump
intake/pump outlet. The elbow connection (4) leads to the opposite pump head via the
pump-head connection piece.
u Unscrew the fixing screws on the straight connections (5) and remove the connec-
tions.
u Remove the O-rings (2) from the connections.
u Remove the non-return valves (6) from the connections.
Reassembling and refitting the pump head
u Insert the non-return valves (6) and O-rings (2) inside the connections (4 and 5).
u Fit the straight connections (5) on the pump heads (the elbow connections are re-
fitted later together with the pump-head connection piece).
u Position the pump head on the membrane and fix in place with the four Allen-head
screws.
u Fit the elbow connections (4) together with the pump-head connection piece and
the GL14 cap nuts between the two pump heads.
u Refit the rubber surrounds on the pump intake and pump outlet inside the housing.
u Refit the pump top cover and fix in place with the knurled-head screws.
Page 38
7 | Cleaning and servicing BÜCHI Labortechnik AG
38/52 Operation Manual Vacuum Pump V-100
7.2.3 Replacing the membrane
The membranes of the V-100 are located on the left and right behind the pump head.
Fig.22: Membrane
1 Membrane
To remove the membrane you require a clamp (see Chapter10.2 "Spare parts and
accessories", page46).
Precondition:
R Pump has been shut down.
u Remove the top cover of the V-100 and remove the pump head (see Chap-
ter7.2.2 "Dismantling and reassembling pump head", page35).
u Grip membrane with clamp and turn counter-clockwise.
u Remove old membrane and insert new membrane.
u Tighten new membrane by turning clockwise with clamp.
u Refit the pump head and pump top cover (see Chapter7.2.2 "Dismantling and re-
assembling pump head", page35).
Fig.23: Membrane and clamp
Page 39
BÜCHI Labortechnik AG Cleaning and servicing | 7
Operation Manual Vacuum Pump V-100 39/52
7.2.4 Replacing valve
1
5
1
1
2
3
4
3
2
Fig.24: Dismantling the pump head
1 O-rings 4 Elbow connection
2 Non-return valves 5 Straight connection
3 Screws for connections
u Remove the pump head (see Chapter7.2.2 "Dismantling and reassembling pump
head", page35).
u Unscrew the screws (3) from the connections (4, 5).
u Remove the elbow connection and the straight connection from the pump head.
u Remove the O-rings (1) and the non-return valves (2) from inside the connections.
u Insert new O-rings and valves into the connections. NOTICE!When inserting the
non-return valves, pay attention to the airflow direction: the air enters on the
funnel-shaped side of the non-return valve. See also the schematic diagram
on the inside of the housing above the pump intake and pump outlet.
u Refit the connections to the pump head.
Page 40
7 | Cleaning and servicing BÜCHI Labortechnik AG
40/52 Operation Manual Vacuum Pump V-100
7.2.5 Replacing tubing
3
4
1
1
2
Fig.25: Pump-head connection piece with GL-14 union nuts between the two pump heads
1 Screws for connections 3 Pump-head connection piece
2 Elbow connection 4 GL14 cap nut
Precondition:
R Pump has been shut down.
u Unscrew the two knurled-head screws and remove the pump top cover.
u Unscrew two screws (1) from each elbow connection (2).
u Remove the two elbow connections together with the pump-head connection piece
(3) from the pump heads.
u Unscrew the GL14 cap nuts (4) on each end of the pump-head connection piece
counter-clockwise and remove the connections (2).
u Pull the GL14 cap nuts off the pump-head connection piece.
u Feed a new pump-head connection piece through the union nuts.
u Screw the GL14 cap nuts onto the connections. Make sure that the FEP pipe
seals under the GL14 cap nuts are in proper contact with the pump-head connection piece and are not damaged.
u Fit the connections together with the pump-head connection piece on the pump
heads.
u Refit the pump top cover and fix in place.
