YOKOGAWA PH202G User Manual

User’s Manual
Model PH202G (S) pH Transmitter
IM 12B6C3-E-E
12th Edition
OKOGAWA
IM 12B6C3-E-E
TABLE OF CONTENTS
PREFACE
1. INTRODUCTION AND GENERAL DESCRIPTION ..................................................................... 1-1
1-1. Instrument check ...................................................................................................................
1-1
1-2. Application ............................................................................................................................... 1-2
2. PH202 SPECIFICATIONS ............................................................................................................. 2-1
2-1. Genera• ................................................................................................................................... 2-1
2-2. Operating specifications ........................................................................................................... 2-2
2-3. Model and suffix codes ............................................................................................................ 2-3
2-4. Intrinsic safety - common specifications ................................................................................... 2-4
2-5. Connection diagrams for power supply .................................................................................... 2-5
3. INSTALLATION AND WIRING ......................................................................................................
3-1
3-1. Installation and dimensions ...................................................................................................... 3-1
3-1-1. Installation site ............................................................................................................ 3-1
3-1-2. Mounting methods ...................................................................................................... 3-1
3-2. Preparation .............................................................................................................................. 3-3
3-2-1. Cables, terminals and glands ...................................................................................... 3-3
3-3. Wiring of sensors ..................................................................................................................... 3-4
3-3-1. General precautions .................................................................................................... 3-4
3-3-2. Additional precautions for installations in hazardous areas .......................................... 3-4
3-3-3. Hazardous area non-incendive PH 202S-N ................................................................ 3-4
3-3-4. Liquid earth ................................................................................................................. 3-5
3-3-5. Access to terminal and cable entry ............................................................................. 3-5
3-4. Wiring of power supply ............................................................................................................ 3-5
3-4-1. General precautions .................................................................................................... 3-5
3-4-2. Connection of the power supply ................................................................................. 3-5
3-4-3. Switching the instrument on ........................................................................................ 3-6
3-5. Wiring the sensor system ......................................................................................................... 3-7
3-5-1. Impedance measurement jumper settings .................................................................. 3-7
3-6. Sensor wiring ........................................................................................................................... 3-8
3-6-1. Connection cable ........................................................................................................ 3-9
3-6-2. Sensor cable connection with special grommet ........................................................ 3-10
3-6-3. Sensor cable connections using junction box (BA10) and extension cable (WF10) ... 3-11
4. OPERATION; DISPLAY FUNCTIONS AND SETTING .................................................................
4-1
4-1. Operator interface .................................................................................................................... 4-1
4-2. Explanation of operating keys .................................................................................................. 4-2
4-3. Setting passcodes ................................................................................................................... 4-3
4-3-1. Passcode protection ................................................................................................... 4-3
4-4. Display examples .................................................................................................................... 4-3
4-5. Display functions .................................................................................................................... 4-4
4-5-1. Display functions pH (default) ...................................................................................... 4-4
4-5-2. Display functions pH (ORP) ......................................................................................... 4-5
4-5-3. Display functions pH (rH) ............................................................................................. 4-6
5. PARAMETER SETTING ................................................................................................................
5-1
5-1. Maintenance mode .................................................................................................................. 5-1
5-1-1. Manual temperature selection and adjustment ............................................................ 5-2
5-1-2. Process temperature measuring in ORP mode ........................................................... 5-3
5-1-3. Manual activation of HOLD .............................................................................................. 5-4
5-1-4. Manual impedance check ................................................................................................ 5-5
IM 12B6C3-E-E
5-2. Commissioning mode ................................................................................................................... 5-6
5-2-1. Output Range .................................................................................................................. 5-7
5-2-2. Hold ................................................................................................................................ 5-8
5-2-3. Service .......................................................................................................................... 5-10
5-3. Notes for guidance in the use of service coded settings ............................................................. 5-11
5-3-1. Parameter specific functions .......................................................................................... 5-12
5-3-2. Temperature compensation and measuring functions ................................................... 5-14
5-3-3. Calibration functions ...................................................................................................... 5-16
5-3-4. mA Output functions ..................................................................................................... 5-18
5-3-5. User interface ................................................................................................................ 5-20
5-3-6. Communication setup ................................................................................................... 5-22
5-3-7. Genera• ........................................................................................................................ 5-22
5-3-8. Test and setup mode .................................................................................................... 5-22
6. CALIBRATION ................................................................................................................................
6-1
6-1. Automatic calibration ............................................................................................................... 6-1
6-2. Manual calibration .................................................................................................................... 6-1
6-3. Sample calibration ................................................................................................................... 6-1
6-4. Data entry ................................................................................................................................ 6-1
6-5. Calibration procedures ............................................................................................................. 6-2
6-5-1. Automatic calibration .................................................................................................. 6-2
6-5-2. Automatic calibration with HOLD active ...................................................................... 6-3
6-5-3. Manual calibration (2nd parameter calibration) ............................................................ 6-4
6-5-4. Sample calibration ...................................................................................................... 6-6
7. MAINTENANCE ..............................................................................................................................
7-1
7-1. Periodic maintenance for the EXA transmitter .......................................................................... 7-1
7-2. Periodic maintenance for the sensor system ............................................................................ 7-1
8. TROUBLESHOOTING ....................................................................................................................
8-1
8-1. Diagnostics .............................................................................................................................. 8-2
8-1-1. Off-line calibration checks ........................................................................................... 8-2
8-1-2. On-line impedance checks ......................................................................................... 8-2
8-1-3. Error Codes ................................................................................................................ 8-3
9. SPARE PARTS ...............................................................................................................................
9-1
10. APPENDIX ..................................................................................................................................
10-1
10-1. User setting table ................................................................................................................. 10-1
10-2. Configuration checklist for PH202G ..................................................................................... 10-3
10-3. Set up for sensor compatibility ............................................................................................. 10-4
10-3-1. Genera• .................................................................................................................. 10-4
10-3-2. Selection of measurement and reference electrode ................................................ 10-4
10-3-3. Selecting a temperature sensor .............................................................................. 10-4
10-4. Set up for other functions .................................................................................................... 10-5
10-5. Set up for Pfaudler Type 18 sensor ..................................................................................... 10-6
10-5-1. General set up ........................................................................................................ 10-6
10-5-2. Calibration set up .................................................................................................... 10-6
10-6. Device Description (DD) menu structure ............................................................................... 10-7
10-7. Field Change Order .............................................................................................................. 10-8
11. TEST CERTIFICATE ...................................................................................................................
