INFICON MicroFID II Portable Flame Ionization Detector User Manual

OPERATING MANUAL
MicroFID
Flame Ionization Detector
IPN 074-579-P1A
II
The ultimate responsibility of the consequences of use of toxic compounds rests with the user. INFICON’s role is as a supplier of instrumentation to assist in the early detection of hazardous conditions involving such compounds.
It is vitally important to ensure that the MicroFID II is maintained in accordance with INFICON’s instructions and that proper calibration is regularly performed.
MicroFID II service should be performed only by INFICON, Inc., or an authorized INFICON repair center. Unauthorized service may void the Intrinsic Safety Certifications.
As with any complex device, the MicroFID II is subject to failure and, while INFICON has taken, and continues to take, all possible precautions to (a) reduce the possibility of failure, and (b) warn the user in the event of failure, circumstances may occasionally occur in which there is a failure despite such precautions on INFICON’s part. INFICON regrets that it cannot accept liability for damages of any kind caused as a result of either failure of the user to follow instructions or of the MicroFID II to perform.
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Part Number
Release
Publication Date
MN201103
A
6 September 2011
074-579-P1
A
16 October 2012
Release History
Customer Service INFICON Two Technology Place East Syracuse, NY 13057 USA
315-434-1100
www.inficon.com
Notices
The information contained in this document is subject to change without notice. INFICON makes no warranty of any kind with regard to the material, including, but not limited to, the implied warranties of merchantability and fitness for a particular purpose.
INFICON shall not be liable for errors contained herein for incidental or consequential damages in connection with furnishing, performance or use of this material.
Copyright © 2012 by INFICON
MicroFID IITM is a Trademark of INFICON Windows® is a Registered Trademark of Microsoft Corporation Bluetooth® is a registered Trademark of Bluetooth SIG, Inc. Tedlar® and Teflon® are Registered Trademarks of E.I. du Pont de Nemours & Company, Inc. A component of this device is licensed under U.S. Patent No. 7,369,945 B2
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Table of Contents
FOR YOUR SAFETY ............................................................................................................................ 7
NOTICES AND WARNINGS .............................................................................................................. 8
FCC Warning ............................................................................................................................................... 8
MicroFID II Intrinsic Safety Notice ............................................................................................................. 8
DECLARATION OF CONFORMITY ........................................................................................................... 11
1. INTRODUCTION ............................................................................................................................. 13
About this Manual ..................................................................................................................................... 13
UNPACKING THE MicroFID II ................................................................................................................... 14
WARNINGS AND SAFETY PRACTICES .................................................................................................. 14
Excessive Heat and Cold ........................................................................................................................ 14
Flame Ionization Detector Operation ...................................................................................................... 15
Detector Response ................................................................................................................................. 16
Support Equipment and Consumables ................................................................................................... 16
Compressed Gases ................................................................................................................................ 16
Regulators for Compressed Gases ......................................................................................................... 17
Hydrogen Gas ......................................................................................................................................... 17
Calibration Gas ....................................................................................................................................... 18
Oxygen Concentration Limits .................................................................................................................. 18
Flammable Gases ................................................................................................................................... 18
ACCESSORIES .......................................................................................................................................... 19
Computer ................................................................................................................................................. 19
Gas Sampling Bag .................................................................................................................................. 19
Charcoal Filters ....................................................................................................................................... 19
2. USING THE MICROFID II ............................................................................................................. 21
MicroFID II Feature Layout ....................................................................................................................... 21
Filling the Hydrogen Fuel Cylinder ......................................................................................................... 25
Attaching the Telescoping Probe to the MicroFID II ............................................................................. 33
Basic Operating Instructions ................................................................................................................... 33
Calibration.................................................................................................................................................. 34
Data Communication ................................................................................................................................ 34
Response Factors for Gases and Vapors ............................................................................................... 34
To use the response factors:................................................................................................................... 34
Preparing for Field Operation .................................................................................................................. 35
Field Check List ....................................................................................................................................... 35
Operational Check List ............................................................................................................................ 36
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3. USER FUNCTIONS ....................................................................................................................... 37
Display ........................................................................................................................................................ 37
Graphic Display ....................................................................................................................................... 37
Keys ............................................................................................................................................................ 41
Fixed ON/OFF Key .................................................................................................................................. 41
Soft Keys ................................................................................................................................................. 41
Beginning Operation ................................................................................................................................. 41
Turning on the MicroFID II ...................................................................................................................... 41
Default Display ........................................................................................................................................ 41
