PolyScience AD07R-20, AD07R-40, AD7LR-20, AD15R-30, AD15R-40 Operating Manual

...
4.1 (8)

Circulating Baths with Advanced Digital Temperature Controller

Operator’s Manual

Models:

AD07R-20

AD07R-40

AD7LR-20

AD15R-30

AD15R-40

AD20R-30

AD28R-30

AD45R-20

AD07H200

AD15H200

AD20H200

AD28H200

AD06S150

AD10S150

AD28S150

AD29VB3S

AD29VB5R

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Table of Contents

 

Introduction .................................................................................................................................................

4

PolyScience Circulating Baths with the Advanced Digital Temperature Controller .................................

4

General Safety Information.......................................................................................................................

5

Safety Recommendations.........................................................................................................................

6

Regulatory Compliance & Testing ............................................................................................................

7

Unpacking Your Circulator........................................................................................................................

8

Contents ...................................................................................................................................................

8

Controls & Components............................................................................................................................

9

Advanced Digital Controller..................................................................................................................

9

Refrigerating/Heating Baths ...............................................................................................................

10

Heating Only Baths.............................................................................................................................

11

Open Bath Systems (Stainless Steel) ................................................................................................

12

Viscosity Bath (Polycarbonate) ..........................................................................................................

12

Quick-Start.................................................................................................................................................

13

Installation & Startup ................................................................................................................................

15

General Site Requirements ....................................................................................................................

15

Adding Liquid to the Bath Reservoir .......................................................................................................

15

Pump Inlet and Outlet Connections........................................................................................................

16

External Closed Loop Circulation ...........................................................................................................

17

Open Loop Circulation ............................................................................................................................

17

Refrigeration Control Connections (Refrigerating/Heating Circulators only)..........................................

18

Electrical Power ......................................................................................................................................

18

Refrigerating/Heating Circulators .......................................................................................................

18

Heat Only Circulators and Open Bath Systems .................................................................................

19

Communication.......................................................................................................................................

20

USB Communication ..........................................................................................................................

21

Ethernet ..............................................................................................................................................

21

RS232 / RS485 Serial Communication ..............................................................................................

21

External (P2) Temperature Probe ..........................................................................................................

21

Controller Setup......................................................................................................................................

22

Power .................................................................................................................................................

22

Safety Set Temperature .....................................................................................................................

23

Normal Operation......................................................................................................................................

24

Keys and Controls ..................................................................................................................................

24

Turning Your Circulator ON ....................................................................................................................

24

Main Operational Display........................................................................................................................

25

Set-Up Sub-Menus .................................................................................................................................

27

Adjusting the Temperature Set Point......................................................................................................

28

Selecting the Temperature Unit..............................................................................................................

29

Selecting the Pump Speed .....................................................................................................................

30

Setting the High Limit Temperature........................................................................................................

31

Setting the Low Limit Temperature.........................................................................................................

32

Setting the Differential Temperature.......................................................................................................

33

Setting the Auto Cool Temperature ........................................................................................................

34

Setting the Specific Heat Capacity (SHC) ..............................................................................................

35

Selecting Internal or External Control.....................................................................................................

36

Calibrating Your Circulator (Offset) ........................................................................................................

37

Displaying the Safety Set Temperature..................................................................................................

38

Selecting a Remote Communication and Control Protocol ....................................................................

39

Using the Timer ......................................................................................................................................

40

Entering a Password...............................................................................................................................

41

Enabling / Disabling Data Logging .........................................................................................................

42

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Selecting the Operational Language ......................................................................................................

43

Setting Auto Restart................................................................................................................................

44

Resetting the Factory Default Values .....................................................................................................

44

Changing Your Circulator's Viewing Angle.............................................................................................

45

Inert Gas Purge ......................................................................................................................................

45

Tap Water Cooling..................................................................................................................................

45

Reservoir Cover Storage ........................................................................................................................

46

Display Messages and Alarms ................................................................................................................

47

Routine Maintenance & Troubleshooting...............................................................................................

48

Maintaining Clear Bath Water.................................................................................................................

