YSI DO200A User Manual [en, es, fr]

Operations Manual
®
EcoSense
DO200A
Dissolved Oxygen
and Temperature
English Français Español
Instrument
Português
WARRANTY
The EcoSense® DO200A Instrument is warranted for one year from date of purchase by the end user against defects in materials and workmanship. DO200A probes and cables are warranted for one year from date of purchase by the end user against defects in material and workmanship. Within the warranty period, YSI will repair or replace, at its sole discretion, free of charge, any product that YSI determines to be covered by this warranty.
To exercise this warranty, write or call your local YSI representative, or contact YSI Customer Service in Yellow Springs, Ohio. Send the product and proof of purchase, transportation prepaid, to the Authorized Service Center selected by YSI. Repair or replacement will be made and the product returned, transportation prepaid. Repaired or replaced products are warranted for the balance of the original warranty period, or at least 90 days from date of repair or replacement.
Limitation of Warranty This Warranty does not apply to any YSI product damage or failure caused by: (i)
failure to install, operate or use the product in accordance with YSI’s written instructions; (ii) abuse or misuse of the product; (iii) failure to maintain the product in accordance with YSI’s written instructions or standard industry procedure; (iv) any improper repairs to the product; (v) use by you of defective or improper components or parts in servicing or repairing the product; or (vi) modification of the product in any way not expressly authorized by YSI.
THIS WARRANTY IS IN LIEU OF ALL OTHER WARRANTIES, EXPRESSED OR IMPLIED, INCLUDING ANY WARRANTY OF MERCHANTABILITY OR FITNESS FOR A PARTICULAR PURPOSE. YSI’s LIABILITY UNDER THIS WARRANTY IS LIMITED TO REPAIR OR REPLACEMENT OF THE PRODUCT, AND THIS SHALL BE YOUR SOLE AND EXCLUSIVE REMEDY FOR ANY DEFECTIVE PRODUCT COVERED BY THIS WARRANTY. IN NO EVENT SHALL YSI BE LIABLE FOR ANY SPECIAL, INDIRECT, INCIDENTAL OR CONSEQUENTIAL DAMAGES RESULTING FROM ANY DEFECTIVE PRODUCT COVERED BY THIS WARRANTY.
CONTACT INFORMATION
YSI 1725 Brannum Lane Yellow Springs OH, 45387, USA Tel: 800-897-4151 • 937-767-7241; Fax: 937-767-1058 E-mail : environmental@ysi.com Web : www.ysi.com
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CONTENTS
WARRANTY ............................................................................................................ 1
CONTACT INFORMATION .................................................................................. 1
GENERAL INTRODUCTION ................................................................................. 3
INITIAL INSPECTION ............................................................................................ 3
PRECAUTIONS ...................................................................................................... 3
The Case ......................................................................................................... 3
The Probes (Field & Lab) ............................................................................... 3
PROBE PREPARATION ......................................................................................... 4
BATTERY INSTALLATION .................................................................................... 4
Battery Disposal ............................................................................................. 4
THE KEYPAD .......................................................................................................... 4
THE LCD DISPLAY ................................................................................................. 4
OPERATIONAL PROCEDURES ........................................................................... 5
MEASUREMENT MODES ..................................................................................... 5
SAVING, VIEWING AND DELETING DATA
.................................................... 5
CALIBRATION SET-UP .......................................................................................... 5
Requirements ................................................................................................. 5
Procedure ....................................................................................................... 5
PROBE MAINTENANCE ....................................................................................... 6
TROUBLESHOOTING ........................................................................................... 7
SPECIFICATIONS .................................................................................................. 7
CONVERSIONS ..................................................................................................... 7
RECOMMENDED SPARE PARTS LIST ................................................................ 7
2
GENERAL INTRODUCTION
The DO200A is a precise tool that measures temperature and dissolved oxygen in % and ppm (mg/L) .
This instrument has a waterproof IP67 case when the connector cap is installed. The keys are highly reliable with tactile and audio feedback. This instrument uses one 9V battery. Re­calibration is not required after turning the instrument off and on.
The front of the instrument has a large LCD that displays DO %, ppm, and temperature simultaneously along with user prompts and mode indicators. The unit prompts the user through calibration and measurement procedures.