Numeric Value, Duration, Time and Date Entry ...................................................................................... 42
System Alerts and Alarms ....................................................................................................................... 43
User Interface – Basic Menu .................................................................................................................... 44
Passcode.................................................................................................................................................... 44
User Modes ................................................................................................................................................ 44
Location Mode Display ............................................................................................................................. 45
Interval Mode ............................................................................................................................................. 45
Method 21 Mode .................................................................................................................................... 46
Logging Off .............................................................................................................................................. 48
Data Logging ............................................................................................................................................. 48
Interval Mode - Data Logging .................................................................................................................. 49
MicroFID II Setup Functions ..................................................................................................................... 52
Pump ....................................................................................................................................................... 52
Backlight .................................................................................................................................................. 53
User Mode ............................................................................................................................................... 53
Date Format ............................................................................................................................................ 55
Password ................................................................................................................................................. 55
Language – Note: This feature is not yet available. ................................................................................ 55
Units ........................................................................................................................................................ 55
Real Time Data ....................................................................................................................................... 55
Alternative Calibration with Gas Bag ...................................................................................................... 61
Calibrating the MicroFID II (General) ....................................................................................................... 63
TARE selection .......................................................................................................................................... 71
4. WIRELESS COMMUNICATION ................................................................................................ 71
Wireless Communication Range ............................................................................................................. 71
Pairing ........................................................................................................................................................ 71
Enabling Blue Tooth Communication ..................................................................................................... 72
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5. ROUTINE MAINTENANCE ........................................................................................................ 74
Maintenance Intervals ............................................................................................................................... 74
Battery Charging ....................................................................................................................................... 74
Maintenance of the Flame Ionization Detector ....................................................................................... 75
Replacing Inlet Filter ................................................................................................................................. 75
Replacing the Sintered Filter (Exhaust Filter) ........................................................................................ 76
Calibration.................................................................................................................................................. 76
Maintenance Schedule Table ................................................................................................................... 77
Waste Electrical and Electronic Equipment (WEEE) ............................................................................. 77
7. TROUBLE SHOOTING ................................................................................................................. 78
General Information .................................................................................................................................. 78
MicroFID II Fault Messages ...................................................................................................................... 78
MicroFID II Troubleshooting .................................................................................................................... 80
8. APPENDICES ................................................................................................................................. 84
Monitoring Software ................................................................................................................................. 85
MicroFID II Telescoping Probe Holder Installation Guide ..................................................................... 86
MicroFID II Shoulder Strap Adaptor Kit Installation Guide ................................................................... 87
Warranty ..................................................................................................................................................... 88
Contacting INFICON .................................................................................................................................. 89
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For Your Safety
Strictly follow the Instructions for Use
Any use of this instrument requires a full understanding and strict adherence to these instructions. The instrument is only to be used for the purposes specified in this manual.
Maintenance
The MicroFID II must be inspected and serviced by trained service personnel at regular intervals. Repair of the MicroFID II may only be carried out by INFICON factory authorized service personnel. Only authentic INFICON spare parts may be used for maintenance. Review the chapter “Maintenance Intervals.
Use in areas subject to explosion hazards
The MicroFID II has been tested and approved according to EMI and intrinsic safety requirements defined by the US (FCC Pt. 15 and UL 913 5th edition). Declarations of conformity are found on page 11.
Modifications of components or the use of faulty or incomplete parts is not permitted. When making repairs to equipment or components of this type, Intrinsic Safety Certifications may be violated if the MicroFID II is serviced by individuals or organizations that are not INFICON factory certified for repair services.
Liability
The liability for the proper functioning of the MicroFID II is irrevocably transferred to the owner or operator to the extent that the instrument is improperly serviced or repaired by personnel not employed or authorized by INFICON, or if the MicroFID II is used in a manner not conforming to its intended use.
INFICON cannot be held responsible for damage caused by non-compliance with the recommendations given above.
The warranty and liability limitations provisions of the terms of sale and delivery of INFICON, are likewise not modified by the recommendations given above.
Copyright Information
This document contains proprietary information that is protected by copyright. All rights are reserved. No part of this publication may be reproduced in any form whatsoever or translated into any language without the prior written permission of INFICON.
Trademarks
Registered names, trademarks, etc. used in this document, even when not specifically marked as such, are protected by law.
