INFICON HAPSITE ER Chemical Identification System User Manual

Name: INFICON HAPSITE ER Chemical Identification System
Brand: INFICON
SKU: 1596256
Rating: 4 (2 reviews)

4 (2)

O P E R A T I N G M A N U A L

HAPSITE® ER

Chemical Identification System

IPN 074-471-P1B

O P E R A T I N G M A N U A L

HAPSITE® ER

Chemical Identification System

IPN 074-471-P1B

www.inficon.com reachus@inficon.com

Trademarks

The trademarks of the products mentioned in this manual are held by the companies that produce them.

ConFlat® is a registered trademark of Varian, Inc.

Dell™ is a trademark of Dell Inc.

ER IQ™, SituProbe™, INFICON® and HAPSITE® are trademarks of INFICON.

Loctite® is a registered trademark of Henkel Technologies.

LEMO® is a registered trademark of LEMO SA.

MicroDuster® is a registered trademark of Acctech LLC.

Microsoft®, Windows® and Excel® are either registered trademarks or trademarks of Microsoft Corporation in the United States and/or other countries

PEEK™ is a trademarks of Victrex plc.

Swagelok® is a registered trademark of Swagelok Co.

Tedlar®, DuPont™, and Vespel® are trademarks of E. I. du Pont de Nemours and Company or its affiliate

Viton® is a registered trademark of DuPont Performance Elastomers

All other brand and product names are trademarks or registered trademarks of their respective companies.

The HAPSITE ER runs a Linux® Operating System. The source code for the Operating System is available from INFICON by request for a nominal operating fee.

Linux® is the registered trademark of Linus Torvalds in the U.S. and other countries.

Disclaimer

The information contained in this manual is believed to be accurate and reliable. However, INFICON assumes no responsibility for its use and shall not be liable for any special, incidental, or consequential damages related to the use of this product.

Due to our continuing program of product improvements, specifications are subject to change without notice.

Reproduction or adaptation of any part of this document without permission is unlawful.

DECLARATION

CONFORMITY

This is to certify that this equipment, designed and manufactured by:

INFICON Inc.

Two Technology Place

East Syracuse, NY 13057

USA

meets the essential safety requirements of the European Union and is placedon the market accordingly. It has been constructed in accordance with good engineering practice in safety matters in force in the Community and does not endanger the safety of persons, domestic animals or property when properly installed and maintained and used in applications for which it was made.

In addition, this is to certify that this equipment has also been designed and manufactured, having regard to the state of the art, to ensure complies with the Protection Requirements of EMC directive 2004/108/EC.

A Technical Documentation File is also available for review by competent authorities and will be maintained for a period of ten years after the date whichon the equipment was last manufactured. In additional to this file, technical, installation, maintenance and application information concerning this equipment can also be found in the Operating Manual(s) for this product or product family.

Equipment Description: HAPSITE ER Portable GC/MS with wireless communications, including the HAPSITE Service Module, NEG Pump, Battery and AC to DC HAPSITE Adapter, Headspace Accessory, Situ-Probe Accessory, and SPME Accessory.

Applicable Directives:	2006/95/EC	(LVD)
	1999/5/EC (R&TTE / EMC)
	(The required compliance statement concerning this directive can be found in
	Chapter 4 of this manual.)
	2004/108/EC	(General	EMC)

2002/95/EC (RoHS)

Applicable Standards:
Safety:	EN	61010-1:2001
Emissions:	ETSI EN 300 328-2 V1.4.1: 2003 (R&TTE Emissions)
	(ERM for equipment operating in the 2.4 GHz ISM band)

ETSI EN 301 489-17 V1.2.1: 2002 (Flicker & Harmonics) (ERM - Specific conditions for 2.4 GHz)

EN 61326:2006 (Radiated & Conducted Emissions) Class A: Emissions per Table 3

(EMC – Measurement, Control & Laboratory Equipment)

Immunity:	EN	61326:2006
	(EMC – Measurement, Control & Laboratory Equipment)
	Class A: Immunity per Table A.1
	ETSI EN 301 489-17 V1.2.1: 2002 (General EMI)
	(ERM - EMC - Specific conditions for 2.4 GHz)
RoHS:	Due to the classification of this product it is currently exempt from the RoHS
	directive.

Wireless Restrictions:

	Countries		Restrictions

	France		Outdoor use limited to 10mW e.i.r.p. within the band
			2454 to 2483.5 MHz.
	Italy		If used outside of own premises, general
			authorization is required.
	Luxembourg		General authorization is required for public service.
	Romania		On a secondary basis. Individual license required.
	Austria, Denmark, Finland,		None
	Germany, Greece, Iceland,
	Ireland, Liechtenstein,
	Luxembourg, The Netherlands,
	Norway, Portugal, Spain,
	Sweden, Switzerland, The
	United Kingdom
CE Implementation Date:		July 18, 2008
Amended:		June15, 2009 (Includes Accessories)
Authorized Representative:		Jerry	Wander	Chabot	Stephen

Business Line Manager, ISS		Vice-President, Operations
INFICON	Inc.	Inc INFICON,

ANY QUESTIONS RELATIVE TO THIS DECLARATION OR TO TH E SAFETY OF INFICON'S PRODUCTS SHOULD BE DIRECTED, IN WRITING, TO THE VICE-PRESIDENT OF OPERATIONS AT THE ABOVE ADDRESS.

Revised 11/04/08 (Rev C)

DECLARATION

CONFORMITY

This is to certify that this equipment, designed and manufactured by:

INFICON Inc.