The model DO200A field and lab probes use a polarographic electrode with convenient screw-on cap membranes. The 200-4 and 200-10 field probes come with a built-in temperature probe for automatic temperature compensation, as well as a stainless steel body for added weight. The self stirring 200-BOD lab probe comes with a power supply and has replaceable electrodes.
Other features include long battery life and high 50/60 Hz AC noise rejection. This instrument is universal and user-friendly for field, industrial, and laboratory applications.
INITIAL INSPECTION
Carefully unpack the unit and accessories, and inspect for shipping damages. Compare received parts with materials listed on the packing list. Notify YSI immediately of any damage or missing parts. Save all packing materials until satisfactory operation is confirmed.
PRECAUTIONS The Case
Though the instrument is housed in a water-proof IP67 case, DO NOT use it underwater. The connector is not waterproof unless the cap is installed. In case of submersion without the cap connected, follow these steps immediately:
1. Dry the connector if necessary. Rinse unit carefully with distilled water. After rinsing and
drying, inspect and clean connectors to remove all contaminants that may affect probe
connections.
2. Wait for unit and connectors to dry completely before resuming operation.
3. If the unit does not function correctly after steps 1 and 2, call YSI for possible repair or
replacement.
The Probes (Field & Lab)
1. Membranes last longer if properly installed and regularly maintained. Erratic readings
can result from damaged or fouled membranes or from large bubbles in the electrolyte
reservoir. If unstable readings or membrane damage occurs, replace both the
membrane cap and Oxygen Probe solution (O2 Probe Electrolyte). The average
membrane replacement interval is 4 to 8 weeks, although they may last longer if kept
clean. Harsh environments, such as wastewater, may require membrane replacement
every 2 to 4 weeks. Unstable readings may occur if membrane cap is coated with oxygen
consuming or producing organisms such as bacteria or algae.
2. Chlorine, sulfur dioxide, nitric oxide and nitrous oxide can affect readings by behaving
like oxygen at the probe.
3. Avoid substances that may damage probe materials such as concentrated acid, caustics
and strong solvents. Probe materials include Stainless steel, epoxy and ABS Plastic.
4. Keep the probe’s gold cathode clean and textured (when properly maintained it has a
matte finish). If it is tarnished (from contact with certain gases), or plated with silver (from
extended use with a loose or wrinkled membrane), then clean it, following the
instructions in “Probe Maintenance”.
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5. To prevent the membrane and electrolyte from drying out, store the field probe in the
A
calibration bottle with the moistened, clean sponge and the lab probe in a clean BOD
bottle with 1 inch of water to keep them in a saturated air environment.
PROBE PREPARATION
The DO200A probe ships with a dry, protective membrane. To install a new membrane cap on the probe:
1. Unscrew probe membrane cap and discard.
2. Fill a new cap with Oxygen Probe Solution. If using the probe solution for the first time,
prepare it according to directions on the bottle.
3. Thread filled membrane cap onto sensor.
4. Allow sufficient warm-up time for initial use (10-15 min). During this time an “ovEr”
message may appear on the display. This is normal. After the warm up is complete the
message will disappear.
BATTERY INSTALLATION
An initial display of “LOW BAT” on the LCD indicates approximately one hour of battery life for unit operation within specifications. Replace battery when “LOW BAT” appears on the LCD.
To replace battery, remove the two battery cover screws and the
battery cover and o-ring. Replace the 9V battery. Replace the battery cover and o-ring (be sure to align the o-ring correctly to prevent a bad seal) and fasten the two battery cover screws for
Figure 1.
Battery Installation
the water-proof feature.
Battery Disposal
This instrument is powered by a 9 volt battery, which the user must remove and dispose of when the batteries no longer power the instrument. Disposal requirements vary by country and region, and users are expected to understand and follow the battery disposal requirements for their specific locale.
THE KEYPAD
1. : Turns the unit on or off.
2. MODE: In normal operation, toggles display between Dissolved Oxygen in % air
saturation, Dissolved Oxygen in ppm (mg/L), Delete and Recall. In Calibration mode,
exits current calibration and displays the next calibration parameter.