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Notices and Warnings
FCC Warning
This equipment has been tested and found to comply with the limits for a Class B Digital Device, pursuant to Subpart B, Class B of Part 15 of the FCC rules. These limits are designed to provide reasonable protection against harmful interference when the equipment is operated in a commercial environment. This equipment generates, uses, and can radiate radio frequency energy and if not installed and used in accordance with the instruction manual, may cause harmful interference to radio communications. Operation of this equipment in a residential area is likely to cause harmful interference in which case the user will be required to correct the interference at their expense.
MicroFID II Intrinsic Safety Notice
THE MicroFID II IS CLASSIFIED FOR USE IN CLASS I, DIVISION 1, GROUPS A, B, C, D HAZARDOUS LOCATIONS. T4 (135°C) RATING.
The MicroFID II has been listed by Intertek, Inc., to comply with Underwriters Laboratories® Inc. UL® 913 Standard for Intrinsically Safe Apparatus and Associated Apparatus for use in Class I, Division 1, Groups A, B, C, D Hazardous (Classified) Locations.
MicroFID II Safety Label
NOTE: The MicroFID II and MicroFID II are based on the same platform and contain the same
components. The terms may be used interchangeably throughout this manual.
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WARNING
If there is any indication of physical damage to the MicroFID II after it has been dropped, the unit must be checked out by a service technician to ensure instrument integrity.
.
WARNING
Do not use any other accessories with the MicroFID II in a hazardous location
Substitution of components may affect the safety rating.
THE MicroFID II IS NOT INTENDED TO DETECT COMBUSTIBLE LEVELS OF GASES. THE MicroFID II IS CLASSIFIED FOR USE IN ATMOSPHERES CONTAINING COMBUSTIBLE LEVELS
OF GASES.
CAUTION
To reduce the risk of fire or injury to persons, read and follow these instructions:
1. All calibration, maintenance and servicing of this device, including battery charging, must be performed in a safe area away from hazardous locations. Disconnect all power before servicing.
2. There are no operator replaceable parts for the MicroFID II except the exhaust frit, and sample inlet filter.
3. There are no operator serviceable parts inside the MicroFID II.
WARNING
1. Do not dispose of the battery pack in a fire. The cells may explode. The battery pack must be disposed of properly. Check with local codes for possible special disposal instructions.
2. Do not open or mutilate the battery pack. If the MicroFID II is used in a manner not specified, the protection provided by the MicroFID II may be impaired.
3. Exercise care in handling battery packs in order not to short the terminals with conducting materials such as rings, bracelets and keys. The battery or conductor may overheat and cause burns.
4. Do not defeat proper polarity orientation between the battery pack and battery charger.
5. Charge the battery pack using the AC battery charger provided with or identified for use with this product only in accordance with the instructions and limitations specified in this manual. To charge the battery, use only the Universal Battery Charger Part No. A1201221. When using the battery charger, do not block access to the mains outlet in use with adapter. The
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AC battery charger is not to be used in a hazardous area.
WARNING
Do not open the MicroFID II housings to access the internal components. This action will invalidate the Intrinsic Safety rating for these products
WARNING
1. All calibration, maintenance and servicing of this device, including battery charging, must be
performed in a safe area away from hazardous locations.
2. Disconnect all power before servicing.
3. Do not open the MicroFID II exhaust frit when the unit is operating.
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DECLARATION OF CONFORMITY
This is to certify that this equipment, designed and manufactured by:
INFICON Inc.
Two Technology Place
East Syracuse, NY 13057
USA
meets the essential safety requirements of the European Union and is placed on the market accordingly. It has been constructed in accordance with good engineering practice in safety matters in force in the Community and does not endanger the safety of persons, domestic animals or property when properly installed and maintained and used in applications for which it was made.
In addition, this is to certify that this equipment has also been designed and manufactured, having regard to the state of the art, to ensure compliance with the Protection Requirements of EMC directive 2004/108/EC.
A Technical Documentation File is also available for review by competent authorities and will be maintained for a period of ten years after the date on which the equipment was last manufactured. In addition to this file, technical, installation, maintenance and application information concerning this equipment can also be found in the Operating Manual(s) for this product or product family.