Two Technology Place

East Syracuse, NY 13057

USA

Equipment Description:	SituProbe
	(when used with the HAPSITE Smart Portable GC/MS System)
Applicable Directives:	2006/95/EC	(LVD)
	2004/108/EC	(General	EMC)

2002/95/EC (RoHS)

Applicable Standards:
Safety:	EN	61010-1:2001
Emissions:	EN 61326-1:1997/A1: 1998/A2: 2001 (Radiated & Conducted Emissions)
	Class A: Emissions per Table 3
	(EMC – Measurement, Control & Laboratory Equipment)
Immunity:	EN 61326-1:1997/A1: 1998/A2: 2001 (General EMC)
	Class A: Immunity per Table A.1
	(EMC – Measurement, Control & Laboratory Equipment)
RoHS:	Due to the classification of this product it is currently exempt from the RoHS
	directive.

CE Implementation Date:

March 31, 2006

Authorized Representative: Duane H. Wright

Operations Quality Manager, ISS

INFICON Inc.

ANY QUESTIONS RELATIVE TO THIS DECLARATION OR TO TH E SAFETY OF INFICON'S PRODUCTS SHOULD BE DIRECTED, IN WRITING, TO THE VICE-PRESIDENT OF OPERATIONS AT THE ABOVE ADDRESS.

Revised 11/04/08 (Rev C)

DECLARATION

CONFORMITY

This is to certify that this equipment, designed and manufactured by:

INFICON Inc.

Two Technology Place

East Syracuse, NY 13057

USA

Equipment Description:	Headspace
	(when used with the HAPSITE Smart Portable GC/MS System)
Applicable Directives:	2006/95/EC	(LVD)
	2004/108/EC	(General	EMC)

2002/95/EC (RoHS)

Applicable Standards:
Safety:	EN	61010-1:2001
Emissions:	EN 61326-1:1997/A1: 1998/A2: 2001 (Radiated & Conducted Emissions)
	Class A: Emissions per Table 3
	(EMC – Measurement, Control & Laboratory Equipment)
Immunity:	EN 61326-1:1997/A1: 1998/A2: 2001 (General EMC)
	Class A: Immunity per Table A.1
	(EMC – Measurement, Control & Laboratory Equipment)
RoHS:	Due to the classification of this product it is currently exempt from the RoHS
	directive.

CE Implementation Date:

October 2004

Authorized Representative: Duane H. Wright

Operations Quality Manager, ISS

INFICON Inc.

ANY QUESTIONS RELATIVE TO THIS DECLARATION OR TO TH E SAFETY OF INFICON'S PRODUCTS SHOULD BE DIRECTED, IN WRITING, TO THE VICE-PRESIDENT OF OPERATIONS AT THE ABOVE ADDRESS.

Revised 11/04/08 (Rev B)

Warranty

WARRANTY AND LIABILITY - LIMITATION: Seller warrants the products manufactured by it, or by an affiliated company and sold by it, and described on the reverse hereof, to be, for the period of warranty coverage specified below, free from defects of materials or workmanship under normal proper use and service. The period of warranty coverage is specified for the respective products in the respective Seller instruction manuals for those products but shall not be less than two (2) years from the date of shipment thereof by Seller. Seller's liability under this warranty is limited to such of the above products or parts thereof as are returned, transportation prepaid, to Seller's plant, not later than thirty (30) days after the expiration of the period of warranty coverage in respect thereof and are found by Seller's examination to have failed to function properly because of defective workmanship or materials and not because of improper installation or misuse and is limited to, at Seller's election, either (a) repairing and returning the product or part thereof, or (b) furnishing a replacement product or part thereof, transportation prepaid by Seller in either case. In the event Buyer discovers or learns that a product does not conform to warranty, Buyer shall immediately notify Seller in writing of such non-conformity, specifying in reasonable detail the nature of such non-conformity. If Seller is not provided with such written notification, Seller shall not be liable for any further damages which could have been avoided if Seller had been provided with immediate written notification.

THIS WARRANTY IS MADE AND ACCEPTED IN LIEU OF ALL OTHER WARRANTIES, EXPRESS OR IMPLIED, WHETHER OF MERCHANTABILITY OR OF FITNESS FOR A PARTICULAR PURPOSE OR OTHERWISE, AS BUYER'S EXCLUSIVE REMEDY FOR ANY DEFECTS IN THE PRODUCTS TO BE SOLD HEREUNDER. All other obligations and liabilities of Seller, whether in contract or tort (including negligence) or otherwise, are expressly EXCLUDED. In no event shall Seller be liable for any costs, expenses or damages, whether direct or indirect, special, incidental, consequential, or other, on any claim of any defective product, in excess of the price paid by Buyer for the product plus return transportation charges prepaid.

No warranty is made by Seller of any Seller product which has been installed, used or operated contrary to Seller's written instruction manual or which has been subjected to misuse, negligence or accident or has been repaired or altered by anyone other than Seller or which has been used in a manner or for a purpose for which the Seller product was not designed nor against any defects due to plans or instructions supplied to Seller by or for Buyer.

This manual is intended for private use by INFICON® Inc. and its customers. Contact INFICON before reproducing its contents.

NOTE: These instructions do not provide for every contingency that may arise in connection with the installation, operation or maintenance of this equipment. Should you require further assistance, please contact INFICON.

www.inficon.com reachus@inficon.com

IPN 074-471-P1B

HAPSITE ER Operating Manual

Definition of

Note, Hint, Danger, Warning and Caution Paragraphs

NOTE: This is a note paragraph. Notes provide additional information about the current topic.

HINT: This is a hint paragraph. Hints provide insight into product usage

DANGER

This is a Danger paragraph. Failure to heed these messages has a high likelihood of resulting in serious personal injury or even death!

WARNING

This is a Warning paragraph. It warns of actions that may cause physical injury.

WARNING - Risk Of Electric Shock

This Warning paragraph warns of the presence of electrical voltages which may cause physical injury.