48

Draining the Bath Reservoir ...................................................................................................................

48

Refrigerated / Heating and Heat only Circulating Baths.....................................................................

48

Polycarbonate Viscosity Baths ...........................................................................................................

49

Checking the Over-Temperature / Low Liquid Level Safety Systems....................................................

50

Over-Temperature Protection.............................................................................................................

50

Low Liquid-Level Protection ...............................................................................................................

50

Cleaning Your Circulator.........................................................................................................................

51

Temperature Controller ......................................................................................................................

51

Bath Reservoir....................................................................................................................................

51

Pump Impeller ....................................................................................................................................

51

Condenser, Air Vents, and Reusable Filter (Refrigerating / Heating Circulators only) ......................

51

Temperature Controller Removal and Re-Installation ............................................................................

52

Removal .............................................................................................................................................

52

Re-Installation.....................................................................................................................................

53

Viewing Component Operating Time......................................................................................................

54

Troubleshooting Chart ............................................................................................................................

55

Technical Information...............................................................................................................................

57

Performance Specifications....................................................................................................................

57

Reservoir Fluids......................................................................................................................................

58

Application Notes....................................................................................................................................

60

Tubing and Fitting Temperature Ranges................................................................................................

60

Fluid Compatibility ..................................................................................................................................

60

RS232/RS485 Configuration ..................................................................................................................

61

RS232/RS485 Communications.............................................................................................................

63

USB Data Logging ..................................................................................................................................

65

USB B Setup, Monitoring, and Control ...................................................................................................

65

Initial Setup.........................................................................................................................................

65

Monitoring and Control .......................................................................................................................

66

Configuring the Ethernet Connection .....................................................................................................

66

Direct Computer to Controller Configuration ......................................................................................

66

Wired or Wireless Network Configuration ..........................................................................................

66

Equipment Disposal (WEEE Directive) ...................................................................................................

70

Replacement Parts & Accessories..........................................................................................................

71

PolyScience Circulating Bath Fluids ......................................................................................................

73

Service & Technical Support ...................................................................................................................

73

Warranty.....................................................................................................................................................

74

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Introduction

Thank you for choosing a PolyScience Circulating Bath. It is intended for the precise temperature control of suitable liquids in a reservoir. Extremely easy to use and maintain, your Circulating Bath combines design innovation with highly intuitive operation to deliver convenient and reliable liquid temperature control for a wide range of applications.

WARNING: PolyScience Circulating Baths are not intended for directly controlling the temperature of foods, pharmaceuticals, medicines, or other objects which may be ingested by or injected in humans or animals. Any such objects must be isolated from contact with the bath fluid and bath surfaces.

Here are some of the features that make your Circulating Bath so user-friendly:

Simple, intuitive operation

Extra-large digital readout that displays actual and set point temperature simultaneously

Powerful variable speed duplex pump with openand closed-loop external circulation capability

180° viewing radius (Swivel 180™ rotating control head)

DuraTop™ heat and chemical resistant top plate

LidDock™ self-storing reservoir cover (integrated baths only)

Built-in temperature protection

Suitable for use with Class III flammable fluids per DIN 12876-1

It will take you very little time to get your new Circulating Bath installed and running. This Operator’s Manual is designed to guide you quickly through the process. We recommend that you read it thoroughly before you begin.

PolyScience Circulating Baths with the Advanced Digital Temperature Controller

Model Type

Reservoir

Temperature Range

Capacity

°C

°F

 

 

 

 

 

AD07R-20 Refrigerating / Heating Bath

7 liters

-20° to 200°C

-4° to 392°F

 

 

 

 

AD07R-40 Refrigerating / Heating Bath

7 liters

-40° to 200°C

-40° to 392°F

 

 

 

 

AD7LR-20 Refrigerating / Heating Bath

7 liters

-20° to 200°C

-4° to 392°F

 

 

 

 

AD15R-30 Refrigerating / Heating Bath

15 liters

-30° to 200°C

-22° to 392°F

 

 

 

 