Equipment Description: MicroFID II, MicroFID II, SiteFID. Applicable Directives: 2006/95/EC (LVD)
1999/5/EC (R&TTE / EMC) 2004/108/EC (General EMC)
2011/65/EC (RoHS)
Applicable Standards:
Safety: UL 913, Fifth Edition; Dated February 21, 1997; with Revisions through
and including February 24, 1997, UL Standard for Safety for Intrinsically
Safe Apparatus and Associated Apparatus for Use in Class I, II, and III, Division 1, Hazardous (Classified) Locations
ANSI/UL 1203-2006; Fourth Edition; Dated September 15, 2006,
UL Standard for Safety for Explosion-Proof and Dust-Ignition-Proof Electrical Equipment for Use in Hazardous (Classified) Locations
ANSI/UL 61010-1-2008; Second Edition; Dated July 12, 2004, (UL Standard for Safety for Electrical Equipment for Measurement, Control and Laboratory Use)
Emissions: EN 61326-1:2006: FCC 47 CFR Part 15 Subpart B
(Radiated & Conducted Emissions)
Class B: Emissions per Table 3 (EMC – Measurement, Control & Laboratory Equipment)
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Countries
Restrictions
France
Outdoor use limited to 10mW e.i.r.p. within the band 2454 to 2483.5 MHz.
Italy
If used outside of own premises, general authorization is required.
Luxembourg
General authorization is required for public service.
Romania
On a secondary basis. Individual license required.
Austria, Denmark, Finland, Germany, Greece, Iceland, Ireland, Liechtenstein, Luxembourg, The Netherlands, Norway, Portugal, Spain, Sweden, Switzerland, The United Kingdom
None
RoHS: INFICON hereby declares that the above mentioned products are
assigned to the classification of Category 9, Industrial Test and Measurement Equipment, it is exempt from the RoHS directive pursuant to Article 4, paragraph 4, section e), until 22 July 2017.
Immunity: EN 61000-4-5:1995+A1:1998+A2:2001 Electro Static Discharge (+4kV Contact discharge, + 8kV Air discharge) EN61000-4-4:2004
Radiated RF Susceptibility (80-270 MHz @ 3 V/m, 1kHz AM 80% Modulation)
Wireless Restrictions:
CE Implementation Date: May 15, 2012
Authorized Representative:
Name: Stephen Chabot Title: Vice President of Operations and Quality Done at East Syracuse, NY USA
On 13 August 2012
ANY QUESTIONS RELATIVE TO THIS DECLARATION OR TO THE SAFETY OF INFICON'S PRODUCTS SHOULD BE DIRECTED, IN WRITING, TO THE VICE-PRESIDENT OF OPERATIONS AT THE ABOVE ADDRESS.
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WARNING
A warning indicates an operation that could cause personal injury if
precautions are not followed.
CAUTION
A caution indicates an operation that could cause damage to the
instrument if precautions are not followed.
NOTE
A note indicates significant information.
1. INTRODUCTION
About this Manual
This manual provides detailed instructions for the setup, operation and maintenance of the MicroFID II Portable Flame Ionization Detector.
NOTE: The MicroFID II and MicroFID II are based on the same platform and contain the same components. The terms may be used interchangeably throughout this manual.
Before unpacking the instrument, please read the Warnings and Safety Practices. This section describes possible hazards that may injure the user, damage the instrument or compromise its operation. Some general safety information is also provided.
The MicroFID II manual uses a few conventions for key names on the keypad and for text that is shown on the display.
UPPERCASE Key names are denoted by uppercase text. An ARROW key is the
collective name for the UP ARROW and DOWN ARROW keys. “Display Text” Text that appears on the MicroFID II display is in quotation marks. <Angle Brackets> Computer keyboard names are denoted by angle brackets, e.g. <Ctrl>. FID Text that must be typed in using the computer keyboard is shown in
italics.
In the User Manual text various warnings and notes are displayed, including:
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WARNING
The MicroFID II only measures the concentration of airborne gases and
vapors that can be ionized by a flame ionization detector.
The MicroFID II automatically displays and can record the concentration
values.
The reading displayed represents the total concentration of all flame ionizable chemicals present in the sample. The MicroFID II can display concentration values in ppm and ppb.
WARNING
Do not expose the instrument to intense sunlight for prolonged periods.
Exposure to excessive heat may result in erroneous readings.
At low temperatures, water vapor, a by-product of the hydrogen flame, may
condense at the exhaust port. At sub-zero temperatures the water vapor
will freeze and obstruct the exhaust port. If the exhaust port becomes
obstructed, pump operation will be inhibited. Flame out may also result.