CAUTION

This is a Caution paragraph. It cautions against actions which may damage the instrument or lead to the loss of data.

HAPSITE ER Operating Manual

Operating Manual Style Conventions

The following information describes the conventions used throughout this manual.

When holding down a key and then pressing another key, this is expressed as (for example) Press Ctrl+C

It is assumed that the floppy drive used is drive a. If using another drive, substitute the floppy drive letter being used for “a:”.

It is assumed that the hard drive used is drive c. If using another drive, substitute the hard drive letter being used for “c:”.

Left-click means to press and release the left mouse button (LMB) and right-click means to press and release the right mouse button (RMB).

The HAPSITE software operates in the Windows environment using the Windows® Graphical User Interface (GUI). Actions in the HAPSITE software GUI that are common to the Windows GUI are not explained in detail in this manual. Refer to the Windows documentation supplied by Microsoft®.

IPN 074-471-P1B

HAPSITE ER Operating Manual

Trademarks

Definition of Note, Hint, Danger, Warning and Caution Paragraphs Operating Manual Style Conventions

Chapter 1

Introduction

1.1 The HAPSITE ER System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-1 1.2 Performance Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-2 1.3 Serial Number Location . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-2 1.4 Theory of Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-3 1.5 Instrument Overview. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-4 1.6 Description Of Subsystems . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-4

1.6.1 Gas Chromatograph . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-4 1.6.1.1 Membrane Isolation Valve . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-6 1.6.2 Mass Spectrometer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-6 1.6.3 Vacuum System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-8 1.6.4 Electronic Systems . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-9 1.6.4.1 Mass Spectrometer Control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-9 1.6.4.2 Gas Chromatograph Control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-9 1.6.4.3 Main Processor. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-9 1.6.4.4 Interfaces . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-9 1.6.5 Software Systems. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-10

Chapter 2

HAPSITE Components and Assemblies

2.1 Ship Kit Packing Lists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-1 2.1.1 930-850-G9, G12 Ship Kit Contents. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-1 2.1.2 930-850-G10, G11 Ship Kit Contents. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-3 2.1.3 Ship Kits Box 3 and 4 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-5 2.2 Basic Assembly . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-5 2.2.1 Attaching the Probe . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-6 2.2.2 Installing the Gas Canisters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-7 2.2.2.1 How to Change or Remove a Gas Canister . . . . . . . . . . . . . . . . . . . . . . . . . 2-8 2.2.3 Install Battery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-9 2.2.4 Connect the AC To DC Power Converter Power Supply . . . . . . . . . . . . . . . 2-9 2.2.5 Connect Laptop (if desired) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-10 2.2.5.1 Connect Laptop with Black Crossover Cable . . . . . . . . . . . . . . . . . . . . . . . 2-10 2.2.5.2 Connect Laptop with Wireless Connection. . . . . . . . . . . . . . . . . . . . . . . . . 2-10

TOC - 1

HAPSITE ER Operating Manual

2.3 Helpful Guidelines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-11 2.4 HAPSITE Configurations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-12 2.5 Headspace Sampling System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-12 2.5.1 Headspace Sampling System - Components Received. . . . . . . . . . . . . . . 2-12 2.5.2 Installing the Headspace Sampling System . . . . . . . . . . . . . . . . . . . . . . . . 2-13 2.6 Service Module. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-17 2.6.1 Setting Up the Service Module. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-17 2.6.2 Placing the HAPSITE on the Service Module . . . . . . . . . . . . . . . . . . . . . . 2-21 2.6.3 Detaching the HAPSITE from the Service Module. . . . . . . . . . . . . . . . . . . 2-24 2.7 SituProbe . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-24 2.7.1 Installing the Tri-Bed or Tenax Concentrator . . . . . . . . . . . . . . . . . . . . . . . 2-27 2.7.2 Removing the Concentrator . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-32 2.8 Probe Sampling Options and Attachments . . . . . . . . . . . . . . . . . . . . . . . . 2-33 2.8.1 Probe Nut Assembly. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-33 2.8.2 Attaching a Bag Sample. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-34 2.8.3 VX / R-33 Conversion Tube . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-35 2.8.3.1 VX/R-33 Conversion Tube Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-35 2.8.3.2 VX-G Conversion Tube Removal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-36 2.9 Batteries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-37 2.9.1 How to Remove a Battery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-37 2.9.2 Battery Charger . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-38 2.9.2.1 Battery Charger Components. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-39 2.9.2.2 Battery Charger Connections and Startup . . . . . . . . . . . . . . . . . . . . . . . . . 2-39 2.9.2.3 Loading the Battery Charger . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-39 2.9.2.4 Understanding the Battery Charger Indicators . . . . . . . . . . . . . . . . . . . . . . 2-39 2.10 Portable Accessories . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-41 2.10.1 HAPSITE and Headspace Sampling System Strap . . . . . . . . . . . . . . . . . . 2-41 2.10.2 HAPSITE Backpack . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-42

2.10.2.1 Adjustment of the Backpack. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-42 2.10.2.2 Care of the Backpack . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-43 2.11 Hot Swap Cable (IPN 930-246-G1) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-43 2.11.1 Connecting the Hot Swap Cable . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-43 2.11.2 Storing the Hot Swap Cable . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-45 2.11.3 Use as an Additional Battery Source . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-45