AD15R-40 Refrigerating / Heating Bath

15 liters

-40° to 200°C

-40° to 392°F

 

 

 

 

AD20R-30 Refrigerating / Heating Bath

20 liters

-30° to 200°C

-22° to 392°F

 

 

 

 

AD28R-30 Refrigerating / Heating Bath

28 liters

-30° to 200°C

-22° to 392°F

 

 

 

 

AD45R-20 Refrigerating / Heating Bath

45 liters

-25° to 135°C

-13° to 275°F

 

 

 

 

AD07H200 Heating Only Bath

7 liters

Ambient +10° to 200°C

Ambient +20° to 392°F

AD15H200 Heating Only Bath

15 liters

Ambient +10° to 200°C

Ambient +20° to 392°F

 

 

 

 

AD20H200 Heating Only Bath

20 liters

Ambient +10° to 200°C

Ambient +20° to 392°F

 

 

 

 

AD28H200 Heating Only Bath

28 liters

Ambient +10° to 200°C

Ambient +20° to 392°F

 

 

 

 

AD06S150 Open Bath System

6 liters

Ambient +10° to 150°C (1)

Ambient +20° to 302°F (1)

AD10S150 Open Bath System

10 liters

Ambient +10° to 150°C (1)

Ambient +20° to 302°F (1)

AD20S150 Open Bath System

20 liters

Ambient +10° to 150°C (1)

Ambient +20° to 302°F (1)

AD28S150 Open Bath System

28 liters

Ambient +10° to 150°C (1)

Ambient +20° to 302°F (1)

AD29VB5R Polycarbonate Viscosity

29 liters

Ambient +10° to 85°C (2)

Ambient +20° to 185°F (2)

AD29VB3S Polycarbonate Viscosity

29 liters

Ambient +10° to 85°C (2)

Ambient +20° to 185°F (2)

1.Maximum operating temperature at which ±0.01°C temperature stability can be maintained; Advanced Digital Controller is capable of higher temperatures.

2.Maximum operating temperature for polycarbonate tank. Advanced Digital Controller is capable of higher temperatures.

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General Safety Information

When installed, operated, and maintained according to the directions in this manual and common safety procedures, your Circulating Bath should provide safe and reliable temperature control. Please ensure that all individuals involved in the installation, operation, or maintenance of this Circulating Bath read this manual thoroughly prior to working with the unit.

This symbol alerts you to a wide range of potential dangers.

This symbol advises you of danger from electricity or electric shock.

This symbol indicates that a hot surface may be present.

This symbol marks information that is particularly important.

This symbol indicates alternating current.

/These symbols on the Power Switch / Circuit Breaker indicate that they place the main power supply ON / OFF.

This symbol on the Power Key indicates that it places the unit in a standby mode. It DOES NOT fully disconnect the unit from the power supply.

This symbol indicates a protective conductor terminal.

Read all instructions pertaining to safety, set-up, and operation.

Proper operation and maintenance is the user’s responsibility.

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Safety Recommendations

To prevent injury to personnel and/or damage to property, always follow your workplace’s safety procedures when operating this equipment. You should also comply with the following safety recommendations:

WARNING:

This Circulating Bath is suitable for use with Class III flammable fluids per DIN 12876-1. A fire hazard may be present.

Be aware of the chemical hazards that may be associated with the bath fluid used. Observe all safety warnings for the fluids used as well as those contained in the material safety data sheet.

Explosive gas mixtures may accumulate if used with insufficient ventilation. Use this Circulating Bath in a well ventilated area or beneath a suitable fume hood only.

Use only recommended bath fluids; see Technical Information in the rear of this manual for recommended fluids.

Use only non-acid bath fluids.

WARNING: When using Class III flammable fluids per DIN 12876-1, the user must attach the following warning labels to the front of the unit so that they are well visible:

Warning Label

 

Danger Area.

W09

 

Attention! Observe instructions

Colors: Yellow/black

 

(operating manual, safety data sheet)

 

 

 

Mandatory Label

 

Carefully read the user information prior to

M018

 

beginning operation.

