In-Situ S2XP User Manual

Instruction Sheet
TROLL®9500 S2XP Restrictor Installation and Calibration
Part number 0085490, Rental R79420

Overview

The S2XP restrictor is shipped in two pieces. The restrictor must be installed in separate steps to allow for sensor calibration.
It is recommended you follow all steps in this instruction sheet to properly set up your TROLL 9500 S2XP system.

Contents

Figure 1.1 Contents of the shipping container
1 TROLL 9500 Instrument

pH, ORP, and Conductivity Calibration

1. Detach the Cal Cup from the TROLL 9500. The Cal Cup contains a small amount of liquid to hydrate the pH sensor during shipment. Discard this liquid.
2. Thoroughly rinse the sensors with clean water.
3. Fill the Cal Cup to the fill line with Quick Cal solution. Reinstall the Cal Cup on the TROLL 9500. See Figure 1.2. Do not over-tighten.
2 S2XP restrictor, part A
3 Quick Cal solution
4 S2XP restrictor, part B
5 Sodium sulfite solution
6 Accessories kit
7 RDO sensor; TROLL Com
8 Bubbler (not shown)
Units may contain other equipment.
Information subject to change without notice. In-Situ, In-Situ logo, Baro Merge, BaroTROLL, HERMIT, iSitu, Pocket-Situ, RDO, RuggedCable, RuggedReader, TROLL, andWin-Situ are trademarks or registered trademarks of In-Situ Inc.©2013. A ll rights reserved.
Figure 1.2 Calibration using Quick Cal in the Cal Cup
4. In Win-Situ 4, click on Parameters in the Navigation tree.
5. Click Quick Cal. Select pH, ORP, and Conductivity.
6. Click Start. You must hold the TROLL 9500 vertically for proper calibration.
7. Allow the calibration to run until indicators reach Stable. Check calibration coefficients to ensure a proper calibration.
08/2013| Rev. 005 | 0085492
pH slope Between -50 to -66 mV/pH
pH offset 350 - 450 mV
ORP offset Between -20 and +20 mV
6. Remove the RDO sensor port plug from the center port using the removal tool. See Figure 1.5.
Save the port plug for return shipping.
K Cell Low 0.30 - 0.39 cm
K Cell High 4.4 - 5.8 cm
-1
-1

Initial Installation

1. Remove the Cal Cup. Dispose of the Quick Cal solution.
2. Thoroughly rinse the sensors with clean water.
3. Gently dry sensors with a paper towel.
4. Remove the pH/ORP sensor by inserting the removal tool (located in the accessories kit) underneath the sensor. See Figure 1.3. Note the sensor's port location (port 1) for reinstallation.
Instruction Sheet
Figure 1.5 Removing the RDO sensor port plug
7. Feed the RDO cable through the restrictor cap of restrictor B. See Figure 1.6.
Figure 1.3 Removing the pH/ORP sensor
5. Remove the conductivity sensor using the removal tool. See Figure 1.4. Note the sensor's port location (port 4) for reinstallation.
Figure 1.4 Removing the conductivity sensor
Figure 1.6 Feeding the RDO cable through the restrictor cap of restrictor B
8. Connect the RDO cable to the TROLL 9500 in port 3 (the center port). See Figure 1.7.
Figure 1.7 Connecting the RDO to sensor port 3
9. Reinstall the pH/ORP sensor to port 1 and the conductivity sensor to port 4. A diagram on the TROLL 9500 body designates port locations. Be sure the sensors are fully inserted before proceeding.
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10. Refresh Win-Situ 4 to ensure all sensors are correctly attached to the TROLL 9500. pH, ORP, Conductivity, and Rugged Dissolved Oxygen should appear under Parameters in the Navigation tree.
11. Rotate restrictor B onto the TROLL 9500 body. Do not fully attach the RDO sensor to the restrictor cap yet.

RDO Calibration

5. In Win-Situ 4, select Rugged Dissolved Oxygen in the Parameters list.
6. Before the DO Calibration Wizard starts, you will be asked how you want to handle barometric pressure. If the TROLL 9500 will be deployed on a vented cable,
Instruction Sheet
click No. If it will be deployed on a non-vented cable, click Yes.
7. Three calibration options appear. Select the first or second option:
The RDO sensor should be calibrated prior to being fully installed into the S2XP restrictor. Normally, a one-point 100% saturation calibration is sufficient.
A two-point (100% and 0% saturation) calibration is recommended when very low DO values (<1 mg/L) are expected, or after the sensor cap has been replaced. Standard Operating Procedures may also require a two-point calibration.