IPN 074-471-P1B

TOC - 2

IPN 074-471-P1B

HAPSITE ER Operating Manual

Chapter 3

Operating HAPSITE in Portable Mode

3.1 Starting the HAPSITE in Portable Mode. . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-1 3.1.1 Emergency Mode (EMER MODE) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-6 3.1.2 Concentrator Options (CONC OPTIONS) . . . . . . . . . . . . . . . . . . . . . . . . . . 3-8 3.1.2.1 Concentrator Cleanout . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-8 3.1.2.2 Skip Cleanout . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-10 3.1.3 Concentrator Cleanout Failure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-11 3.1.4 Quick Reference SOP - Heat-up and Tune . . . . . . . . . . . . . . . . . . . . . . . . 3-12 3.2 Selecting a Different Method Using the SELECT METHOD Icon. . . . . . . . 3-13 3.2.1 Changing the Default Method. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-16 3.2.2 Show All . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-17 3.3 Survey Mode . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-17 3.3.1 Quick Reference SOP — Survey Method . . . . . . . . . . . . . . . . . . . . . . . . . 3-24 3.4 ANALYZE (GC/MS) Mode with the Concentrator. . . . . . . . . . . . . . . . . . . . 3-25 3.4.1 The TriBed Concentrator . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-25 3.4.2 The Tenax Concentrator. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-25 3.4.3 Procedure for Running Concentrator Methods. . . . . . . . . . . . . . . . . . . . . . 3-25 3.4.4 Quick Reference SOP —Concentrator Methods . . . . . . . . . . . . . . . . . . . . 3-30 3.5 Detecting Hazardous Chemicals . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-31 3.5.1 View Results/View Reports . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-32 3.6 The Help Icon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-41 3.7 The Info Icon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-42 3.7.1 HAPSITE Icon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-49 3.7.1.1 Battery Icon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-50 3.7.1.2 Carrier Gas Icon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-50 3.7.1.3 Internal Standard Icon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-51 3.7.1.4 HEATERS Icon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-51

3.7.1.4.1 HEATERS Icon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-52 3.7.1.4.2 NEG Button . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-52 3.7.1.4.3 CONC Button . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-53 3.7.1.5 TUNE STATUS Icon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-54 3.7.1.5.1 TUNE REPORTS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-55 3.7.1.6 GPS Icon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-56 3.7.1.7 HAPSITE SYSTEM Icon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-56 3.7.1.7.1 HAPS Button . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-57 3.7.1.7.2 FIRMWARE Button. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-57 3.7.1.7.3 DATE TIME Button . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-58 3.7.1.7.4 NET Button . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-58

TOC - 3

HAPSITE ER Operating Manual

3.7.2 Attachments . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-58

3.8 EXIT Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-59

3.8.1 Extended Standby . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-61

3.8.1.1 End Standby. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-64

3.9Analyze (GC/MS) Mode with Headspace Sampling

System in Portable Mode . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-65

3.9.1Quick Reference SOP —

GC/MS Mode with HSS in Portable Mode . . . . . . . . . . . . . . . . . . . . . . . . . 3-70 3.10 SituProbe . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-71 3.10.1 Procedure for SituProbe Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-71

3.10.2Quick Reference SOP —

GC/MS Mode with SituProbe in Portable Mode . . . . . . . . . . . . . . . . . . . . . 3-75

Chapter 4

Wireless and Touch Screen Options

4.1 Wireless Option . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-1 4.1.1 Introduction. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-1 4.1.2 Regulatory Compliance Information for UNITED STATES Users . . . . . . . . 4-1 4.1.2.1 FCC Statement. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-2 4.1.2.2 FCC RF Exposure Statement. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-2 4.1.3 Regulatory Compliance Information for CANADIAN Users . . . . . . . . . . . . . 4-3 4.1.3.1 Industry Canada (IC) Notices . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-3 4.1.4 Regulatory Compliance Information for EUROPEAN Users . . . . . . . . . . . . 4-4 4.1.4.1 European Usage Restrictions. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-4 4.1.4.2 European EMC Compliance Statement . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-5 4.1.4.3 European Safety Compliance Statement . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-6 4.1.5 Wireless Range . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-7 4.1.6 Turning On the Radio . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-7 4.1.7 Establishing Communication . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-8 4.1.7.1 Setting the User Access Level . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-9 4.1.7.2 Setting Up ER IQ for Communication with the HAPSITE. . . . . . . . . . . . . . . 4-9 4.1.8 Wireless Module Indicator Lights . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-10 4.1.9 Turning Off the Radio . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-10 4.2 The MAIN Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-12 4.2.1 Smart Interface. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-12 4.2.2 Adjust Brightness . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-14 4.3 Touch Screen Options . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-17 4.3.1 Calibrating The Touch Screen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-17 4.3.2 Enabling/ Disabling the Touch Screen . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-20 4.3.2.1 Disabling the Touch Screen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-20 4.3.2.2 Enabling the Touch Screen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-22

TOC - 4

IPN 074-471-P1B

HAPSITE ER Operating Manual

4.4 The USB Drive . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-23 4.4.1 Copying Files to the USB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-23 4.4.2 Copying Files From the USB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-27 4.4.3 Updating the Front Panel Software from the USB . . . . . . . . . . . . . . . . . . . 4-30 4.4.4 Retrieving Files from the USB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-33

Chapter 5

Operating HAPSITE in Laptop Mode

5.1 Starting the HAPSITE in Laptop Mode . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-1 5.2 Survey Mode . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-2 5.2.1 Quick Reference SOP — Running Survey Mode . . . . . . . . . . . . . . . . . . . . . 5-6 5.3 Selecting a New Method. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-7 5.4 Analyze (GC/MS) Mode with Concentrator . . . . . . . . . . . . . . . . . . . . . . . . 5-10 5.4.1 The TriBed Concentrator . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-10 5.4.2 The Tenax Concentrator. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-10 5.4.3 Quick Reference SOP — Tri-Bed Concentrator Method . . . . . . . . . . . . . . 5-14 5.5 Analyze (GC/MS) Mode with Headspace Sampling System . . . . . . . . . . . 5-15 5.5.1 Quick Reference SOP — GC/MS Mode with HSS . . . . . . . . . . . . . . . . . . . 5-19 5.6 SituProbe Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-20 5.6.1 Procedure for SituProbe Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-20 5.6.2 Quick Reference SOP — Analyze Mode with SituProbe . . . . . . . . . . . . . . 5-23 5.7 Front Panel Emulator . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-24