3. CAL: In normal operation, changes the mode from Normal to Calibration. See
Calibration Set-up.
: In Calibration Set-up, press this key to save the current parameter to memory.
4.
5. and  Keys: Increases or decreases the display value as desired.
THE LCD DISPLAY
1. BAT: Low battery indicator.
2. CAL: Calibration mode indicator.
3. SAL ppt: Displays during calibration
when user is prompted for the
approximate salinity of the sample in
parts per thousand (ppt).
4. mBar: Displays during calibration to
prompt user for barometric pressure.
5. Main display for dissolved oxygen
values.
6. %/ppm: Unit indicators.
1
2
4
BAT
CAL
Figure2. LCD Display
SAL ppt
mBar
% ppm
C
3
4
5
6
7
7. ºC: Temperature display.
OPERATIONAL PROCEDURES
Press to turn the unit on or off. The instrument will perform a self-diagnostic test, during which an “ovEr” message may appear on the display. This is normal. After the warm up is complete the message will disappear. After the self-diagnostic test completes, the temperature displays in the lower right of the display, and the unit is ready for operation. Immerse the probe into the sample solution. If possible, do not allow probe to touch any solid object in the solution. Avoid air bubbles bursting on the membrane surface. When the unit is not in use, turn it off to save battery life. The instrument has a 30 minute auto shut off feature when not in use.
NOTE: During an oxygen measurement, the probe must be moved approximately 1/2 ft per second to overcome the consumption of oxygen by the sensor. When using the 200-BOD lab probe, however, simply use the probe’s self-stirring feature.
MEASUREMENT MODES
This unit provides three distinct measurements:
1. Temperature - Current solution temperature continually displays.
2. Dissolved Oxygen % - Measurement of oxygen in percent saturation.
3. Dissolved Oxygen ppm - Measurement of oxygen in ppm (mg/L).
Carefully observe the units displayed at the far side of the LCD to determine the desired mode.
SAVING, VIEWING AND DELETING DATA
The DO200A can save 50 data records. When in measurement mode, press to save a record. The instrument will confirm the saved data by displaying SAVE and the record number for one second. “Full” is displayed when trying to save data and the memory is full.
To view saved data, press mode until RECALL is displayed and then press . Use the Up or Down arrow keys to review different saved records. Press Mode to escape back to measurement mode.
To delete data records, press Mode while in measurement mode until DELETE is displayed. Press . “All” will be displayed and blinking. Press the Up or Down arrow key to switch between delete ‘All’ or ‘Each’ options. Select either ‘All’ or ‘Each’ by pressing while that option is displayed.
If ‘All’ is selected, all records will be deleted from memory and ‘None’ will be displayed. Press Mode twice to return to the measurement mode.
If ‘Each’ is selected, the Up and Down arrow keys will allow you to scroll through the saved data records. Press to delete the selected record. All records after the deleted record will shift up to keep the records in sequential order. For example, if record 3 is deleted, record 4 will become record 3 and record 5 will become record 4. Press Mode twice to return to the measurement mode.
CALIBRATION SET-UP Requirements
1. The approximate pressure (in millibars [mBar]) of the location at the time of calibration.
2. The approximate salinity of the water to be analyzed. Fresh water has an approximate
salinity of zero parts per thousand (ppt). Seawater has an approximate salinity of 35 ppt.
Procedure
1. For the field probe, place 5-6 drops of clean water (tap, distilled, or deionized) into the
sponge inside the calibration bottle. Turn the bottle over and allow any excess water to
drain out of the bottle. The wet sponge creates a 100% water-saturated air environment
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for the probe, which is ideal for calibration, transport, and storage of the Model DO200A
probe. For calibration, the probe remains in a water saturated air atmosphere and is not
submersed.
For the lab probe, simply use the same bottle the probe is stored in with approximately
1 inch of water in the bottom. This creates a 100% water-saturated air environment for
the probe, which is ideal for calibration and storage of the Model 200-BOD probe. For
calibration, the probe remains in a water saturated air atmosphere and is not
submersed.
2. For the field probe, slide it into the calibration bottle. Be sure the membrane does not
touch the sponge.