UNPACKING THE MicroFID II
The following accessories are included with your MicroFID II: MicroFID II Instrument CD Manual
70 Liter hydrogen cylinder MicroFID II Multi-Tool Universal Battery Charger with Line Cord Replacement Fluoropore Membrane Filters for Sample Inlet
Ensure all of these accessories have been included with the instrument. If any items are missing or damaged, contact INFICON immediately.
WARNINGS AND SAFETY PRACTICES
Please read this section before operating the MicroFID II. Throughout this manual notes are provided to inform you of the limitations of usage for the MicroFID II.
Intended Use
Excessive Heat and Cold
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Electrometer
Repeller Electrode
(Jet +75 Volts)
Collector Electrode
Sample In
Exhaust Out
Flame Arrestor
Flame Arrestor
Microprocessor
Combustion Chamber
Glow PlugThermocouple
Flame Ionization Detector Operation
The MicroFID II uses a flame ionization detector for the measurement of combustible organic compounds in air at parts-per million levels. The permanent air gases (argon, carbon dioxide, nitrogen, oxygen, water vapor, etc.) are not ionized by the flame.
When the MicroFID II is flamed on, the internal pump draws air in through the MicroFID II inlet. This sample air provides the oxygen necessary for combustion in the hydrogen fed flame.
Figure 1. Flame Ionization Detector
When the proper ratio of hydrogen to air is present in the combustion chamber, the flame is started automatically with a glow plug. A thermocouple is used to monitor the status of the flame.
When the sample passes through the flame, the combustible organic compounds in the sample will be ionized. After the compounds have been ionized by the flame, the ionized particles are subjected to a continuous electric field between the repeller electrode at the jet (+75V) and the collector electrode.
The ions move in the electric field, generating a current, which is proportional to the concentration of the ionized molecules in the ionization chamber. An electrometer circuit converts the current to a voltage that is then fed to the microprocessor.
After the sample passes through the flame and has become ionized, it is vented from the detector through a flame arrestor. The flame arrestor prevents the flame from igniting any flammable gases present in the sampling location.
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Display and
I/O Connector
Keypad
Microprocessor
Power
Supply
Electrical Connections
Sample Flow
Pump
Sample
In
Inlet
Filter
Flame Ionization
Detector
Detector
Out
Figure 2. Block Diagram
Detector Response
The MicroFID II is strictly an organic compound detector. It does not respond to inorganic compounds. The MicroFID II’s sensitivity is highly dependent on chemical structure and bonding characteristics. The combustion efficiency of a compound determines its sensitivity.
Simple saturated hydrocarbons (methane, ethane etc.) possess high combustion efficiencies and are among the compounds that produce the highest MicroFID II response. Organic fuels (acetylene, refined petroleum products), burn easily and are also extremely well detected.
The presence of substituted functional groups (amino, hydroxyl, halogens) on a simple hydrocarbon reduces its combustion efficiency and thus MicroFID II’s sensitivity to the compounds methanol and chloromethane, for example, are detectable with the MicroFID II but not as well as methane. A greater number of carbon atoms can offset this loss of sensitivity due to substitution. For example, the MicroFID II is more sensitive to n-butanol than it is to methanol.
NOTE: The FID Response Factors Technical Note is maintained on the INFICON web site:
www.inficon.com.
Support Equipment and Consumables
Compressed Gases
Cylinders of compressed gas, such as hydrogen and calibration gas, must be handled with extreme care. When using the calibration gas bag adapter, take care not to kink or stress the tubing. For safety, the hydrogen and calibration gas cylinders must be secured before use.
Please observe the following handling procedures: Do not mutilate cylinders. Do not expose the cylinders to direct sunlight. Do not heat the cylinders. The cylinders may rupture at high temperatures.
Use only the specified regulator for the calibration gas. Confirm regulator type and material with
your specialty gas supplier.
Use only the MicroFID II Hydrogen Filling Station for the hydrogen cylinder, Part No. A1201222.
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WARNING
Hydrogen gas is a fire and explosion hazard when exposed to heat or flame. The lower explosive limit (LEL) is 4%. The lower explosive limit is the minimum concentration of gas or vapor in air that will ignite in the presence of a source of heat or sparks.
Refer to the Material Safety Data Sheet (MSDS) before handling this gas. The MSDS will be provided by the gas supplier when the gas is ordered.
Always secure cylinders before removing the cylinder valve protection cap.