Chapter 6

Methods

6.1 Introduction to Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-1 6.1.1 Sensitivity . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-1 6.1.2 Survey Method . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-1 6.1.3 Building a Survey Method Library File . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-3 6.1.3.1 Creating Survey Methods for Target Compounds . . . . . . . . . . . . . . . . . . . . 6-3 6.1.3.2 Building a Survey Target Compound Library . . . . . . . . . . . . . . . . . . . . . . . . 6-3 6.2 Analyze (GC/MS) Methods. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-7

6.2.1Building an Analyze (GC/MS) Method and

Target Compound Library File . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-8

Chapter 7

Tune

7.1 Introduction to AutoTune and Manual Tune . . . . . . . . . . . . . . . . . . . . . . . . . 7-1 7.2 AutoTune . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-2

7.2.1Starting AutoTune from the Manual Tune Screen

on the Laptop Computer. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-3 7.3 Viewing a Tune Report . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-4 7.4 AutoTune Failure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-6

TOC - 5

HAPSITE ER Operating Manual

7.5 Manual Tune Settings and Controls . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-9 7.5.1 Tool Bar . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-10 7.5.2 Tune Drop Down Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-11 7.5.2.1 Tune Properties Window . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-12 7.5.3 Tune Control Panel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-14 7.5.3.1 Tune Parameters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-15 7.5.4 Peak Scan Window . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-16 7.5.4.1 Peak Scan Window Controls . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-17 7.5.5 Full Scan Window. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-18 7.5.6 Tune and Mass Calibration Status . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-19 7.5.7 Mass Calibration Status . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-21 7.5.8 Right Mouse Button (RMB) Menus. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-23 7.5.8.1 RMB in Scan Window. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-23 7.5.8.2 RMB in Tune Status Window . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-24 7.5.8.3 RMB on Y Axis . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-24 7.6 Performing Manual Tune . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-25 7.6.1 Adjusting Base Peak Gain . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-25 7.6.2 Adjusting Resolution. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-29 7.6.3 Adjusting the Ion Energy . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-30

Chapter 8

ER IQ Software

8.1 The HAPSITE Software - ER IQ. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-1 8.2 Computer System Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-2

8.3Installing and Updating the HAPSITE

Analytical Module Software . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-2 8.3.1 Updating the HAPSITE Analytical Module Software . . . . . . . . . . . . . . . . . . 8-2 8.4 Reloading Default HAPSITE Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-3 8.4.1 Locating Default Methods. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-3 8.4.2 Loading a Default Method to the HAPSITE . . . . . . . . . . . . . . . . . . . . . . . . . 8-5

8.5Establishing Communications between the

HAPSITE and Laptop Computer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-8 8.5.1 Setting Up Communications. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-8 8.5.2 Configuring the HAPSITE for Communications . . . . . . . . . . . . . . . . . . . . . 8-10 8.5.3 Establishing Communication with the Service Module. . . . . . . . . . . . . . . . 8-14

8.6Establishing Communications between the

HAPSITE and Laptop Computer Using the Wireless Connection . . . . . . . 8-16 8.7 Setting the HAPSITE Time Zone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-16 8.8 Access Levels . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-17 8.8.1 Changing Access Levels . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-18 8.8.2 Setting or Changing the Access Level Password. . . . . . . . . . . . . . . . . . . . 8-19

TOC - 6

IPN 074-471-P1B

HAPSITE ER Operating Manual

8.9 ER IQ Controls . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-20 8.9.1 System Setup Main Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-20 8.9.1.1 File . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-21 8.9.1.2 Functions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-21 8.9.1.3 System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-21 8.9.1.4 Tools Menu. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-21 8.9.1.5 View Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-22 8.9.1.6 Window Menu. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-22 8.9.1.7 Help Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-22 8.10 Software Versions for the HAPSITE and Laptop . . . . . . . . . . . . . . . . . . . . 8-22 8.11 HAPSITE Icons. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-23

Chapter 9

Data Review

9.1 Introduction to Data Review . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-1 9.2 Accessing the Data Review Feature . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-2 9.3 Data Review Toolbar . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-5 9.4 RMB (Right Mouse Button) Menus within Data Review . . . . . . . . . . . . . . . . 9-6 9.4.1 RMB in the TIC/RIC Window . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-6 9.4.2 RMB in the Spectrum Display Window. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-9 9.5 The TIC/RIC Display Functions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-11 9.5.1 How to Access the Scan Cursor. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-11 9.5.2 How to Use Background Subtraction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-12 9.5.2.1 Steps Required to Perform a One Point Background Subtraction . . . . . . . 9-12 9.5.2.2 Background Subtraction Using a Range of Points . . . . . . . . . . . . . . . . . . . 9-14 9.5.2.3 Additional Features of the Background Tool . . . . . . . . . . . . . . . . . . . . . . . 9-15 9.5.3 Utilizing the Range Tool . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-15 9.5.3.1 Steps Required to Range Acquisition. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-16 9.5.3.2 Additional Features of the Range Tool . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-16 9.6 Using the Zoom Function . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-17 9.6.1 Using the Zoom Function in the TIC/RIC Window . . . . . . . . . . . . . . . . . . . 9-17 9.6.2 Using The Zoom Spectrum Function . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-19 9.7 Displaying Reconstructed Ion Chromatograms (RIC) . . . . . . . . . . . . . . . . 9-20 9.7.1 RIC Plot to Locate Specific Compounds . . . . . . . . . . . . . . . . . . . . . . . . . . 9-21 9.8 NIST Library Searches . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-23 9.8.1 Searching Peaks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-25 9.8.2 Analyzing Data Using AMDIS. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-29 9.8.3 How To Access AMDIS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-29 9.8.3.1 Accessing NIST from AMDIS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-31 9.8.4 Analyzing Data Using NIST . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-32