3. Turn on the DO200A by pressing . Wait 10 to 15 minutes for the dissolved oxygen and
temperature readings to stabilize.
4. Press CAL.
5. The LCD prompts for the local pressure in mBar. Use the and keys to increase or
decrease the pressure value respectively. See the section titled ‘Conversions’ to convert
barometric pressure units to mBars.
6. When the proper pressure displays, press
lower right of the display. Once the value in the main display stabilizes, press
move to the salinity compensation procedure.
7. The display prompts for the approximate salinity of the water to be analyzed. Use the
and keys to increase or decrease the salinity compensation value to the value of your
sample (between 0 to 40 parts per thousand [ppt]). When the correct salinity displays,
.
press
8. The unit holds calibration even if it is powered off. However, it is recommended to check
calibration with each use and recalibrate as necessary to prevent drift. Dissolved oxygen
readings are only as good as the calibration.
once to view the calibration value in the
again to
PROBE MAINTENANCE
Clean the probe whenever it won’t calibrate or the readings are unstable and changing the membrane does not solve either issue. On average, the probe should only be cleaned about once or twice per year. To clean the probe, sand the electrodes according the directions below. In addition to sanding, a chemical soak may be necessary (direction below). Always sand the electrodes after performing a chemical soak.
1. Turn unit off, or disconnect probe.
2. Remove membrane cap and rinse the probe with clean water (tap, distilled, or
deionized).
3. Obtain either:
14 % lab strength ammonium hydroxide and soak for 2-3 minutes
4. Rinse ammonium hydroxide/ammonia completely from probe.
5. Use sandpaper (400 grit wet/dry, supplied with 5238 kit and with the 5908 membrane
6. Install a new membrane cap.
Never use chemicals or abrasives not recommended by YSI.
3% household cleaning strength ammonia and soak overnight (8-12 hours)
kit) to buff (wet sand) excess deposits from probe. Perform a circular sand on the gold
cathode (tip) and also wrap the sand paper around the silver anode (shaft) and twist.
Rinse with clean water (tap, distilled, or deionized).
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TROUBLESHOOTING
Y
Y
Main Display reads: Possible Solutions:
“ovEr” or “undr”
Check membrane and electrolyte solution. Clean anode and cathode. Return product for service.
Secondary Display reads: Possible Solutions:
“undr”
“ovEr”
Heat the sample to above –6.0 °C Return product for service.
Cool sample to below 46.0 °C Return product for service
SPECIFICATIONS
Display Range Accuracy Resolution
Dissolved O2
(ppm or mg/L)
Dissolved O2
% air-sat
Temperature °C -6.0 to 46.0 °C
Pressure Compensation 600 to 1100 mBar (450 to 825 mmHg) Salinity Compensation From 0.0 to 40.0 ppt ATC Probe Calibration Backup Audio Feedback Power Source One 9V battery Operating Temperature Instrument Casing Waterproof IP 67 Weight (with battery) 270 grams (.61 lbs) Dimensions (L x W x D) 18.7 cm x 7.6 cm x 3.8 cm (7.3 in x 3 in x 1.5 in)
0 to 20.00 ppm (mg/L) ±2 % of the reading or ±2% air
0 to 200.0 % ±2% of the reading or ±0.2 ppm,
21 to 115 °F
saturation, whichever is greater
whichever is greater.
±0.3 °C ±1 digit 0.1 °C
Thermistor, 10K, at 25C
es es, on all keys
0 to 50C (32 to
122 °F)
0.01 mg/L
0.1 %
CONVERSIONS
To Convert: Multiply by: Inches of Hg to mBar 33.864 Inches of Hg to mmHg 25.4 mmHg to mBar 1.333
RECOMMENDED SPARE PARTS LIST
PART # DESCRIPTION
200-4 4 meter (approx. 13 feet) probe and cable assembly
200-10 10 meter (approx. 33 feet) probe and cable assembly
200-BOD Self-stirring BOD lab probe and cable assembly with power supply
485 DO carrying case, soft sided
606036 DO carrying case, hard sided
5908 Membrane kit, 1.25 mil PE (605306), six cap membranes and KCl solution
Item #606035REF
Revision A; July 2012
For the latest version of this manual, visit www.ysi.com
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GARANTIE
L’appareil EcoSense® DO200A est garanti pour une période d’un an, à compter de la date d’achat par l’utilisateur final, contre tout défaut matériel et de fabrication. Les sondes et les câbles de DO200A sont garantis pour une période d’un an, à compter de la date d’achat par l’utilisateur final, contre tout défaut matériel et de fabrication. Pendant la période de garantie, YSI s’engage à réparer ou à remplacer, gratuitement et à sa discrétion, tout produit qu’YSI peut établir comme étant couvert par la garantie.