10-1
In this manual a
mA
sign appears if it concerns the pH202G(S)-E/C/U/N
IM 12B6C3-E-E
PREFACE
Electric discharge
The EXA analyzer contains devices that can be damaged by electrostatic discharge. When servicing this equipment, please observe proper procedures to prevent such damage. Replacement components should be shipped in conductive packaging. Repair work should be done at grounded workstations using grounded soldering irons and wrist straps to avoid electrostatic discharge.
Installation and wiring
The EXA analyzer should only be used with equipment that meets the relevant IEC, American or Canadian standards. Yokogawa accepts no responsibility for the misuse of this unit.
The Instrument is packed carefully with shock absorbing materials, nevertheless, the instrument may be damaged or broken if subjected to strong shock, such as if the instrument is dropped. Handle with care.
Although the instrument has a weatherproof construction, the transmitter can be harmed if it becomes submerged in water or becomes excessively wet.
Do not use an abrasive or solvent in cleaning the instrument.
Notice
Contents of this manual are subject to change without notice. Yokogawa is not responsible for damage to the instrument, poor performance of the instrument or losses resulting from such, if the problems are caused by:
Improper operation by the user.
Use of the instrument in improper applications
Use of the instrument in an improper environment or improper utility program
Repair or modification of the related instrument by an engineer not authorized by Yokogawa.
Warranty and service
Yokogawa products and parts are guaranteed free from defects in workmanship and material under normal use and service for a period of (typically) 12 months from the date of shipment from the manufacturer. Individual sales organizations can deviate from the typical warranty period, and the conditions of sale relating to the original purchase order should be consulted. Damage caused by wear and tear, inadequate maintenance, corrosion, or by the effects of chemical processes are excluded from this warranty coverage.
In the event of warranty claim, the defective goods should be sent (freight paid) to the service department of the relevant sales organization for repair or replacement (at Yokogawa discretion). The following information must be included in the letter accompanying the returned goods:
Part number, model code and serial number
Original purchase order and date
Length of time in service and a description of the process
Description of the fault, and the circumstances of failure
Process/environmental conditions that may be related to the installation failure of the device
A statement whether warranty or non-warranty service is requested
Complete shipping and billing instructions for return of material, plus the name and phone number of a
contact person who can be reached for further information.
Returned goods that have been in contact with process fluids must be decontaminated/disinfected before shipment. Goods should carry a certificate to this effect, for the health and safety of our employees. Material safety data sheets should also be included for all components of the processes to which the equipment has been exposed.
WARNING
CAUTION
Introduction 1-1
IM 12B6C3-E-E
1. INTRODUCTION AND GENERAL DESCRIPTION
The Yokogawa EXA 202 is a 2-wire transmitter designed for industrial process monitoring, measurement and control applications. This user’s manual contains the information needed to install, set up, operate and maintain the unit correctly. This manual also includes a basic troubleshooting guide to answer typical user questions.
Yokogawa can not be responsible for the performance of the EXA analyzer if these instructions are not followed.
1-1. Instrument check
Upon delivery, unpack the instrument carefully and inspect it to ensure that it was not damaged during shipment. If damage is found, retain the original packing materials (including the outer box) and then immediately notify the carrier and the relevant Yokogawa sales office.
Make sure the model number on the textplate affixed to the side of the instrument agrees with your order. Examples of nameplates are shown.
Figure 1-1. Nameplate
N200
pH / ORP TRANSMITTER
PROFIBUS - PA
-10 TO 55 ºC
SUPPLY
OUTPUT
AMB.TEMP. [Ta]
SERIAL No.
EEx ib [ia] IIC T4 for Ta -10 to 55 ºC EEx ib [ia] IIC T6 for Ta -10 to 40 ºC KEMA 00ATEX1068 X
IS CL I, DIV 1, GP ABCD T3B for Ta -10 to 55 ºC
T4 for Ta -10 to 40 ºC
MODEL
EXA PH202S
0344
II 2 (1) G
24VDC/250mA/1,2W
FISCO 17,5VDC/380mA/5,32W
Li=2,6µH Ci=737pF
or
HAZ LOC per Control Drawing FF1-PH202S-00
Amersfoort, The Netherlands
PH202S CSA
WARNING
Substitution of components may impair intrinsic safety
AVERTISSEMENT
La substitution de composants peut compromettre la sècurite intrinsëque.
Refer to Installation Drawing
T4 for Ta -10 to 55 ºC T6 for Ta -10 to 40 ºC
Ex ia CL I, DIV 1, GP ABCD,
IM 12B6C3-E-E
1-2 Introduction
NOTE: The nameplate will also contain the serial number and any relevant
certification marks. Be sure to apply correct power to the unit. The first two characters of the serial number refers to the year and month of manufacturing
Check that all the parts are present, including mounting hardware, as specified in the option codes at the end of the model number. For a description of the model codes, refer to Chapter 2 of this manual under General Specifications.
Basic Parts List: Transmitter PH202 User’s Manual (See model code for language) Optional mounting hardware when specified (See model code)
NOTE: mounting screws and special grommet are packed in the terminal compartment,
together with a second link for impedance selection.
1-2. Application
The EXA converter is intended to be used for continuous on-line measurement in industrial installations. The unit combines simple operation and microprocessor-based performance with advanced self-diagnostics and enhanced communications capability to meet the most advanced requirements. The measurement can be used as part of an automated process control system. It can also be used to indicate dangerous limits of a process, to monitor product quality, or to function as a simple controller for a dosing/neutralization system.
Yokogawa designed the EXA analyzer to withstand harsh environments. The converter may be installed either indoors or outside because the IP65 (NEMA4X) housing and cabling glands ensure the unit is adequately protected. The flexible polycarbonate window on the front door of the EXA allows pushbutton access to the keypad, thus preserving the water and dust protection of the unit even during routine maintenance operations. A variety of EXA hardware is optionally available to allow wall, pipe, or panel mounting. Selecting a proper installation site will permit ease of operation. Sensors should normally be mounted close to the converter in order to ensure easy calibration and peak performance. If the unit must be mounted remotely from the sensors, WF10 extension cable can be used up to a maximum of 50 metres (150 feet) with a BA10 junction box. Except installations with dual high impedance sensors, where the maximum cable length is 20 metres using integral cable only (no junction box).