Page 41
BÜCHI Labortechnik AG Help with faults | 8
Operation Manual Vacuum Pump V-100 41/52
8 Help with faults
8.1 Faults, possible causes and remedies
Fault Possible cause Remedy
Device does not work. Master switch is off. u Switch on master switch.
Device is not connected
to a power supply.
u Check power supply.
System is not air-tight
and cannot achieve terminal vacuum.
Pipe clips not properly
fitted or are damaged.
u Check pipe clips (see Chap-
ter7.2.5 "Replacing tubing",
page40).
Tubing leaking (and
brittle)
u Replace tubing (see Chap-
ter7.2.5 "Replacing tubing",
page40).
Membrane and/or
valves dirty
u Clean or replace membrane
and/or valves (see Chapter7.2.3 "Replacing the
membrane", page38 and
Chapter7.2.4 "Replacing
valve", page39).
Valve O-rings are leaking.
u Replace O-rings (see Chap-
ter7.2.4 "Replacing valve",
page39).
Pump fails to start. Switch on pump top
cover not closing.
u Check seating of pump top
cover and correct if necessary. The cover is fixed by
two knurled-head screws.
Page 42
8 | Help with faults BÜCHI Labortechnik AG
42/52 Operation Manual Vacuum Pump V-100
8.2 Customer service
Repairs to the device may only be carried out by authorized service technicians. The
service technicians have been comprehensively technically trained and are aware of
the potential hazards that can arise from the device.
The addresses of the official BUCHI Customer Service offices can be found on the
BUCHI website at: www.buchi.com. If you have any questions regarding technical issues or faults, please contact those offices.
Customer Services can offer you:
supply of spare parts
repairs
technical advice
Page 43
BÜCHI Labortechnik AG Taking out of service and disposal | 9
Operation Manual Vacuum Pump V-100 43/52
9 Taking out of service and disposal
9.1 Taking out of service
u Remove all tubing and communication cables from the device.
u Run the pump to dry out tubing and diaphragms inside the pump.
u Switch off the pump and disconnect it from the mains power supply.
9.2 Disposal
The operator is responsible for proper disposal of the Vacuum Pump.
u When disposing of equipment observe the local regulations and statutory require-
ments regarding waste disposal.
Page 44
10 | Appendix BÜCHI Labortechnik AG
44/52 Operation Manual Vacuum Pump V-100
10 Appendix
10.1 Solvent table
Solvent Formula Molar
mass in g/
mol
Evaporation energy in J/g
Boiling
point in °C
at 1013
mbar
Density in
g/cm
3
Vacuum in
mbar for
40°C boiling point
Acetone CH3H6O 58.1 553 56 0.790 556
n-Amyl alcohol,
n-pentanol
C5H12O 88.1 595 37 0.814 11
Benzene C6H
6
78.1 548 80 0.877 236
n-butanol C4H10O 74.1 620 118 0.810 25
Tert butyl alcohol (2methyl-2-propanol)
C4H10O 74.1 590 82 0.789 130
Chlorobenzene C6H5Cl 112.6 377 132 1.106 36
Chloroform CHCl
3
119.4 264 62 1.483 474
Cyclohexane C6H
12
84.0 389 81 0.779 235
Diethyl ether C4H10O 74.0 389 35 0.714 850
1,2-dichloroethane C2H4Cl
2
99.0 335 84 1.235 210
cis-1,2-dichloroethylene
C2H2Cl
2
97.0 322 60 1.284 479
trans-1,2dichloroethylene
C2H2Cl
2
97.0 314 48 1.257 751
Di-isopropyl ether C6H14O 102.0 318 68 0.724 375
Dioxane C4H8O
2
88.1 406 101 1.034 107
DMF (dimethylformamide)
C3H7NO 73.1 – 153 0.949 11
Acetic acid C2H4O
2