Do not drag or roll cylinders. Use a cylinder hand truck to move large cylinders. Wear safety glasses when working with compressed gases. Store cylinders in an upright position. Do not store cylinders in a hazardous location. Store cylinders away from possible sources of ignition.
Keep regulators and related equipment in the same gas service. Do not change service or adapt
equipment without consulting your gas supplier.
Refer to local shipping regulations for hydrogen supply cylinder shipping instructions.
Regulators for Compressed Gases
When connecting a regulator to a large cylinder: Ensure the cylinder valve and regulator connection match.
Ensure the regulator construction materials are compatible with the gas, and that the cylinder
pressure gauge will withstand the cylinder pressure.
Never use the regulator as a shut-off valve. Close the cylinder valve when it is not in use. Do not subject the regulator to an inlet pressure greater than recommended.
Do not move or detach the regulator when it is pressurized or when it is in use.
Before connection, ensure the gas cylinder valve and the regulator CGA connection are clean.
Turn the pressure control valve on the cylinder all the way out (close the cylinder). Turn the
regulator outlet to off. Open the gas cylinder valve slowly and check for leaks. Adjust the delivery
pressure and then open the regulator outlet valve.
Hydrogen Gas
The MicroFID II detector uses a hydrogen flame to ionize samples and produce Total Volatile Organic Compound (TVOC) readings. The quality and purity of the Hydrogen gas is very important to the accuracy of the detector.
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You must obtain a tank of hydrogen from which you can fill the internal cylinder. When ordering hydrogen, specify ultra-high purity hydrogen, 99.999% pure. This grade of hydrogen is also referred to as Grade 5 or Ultra zero grade. The hydrogen must have less than 0.1 ppm hydrocarbon contamination.
You can obtain the hydrogen in various size cylinders and pressures. Specify a tank with no more than 2400 psig (16547 kPa).
The hydrogen cylinder must also have CGA 350, male outlet.
The MicroFID II Hydrogen Filling Station Part No.A1201222 is required to fill the MicroFID II hydrogen fuel cylinder. You cannot fill the MicroFID II hydrogen cylinder without the MicroFID II hydrogen filling station.
Calibration Gas
Adequate ventilation must be provided when the MicroFID II is being calibrated. If compound threshold limit values (TLV) are exceeded, you should use a gas bag for sampling and
calibration. To determine the TLV of the compounds contained in the calibration gas, refer to the Material Safety Data
Sheet (MSDS) supplied with your calibration gas cylinder.
Oxygen Concentration Limits
A minimum of 17% oxygen is required to start the hydrogen flame. The oxygen is supplied from the sample as it is drawn in by the pump. A minimum of 10% oxygen is required to maintain the hydrogen flame. An oxygen deficiency will reduce the height of the flame or cause the flame to be extinguished and may affect the displayed reading.
If the MicroFID II is used in a highly contaminated area where it is possible that the oxygen content is below 10%, watch for indications of reduced flame height such as lowered detection limits or a flame out fault.
Flammable Gases
High concentrations of flammable gases (gases within their flammable range) can act as an additional fuel source. When this happens, the flame height may increase beyond the confines of the combustion chamber. The hydrogen supply will then be cut off and the flame will go out.
Flame out may also occur when the concentration of sample gas is so great that it causes an oxygen deficiency. This may occur when sampling enclosed or confined spaces where vapors and gases cannot escape. Watch for indications of increased flame height such as erratic readings or sudden high concentrations followed by a flame out fault.
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WARNING
The MicroFID II is not classified for use in hazardous locations with non­intrinsically safe rated computers.
ACCESSORIES
Computer
The MicroFID II will send information stored in its logged memory or will continuously stream data to a computer or PDA via Bluetooth wireless communication. This feature may be used if you need to prepare reports based on the MicroFID II recorded data.
Information prepared on a PC such as “routing or tag information” may be uploaded to the MicroFID II via Bluetooth as well.
Gas Sampling Bag
A gas sampling bag can be used for calibration of the MicroFID II. If you are unsure of the quality of ambient air you should use an additional gas bag filled with zero air. Connect the sample bag to the inlet fitting with the gas bag adapter. See Calibration section for more information.
One sampling bag is included in the MicroFID II calibration kit Part No. MX396011. Additional gas bags are also available (Part No. MX396017).
Charcoal Filters
A charcoal filter (Part No.MX396022, package of 10) may be connected to the MicroFID II during calibration and sampling to provide clean air to the MicroFID II. The filter will remove hydrocarbon contamination from room air to provide zero grade air to the MicroFID II.