The EXA is delivered with a general purpose default setting for programmable items. (Default settings are listed in Chapter 5 and again in Chapter 10). While this initial configuration allows easy start-up, the configuration should be adjusted to suit each particular application. An example of an adjustable item is the type of temperature sensor used. The EXA can be adjusted for any one of eight different types of temperature sensors.
To record such configuration adjustments, write changes in the space provided in Chapter 10 of this manual. Because the EXA is suitable for use as a monitor, a controller or an alarm instrument, program configuration possibilities are numerous.
Details provided in this user’s manual are sufficient to operate the EXA with all Yokogawa sensor systems and a wide range of third-party commercially available probes. For best results, read this manual in conjunction with the corresponding sensor user’s manual.
Yokogawa designed and built the EXA to meet the CE regulatory standards. The unit meets or exceeds stringent requirements of EN 55082-2, EN55022 Class A without compromise, to assure the user of continued accurate performance in even the most demanding industrial installations.
Y = Year M = Month
2000 M January 1 2001 N February 2 2002 P March 3 2003 R Apri• 4
........ .. .......... ..
2008 W September 9 2009 X October O 2010 A November N 2011 B December D
IM 12B6C3-E-E
2-1. General A. Input specifications : Dual high impedance inputs
(2 x 1013) with provision for liquid earth connection. Suitable for inputs from glass or enamel pH & reference sensors and ORP metal electrodes.
B. Input ranges
- pH : -2 to 16 pH
- ORP : -1500 to 1500 mV
- rH : 0 to 55 rH
- Temperature : -30 ºC - 140 ºC (-20 - 300 ºF)
- 8k55 sensor : -10 ºC - 120 ºC (10 - 250 ºF)
- PTC10k : -20 ºC - 140 ºC (0 - 300 ºF)
C. Span
- pH : min 1 max 20 pH
- ORP : min 100 max 3000 mV
- rH : min 2 max 55 rH
D. Output signa• : 4-20 mA loop powered,
isolated from input, maximum load 425 at 24 V DC. With the possibility of 22 mA “FAIL” signal (burn up) and 3.9 mA (burn down).
E. Temperature compensation
- Range : Automatic or manual compensation to Nernst equation. Process compensation by configurable coefficient. Compensation for total range of selected temperature sensors (see B) Adjustable ITP (Iso-thermal point of intersection).
F. Calibration : Semi-automatic using pre-
configured NIST buffer tables 4, 7 & 9, of with user defined buffer tables, with automatic stability check. Manual adjustment to grab sample. Slope and Asymmetry Potential setting. Zero point can be selected for calibration and display instead or As. Pot. (IEC746-2)
G. Serial communication
: Bi-directional HART® digital
communication superimposed on the 4-20 mA signal.
H. Logbook : Software record of important
events and diagnostic data. Available through HART link, with key diagnostic information available in the display.
I. Display : Custom liquid crystal display,
with a main display of 31/2 digits 12.5 mm high. Message display of 6 alphanumeric characters, 7 mm high. Warning flags and units (pH and mV).
J. Power supply : Nominal 24 volt DC loop
powered system.
- PH202G : Up to 40 volts.
- PH202S : Up to 31.5 volts.
NOTE: The transmitter contains a switched power
supply. The transmitter requires a minimum Power voltage in order to work correctly, which is dependant on the load. Please refer to figures 2-1 and 2-2 for the correct power supply.
2. PH202 SPECIFICATIONS
Fig. 2-1. Supply voltage/ load diagram
Fig. 2-2. Minimum terminal voltage at the PH202
0.0
20
0.0
40
0.0
60
0.0
80
0.0
1000.0
1200.0
12 14 16 18 20 22 24 26 28 30 32 34 36 38 40
4 mA
22 mA
425.0
775.0
31.5 V
(limit for IS version)
Voltage (V)
Load Resistance ()
230.0
1100.0
Communication
Range
17 Volts
14.5 Volts
4 mA 7 mA 20 mA
Te
rminal voltage (V)
Output Current (mA)
mA
mA
Specification 2-1
mA
IM 12B6C3-E-E
2-2 Specification
K. Input isolation : 1000V DC
2-2. Operating specifications A. Performance : pH
- Linearity :
0.01 pH ± 0.02 mA
- Repeatability : <0.01 pH ± 0.02 mA
- Accuracy : 0.01 pH ± 0.02 mA
Performance : ORP
- Linearity : 1 mV ± 0.02 mA
- Repeatability : <1 mV ± 0.02 mA
- Accuracy : 1 mV ± 0.02 mA Performance :
Temperature with Pt1000 ,
3U Balco, 5kU, 35U, 6kU ,
PTC10k & 8k55
- Linearity : 0.3 ˚C ± 0.02 mA
- Repeatability : <0.1 ˚C ± 0.02 mA
- Accuracy : 0.3 ˚C ± 0.02 mA
Performance : Temperature with Pt100
- Linearity : 0.4 ˚C ± 0.02 mA
- Repeatability : <0.1 ˚C ± 0.02 mA
- Accuracy : 0.4 ˚C ± 0.02 mA
B. Ambient operating temperature
: -10 to + 55 ˚C (10 to 131 ˚F)
Excursions to -30˚C (-20 ˚F) do not influence the current output function, and excursions to + 70˚C (160˚F) are acceptable too.
C. Storage temperature : -30 to +70 ˚C (-20 to 160 ˚F)
D. Humidity : 10 to 90% RH
E. HART specification
- Min. cable diameter : 0.51 mm, 24 AWG
- Max. cable length : 1500 m
- Detailed information can be found at: www.hartcomm.org
F. Housing : Cast aluminium case
with chemically resistant coating, cover with flexible polycarbonate window. Case color is off-white and cover is moss green. Cable entry is via two
1
/2” polyamide glands. Cable terminals are provided for up to 2.5 mm2 finished wires. Weather resistant to IP65 and NEMA 4X standards. Pipe wall or panel mounting, using optional hardware.
G. Shipping details : Package size w x h x d
290 x 225 x 170 mm.
11.5 x 8.9 x 6.7 in. Packed weight approximately
2.5 kg (5lb).
H. Data protection : EEPROM for configuration and
logbook, and lithium cell for clock.
I. Watchdog timer : Checks microprocessor
J. Automatic safeguard : Return to measuring mode
when no keystroke is made for 10 min.
K. Operation protection
: 3-digit programmable
password.