60.0 695 118 1.049 44
Ethanol C2H6O 46.0 879 79 0.789 175
Ethylacetate C4H8O
2
88.1 394 77 0.900 240
Heptane C7H
16
100.2 373 98 0.684 120
Hexane C6H
14
86.2 368 69 0.660 360
Isopropylalcohol C3H8O 60.1 699 82 0.786 137
Isoamylalcohol (3methyl-1-butanol)
C5H12O 88.1 595 129 0.809 14
Methylethylketone C4H8O 72.1 473 80 0.805 243
Methanol CH4O 32.0 1227 65 0.791 337
Methylene chloride,
dichloromethane
CH2CI
2
84.9 373 40 1.327 850
Pentane C5H
12
72.1 381 36 0.626 850
n-propylalcohol C3H8O 60.1 787 97 0.804 67
Pentachloroethane C2HCl
5
202.3 201 162 1.680 13
Page 45
BÜCHI Labortechnik AG Appendix | 10
Operation Manual Vacuum Pump V-100 45/52
Solvent Formula Molar
mass in g/
mol
Evaporation energy in J/g
Boiling
point in °C
at 1013
mbar
Density in
g/cm
3
Vacuum in
mbar for
40°C boiling point
1,1,2,2-tetrachloroethane
C2H2Cl
4
167.9 247 146 1.595 20
Carbon tetrachloride CCl
4
153.8 226 77 1.594 271
1,1,1-trichloroethane C2H3Cl
3
133.4 251 74 1.339 300
Tetrachloroethylene C2Cl
4
165.8 234 121 1.623 53
THF (tetrahydrofurane)
C4H8O 72.1 – 67 0.889 374
Toluene C7H
8
92.2 427 111 0.867 77
Trichloroethylene C2HCl
3
131.3 264 87 1.464 183
Water H2O 18.0 2261 100 1.000 72
Xylene (mixture) C8H
10
106.2 389 – – 25
o-xylene C8H
10
106.2 – 144 0.880 –
m-xylene C8H
10
106.2 – 139 0.864 –
p-xylene C8H
10
106.2 – 138 0.861 –
Page 46
10 | Appendix BÜCHI Labortechnik AG
46/52 Operation Manual Vacuum Pump V-100
10.2 Spare parts and accessories
u Use only genuine BUCHI consumables and spare parts in order to ensure correct,
safe and reliable operation of the system.
NOTE
Any modifications of spare parts or assemblies are only allowed with the prior written
permission of BUCHI.
10.2.1 Accessories
Secondary condensers
Secondary condenser C. Cold trap, P+G, incl. holder
Condenses vapor before getting into the pump. In use with ice or dry
ice. Contents: 500 mL receiving flask, connection piece, holder for the
vacuum pump
047190
Secondary condenser V. Vertical condenser, incl. insulator, holder
Condenses vapor before getting into the pump. Used with recirculating
chiller or tap water. Contents: 500 mL receiving flask, connection piece,
holder for the vacuum pump
047180
Tubing
FEP, Ø6/8mm, transparent, per m
Utilization: Vacuum, cooling media
027900
Natural rubber, Ø6/16mm, red, per m
Utilization: Vacuum
017622
Nyflex, PVC-P, Ø8/14mm, transparent, per m
Utilization: Vacuum, cooling media, feeding (industrial Rotavapor)
004113
PTFE, Ø8/10mm, white, per m
Utilization: Vacuum, feeding (industrial Rotavapor)
027277
Silicone rubber, Ø6/9mm, transparent, per m
Utilization: Cooling media
004133
Communication cables
Mini-DIN, 0.6m
Connection between interface and vacuum pump
11060882
Mini-DIN, Y-shielded, 650mm
Used when connecting vacuum pump with two vacuum controllers
031920
Receiving flasks
Glass, BJ35/20, 250mL 000423
Glass, BJ35/20, 250mL, P+G 11060907
Glass, BJ35/20, 500mL 000424
Glass, BJ35/20, 500mL, P+G 025264
Page 47
BÜCHI Labortechnik AG Appendix | 10
Operation Manual Vacuum Pump V-100 47/52
Further accessories
Manometer with needle valve. Incl. holder for pump, valve, vacuum gauge
For manual vacuum adjustment
047291
Manometer with needle valve. Incl. valve, vacuum gauge, not incl.