NOTE: The charcoal filter does not filter methane or ethane. If these compounds are present, you should use a gas bag with a supply of commercial zero air for calibration purposes.
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1/4" Nut
Connect
to MicroFID
Charcoal Filter
Front Ferrule
Back Ferrule
To connect a charcoal filter:
1. Load the Teflon ferrules into the nut. The nut and ferrules are supplied with the filter. See
Figure 3.
2. Connect the nut to the MicroFID II inlet. Do not tighten the nut.
CAUTION: Over-tightening the Teflon ferrules will result in damage to the ferrules.
3. Remove the charcoal filter from its plastic bag and insert it into the nut. Finger-tighten the nut
onto the inlet. If the filter is not secure, ensure you have inserted the tube stub far enough into
nut. Do not over-tighten the fitting.
Figure 3 Connecting the Charcoal Filter
The charcoal filter will remove hydrocarbon contaminants for up to 4000 ppm hours. This means that the filter will be good for 1 hour removing 4000 ppm of hydrocarbon contaminants or will last for 4 hours removing 1000 ppm. The exact time will be determined by the operating environment. You will notice an increased hydrocarbon background when the filter requires replacement.
To replace the charcoal filter:
1. Loosen the nut on the MicroFID II inlet.
2. Remove the used filter.
3. Insert the new charcoal filter into the nut and finger-tighten the nut onto the inlet. Do not over-
tighten the fitting.
4. When the charcoal filter is not in use, place it in its plastic bag and store it in a clean, dry place.
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Hydrogen Fuel Cylinder Retention Plate
Handle
Inlet
On/Off Switch
AC Charging Connector Cap
Digital Display and Soft Keys
Hydrogen Fuel Cylinder
Alarm Speaker
Exhaust Frit
2. USING THE MicroFID II
MicroFID II Feature Layout
The photograph below shows the basic layout of the MicroFID II Version components. The MicroFID II is also supplied with an optional telescoping probe that can be removed from its holder for access to hard to reach spaces.
NOTE: The cover must be attached for the MicroFID II to operate and to maintain the intrinsic safety rating.
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MicroFID II with probe in probe holder position
MicroFID II with probe in telescoping position
Using the MicroFID II Battery Charger
READ THESE INSTRUCTIONS BEFORE USING THE CHARGER
The MicroFID II battery charger is only designed for indoor use and should not come into contact with water or dust. In order to avoid overheating, the charger should not be covered when it is in use.
The charger is turned on by connecting it to the mains socket. Disconnecting it from the mains socket turns the charger off. If
the charger is equipped with a mains cord, verify that the cord has not been damaged. If the cord is damaged, the charger must not be used.
The charger contains dangerous voltages and the cover should not be removed.
CHARGER FUNCTIONALITY
This charger is a fast charger for NiMH batteries. The charger will automatically charge the battery at a fast rate, and then charge to a slow rate near the end of the cycle. This prevents over-charging.
CAUTION: Do not charge batteries at too high or too low temperatures. Charge only in areas between 38-110°F (3-43°C).
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LED
MODE
Orange
Battery not connected
Orange
Battery initialization & analysis
Red
Fast Charge
Green with intermittent orange flash
Top-off charge
Green
Trickle charge
Alternating red-green
Error
HOW TO USE THE CHARGER
The Charger is started by connecting the battery pack to the charger. Once connected, the indicator LED will start Orange, for the Initialization and Analysis Phase, before switching to Red for the Fast Charge Phase. When the batteries are fully charged, the charger will go into a top-off charge mode before it goes over to trickle charge mode. During top-off charge, the LED will be Green with short intermittent Orange light. When the top-off charge is completed, the charger will go into trickle charge mode and the LED will be Green. The charge current is now reduced to a safe level, which allows the charger to stay connected to the NiMH batteries without damaging the battery. If the battery voltage is far below normal, the charger
will cut off the fast charge current and go to trickle charge mode. The LED will then indicate ‘error’ by
flickering Green and Red light. If the mains is turned off, the charger will reset and start a new charge cycle if the mains is turned on again. If new batteries are to be connected, the charger must idle for approximately 15 seconds to make sure all parameters in the microprocessor have been reset. The LED changing to Orange light shows this and a new charge cycle can begin.
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CHARGE CYCLE AND LED INDICATIONS
With mains connected, the LED will be orange the first 5-7 seconds, and will be orange when the initialization and analysis starts. If a battery is connected, the actual charging will start a few seconds later when the LED changes to red.