L. Sensor impedance checking
: Independent impedance
check on measuring and reference sensor elements, with temperature compensation. Display of sensor impedance on message line of display. FAIL flag in event of “out of limits” impedance, and the possibility of 22 mA or 3.9 mA error signal.
M. DD Specification
: The PH202 Device Description is available ena­ bling communications with the Handheld communicator
(HHC) and compatible devices. For more information contact your local Yokogawa sales offices.
mA
IM 12B6C3-E-E
Mode• Suffix Code Option code Description
PH202G PH/ORP Transmitter, General Purpose version Type - E Milli-amp (+HART) version, European style
- C Milli-amp (+HART) version, Canadian style
- U Milli-amp (+HART) version, North American style
- F FOUNDATION ® Fieldbus version
- P Profibus PA version
- E Always E Options /H Hood for Sun Protection /U Pipe & Wall mounting hardware /SCT Stainless steel tagplate /Q Calibration certificate
Mode• Suffix Code Option code Description
PH202S PH/ORP Transmitter, Intrinsic Safe version Type - E Milli-amp (+HART) version, European style
- C Milli-amp (+HART) version, Canadian style
- U Milli-amp (+HART) version, North American style
- F FOUNDATION ® Fieldbus version
- P Profibus PA version
- N Non-Incendive Milli-amp (+HART) version
- B Non-Incendive FOUNDATION ® Fieldbus version
- D Non-Incendive Profibus PA version
- E Always E Options /H Hood for Sun Protection /U Pipe & Wall mounting hardware /SCT Stainless steel tagplate /Q Calibration certificate
2-3. Model and suffix codes
N. Regulatory compliance
- EMC : meets council directive 89/336/EEC
- Emmission : meets EN 55022 Class A
- Immunity : meets EN 61000-6-2
O. Intrinsic safety
- ATEX
: EEx ib [ia] IIC T4 for Ta -10 to 55 ºC
EEx ib [ia] IIC T6 for Ta -10 to 40 ºC
II 2 (1) G
KEMA 00ATEX1068 X
- CSA : Ex ia CL 1, DIV 1, GP C&D, T3C for Ta -10 to 55 ºC Refer to Installation Drawing PH202S CSA
- FM : IS CL 1, DIV 1, GP ABCD T3B for Ta -10 to 55 ºC T4 for Ta -10 to 40 ºC HAZ LOC per Control Drawing FF1-PH202S-00
P. Non-Incendive
- FM : NI CL 1, DIV 2, GP ABCD
T3B for Ta -10 to 55 ºC T4 for Ta -10 to 40 ºC HAZ LOC per Control Drawing FF1-PH202S-00
- ATEX : EEx nA [L] IIC T4 for Ta -10 to 55 ºC EEx nA [L] IIC T6 for Ta -10 to 40 ºC
II 3 G
KEMA 00ATEX1115 X
Specification 2-3
IM 12B6C3-E-E
2-4 Specification
Stamp Company : Stamp Certification Institute :
Signature : Remarks :
Model EXA PH202S
Title : Control Drawing PH202S Cenelec
Number : FF1-PH202S-00 Page : 1 of 10
Revision : 5.4
EXA PH202S
(pH/ORP-transmitter)
Safe area
Uo = 31.5 Volt DC
Io = 100 mA
Po = 1.2 Watt
EEX ib Certified Repeater
Power Supply
(HART Compatible)
Output
Supply
SENSOR(S)
terminals 11-19
+_G
SENSOR(S)
terminals 11-19
Zone 0 or 1 Zone 1
Hazardous area
Safe area
+_G
Protective
earth
Protective
earth
Intrinsically safe design
CENELEC standard EEX ib [ia] IIC: T4 for ambient temp. < 55¡C
T6 for ambient temp. < 40¡C
Certificate nr. 00ATEX1068 X
EXA PH202S
+
_
Load
Resistance
EEX ib
Certified safety barrier or power
with Rint=300
Io = 100 mA
Uo = 31.5 Volt DC
Zone 0 or 1
Zone 1
Hazardous area
Protective
earth
+
_
24 volts DC Nominal
Supply Voltage.
Intrinsically safe design
CENELEC standard EEX ib [ia] IIC: T4 for ambient temp. < 55¡C
T6 for ambient temp.< 40¡C
Certificate nr. 00ATEX1068 X
(HART compatible)
(pH/ORP-transmitter)
Sensor(s) are of a passive type to be regarded as simple apparatus , devices which comply with clause 1.3 of the
EN 50014.
Electrical data of the EXAPH202S.
- Supply and output circuit (terminals + and -):
Maximum input voltage U
i
= 31.5 V.
Maximum input current I
i
= 100 mA.
Maximum input power P
i
= 1.2 W.
Effective internal capacitance C
i
= 22 nF.
Effective internal inductance L
i
= 22 µH.
- Sensor input circuit (terminals 11 through 19):
Maximum output voltage U
o
= 14.4 V.
Maximum output current I
o
= 32.3 mA.
Maximum allowed external capacitance C
o
= 600 nF.
Maximum allowed external inductance L
o
= 36 mH.
Barriers and power supply specification must not exceed the maximum values as shown in the diagram above.
These safety descriptions cover most of the commonly used industry standard barriers, isolators and power
supplies.
The Hand Held Communicator must be of a ATEX certified intrinsically safe type in case it is used on the
intrinsically safe circuit in the hazardous area or of a ATEX certified non-incendive type in case it is used in the
non-incendive circuit in the hazardous area.
YOKOGAWA EUROPE B.V.
Date : 01/07/2004
IM 12B6C3-E-E
Specification 2-5
Stamp Company : Stamp Certification Institute :
Signature : Remarks :
Model EXA PH202S
Title : Control Drawing PH202S Cenelec
Number : FF1-PH202S-00 Page : 2 of 10
Revision : 5.4
YOKOGAWA EUROPE B.V.
Date : 01/07/2004
Sensor(s) are of a passive type to be regarded as ’simple apparatus’, devices which
comply with clause 1.3 of the EN 50014.
Electrical data of the EXA PH202S-F & PH202S-P:
- Supply and output circuit::
Maximum input voltage Ui=24 V or Maximum input voltage Ui=17.5 V
Maximum input current Ii=250 mA Maximum input current Ii=380 mA
Maximum input power Pi=1.2 W Maximum input power Pi=5.32 W
Effective internal capacitance Ci=737 pF; Effective internal i nductance Li=2.6
µH.