Pour faire valoir cette garantie, écrivez ou appelez votre représentant YSI ou contactez le Service clientèle d’YSI à Yellow Springs, Ohio, États-Unis. Envoyez le produit et son justificatif d’achat en port payé au Centre de service homologué sélectionné par YSI. La réparation ou le remplacement seront effectués et le produit vous sera retourné en port payé. Les produits réparés ou remplacés sont garantis jusqu’à expiration de la période de garantie originale ou au moins 90 jours à compter de la date de réparation ou de remplacement.
Limitation de garantie Cette garantie ne s’applique pas aux produits YSI endommagés ou présentant des
dysfonctionnements pour les raisons suivantes : (i) installation, exploitation ou utilisation du produit d’une façon non conforme aux instructions écrites d’YSI ; (ii) abus ou mésusage du produit ; (iii) manquement à l’entretien du produit conformément aux instructions écrites d’YSI ou aux procédures industrielles normales ; (iv) réparation non conforme du produit ; (v) utilisation par vous de pièces ou de composants défectueux ou non conformes lors de l’entretien ou de la réparation du produit ; ou, (vi) modification du produit d’une façon non expressément autorisée par YSI.
CETTE GARANTIE REMPLACE TOUTES LES AUTRES GARANTIES, EXPRESSES OU INDUITES, Y COMPRIS LES GARANTIES DE COMMERCIABILITÉ OU D’ADAPTATION À UN USAGE PARTICULIER. LA RESPONSABILITÉ D’YSI SELON LES TERMES DE CETTE GARANTIE SE LIMITE À LA RÉPARATION OU AU REMPLACEMENT DU PRODUIT, CONSTITUANT VOTRE SEUL ET UNIQUE RECOURS POUR TOUT PRODUIT DÉFECTUEUX COUVERT PAR CETTE GARANTIE. YSI NE POURRA EN AUCUN CAS ÊTRE TENU RESPONSABLE DE DOMMAGES SPÉCIAUX, INDIRECTS, ACCIDENTELS OU CONSÉCUTIFS RÉSULTANT DE L’UTILISATION DE TOUT PRODUIT DÉFECTUEUX COUVERT PAR CETTE GARANTIE.
COMMENT NOUS CONTACTER
YSI 1725 Brannum Lane Yellow Springs OH, 45387, États-Unis 800-897-4151 • 937-767-7241 • Télécopie : 937-767-1058 E-mail : environmental@ysi.com Web : www.ysi.com
1
TABLE DES MATIÈRES
GARANTIE .............................................................................................................. 1
TABLE DES MATIÈRES ......................................................................................... 2
INFORMATIONS GÉNÉRALES ............................................................................ 3
INSPECTION INITIALE .......................................................................................... 3
PRÉCAUTIONS ...................................................................................................... 3
PRÉPARATION DE LA SONDE ............................................................................ 4
INSTALLATION DE LA PILE ................................................................................. 4
CLAVIER ................................................................................................................. 4
ÉCRAN À CRISTAUX LIQUIDES .......................................................................... 5
PROCÉDURES D’UTILISATION ........................................................................... 5
MODES DE MESURE ............................................................................................ 5
ENREGISTREMENT, AFFICHAGE ET SUPPRESSION DES DONNÉES ........... 5
CONFIGURATION DE L’ÉTALONNAGE ............................................................ 6
ENTRETIEN DE LA SONDE .................................................................................. 7
DÉPANNAGE ......................................................................................................... 7
SPÉCIFICATIONS .................................................................................................. 8
CONVERSIONS ..................................................................................................... 8
LISTE DES PIÈCES DÉTACHÉES RECOMMANDÉES ........................................ 8
2
INFORMATIONS GÉNÉRALES
L’ DO200A est un outil de précision mesurant l’oxygène dissous en pourcentage, ppm (mg/l) ainsi que sa température. Un microprocesseur incorporé stocke, calcule et compense tous les paramètres relatifs aux déterminations liées à l’oxygène dissous, y compris les caractéristiques de température des électrodes de détection de l’oxygène dissous.