TOC - 7

HAPSITE ER Operating Manual

9.8.5 How to Grab Spectra/Utilize the Full NIST Program . . . . . . . . . . . . . . . . . 9-33 9.8.6 Method Generated Reports . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-34 9.9 ER IQ Hot Keys . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-36

Chapter 10

Saving and Managing Files

10.1 Saving Files on the HAPSITE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-1 10.1.1 Method Files. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-1 10.1.2 Event Log Files. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-3 10.1.3 Data Files . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-3 10.1.4 Tune Files. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-4 10.1.5 Data Review . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-7

10.2 Saving Files . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-9 10.2.1 Method Files. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-9 10.2.2 Event Log Files. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-10 10.2.3 Data Files . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-11 10.2.4 Tune Files. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-11 10.2.5 Report Files . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-11

10.3 Transferring Files Between the HAPSITE and Laptop . . . . . . . . . . . . . . . 10-11

Chapter 11

Method Editor

11.1 The Method Editor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-1 11.2 Accessing Method Editor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-4 11.3 Description Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-4 11.3.1 Full Scan Method . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-7 11.3.2 SIM Method . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-8 11.4 Startup Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-9 11.4.1 Headspace . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-12 11.4.2 SituProbe . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-13 11.5 Inlet Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-14 11.5.1 Inlet States . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-16 11.5.2 GC Temperature Profile . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-23 11.5.3 Use Internal Standard . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-23 11.5.4 Scan Events . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-24 11.5.5 Concentrator Selection. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-25 11.5.6 Headspace Flow Parameter. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-25 11.5.7 SituProbe Flow Parameter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-25 11.6 Tune Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-26 11.6.1 Param Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-26 11.6.2 Report Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-26

TOC - 8

IPN 074-471-P1B

HAPSITE ER Operating Manual

11.7 Full Scan Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-29 11.8 SIM Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-31 11.8.1 SIM for Analyze (GC/MS) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-31 11.8.2 SIM for Survey . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-34 11.9 Search Page. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-36 11.9.1 Setting Up a Qualitative Search . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-37 11.9.2 Setting Up a Quantitative Search . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-42 11.10 Data Page. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-47 11.11 Summary Page. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-50 11.12 How to Create a Method. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-51 11.12.1 Creating a New Custom Method from an Existing Method. . . . . . . . . . . . 11-51 11.13 How to Sequence Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11-54

Chapter 12

Target Compound Methods

12.1 Introduction To Quantitative Analysis . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-1 12.2 Definition of Terms in the Calibrate Window . . . . . . . . . . . . . . . . . . . . . . . 12-2 12.2.1 Method . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-2 12.2.2 Data Files . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-2 12.2.3 Peak Search . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-3 12.2.4 Analytes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-4 12.2.5 Reports . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-4 12.2.6 Extracted Mass Peaks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-5 12.2.7 Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-5 12.3 Definition of Terms in the ID Unknowns Window . . . . . . . . . . . . . . . . . . . . 12-6 12.3.1 Method . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-6 12.3.2 Data Files . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-6 12.3.3 Peak Search . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-7 12.3.4 Analytes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-7 12.3.5 Reports . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-7 12.3.6 Extracted Mass Peaks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-8 12.3.7 Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-8 12.4 Display Function . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-9 12.5 Using the Calibrate Function . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-10 12.6 Using the ID Unknown Function . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-18

Chapter 13

Headspace Sampling System

13.1 Introduction. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-1 13.1.1 How the HSS Operates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-2 13.1.2 Performance Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-3

TOC - 9

HAPSITE ER Operating Manual

13.1.3 HSS Indicators . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-3 13.1.4 Consumables Required . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-4 13.1.5 Connecting the HSS to the HAPSITE . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-5 13.1.6 Providing Power to the HSS. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-5 13.1.6.1 If AC Power is Available . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-5 13.1.6.2 If AC Power is Not Available . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-5 13.2 Using the HAPSITE with HSS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-6 13.2.1 Powering on the HSS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-6 13.2.2 Loading the Vials . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-7 13.2.3 Loading the Wells. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-11 13.2.4 Cycling the Vials. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-12 13.2.5 Making the Measurement. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-13 13.3 Maintenance of the HSS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-13 13.3.1 Clean Out after a High Concentration Sample . . . . . . . . . . . . . . . . . . . . . 13-13 13.3.1.1 Purge Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-13 13.3.2 Cleaning Up a High Background . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-13 13.3.2.1 Flush Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-14 13.3.3 Cleaning the HSS Wells . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-15 13.3.4 Decontaminating the HSS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-16 13.3.5 Replacing The HSS Battery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-17 13.3.6 Replacing The HSS Nitrogen Canister. . . . . . . . . . . . . . . . . . . . . . . . . . . 13-18 13.4 Shipping the HSS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-18 13.5 Charging the HAPSITE Battery using the HSS . . . . . . . . . . . . . . . . . . . . 13-19

Chapter 14

SituProbe

14.1 SituProbe . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-1 14.2 Theory . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-1 14.3 Physical Specifications. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-2 14.4 Operating Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-3 14.5 Consumables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-4

14.5.1 Compressed Nitrogen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-4 14.6 Heated Zones. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-5 14.7 Valves and Sequences. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-6 14.7.1 Headspace . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-6 14.7.2 Purge . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-6 14.7.3 Dry Purge . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-7 14.8 SituProbe Operation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-7 14.8.1 Headspace Creation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-7 14.8.2 Purge Rate Adjustment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-7