holder
047391
Valve unit. Incl. Woulff bottle, 125mL, P+G, holder
The valve is only to use in combination with a vacuum controller/interface
047160
Woulff bottle. 125mL, P+G, incl. holder
For trapping particles and droplets and for pressure equalization
047170
Woulff bottle. 3-neck, 800mL, P+G
For trapping particles and droplets and for pressure equalization
025519
10.2.2 Wear parts
Seals
For cap nut, GL14, FEP 038225
Set. 10pcs, for hose barbs, GL14, EPDM, black 040029
Set. 10pcs, for hose barbs, GL14, FPM, green 040040
Set. 20pcs, for hose barbs, GL14, silicone, red 040023
Hose barbs
Bent, GL14, incl. silicone seal 018916
Set. 3pcs, bent, GL14, silicone seal
Content: Hose barbs, seals
041987
Set. 4pcs, bent, GL14, EPDM seal
Content: Hose barbs, cap nuts, seals
043129
Set. 4pcs, bent, GL14, FEP seal
Content: Hose barbs, cap nuts, seals
040295
Set. 4pcs, bent, GL14, silicone seal, incl. cap nut
Content: Hose barbs, cap nuts, seals
037287
Set. 4pcs, bent, GL14, silicone seal, incl. cap nut
Content: Hose barbs, cap nuts, seals
043128
Set. 4pcs, straight, GL14, EPDM seal
Content: Hose barbs, cap nuts, seals
040296
Set. 4pcs, straight, GL14, silicone seal
Content: Hose barbs, cap nuts, seals
037642
Set. 6pcs, bent (4), straight (2), GL14, silicone seal
Content: Hose barbs, cap nuts, seals
038000
Further wear parts
Membrane. For pump head, incl. clamp, support ring 047153
Membranes, set. 10pcs, for pump head, incl. clamp, support ring 11055214
O-ring. For secondary condenser, FKM/FEP, Ø28.2/2.6mm 11057661
O-rings, set. 4pcs, FFKM, Ø15.4/1.55mm, white 11057136
Page 48
10 | Appendix BÜCHI Labortechnik AG
48/52 Operation Manual Vacuum Pump V-100
Check valves, set. 4pcs, incl. O-ring 047156
Check valves, set. 4pcs, without O-rings 11058389
Screw caps, set. 5pcs, GL14 040624
Cap nuts, set. 10pcs, screw cap with hole, GL14, incl. FEP seal
Content: Hose barbs, cap nuts, seals
041999
Cap nuts, set. 10pcs, cap nuts with hole, GL14 041956
10.2.3 Spare parts
Connection piece. Straight, for pump head
Content: Connection straight, valve, O-ring, cap nut, GL14, FEP seal
11061580
Connection piece. Bent, for pump head
Content: Connection bent, valve, O-ring, cap nut, GL14, FEP seal
11061579
Lid. For cold trap, Ø68mm 047193
Insulator. For secondary condenser
Prevents formation of condensed water
047183
Ball joint clamp. For BJ35/20 003275
Secondary condenser V. Vertical condenser
Condenses remaining vapors after the vacuum pump outlet. Used
along with a recirculating chiller or tap water
047181
Secondary condenser V. Vertical condenser
Condenses remaining vapors after the vacuum pump outlet. Used
along with a recirculating chiller or tap water
11061840
Pump head. For Vacuum Pump V-100/V-700/V-710 11061578
Pump head, set. For Vacuum Pump V-100
Content: Pump head, set connection piece straight, set connection
piece angled
11061577
Silencer. Incl. cap nut, GL14, FEP seal
For Vacuum Pump V-100 / V-700 or V-710
047090
Tubing. Silicone rubber, Ø6/16, red, 2m
Utilization: Vacuum
040459
Support secondary condenser V. Incl. holder, FEP seal, connection piece
11055584
Support condenser V/C. Holder 047182
Connection piece. PTFE, Ø6/8mm, 162mm
Tubing between vacuum controller/interface and Woulff bottle
047154
Connection piece. PTFE, Ø6/8mm, 77mm
Tubing between vacuum pump and Woulff bottle
047066
Packaging. V-100/V-700, with glass assembly 045617
Packaging. V-100/V-700, without glass assembly 045616
Page 49
BÜCHI Labortechnik AG Appendix | 10
Operation Manual Vacuum Pump V-100 49/52
10.3 List of abbreviations
Abbreviation Meaning
ADR Accord européen relatif au transport international des marchan-
dises dangereuses par route (European Agreement concerning the
International Carriage of Dangerous Goods by Road)