Colors: Blue/white

 

Scope: EU

or

 

 

Semi S1-0701

 

Carefully read the user information prior to

Table A1-2 #9

 

beginning operation.

Colors: Blue/white

 

Scope: NAFTA

 

 

 

WARNING:

Always connect the power cord on this Circulator to a grounded (3-prong) power outlet. Make certain that the outlet is the same voltage and frequency as your unit.

Never operate the Circulator with a damaged power cord.

Always turn the Circulator OFF and disconnect mains power before performing any maintenance or service.

WARNING:

Never operate the Circulator without bath fluid in the reservoir. Periodically check the reservoir to ensure that the liquid depth is within acceptable levels. Always refill the reservoir using the same bath fluid type that is already in the reservoir. Bath oil must not contain any water contaminants and should be preheated to the actual bath temperature before adding as there is an explosion hazard at high temperatures.

Always drain all fluid from the reservoir before moving or lifting your Circulator. Be sure to follow your organization’s procedures and practices regarding the safe lifting and relocation of heavy objects.

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WARNING:

Always allow the bath fluid to cool to ambient temperature before draining.

The reservoir cover, top deck, and/or external pump connections may become hot with continuous use. Exercise caution when touching these parts.

Always keep within the 85°C maximum operating temperature limit if using a polycarbonate tank.

WARNING: It is the user’s responsibility to properly decontaminate the unit in the event hazardous materials are spilled on exterior or interior surfaces. Consult manufacturer if there is any doubt regarding the compatibility of decontamination or cleaning agents.

Regulatory Compliance and Testing

This equipment is compliant with the European Directive 2002/95/EC and its latest amendments on Restrictions on Hazardous Substances (RoHS) and below the given limits of hazardous substances.

ETL Intertek (60 Hz units)

UL 61010-1 / CSA C22.2 No. 61010-1 — Safety Requirements for Measurement, Control, and Laboratory Use; Part 1: General Requirements

UL 61010A-2-010 / CSA C22.2 No. 61010-2-010:04 — Safety Requirements for Measurement, Control, and Laboratory Use; Part 2-010: Particular Requirements for Laboratory Equipment for the Heating of Materials

UL 61010A-2-051 / CSA C22.2 No. 61010-2-051:04 — Safety Requirements for Measurement, Control, and Laboratory Use; Part 2-051: Particular Requirements for Laboratory Equipment for the Mixing and Stirring

CE (all units)

EC Low Voltage Directive 2006/95/EC

EC Electromagnetic Compatibility Directive 2004/108/EC

IEC 61010-1-2001

IEC 61010-2-2001

IEC 61326:2005 / EN 61326 : 2006

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Unpacking Your Circulator

Your Circulator was packed in a special carton or cartons. You should keep the packaging, along with all packing materials, until the unit has been installed and you are certain it is working properly.

CAUTION: Remove any loose packing material that may have fallen into the heater/pump housing during shipping. Before powering up, check that nothing remains around the heater or Circulator pump.

We recommend that you begin using your Circulator immediately to confirm proper operation, since beyond one week you may be eligible for warranty repair only (rather than replacement). You’ll find complete warranty information in the back of this manual.

In the unlikely event that the unit was damaged or does not operate properly, contact the transportation company, file a damage claim, and contact the company where your Circulator was purchased.

Contents

The items included with your Circulator will vary depending on which model Circulating Bath you purchased.

 

Refrigerating /

 

Heating Only

 

Open Bath

Viscosity

 

Heating Bath

 

Bath

 

System

Bath

Resource Disk with

 

 

Operator’s Manual

 

 

 

 

 

 

 

 

Reservoir Lid

 

 

N/A

 

 

 

 

 

 

 

3-ft / 0.91 m IEC to

 

N/A

 

N/A

N/A

IEC Power Cord

 

 

 

 

 

 

 

 

6-ft / 1.82 m IEC to

 

 

Mains Power Cord

 

 

 

 

 

 

 

 

Refrigeration Control

 

N/A

 

N/A

N/A

Cable

 

 