Oxygen Saturation Point (100%) Calibration

1. Remove the two batteries from inside the bubbler and install them into the air pump, as shown on the diagram on the inside of the air pump lid.
2. Fill the bubbler with clean water that is similar in temperature to what is expected in the field.
3. Turn on the bubbler. Open the pinch valve on the bubbler tubing and allow the bubbler to run for 10 minutes. For best results, run at the full flow rate to achieve saturation; after 10 minutes you can use the control valve to match the water turbulence conditions expected in the field.
4. Lay the TROLL 9500 on its side and insert the RDO sensor into the bubbler. See Figure 1.8. Ensure that the sensing element is not in the direct path of the bubbles.
l Calibrate: Starting from values stored in the sensor
(user-set or factory defaults) for the 0% and 100% calibration, this allows the user to redo one or both calibration points.
l Restore defaults, then calibrate: Restores factory
defaults for both 0% and 100%, then allows the user to redo one or both calibration points.
l Restore defaults, don't calibrate: Restores factory
defaults for both 0% and 100% saturation and closes the Calibration Wizard.
8. Click Run. Follow the on-screen instructions to complete the 100% calibration point.
9. When readings have stabilized, you will have several choices:
l Select Next to continue with the zero oxygen point if
you are performing a two-point calibration. Zero point oxygen calibration steps are listed below.
l Select Next, then Next again, then click Finish to
finalize the one-point calibration.
l Select Run to repeat the one-point calibration. Follow
steps 5-9 to repeat the calibration.

Zero Oxygen Point (0%) Calibration

Perform a 0% calibration only after completing the steps listed above.
1. Remove the RDO sensor from the bubbler.
2. Fill the Cal Cup 1/2 full with sodium sulfite solution.
3. Submerge the RDO sensor in the solution, and ensure there are no air bubbles on the sensing element.
Figure 1.8 Calibrating the RDO sensor
4. Allow 15 minutes for temperature equilibration.
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5. In Win-Situ 4, click Run in the Zero Oxygen Point screen. Follow the on-screen instructions to complete the 0% calibration point.
6. When readings have stabilized, you will have several choices:
l Select Next, then click Finish to finalize the calibration.
l Select Back to repeat the oxygen saturation point
(100%) calibration.
l Select Run to repeat the zero oxygen point (0%)
calibration. Follows steps 5-6 to repeat the calibration.

Final Installation

1. Remove the RDO sensor from the calibration solution. Rinse the RDO sensor thoroughly.
2. Loop the RDO cable that extends from the restrictor cap and hold it so that it abuts the RDO sensor. See Figure 1.9.
Instruction Sheet
Figure 1.11 Installing restrictor A —do not rotate restrictor B

Restrictor Removal and TROLL 9500 Shipping

1. Grip restrictor B firmly. Remove restrictor A from the restrictor cap. Do not allow restrictor B to rotate, as the RDO cable can become twisted or damage the other sensors. See Figure 1.12.
Figure 1.9 Looping the RDO cable for installation
3. Insert the RDO sensor and cable loop into the restrictor cap, using the hole for the sensor and the slot for the cable.
4. Push the sensor in until it snaps into the restrictor cap. Push the cable down into the slot until a small loop remains. See Figure 1.10.
Figure 1.10 RDO sensor and cable fully installed
5. Grip restrictor B firmly. Attach restrictor A to the restrictor cap. Do not allow restrictor B to rotate, as the RDO cable can become twisted or damage the other sensors. See Figure 1.11.
Figure 1.12 Removing restrictor A —do not rotate restrictor B
2. Remove the RDO sensor and cable loop from the restrictor cap. The end of the RDO cable will still be attached to the TROLL 9500 body. See Figure 1.13.
Figure 1.13 RDO sensor removed from the restrictor cap
3. Grip the TROLL 9500 body firmly. Remove restrictor B, being careful not to twist the RDO cable.
4. Remove the pH/ORP sensor by inserting the removal tool (located in the accessories kit) underneath the sensor. Note the sensor's port location (port 1) for reinstallation. See Figure 1.14.
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Figure 1.14 Removing the pH/ORP sensor
5. Remove the conductivity sensor using the removal tool. Note the sensor's port location (port 4) for reinstallation.
6. Remove the RDO sensor by pulling the connector out of the TROLL 9500 body. Never remove the sensor by pulling on the cable.
7. Reinstall all sensor port plugs.*
8. Reinstall the pH/ORP sensor and conductivity sensor. Ensure both sensors are completely inserted.
9. Check all sensor ports. Never ship the TROLL 9500 with open sensor ports. *
10. Fill the Cal Cup with a small amount of Quick Cal solution. Install the CalCup onto the TROLL 9500. *
Instruction Sheet
11. Replace red dust caps on the RDO probe and TROLL 9500 connectors.
* All sensor ports should be occupied by a sensor or port plug prior to shipping.
DONOTINSTALLTHECALCUP WITHANYLIQUIDINITIFYOU HAVELOSTPORTPLUGS.
Liquid will enter and damage the instrument.
YOUWILLBECHARGEDFOR INSTRUMENTREPLACEMENTIF YOUDAMAGETHEINSTRUMENT.
Contact In-Situ if you have questions regarding proper shipping.
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