TOC - 10

IPN 074-471-P1B

HAPSITE ER Operating Manual

14.8.3 Method Events . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-8

14.9 Background Cleanup . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-9

14.9.1 Introduction. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-9

14.9.2 Cleanup Steps . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-9

14.10 Operating Tips . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-11

14.10.1 Reducing Background . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-11

14.10.1.1 Sampling Precautions. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-11

14.10.1.2 Expected Concentration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-11

14.10.2 Nitrogen Usage. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-11

14.11 Calibration Standards . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-12

14.11.1 Introduction. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-12

14.11.2 Standard Preparation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-12

14.11.3 Calculations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-14

14.12 Calibration Curves . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-14

14.13 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-15

14.13.1 Surface Cleaning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14-15

Chapter 15

Service Module

15.1 Introduction. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-1

15.2 Service Module Input Power. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-2

15.2.1 Service Module 110/220 V(ac) Input . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-2

15.2.2 Service Module 24 V(dc) Input . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-2

15.3 Components of the Service Module . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-3

15.3.1 Backup Batteries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-3

15.3.2 MDP/Turbo Pump. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-3

15.3.3 Manifold Vent Valve . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-3

15.3.4 Foreline Vent Valve . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-4

15.3.5 Roughing Pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-4

15.3.6 Vacuum Interconnect Valve Actuator . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-4

15.3.7 Battery Charger . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-4

15.3.8 Power Supply . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-5

15.3.9 Communications. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-5

15.4 When to Use the Service Module . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-6

15.5 ER IQ Software for the Service Module . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-7

15.5.1 The Service Module Tab in Properties Window . . . . . . . . . . . . . . . . . . . . . 15-8

15.6 Starting Up HAPSITE on the Service Module . . . . . . . . . . . . . . . . . . . . . 15-11

15.7 Attaching the HAPSITE to the Service Module . . . . . . . . . . . . . . . . . . . . 15-12

15.7.1Attaching the HAPSITE to the Service Module using the

ER IQ Software. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-13

TOC - 11

HAPSITE ER Operating Manual

15.7.2Attaching the HAPSITE to the Service Module using the

HAPSITE Front Panel Controls . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-14 15.8 Detaching the HAPSITE. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-16 15.8.1 Using ER IQ Software to Detach . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-17 15.8.2 Using the Front Panel Display to Detach . . . . . . . . . . . . . . . . . . . . . . . . . 15-18 15.9 Physically Removing the HAPSITE from the Service Module . . . . . . . . . 15-19 15.10 Storing the Service Module . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-20 15.11 When Power to the Service Module is Lost . . . . . . . . . . . . . . . . . . . . . . . 15-23 15.12 Routine Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15-23

Chapter 16

Maintenance

16.1 Introduction. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-1 16.2 Safety Considerations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-2 16.3 HAPSITE Symptom - Cause - Remedy Chart . . . . . . . . . . . . . . . . . . . . . . 16-3 16.4 Required Environment for General Maintenance . . . . . . . . . . . . . . . . . . . . 16-7 16.5 Contamination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-7

16.5.1 Contamination of the Mass Spectrometer . . . . . . . . . . . . . . . . . . . . . . . . . 16-8 16.5.1.1 Symptoms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-8 16.5.1.2 Decontamination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-8 16.5.2 Contamination of the Gas Chromatograph. . . . . . . . . . . . . . . . . . . . . . . . . 16-8 16.5.2.1 Symptoms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-8 16.5.2.2 Decontaminate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-8 16.5.3 Contamination of the Probe and Probe Line . . . . . . . . . . . . . . . . . . . . . . . 16-9 16.5.3.1 Symptoms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-9 16.5.3.2 Decontaminate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-9 16.5.4 Decontaminating the Outside of the Analytical Module . . . . . . . . . . . . . . 16-11 16.6 NEG Troubleshooting. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-13 16.6.1 Bakeout Procedure. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-15 16.6.2 Reactivating the NEG Pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-16 16.7 NEG Pump Removal, Installation and Activation . . . . . . . . . . . . . . . . . . . 16-17 16.7.1 Required Tools and Equipment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-18 16.7.2 Part 1: NEG Pump Removal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-19 16.7.3 Part 2: Service Module Vacuum Interconnect (VI) Valve Cleaning . . . . . 16-21 16.7.4 Part 3: Install the New NEG Pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-24 16.7.5 Part 4: Leak Check of the Vacuum System . . . . . . . . . . . . . . . . . . . . . . . 16-30 16.7.6 Part 5: Activation of the NEG Pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-34 16.8 Replacing the Ionizer of the Mass Spectrometer . . . . . . . . . . . . . . . . . . . 16-35 16.9 Replacing the HSS Needle. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-41 16.10 Cleaning the Air Filters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-43

TOC - 12

IPN 074-471-P1B

HAPSITE ER Operating Manual

16.11 Battery Charger Maintenance and Troubleshooting. . . . . . . . . . . . . . . . . 16-44 16.11.1 Cleaning The Battery Charger . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-44 16.11.2 Troubleshooting The Battery Charger . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-44 16.11.2.1 No Indicators are Illuminated . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-44 16.11.2.2 If the Red Indicator is Flashing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16-45 16.11.2.3 If a Battery Does Not Accept a Charge . . . . . . . . . . . . . . . . . . . . . . . . . . 16-45

Chapter 17

Customer Support

17.1 How To Contact Customer Support . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17-1 17.2 Returning Your Instrument to INFICON . . . . . . . . . . . . . . . . . . . . . . . . . . . 17-1

Chapter 18

Part Numbers

18.1 HAPSITE Part Number. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18-1 18.2 HAPSITE ER Accessories . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18-2 18.3 HAPSITE Consumables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18-3 18.4 Headspace Spare Parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18-4 18.5 Service Module Spare Parts. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18-5 18.6 HAPSITE SituProbe Spare Parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18-5