 

 

 

 

 

 

Fittings

1/4 in. NPT to 3/16 in. barbed adapter (1)

 

 

1/4 in. NPT to 1/4 in. barbed adapter (1)

 

 

 

1/4 in. NPT to 3/8 in. barbed adapter (1)

 

 

 

 

1/4 in. NPT to M16 barbed adapter (2)

 

 

Cooling Coil

N/A

 

Integral

 

Optional

Certificate of

 

 

Compliance

 

 

 

 

 

 

 

 

Quick-Start Guide

 

 

 

 

 

 

 

 

 

1.60Hz and 50Hz models

2.50Hz models only

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Controls and Components

Advanced Digital Controller

3.75” (9.5 cm)

Color LCD

Power Key

Home Key

Power Switch /

Circuit Breaker (located on Refrigeration Power Module on Refrigerating/Heating Circulators)

Safety Set

Thermostat

IEC Electrical

Connection

IEC Power Cord

Fluid Inlet Connection

Inert Gas Injection Port

Touch Scroll Bar

Set Key

Menu Key

Swivel 180

Latch Release

USB A Connection

USB B Connection

Ethernet Connection

RS232/RS485 Serial Port

External (P2)

Temperature Probe

Connection

Refrigeration Control

Connection (functional on

Refrigerating/Heating

Circulators only)

Fluid Outlet Connection

Bypass Hose

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Refrigerating/Heating Baths

Reservoir Drain Valve and Port

(behind access panel) Side access on AD7LR-20)

Washable Air Filter

(behind access panel)

IEC Power Connection to

Refrigeration Power Module

Refrigeration Power Module

Power Switch / Circuit Breaker

Advanced Digital

Temperature Controller

Reservoir Cover

Drain Valve and Port

(right side on AD7LR-20 only)

Refrigeration Control

Connection

Power

Cooling

Cooling Fault

Fan

Cooling System Status Display

Refrigeration Control Connection

IEC Power Connection to Controller

IEC Power Connection to Mains

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Heating Only Baths

Reservoir Drain Valve and Port

(behind access panel)

Power Switch / Circuit Breaker

IEC Connection to Mains

Tap Water Cooling Connection

(inlet)

Advanced Digital

Temperature Controller

Reservoir Cover

Tap Water Cooling Connection

(outlet)

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Open Bath Systems (Stainless Steel)

Advanced Digital

Temperature Controller

Viscosity Bath (Polycarbonate)

Lidded Viscometer Openings

Reservoir Drain Port

Cooling Coil Opening with Cover

(10L, 20L, and 28L models)

Reservoir Cover

Advanced Digital

Temperature

Controller

Tap Water Cooling

Coil

WARNING: The top deck on Open Bath Systems and Viscosity Baths is not attached. Do not remove deck while Circulator is operating. Do not lift bath by grasping the Temperature Controller or top deck. Always disconnect electrical power and drain fluid from bath before moving.

WARNING: The PolyScience Advanced Digital Temperature Controller is designed for use with Class III flammable liquids per DIN 12876-1; however, we strongly recommend that Open Bath Systems and Viscosity Baths be used only with non-flammable fluids.

WARNING: To avoid the potential for burns, allow the Circulator to cool completely before cleaning or performing any maintenance.

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Quick-Start

Unless otherwise specified, quick-start instructions apply to all models. See Installation and Startup for additional information.

Maximum: 1 in. / 2.54 cm below underside of top deck

1 Fill reservoir with fluid

Minimum: 3.0 in. / 7.6 cm below underside of top deck

Heating only models

2

Connect all power cords and

IEC power cord

Refrigerating / Heating

 

control cables

from Controller

 

models

 

 

 

to Refrigeration

 

 

 

 

 

 

 

 

 

 

Power Module

 

 

 

 

 

 

 

 

 

 

 

 

 

Refrigeration control

 

 

 

 

 

cable

 

 

 

 

 

 

 

Heating only models

3Place Power Switch / Circuit Breaker in ON position

Refrigerating / Heating

models

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4 Turn Controller “ON”

5

Set safety thermostat

 

 

 

 

6B.