DKD Deutscher Kalibrierdienst (German Calibration Service)
EPDM Ethylene propylene diene monomer
FEP Fluorinated ethylene propylene
FFKM Perfluoro-elastomer
FPM Fluorinated propylene monomer
GGVE Gefahrgutverordnung Eisenbahn (German Hazardous Goods Reg-
ulations for Railways)
GGVS Gefahrgutverordnung Strasse (German Hazardous Goods Regula-
tions for Road Transport)
PBT Polybutylene terephthalate
PEEK Polyetheretherketone
PP Polypropylene
PTFE Polytetrafluoroethylene
RID Règlement concernant le transport international ferroviaire de
marchandises dangereuses (Regulations concerning the International Carriage of Dangerous Goods by Rail)
10.4 Health and safety approval
To guarantee the health and safety of our staff and to comply with the law and the
regulations for handling hazardous materials, for the purposes of health and safety at
work and safe disposal of waste, no products may be sent back to BÜCHILabortechnikAG or repaired unless we have received the declaration below, completed and
signed.
Products sent to us will not be accepted for repair or DKD calibration until we have received this declaration.
u Copy the form overleaf and complete it.
u Make sure that you know the full details of the substances with which the device
has been in contact and the all questions have been answered fully and correctly.
u Send the completed from to us in advance by post or fax. The declaration must
reach us before the device.
u Enclose a copy of the declaration with the device.
u If the product is contaminated, inform the carrier (in accordance with GGVE/
GGVS/RID/ADR).
If the declaration is missing or the procedure described is not followed, the repairs will
be delayed. We ask for your understanding and cooperation with regard to these
measures.
Page 50
10 | Appendix BÜCHI Labortechnik AG
50/52 Operation Manual Vacuum Pump V-100
10.5 Health and safety
Declaration regarding the safety, hazards and safe disposal of waste
To guarantee the health and safety of our staff and to comply with the law and the
regulations for handling hazardous materials, regarding health and safety at work,
and to comply with safety regulations, health and safety requirements and requirements for safe disposal of waste such as chemical waste, chemical residues or solvents, the form below must be fully completed and signed whenever devices or faulty
components are to be sent back to our factory.
Products or components will not be accepted if this declaration has not been
provided.
Device
Model: Part/Device no.:
Declaration for
non-hazardous ma-
terials
We hereby assure that the products returned
have not been used in the laboratory and are new.
have not been in contact with toxic, corrosive, biologically active, explosive, ra-
dioactive or other hazardous materials.
are not contaminated. The solvents or residues of the substances pumped have
been removed.
Declaration for haz-
ardous materials
In respect of the products returned, we hereby assure that
all substances (toxic, corrosive, biologically active, explosive, radioactive or otherwise hazardous) that have been pumped by the products or have otherwise been
in contact with the products are listed below.
the products have been cleaned, decontaminated, sterilised inside and outside
and all inlets and outlets are sealed.
List of hazardous materials that have been in contact with the products:
Chemical, material Hazard category
Final declaration We hereby declare that
we are fully conversant with the substances that have been in contact with the
products and have answered all questions correctly.
we have taken all measures necessary to prevent potential hazards in respect of
the products returned.
Company name or stamp:
Place, date:
Name (block letters), position
(block letters):
Signature:
Page 51
Page 52
Loading...