CAUTION: Use only Battery Charger P/N 1201221 to charge the MicroFID II.
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Table 1. Battery Charger Indications
To Charge the Battery
1. To charge the MicroFID II battery, unscrew the cover for the charging connector cap.
2. Connect the charge adapter to the MicroFID II charging connector.
3. When the battery charge indicates there is a full charge to the battery, disconnect the charge adapter from the MicroFID II charging connector
4. Install the charging connector cap to the charging connector.
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NOTE: The MicroFID II will not operate without the charging connector cap in place. NOTE: The MicroFID II will not operate with the AC Adapter plugged into the MicroFID II.
Repeat Charging with an AC Charger
If the AC charger has been plugged into an electrical outlet and has been used to charge a FID, and another charging operation is to be performed, please remove the charger from the unit and wait until the status LED on the charger changes from either green or red to orange before plugging it into the second unit.
NOTE: The status change will take up to 15 seconds and the orange LED indicates that the unit is ready to start a new charge cycle.
CAUTION: If the AC charger is not properly reset according to the above instructions, it is possible that the AC charger will remain in trickle charge mode and the FID battery will not
receive a full charge. This will limit the FID’s operating time and may cause problems in lighting
the FID flame due to low voltage.
Filling the Hydrogen Fuel Cylinder
The MicroFID II hydrogen fuel cylinder is a metal hydride design that requires relatively low hydrogen pressure to fill it.
Figure 7. MicroFID II Hydrogen Cylinder
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WARNING
Hydrogen storage on the metal oxide is an Exothermic Reaction. The cylinder may become hot during the initial fill. Care must be taken to avoid injury.
WARNING
DO NOT attempt to fill the hydrogen cylinder without a refill adapter..
The hydrogen fuel cylinder (see Figure 7), when full, will provide the MicroFID II with up to 70 hours of continuous operation in a single fill. To fill the hydrogen fuel cylinder, the MicroFID II hydrogen filling station Part No. A1201222 is required (see Figure 8). The hydrogen fill station is outfitted with a CGA 350 adaptor for use with a high pressure hydrogen cylinder that contains at least 99.999% pure grade hydrogen (also known as ultra high purity hydrogen).
CAUTION: H2S, SO2, Cl2, and CO are contaminating substances for the cylinder alloy. Do not expose the cylinder interior to these substances.
CAUTION: Lower grades of hydrogen will damage the fuel cell with impurities and decrease the overall longevity of the fuel cell. Ensure the hydrogen is ultra high purity.
CAUTION: Do not modify or alter the hydrogen cylinder or fittings.
The Hydrogen Filling Station (Part No.A1201222) consists of an adapter fitting with a left-handed thread for cylinder attachment, an output valve and a hydrogen fuel cylinder quick connect. The Hydrogen Filling Station delivers a fixed 260 psi to the hydrogen fuel cylinder. The output valve is positioned to deliver gas from the cylinder to the hydrogen fuel cylinder. Additionally, in the final stages of filling the hydrogen fuel cylinder, the output valve is used to release gas held in the quick connect after filling.
The MicroFID II Hydrogen Fuel Cylinder is composed of metal hydride material. The process of filling this cylinder involves the low pressure adsorption of hydrogen on the metal hydride surface, rather than the high pressure filling process for conventional hydrogen cylinders. Table 2 illustrates the charge time versus fill time for the MicroFID II hydrogen cylinder.
A 5 minute charge provides 10 hours of usage. Other charge times versus usage are as follows:
5 minutes 10 hours of use 10 minutes 30 hours of use 30 minutes 50 hours of use 60 minutes 65 hours of use
The hydrogen fuel cylinder is over 85% full after one hour. Thereafter, the cylinder charges more slowly up to the full 70+ hours.
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WARNING
Use only the MicroFID II Hydrogen Fill Station p/n A1201222 to fill the hydrogen cylinder. Use of any other filling device will void the warranty.
WARNING
The regulator pressure is set at the factory Do not adjust the regulator on the hydrogen filling station. Adjustment of the hydrogen filling station regulator will void the warranty.
WARNING
Do not exceed 260 psi when filling the MicroFID II Hydrogen Cylinder. The fuel cells in the hydrogen cylinder will be damaged and will void the warranty.
MicroFID II Hydrogen Cylinder Charge Chart
Table 2. Charging Time and Usage Time
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