- Sensor input circuit:
Maximum output voltage Uo=14.4V; Maximum output current Io=32.3 mA
Maximum allowed external capacitance Co=600 nF
Maximum allowed external inductance Lo=36 mH
Any I.S. interface may be used that meets the followi ng requirements:
Uo
24 V or Uo 17.5 V
Io
250 mA Io 380mA
Po 1.2 W Po 5.32 W
Ca
? 737 pF + Ccable; La ? 2.6 µH + Lcable
Safe area
Hazardous area
Zone 1
Zone 0 or 1
Safe area
Apparatus
I.S.
interface
I.S.
certified
Terminator
Sensor
Connections
Ui
=
24 V or Ui
=
17,5 V
Ii
=
250 mA Ii
=
380 mA
Pi
= 1,2 W Pi
=
5,32 W
EEx ib [ia] IIC Certificate no. 00ATEX1068 X
T4 for ambient temp.
55 ϒC
T6 for ambient tem
p
. 40 ϒC
EXA
PH202S-F
& PH202S-P
IM 12B6C3-E-E
2-6 Specification
Stamp Company : Stamp Certification Institute :
Signature : Remarks :
Model EXA PH202S
Title : Installation Drawing PH202S CSA
Number : FF1-PH202S-00 Page : 3 of 10
Revision : 5.4
Safe area
Vmax = 31.5 VoltDC
Imax = 100 mA
Pmax = 1.2 Watt
CSA certified
Power Supply
(HART compatible) )
Output
Supply
SENSOR(S)
terminals 11-19
+_G
SENSOR(S)
terminals 11-19
Hazardous area
Safe area
+_G
Protective
earth
Protective
earth
Intrinsically safe design
(pH/ORP-transmitter)
EXA PH202S
+
_
Load
Resistance
Imax = 100 mA
Vmax = 31.5 VoltDC
Hazardous area
Protective
earth
+
_
24 volts DC Nominal
Supply Voltage.
Intrinsically safe design
CSA Ex ia Class1, Div.1, Group C&D, T3C for ambient temp. < 55¡C
(pH/ORP-transmitter)
EXA PH202S
CSA certified
safety barrier or power supply
Suitable values are:
(HART compatible)
CSA Ex ia Class1, Div.1, Group C&D, T3C for ambient temp. < 55¡C
For electrical data:
see text below.
For electrical data:
see text below.
Suitable values are:
Sensor(s) are thermocouples, RTD s, passive resistive switch devices, or are CSA entity approved and meet
connection requirements.
Electrical data of the EXA PH202S.
- Supply and output circuit (terminals + and -):
Maximum input voltage V
max
= 31.5 V.
Maximum input current I
max
= 100 mA.
Effective internal capacitance C
i
= 22 nF.
Effective internal inductance L
i
= 22 µH.
- Sensor input circuit (terminals 11 through 19):
Maximum output voltage V
oc
= 14.4 V.
Maximum output current I
sc
= 32.3 mA.
Maximum allowed external capacitance Ca = 600 nF.
Maximum allowed external inductance La = 36 mH.
Barriers and power supply should be CSA certified. The specifications must not exceed the maximum values as
shown in the diagram above.
Installation should be in accordance with Canadian Electrical Code, Part I or CEC, Part I.
Maximum safe area voltage should not exceed 250 V
RMS
.
The Hand Held Communicator must be of a CSA certified intrinsically safe type in case it is used on the
intrinsically safe circuit in the hazardous area.
YOKOGAWA EUROPE B.V.
Date : 01/07/2004
IM 12B6C3-E-E
Specification 2-7
Stamp Company : Stamp Certification Institute :
Signature : Remarks :
Model EXA PH202S
Title : Installation Drawing PH202S CSA
Number : FF1-PH202S-00 Page : 4 of 10
Revision : 5.4
YOKOGAWA EUROPE B.V.
Date : 01/07/2004
Sensor(s) are a thermocouple, RTD’s, passive resistive switch devices, or is CSA entity
approved and meet connection requirements.
Electrical data of the EXA PH202S-F & PH202S-P:
- Supply and output circuit::
Maximum input voltage Vmax=24 V or Maximum input voltage Vmax=17.5 V
Maximum input current Imax=250 mA Maximum input current Imax=380 mA
Maximum input power Pmax=1.2 W Maximum input power Pmax=5.32 W
Effective internal capacitance Ci=737 pF; Ef fective internal inductance Li=2.6
µH.
- Sensor input circuit:
Maximum output voltage Voc=14.4V; Maximum output current Isc=32.3 mA
Maximum allowed external capacitance Ca=600 nF
Maximum allowed external inductance La=36 mH
Any CSA approved I.S. interface m ay be used that meets the following requirements:
Vmax
24 V or Vmax 17.5 V
Imax
250 mA Imax 380mA
Pmax
1.2 W Pmax 5.32 W
Ca
? 737 pF + Ccable; La ? 2.6 µH + Lcable
Installation should be in accordance with Canadian Electrical Code, Part I or CEC, Part I.
Maximum safe area voltage should not exceed 250 Vrms.
Safe area
Hazardous area
Zone 1
Zone 0 or 1
Safe area
Apparatus
I.S.
interface
I.S.
certified
Terminator
EXA
PH202S-F
& PH202S-P
Sensor
Connections
V
m
ax
= 24 V or V
max
= 17,5 V
I
max
= 250 mA I
max
= 380 mA
P
m
ax
= 1,2 W P
max
= 5,32 W
CSA Ex ia Class I, DIV. 1, Group C&D
T3C for ambient temp.
55 ϒC
IM 12B6C3-E-E
2-8 Specification
Stamp Company : Stamp Certification Institute :
Signature : Remarks :
Model EXA PH202S
No revision to drawing without prior
FM Approval
Title : FM Control Drawing PH202S (Intrinsic Safety)
Number : FF1-PH202S-00 Page : 5 of 10
Revision : 5.4
Sensor(s)
terminals 11-19
Max. cablelength: 60 mtr.
Cable dia. : 3 12 mm.
Sensor(s)
terminals 11-19
Max. cablelength: 60 mtr.
Cable dia.: 3 12 mm.
n classified Location
FM Approved
Power Supply
(HART compatible)
Output
Supply
+_G
Classified Location
Unclassified Location
+_G
Protective
earth
Protective
earth
Intrinsically safe design
FM Class I, Div.1, Group ABCD, T3B for ambient temp. < 55¡C
T4 for ambient temp. < 40¡C
EXA PH202S analyser
+
-
Load
Resistance
Classified Location
Protective
earth
+
_
24 volts DC Nominal
Supply Voltage.