 

Enter temperature

 

Touch and hold or slide

6

 

finger up/down scroll bar

set point

 

 

 

 

 

 

 

 

 

 

6A.

 

 

Press SET

 

 

 

 

 

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Installation and Startup

Your Circulating Bath with Advanced Digital Temperature Controller is designed to be simple to set-up and install. The only tools required are a No.1 Phillips-head screwdriver and a container for adding water or other suitable fluid to the bath reservoir.

General Site Requirements

Locate your Circulator on a level surface free from drafts and direct sunlight. Do not place it where there are corrosive fumes, excessive moisture, high room temperatures, or in excessively dusty areas.

Refrigerating / Heating Circulators must be 10.2 cm / 4 inches or more away from walls or vertical surfaces so that airflow is not restricted.

Avoid voltage drops by using properly grounded power outlets wired with 14 gauge or larger diameter wire and if possible, be close to the power distribution panel. The use of extension cords is not recommended; this will reduce the potential for problems caused by low line voltage.

Adding Liquid to the Bath Reservoir

WARNING: When using Class III flammable fluids per DIN 12876-1, the user must attach the following warning labels to the front of the unit so that they are well visible:

Warning Label

 

Danger Area.

W09

 

Attention! Observe instructions

Colors: Yellow/black

 

(operating manual, safety data sheet)

 

 

 

Mandatory Label

 

Carefully read the user information prior to

M018

 

beginning operation.

Colors: Blue/white

 

Scope: EU

or

 

 

Semi S1-0701

 

Carefully read the user information prior to

Table A1-2 #9

 

beginning operation.

Colors: Blue/white

 

Scope: NAFTA

 

 

 

WARNING: See Technical Information in the rear of this manual for a list of compatible liquids. WARNING: Read the safety data sheet for the bath fluid being used carefully before filling reservoir.

WARNING: If the proper fluid level is not maintained, the heater coil may become exposed and possibly damaged (fluid level too low) or the bath may overflow (fluid level too high).

The liquid in the reservoir should be maintained at a depth between 1 inch / 2.54 cm and 3.0 inches / 7.6 cm below the underside of the bath’s top deck. Upon start up, it may be necessary to add fluid to the bath to compensate for the fluid required for external circulation. Likewise, be sure to compensate for fluid displacement when placing samples or other materials in the Circulator’s reservoir.

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Maximum Fluid Level =

1 inch / 2.54 cm below underside of top deck

Minimum Fluid Level =

3.0 inches / 7.6 cm below underside of top deck

WARNING: Always drain all fluid from the reservoir before moving or lifting your Circulator. Be sure to follow your organization’s procedures and practices regarding the safe lifting and relocation of heavy objects.

WARNING: To avoid the potential for burns, allow the Circulator to cool completely before cleaning or performing any maintenance.

Pump Inlet and Outlet Connections

WARNING: When connecting tubing to an external application, it is the user’s responsibility to make sure that the tubing and fittings connected to the Circulator are suitable for the fluid being used and the temperature range of operation.

CAUTION: The Circulator’s bypass tubing is secured to the fluid inlet and outlet connections by high temperature nylon hose clamps, which can be removed by carefully cutting them with diagonal cutters.

CAUTION: Secure the tubing to the inlet and outlet fittings using hose clamps with a minimum ID of 7/8 inch (22 mm). Do not operate the unit without hose clamps.

WARNING: If the Circulating Bath will not be used for external circulation, the inlet and outlet ports should remain connected using the Buna N bypass tubing provided with the unit.

The pump inlet and outlet ports are female ¼ inch NPT connections that permit use of barbed tubing adapters or hard plumbing fittings. ½ inch (13 mm) ID tubing may also be slid over these connections and held in place with a hose clamp (minimum 7/8 inch / 22 mm ID).

If the pump inlet and outlet are not used for external circulation, the Bypass Tubing provided with the unit should be left in place in order to optimize fluid mixing within the reservoir.