Chapter 19

Glossary

19.1 Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19-1

Appendix A

HAPSITE Target Compounds

A.1 Compounds In Order Of Elution . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .A-1

Appendix B

Calibrating Gas Mixtures

B.1 Acquisition, Preparation, and Handling . . . . . . . . . . . . . . . . . . . . . . . . . . . .B-1 B.1.1 How to Establish the Desired Concentrations . . . . . . . . . . . . . . . . . . . . . . .B-1 B.1.1.1 Using Cylinders Charged with Each Concentration . . . . . . . . . . . . . . . . . . .B-2 B.1.1.2 Diluting the Gas On Site . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .B-3 B.1.2 Correct Delivery of the Mix to the Inlet of the HAPSITE . . . . . . . . . . . . . . . .B-3 B.1.2.1 Free Flow of Gas . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .B-4 B.1.2.2 Inert Sample Bag . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .B-4 B.1.3 Gas Cylinder Safety, Contamination Checks, and Corrective Steps . . . . . .B-5

TOC - 13

HAPSITE ER Operating Manual

Appendix C

Shipping the HAPSITE and Consumables

C.1 Introduction. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .C-1

C.2 Shipping the Canisters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .C-1

C.3 Empty Canisters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .C-3

Index

IPN 074-471-P1B

TOC - 14

IPN 074-471-P1B

HAPSITE ER Operating Manual

Chapter 1

Introduction

1.1 The HAPSITE ER System

The HAPSITE® ER Portable Gas Chromatograph and Mass Spectrometer (GC/MS) is designed to measure volatile organic hazardous air pollutants at parts-per-trillion (PPT) levels, using pre-programmed sets of instructions known as "methods". The HAPSITE ER is specifically designed for portability and field operation. The HAPSITE ER can collect and analyze samples while operating on battery power using self-contained carrier gas and internal standard gas supplies. The results are displayed and saved on a hard drive. They can also be downloaded to a USB drive or through a data connection to a Laptop for analysis.

NOTE: This manual is specifically for the HAPSITE ER. The terms "HAPSITE" and "HAPSITE ER" are used throughout this manual to refer to the HAPSITE ER.

Several hardware modules comprise the HAPSITE ER System:

HAPSITE . . . . . . . . . . . . . . . . . . . . . Often referred to as the Analytical Module (AM). The AM contains the gas chromatograph and mass spectrometer, cylinders of carrier gas and internal standard gas, high-vacuum chemical pump (for portable operation), control electronics, battery, keypad, display, and a battery charger.

Probe . . . . . . . . . . . . . . . . . . . . . . . . Also known as the Hand Control Unit, this consists of a hand piece and a heated inlet line. The hand piece contains a small display and buttons. The inlet line connects to the HAPSITE and provides a flexible heated sample flow path to the HAPSITE.

Service Module . . . . . . . . . . . . . . . . Also known as the SM, the Service Module contains the turbo-molecular high-vacuum pump, the roughing pump, the mechanism for operating the interconnecting valve, a battery-charger and a power supply.

Headspace Sampling System . . . . Also known as the HSS, the HSS is an accessory to the HAPSITE that allows testing for volatile compounds in solids and liquids, including soil and water.

SituProbe™. . . . . . . . . . . . . . . . . . . The SituProbe accessory is a water purging device that provides continuous testing of water samples in the field.

1 - 1

HAPSITE ER Operating Manual

1.2 Performance Specifications

The performance specifications for the HAPSITE are shown below: Mass range . . . . . . . . . . . . . . . . . . 1-300 AMU

Scan Rate . . . . . . . . . . . . . . . . . . . as much as 1000 AMU/sec @ 10 points per AMU

Ionization Mode . . . . . . . . . . . . . . . 70 eV electron impact Operating temperature range . . . . . 0 oC to 45 oC (32 to 113 oF)

Dimensions (LxWxH) . . . . . . . . . . . 46 x 43 x 18 (cm); 18 x 17 x 7 (in) Weight . . . . . . . . . . . . . . . . . . . . . . 16 kg (35 lb.) without the battery Internal Power Consumption . . . . . 30 watts average, 24 V(dc) Carrier Gas . . . . . . . . . . . . . . . . . . Nitrogen

Column Temperature Range . . . . . 60 oC to 200 oC

Maximum Sample

Moisture Content . . . . . . . . . . . . . . . 8% by weight pH Range of Sample . . . . . . . . . . . . 2 - 11 Boiling Point of Sample (approx) . . . <270 oC

Chemical Composition of Sample . . 1 - 15 Carbon atoms

GC Column . . . . . . . . . . . . . . . . . . . 100% dimethyl polysiloxane phase, 15 m X 0.25 mm ID x 1.0 m film

SIM Channels . . . . . . . . . . . . . . . . 10

External Communications . . . . . . . Ethernet Port, Wireless

Carrier Gas Use-Rate . . . . . . . . . . One 5L canister per 8 hours of operation (This depends on the details of the method being used.)

Internal Standards Gas Use-Rate . One 5L canister per 24 hours of operation (This depends on the details of the method being used.)

Battery Life . . . . . . . . . . . . . . . . . . Approximately 2 to 3 hours

1.3 Serial Number Location

The serial number of the HAPSITE is located on the inside of the front panel and in the front panel software. Touch the HAPSITE icon, followed by the HAPSITE System icon, and then touch HAPS to locate the serial number.

1 - 2

IPN 074-471-P1B

+ 530 hidden pages

INFICON HAPSITE ER Chemical Identification System User Manual

Trademarks

Warranty

Table Of Contents

1.1 The HAPSITE ER System

1.2 Performance Specifications

1.3 Serial Number Location