FM Approved safety barrier or
power supply
with Rint = 300
(HART compatible)
For electrical data:
see text below.
For electrical data:
see text below.
Intrinsically safe design
FM Class I, Div.1, Group ABCD, T3B for ambient temp. < 55¡C
T4 for ambient temp. < 40¡C
EXA PH202S analyser
Figure 1
Figure 2
Electrical data of the EXA PH202S :
- Supply circuit (terminals + and -): - Sensor input circuit (terminals 11 through 19):
Maximum input voltage V
max
= 31.5 V. Maximum output voltage V
t
= 14.4 V.
Maximum input current I
max
= 100 mA. Maximum output current I
t
= 32.3 mA.
Maximum input power P
i
= 1.2 W. Maximum allowed external capacitance C
a
= 600 nF.
Effective internal capacitance C
i
= 22 nF. Maximum allowed external inductance L
a
= 36 mH.
Effective internal inductance L
i
= 22 µH.
If Hand Held Terminal (HHT) is not connected to the power supply lines of the EXA PH202S (see figure 1):
Any FM Approved barrier or power supply may be used that meets the following requirements.
V
oc
or V
t
31.5 V; I
sc
or I
t
100 mA; C
a
22nF + C
cable
; L
a
22µH + L
cable
If HHT is connected to the power supply lines of the EXA PH202S (see figure 2):
The Hand Held Terminal must be FM Approved. Refer to the manufacturers control drawing of the HHT and the barrier/power
supply to determine the cable parameters.
(V
oc
or V
t
) + V
HHT
31.5 V; (I
sc
or I
t
) + I
HHT
100 mA; C
a
22nF + C
cable
+ C
HHT
; L
a
22µH + L
cable
+ L
HHT
When installing this equipment, follow the manufacturer s installation drawing.
Installation should be in accordance with ANSI/ISA RP 12.06.01 Installation of Intrinsically Safe Systems for Hazardous
(Classified) Locations and the National Electrical Code (ANSI/NFPA 70).
Control equipment connected to the barrier/power supply must not use or generate more than 250 Vrms
or Vdc.
Resistance between Intrinsically Safe Ground and earth ground must be less than 1.0 Ohm.
WARNING
- Substitution of components may impair Intrinsic Safety
- To prevent ignition of flammable or combustible atmospheres, disconnect power before servicing or read, understand
and adhere to the manufacturer s live maintenance procedures.
YOKOGAWA EUROPE B.V.
Date : 01/07/2004
IM 12B6C3-E-E
Specification 2-9
Stamp Company : Stamp Certification Institute :
Signature : Remarks :
Model EXA PH202S-N
No revision to drawing without prior
FM Approval
Title : FM Control Drawing PH202S-N (Non-incendive)
Number : FF1-PH202S-00 Page : 6 of 10
Revision : 5.4
Sensor(s)
terminals 11-19
Max. cablelength: 60 mtr.
Cable dia. : 31 2 mm.
Sensor(s)
terminals 11-19
Max. cablelength: 60 mtr.
Cable dia.: 3 12 mm
n classified Location
+_G
Classified Location
Unclassified Location
+_G
Protective
earth
Intrinsically safe design
FM Class I, Div.2, Group ABCD, T3B for ambient temp. < 55¡C
T4 for ambient temp. < 40¡C
EXA PH202S analyser
+
-
Load
Resistance
Classified Location
Protective
earth
FM Approved
power supply
Voc
¡Ü 31.5 VDC
For electrical data:
see text below.
For electrical data:
see text below.
Intrinsically safe design
FM Class I, Div.2, Group ABCD, T3B for ambient temp. < 55¡C
T4 for ambient temp. < 40¡C
EXA PH202S analyser
+
-
FM Approved
power supply
Voc
¡Ü 31.5 VDC
Electrical data of the EXA PH202S :
- Supply circuit (terminals + and -): - Sensor input circuit (terminals 11 through 19):
Maximum input voltage V
max
= 31.5 V. Maximum output voltage V
t
= 14.4 V.
Maximum input power Pi = 1.2 W Maximum output current I
t
= 32.3 mA.
Effective internal capacitance Ci = 22 nF Maximum allowed external capacitance C
a
= 600 nF.
Effective internal inductance Li = 22 H Maximum allowed external inductance L
a
= 36 mH.
The Hand Held Terminal must be FM Approved in case it is used in the classified location.
When installing this equipment, follow the manufacturers installation drawing. Installation shall be in accordance with Article
501.4(B) of the National Electrical Code (ANSI/NFPA 79).
Nonincendive field wiring may be installed in accordance with Article 501.4(B)(3)
Grounding shall be in accordance with Article 250 of the National Electrical code
WARNING
- Substitution of components may impair suitability for Division 2
- Do not remove or replace while circuit is live unless area is know to be non-hazardous
- Explosion Hazard — Do not disconnect equipment unless area is know to be non-hazardous
- Do not reset circuit breaker unless power has been removed from the equipment or the area is know to be non-
hazardous
YOKOGAWA EUROPE B.V.
Date : 01/07/2004
IM 12B6C3-E-E
2-10 Specification
Stamp Company : Stamp Certification Institute :
Signature : Remarks :
Model EXA PH202S-F & PH202S-P
No revision to drawing without prior
FM Approval
Title : FM Control Drawing PH202S-F & PH202S-P (Intrinsic safe Fisco
concept)
Number : FF1-PH202S-00 Page : 7 of 10
Revision : 5.4
YOKOGAWA EUROPE B.V.
Date : 01/07/2004
Sensor(s) are of a passive type to be regarded as ’simple apparatus’, devices which neither store nor
generate voltages over 1.5 V, currents over 0.1 A, power over 25 mW or energy over 20
µJ, or are FM
Approvals entity approved and meet connection requirements.
Electrical data of the EXA PH202S-F & PH202S-P:
- Supply circuit: Vmax=17,5 V; Imax=380 mA; Pi=5,32 W; Ci=737 pF; Li=2.6 µH.
- Sensor input circuit: Vt=14.4 V; It=32.3 mA; Ca=600 nF; La=36 mH
Any FM Approved FISCO barrier may be used that meets the following requirements:
Voc or Vt
17,5 V; Ioc or It 380 mA; Poc or Pt 5,32 W
When installing this equipment, follow the manufacturer s installation drawing.