The nylon barbed tubing adapter fittings supplied with the unit are intended for applications from

-40° to 93°C. For applications above 93°C, brass, stainless steel, or Teflon® fittings are recommended. ¼ inch NPT to M16 stainless steel male adapter fittings are provided with all 50Hz models.

NOTE: The use of quick-connect fittings is not recommended as they typically restrict flow rate.

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External Closed Loop Circulation

Connect the pump inlet and outlet to the external apparatus. To maintain adequate flow, avoid restrictions in the tubing. When connecting the Circulator to more than two closed loops, the use of a manifold made of “Y” adapters to divide the fluid into multiple banks is recommended. After setting up multiple closed loops, check for adequate flow at the return manifold of each loop and check that the bath fluid is at an adequate level. A booster pump may be added to closed loops without damaging the Circulator’s pump.

The temperature control stability of a closed loop system is better at the external apparatus than in the Circulator reservoir (provided the control point of the apparatus represents a constant load and is well insulated). For example, if you circulate fluid through a viscometer at 50°C, the temperature variation observed in the Circulator reservoir may be ±0.1°C while the temperature variation in the viscometer may be only ±0.05°C.

Although temperature stability is generally better at the external apparatus control point, depending on the length of tubing used and the efficiency of the insulation, the actual temperature reading at the external apparatus may be slightly different than the temperature reading at the Circulator reservoir.

Open Loop Circulation

The duplex (pressure/suction) pump permits circulation to and from an external open bath. To prevent siphoning when the Circulating Bath is turned off, position both baths so that the two fluid levels are at the same elevation.

Connect the pump inlet and outlet to the external bath using tubing of the same diameter and length. The same size fittings should also be used on both the inlet (suction) and outlet (pressure). This helps ensure a balanced flow. A restricting valve or pinch clip should be installed in the pressure (outlet) tubing and adjusted to match the return suction (inlet) flow rate. Cut the external end of the suction tube into a “V” shape so that the tube will not seal itself against the wall of the external tank. Both the pressure and suction tubing should be securely fastened to the external tank to prevent movement during use.

When using flexible tubing, the suction tubing must have a wall thickness that will not collapse under vacuum, particularly when going around bends.

Circulating Bath Height Regulation — Position the ends of the pressure and suction tubes at the desired maximum fluid level in the external bath and fill the bath to that level. Fill the Circulating Bath to a height one inch (25mm) below the top of the reservoir. Start the pump and adjust the restricting valve/pinch clip on the pressure tubing until the liquid height in both baths remains constant. Add fluid to the baths as needed to compensate for the fluid in the inlet and outlet lines.

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Refrigeration Control Connections (Refrigerating/Heating Circulators only)

Refrigeration Control Connection

Refrigeration Control Cable

Refrigeration Control Connection

Electrical Power

WARNING: The Circulator’s power cord must be connected to a properly grounded electrical receptacle. Make certain that this electrical outlet is the same voltage and frequency as your Circulator. The correct voltage and frequency for your Circulator are indicated on the identification label on the back of the Controller.

CAUTION: The use of an extension cord is not recommended. If one is necessary, it must be properly grounded and capable of handling the total wattage of the unit. The extension cord must not cause more than a 10% drop in voltage to the unit.

Refrigerating / Heating Circulators

Attach the 3-ft / 0.91 m power cord to the IEC electrical connectors on the Temperature Controller (male) and the Refrigeration Power Module (female).

Attach the 6-ft / 1.8 m power cord to the IEC electrical connection on the Refrigeration Power Module and then plug the male connector into the Mains electrical outlet.

Place the Power Switch / Circuit Breaker on the Refrigeration Power Module in the ON position. The LCD on the Controller will light and “Standby” will appear on the display; the PolyScience logo and the Power Key will also light.

NOTE: To conserve power when not in use, the LCD’s backlighting will go out about 5 seconds after “Standby” appears. The Power Key and PolyScience logo will remain lit to indicate that the Controller is energized and ready to use.

