29
BÜCHI Rotavapor R-200/205
5 Operation
5.8 Solvent table
Solvent Formula Molar Mass Evaporation Boiling point Density Vacuum in mbar for
in g/mol energy in J/g at 1013 mbar in g/cm3boiling point at 40°C
Acetone C3H6O 58.1 553 56 0.790 556
n-amylalcohol, n-pentanol C5H12O 88.1 595 37 0.814 11
Benzene C6H6 78.1 548 80 0.877 236
n-butanol, tert.butanol C4H10O 74.1 620 118 0.810 25
(2-methyl-2-propanol) C4H10O 74.1 590 82 0.789 130
Chlorobenzene C6H5Cl 112.6 377 132 1.106 36
Chloroform CHCl3 119.4 264 62 1.483 474
Cyclohexane C6H12 84.0 389 81 0.779 235
Diethylether C4H10O 74.0 389 35 0.714 Atmospheric
1,2-dichloroethane C2H4Cl2 99.0 335 84 1.235 210
1,2-dichloroethylene (cis) C2H2Cl2 97.0 322 60 1.284 479
1,2-dichloroethylene (trans) C2H2Cl2 97.0 314 48 1.257 751
Diisopropyl ether C6H14O 102.0 318 68 0.724 375
Dioxane C4H8O2 88.1 406 101 1.034 107
DMF (dimethyl-formamide) C3H7NO 73.1 153 0.949 11
Acetic acid C2H4O2 60.0 695 118 1.049 44
Ethanol C2H6O 46.0 879 79 0.789 175
Ethylacetate C4H8O2 88.1 394 77 0.900 240
Heptane C7H16 100.2 373 98 0.684 120
Hexane C6H14 86.2 368 69 0.660 335
Isopropylalcohol C3H8O 60.1 699 82 0.786 137
Isoamylalcohol,
3-methyl-1- butanol C5H12O 88.1 595 129 0.809 14
Methylethylketone C4H8O 72.1 473 80 0.805 243
Methanol CH4O 32.0 1227 65 0.791 337
Methylene chloride,
dichloromethane CH2Cl2 84.9 373 40 1.327 Atmospheric
Pentane C5H12 72.1 381 36 0.626 Atmospheric
n-propylalcohol C3H8O 60.1 787 97 0.804 67
Pentachloroethane C2HCl5 202.3 201 162 1.680 13
1,1,2,2-tetra-chloroethane C2H2Cl4 167.9 247 146 1.595 35
Tetrachlorocarbon CCl4 153.8 226 77 1.594 271
1,1,1-trichloroethane C2H3Cl3 133.4 251 74 1.339 300
Tetra-chloro-ethylene C2Cl4 165.8 234 121 1.623 53
THF (tetrahydrofurane) C4H8O 72.1 67 0.889 357
Toluene C7H8 92.2 427 111 0.867 77
Trichloroethylene C2HCl3 131.3 264 87 1.464 183
Water H2O 18.0 2261 100 1.000 72
Xylene (mixture) C8H10 106.2 389 25
0-xylene C8H10 106.2 144 0.880
m-xylene C8H10 106.2 139 0.864
p-xylene C8H10 106.2 138 0.861
Table 5: Solvent table (CRC Handbook 65th Ed)5.9 Troubleshooting