Installation should be in accordance with ANSI/ISA RP 12 .06.01 Installation of Intrinsically Safe Systems for
Hazardous (Classified) Locations and the National Electrical Code (ANSI/NFPA 70).
Associated apparatus connected to the FISCO barrier must not use or generate more than 250 Vrms
o
r Vdc.
Resistance between FISCO Intrinsically Safe Ground and earth ground must be less than 1.0 Ohm.
The FISCO concept allows the interconnection of several I.S. apparatus not specifically examined in such
combination. The criterion for such interconnection is that the volta ge (Vmax), the current (Imax) and the
power (Pi) which I.S. apparatus can receive and remain intrinsically safe, considering faults, must be equal to
or greater that the voltage (Voc, Vt), the current (Ioc, It) and the power (Poc, Pt) which can be provided e by the
FM approved FISCO barrier. In addition, the maximum unprotected residual capacitance (Ci) and inductance
(Li) of each apparatus (other than the terminator) connected to the Fieldbus must be less than or equal to 5nF
and 10 H respectively.
In each I.S. Fieldbus segment only one active source, normally the FM Approved FISCO barrier, is allowed
to provide the necessary power for the Fieldbus system. All other equipment connected to the bus cable has to
be passive (not providing energy to the system), except to a leakage current of 50 A for each connected
device. Seperately powered equipment needs a galvanic isolation to insure that the I.S. Fieldbus circuit
remains passive.
The cable used to interconnect the devices needs to comply with the following parameters:
Loop resistance R : 15 150 /km; Inductance per unit length L : 0,4 1 mH/km
Capacitance per unit length C : 80 200 nF/km
(C = C line/line + 0,5 C line/screen if both line are floating)
(C = C line/line + C line/screen if the screen is connected to one line)
Length of spur cable: max. 30 m
Length of trunk cable: max. 1 km
Length of splice : max. 1 m
WARNING
- Substitution of components may impair Intrinsic Safety
- To prevent ignition of flammable or combustible atmospheres, disconnect power before servicing or read,
understand and adhere to the manufacturer s live maintenance procedures.
Unclassified Location
Classified Location
Division 1
FM Approved
FISCO barrier
Voc (Vt) ¡Ü17,5 V
Ioc (It)
¡Ü 380 mA
Poc (Pt)
¡Ü 5,32 W
FM Approved
Terminator
R = 90..100
C = 0..2,2 F
EXA
PH202S-F
& PH202S-P
Sensor
Connections
Max. cablelength: 60 mtr.
Cable dia. : 3 1 2 mm.
FM Class I, DIV. 1, Group ABCD
T3B for ambient temp.
55 ϒC
T4 for ambient tem
p
. 40 ϒC
IM 12B6C3-E-E
Specification 2-11
Stamp Company : Stamp Certification Institute :
Signature : Remarks :
Model EXA PH202S-F & PH202S-P
No revision to drawing without prior
FM Approval
Title : FM Control Drawing PH202S-F & PH202S-P (Intrinsic safe Entity
concept)
Number : FF1-PH202S-00 Page : 8 of 10
Revision : 5.4
YOKOGAWA EUROPE B.V.
Date : 01/07/2004
Sensor(s) are of a passive type to be regarded as ’simple apparatus’, devices which
neither store nor generate voltages over 1. 5 V, currents over 0.1 A, power over 25 mW or
energy over 20 µJ, or are FM Approvals entity approved and meet connection
requirements.
Electrical data of the EXA PH202S-F & PH202S-P:
- Supply circuit:
Maximum input voltage Vmax=24 V
Maximum input current Imax=250 mA
Maximum input power Pi=1.2 W
Effective internal capacitance Ci=737 pF; Effective internal inductance Li=2.6
µH.
- Sensor input circuit:
Maximum output voltage Vt=14.4 V; Maximum output current It= 32.3 mA
Maximum allowed external capacitance Ca=600 nF
Maximum allowed external inductance La= 36 mH
Any FM Approved barrier may be used that meets the following requirements:
Voc or Vt
24 V
Ioc or It 250 mA
Poc or Pt
1.2 W
Ca
? 737 pF + Ccable; La ? 2.6 µH + Lcable
When installing this equipment, follow the manufacturer s installation drawing.
Installation should be in accordance with ANSI/ISA RP 12.06.01 Installation of Intrinsically
Safe Systems for Hazardous (Classified) Locations and the National Electrical Code
(ANSI/NFPA 70).
Associated apparatus connected to the barrier must not use or generate more than
250 Vrms
or Vdc.
Resistance between Intrinsically Safe Ground and earth ground must be less than 1.0
Ohm.
WARNING
- Substitution of components may impair Intrinsic Safety
- To prevent ignition of flammable or combustible atmospheres, disconnect power
before servicing or read, understand and adhere to the manufacturer s live
maintenance procedures.
Unclassified Location
Classified Location
Division 1
FM Approved
barrier
Voc (Vt) ¡Ü24 V
Ioc (It)
¡Ü 250 mA
Poc (Pt)
¡Ü 1,2 W
Ca
¡Y 737pF+ Ccable
La
¡Y 2,6 H + Lcable
I.S.
certified
Terminator
EXA
PH202S-F
& PH202S-P
Sensor
Connections
Max. cablelength: 60 mtr.
Cable dia. : 3 1 2 mm.
FM Class I, DIV. 1, Group ABCD
T3B for ambient temp. 55 ϒC
T4 for ambient tem
p
. 40 ϒC
IM 12B6C3-E-E
2-12 Specification
Stamp Company : Stamp Certification Institute :
Signature : Remarks :
Model EXA PH202S-B & PH202S-D
No revision to drawing without prior
FM Approval
Title : FM Control Drawing PH202S-B & PH202S-D (Non-incendive Entity
concept)
Number : FF1-PH202S-00 Page : 10 of 10
Revision : 5.4
YOKOGAWA EUROPE B.V.
Date : 01/07/2004
Sensor(s) are of a passive type to be regarded as ’simple apparatus’, devices which neither store nor
generate voltages over 1.5 V, currents over 0.1 A, power over 25 mW or energy over 20
µJ, or are FM
Approvals entity approved and meet connection requirements.
Electrical data of the EXA PH202S-B & PH202S-D:
- Supply circuit: Vmax=32 V; Pi=1.2 W; Ci= 737 pF; Li= 2.6 H
- Sensor input circuit: Vt=14.4 V; It=32.3 mA; Ca=600 nF; La=36 mH
When installing this equipment, follow the manufacturers installation drawing.