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IEC Power Connection to

Refrigeration Power Module

IEC to IEC Power Cord

Refrigeration Power Module

IEC Power Connection to Controller

Power Switch / Circuit Breaker

 

IEC Power Connection to Mains

 

 

IEC to Mains Power Cord

Heat Only Circulators and Open Bath Systems

Attach the 6-ft / 1.8 m power cord to the IEC electrical connection on the Temperature Controller and then plug the male connector into the Mains electrical outlet.

Place the Power Switch / Circuit Breaker on the Temperature Controller in the ON position. The LCD on the Controller will light and “Standby” will appear on the display; the PolyScience logo and the Power Key will also light.

NOTE: To conserve power when not in use, the LCD will go black about 5 seconds after “Standby” appears. The Power Key and PolyScience logo will remain lit to indicate that the Controller is energized and ready to use.

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PolyScience AD07R-20, AD07R-40, AD7LR-20, AD15R-30, AD15R-40 Operating Manual

Communication

The Advanced Digital Controller features a variety of connectivity options. Following are some typical ways you can use them to monitor and control the operation of your Circulator.

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USB Communication

Two USB ports (A and B) are provided on the rear of the Temperature Controller. USB A is intended for use with a flash drive and allows you to easily log temperature data. USB B allows you to remotely monitor and control your Circulator using a computer. See Normal Operation, Selecting a Remote Communication and Control Protocol and the Technical Information section of this manual for additional information.

Ethernet

An Ethernet port is provided on the back of the Temperature Controller to enable you to connect your Circulator to a computer network. See Normal Operation, Selecting a Remote Communication and Control Protocol and the Technical Information section of this manual for additional information,

RS232 / RS485 Serial Communication

CAUTION: Always turn electrical power to the Circulator OFF before making a connection to the serial (DB9) port.

Your Circulator features RS232 / RS485 serial communication for remote data logging and control capability. A DB9 connector is provided on the rear of the Temperature Controller for this purpose. See

Normal Operation, Selecting a Remote Communication and Control Protocol and the Technical Information section of this manual for additional information.

The serial interface should be connected to a serial communication port on a remote PC using an appropriate cable. Information on the RS232 / RS485 command and communication protocol can be found in the Technical Information section of this manual.

External (P2) Temperature Probe

Your Circulator is capable of controlling temperature based on either the temperature of the internal bath or that of an external vessel or device. The connection for the optional external temperature probe is on the rear of the Temperature Controller. The Temperature Controller automatically detects the external temperature probe when it is connected. See Replacement Parts & Accessories for available lengths and part numbers.

Pin Out Diagrams — External (P2) Temperature Probe Connection

RTD SENSOR: 4 WIRE CIRCUIT, 100 OHMS @ 0 DEGREES C,

MAXIMUM OPERATING TEMPERATURE @ 200 C, CLASS A 0.003850 OHMS/DEGREES C.

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Controller Setup

Power

Press . The Circulator will begin running, actual and set point temperatures will be displayed, and the word “SET” will be continuously lit. The pump symbol will also be lit and the heating or refrigerating symbol may be lit or flashing.

Control probe

Heating symbol

Actual bath

temperature

Refrigerating symbol

Set point temperature

Circulating symbol

Internal (P1) control only – external probe (P2) not connected

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Safety Set Temperature

This is a “Do Not Exceed” temperature setting for your Circulator and is the temperature at which the heater will be turned OFF should the liquid level in the bath drop too low or the heater malfunctions. It is normally set about 5° higher than the desired operating temperature. Setting the Safety Set temperature is a simple 3-step procedure.

WARNING: The Safety Thermostat is user-adjustable from approximately 100° to 220°C / 312° to 428°F. Do not force the indicator dial beyond the stops at either end of the dial’s range.

1. Press the key until SAFETY appears.

Current Safety

Safety Set Set Temperature

sub-menu

2.Using a No.1 Philips head screwdriver, rotate the Safety Thermostat on the rear of the Temperature Controller until the desired Safety Set Temperature is displayed (clockwise to increase; counterclockwise to decrease).

Safety Set Thermostat

3. Press to return to the main operational screen.

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