Cet appareil est étanche (IP67) uniquement lorsque le capuchon recouvre le connecteur est branché. Les touches mécaniques sont très fiables et fournissent une réaction tactile et sonore. Cet appareil utilise une pile de 9 V. Aucun réétalonnage n'est nécessaire lorsque l'alimentation électrique est rétablie
L’avant de l’appareil dispose d’un écran à cristaux liquides affichant simultanément le pourcentage, les mg/l et la température de l’oxygène dissous, ainsi que les invites destinées à l’utilisateur et les indicateurs de mode. L’appareil émet des invites destinées à l’utilisateur lors des procédures d’étalonnage et de mesure.
Le modèle de sonde de terrain et de laboratoire DO200A utilise une électrode polarographique disposant de capuchons à membrane vissables. Les sondes de terrain 200-4 et 200-10 sont équipées d’une sonde de température incorporée permettant la compensation automatique de la température, ainsi que d’un corps en acier inoxydable qui en augmente la masse. La sonde de laboratoire 200-BOD est équipée d’un bloc d’alimentation électrique et comporte des électrodes remplaçables auto-agitées.
Parmi les autres caractéristiques, on notera la longue durée de vie des piles et une élimination du bruit élevée de 50/60 Hz c.a. Cet appareil est convivial et particulièrement souple dans les applications sur le terrain, industrielles et en laboratoire.
INSPECTION INITIALE
Déballez soigneusement l’appareil et les accessoires et vérifiez qu’ils n’ont pas été endommagés lors de l’expédition. Comparez les pièces reçues aux matériaux répertoriés dans le bordereau d’emballage. Notifiez immédiatement YSI s’il s’avère que des pièces sont endommagées ou manquantes. Mettez de côté les matériaux d’emballage jusqu’à ce que le fonctionnement correct de l’appareil soit confirmé.
PRÉCAUTIONS Boîtier
L'appareil est en effet protégé par un boîtier étanche IP67, mais NE doit PAS être utilisé sous l'eau. Le connecteur n’est pas étanche, sauf si le capuchon le recouvre. En cas d’immersion sans capuchon, suivre immédiatement les étapes suivantes:
1. Séchez le connecteur, le cas échéant, et remplacez la sonde d’oxygène dissous. Rincez
soigneusement l’appareil avec de l’eau distillée. Après le rinçage et le séchage,
inspectez et nettoyez les connecteurs en vue d’éliminer tout contaminant pouvant
affecter les connexions de la sonde.
2. Attendez que l’appareil et la sonde soient parfaitement secs avant de reprendre les
opérations.
3. Si l’appareil ne fonctionne pas correctement après les étapes 1 et 2, appelez YSI en vue
d’une réparation ou d’un remplacement éventuels.
Les sondes (de terrain et de laboratoire)
1. Les membranes durent plus longtemps si elles sont correctement installées et
entretenues régulièrement. Des membranes endommagées ou sales et des grosses
bulles dans le réservoir d’électrolyte peuvent entraîner des lectures incohérentes. Si les
lectures sont instables ou la membrane endommagée, remplacez le capuchon à
membrane et la solution de la sonde à oxygène (également appelée « Électrolyte de
sondage d’oxygènométrie », chlorure de potassium ou solution KCl). Les intervalles de
remplacement sont habituellement de 4 à 8 semaines, bien qu’ils puissent se prolonger
s’ils sont conservés en bon état de propreté. Les milieux particulièrement difficiles, tels
que les eaux usées, peuvent exiger que la membrane soit remplacée toutes les 2 à 4
semaines. Des lectures instables peuvent avoir lieu si le capuchon à membrane est
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