Installation shall be in accordance with Article 501.4(B) of the National Electrical Code (ANSI/NFPA 79).
Nonincendive field wiring may be installed in accordance with Article 501.4(B)(3)
Grounding shall be in accordance with Article 250 of the National Electrical code.
WARNING
- Substitution of components may impair suitability for Division 2.
- Do not remove or replace while circuit is live unless area is know to be non -hazardous
- Explosion Hazard — Do not disconnect equipment unless area is know to be non -hazardous
- Do not reset circuit breaker unless power has been removed from the equipment or the area is know to be non -
hazardous
Unclassified Location
Classified Location
Division 2
FM Approved
Power Supply
Voc
¡Ü 32 VDC
FM Approved
Terminator
R = 90..100
C = 0..2,2 F
EXA
PH202S-B
& PH202S-D
Sensor
Connections
Max. cablelength: 60 mtr.
Cable dia.: 3 12 mm.
FM Class I, DIV. 2, Group ABCD
T3B for ambient temp.
55 ϒC
T4 for ambient tem
p
. 40 ϒC
IM 12B6C3-E-E
Specification 2-13
IM 12B6C3-E-E
3-1 Installation and wiring
3. INSTALLATION AND WIRING
3-1. Installation and dimensions
3-1-1. Installation site
The EXA converter is weatherproof and can be installed inside or outside. It should, however, be installed as close as possible to the sensor to avoid long cable runs between sensor and converter. In any case, the cable length should not exceed 50 meters (162 feet). Select an installation site where:
Mechanical vibrations and shocks are negligible
No relay/power switches are in the direct environment
Access is possible to the cable glands (see figure 3-1)
The transmitter is not mounted in direct sunlight or severe weather conditions
Maintenance procedures are possible (avoiding corrosive environments)
The ambient temperature and humidity of the installation environment must be within the limits of the instrument specifications. (See chapter 2).
3-1-2. Mounting methods
Refer to figures 3-2 and 3-3. Note that the EXA converter has universal mounting capabilities:
Panel mounting using two (2) self-tapping screws
Surface mounting on a plate (using bolts from the back)
Wall mounting on a bracket (for example, on a solid wall)
Pipe mounting using a bracket on a horizontal or vertical pipe (maximum pipe diameter 50 mm)
Fig. 3-2. Panel mounting diagramFig. 3-1. Housing dimensions and layout of
glands
Spacing panel cut-out dimension
162 (6.4)
180 (7)
30 (1.2)
77 (3)
115 (4.5)
56 ±0.2
(2.2”)
1/2” supply
M6 bolts (2X)
1/2” input
min. 203
(min. 8.0)
154
(6.06)
2x ø4 (0.16)
30 (1.18)
30 (1.18)
172
(6.77)
min. 229
(min. 9.0)
Unit: mm (inch)
IM 12B6C3-E-E
Figure 3-4. Internal view of EXA wiring compartment
Figure 3-3. Wall and pipe mounting diagram
Pipe mounting (vertical)
Wall mounting
Pipe mounting (horizontal)
2” ND. pipe
56
(2.20)
2x ø6.5
(0.26)
4x ø10
(0.4)
70
(2.75)
115
(4.5)
92
(3.6)
200
(7.87)
Option /U: universal pipe/wall mounting kit
Installation and wiring 3-2
IM 12B6C3-E-E
3-3 Installation and wiring
3-2. Preparation
Refer to figure 3-4. The power/output connections and the sensor connections should be made in accordance with the diagram on page 3-6. The terminals are of a plug in style for ease of mounting.
To open the EXA 202 for wiring:
1. Loosen the four frontplate screws and remove the cover.
2. The terminal strip is now visible.
3. Connect the power supply. Use the gland on the left for this cable.
4. Connect the sensor input, using the gland on the right (see fig. 3-5). Switch on the power. Commission the instrument as required or use the default settings.
5. Replace the cover and secure frontplate with the four screws.
6. Connect the grounding terminals tp protective earth.
7. The optional hose connection is used to guide the cables comming from an immersion fitting through aprotective plastic tubing to the transmitter.
3-2-1. Cables, terminals and glands
The PH202 is equipped with terminals suitable for the connection of finished cables in the size range: 0.13 to 2.5 mm (26 to 14 AWG). The glands will form a tight seal on cables with an outside diameter in the range of 7 to 12 mm (9/32 to 15/32 inches).
Figure 3-5. Glands to be used for cabling
SENSOR
CABLE GLAND
POWER/OUTPUT
CABLE GLAND
GROUNDING TERMINAL
Sensor cable gland
Power/Output cable gland
Grounding terminal
IM 12B6C3-E-E
Figure 3-6. System configuration
3-3. Wiring of sensors
3-3-1. General precautions
Generally, transmission of signals from pH sensors is at a very low voltage and high impedance level. Thus a lot of care must be taken to avoid interference. Before connecting sensor cables to the transmitter make sure that next conditions are met: – the sensor cables are not mounted in tracks together with high voltage and or power switching cables – only standard coaxial electrode cables or extension cable are used – the transmitter is mounted within the distance of the sensor cables (max. 10 m) – the setup is kept flexible for easy insertion and retraction of the sensors in the fitting.
3-3-2. Additional precautions for installations in hazardous areas
Make sure that the total of capacitances and inductances connected to the input terminals of the EXA PH202S do not exceed the limits given in the certificate. This sets a limit to the cable and extensions used. – The intrinsic safe version of the PH202S instrument can be mounted in Zone 1. – The sensors can be installed in Zone 0 or Zone 1 if a safety barrier according to the limits given in the
system certificate is used.
– Ensure that the total of capacitances and inductances connected to the terminals of the EXA PH202S do
not exceed the limits given in the certificate of the safety barrier or distributor. – The cable used should preferably have a BLUE colour or marking on the outside. – Installation for (sensors in Zone 0 or 1): Generally, the distributor with input/output isolation has no external earth connection. If there is an earth
connection on the distributor and the external connection of the transmitter is connected to “protective”
earth, the shield of the 2-wire cable may NOT be connected to “protective” earth at the distributor too.
1 2
18
0
10
0
0
NO MODEYES
>
ENT
>
FAILHOLD
YES
NO
ENT
MEASURE
MAN.CAL DISPLAY
HOLD
YOKOGAWA
MODE
TEMP
AUT.CAL
TEMP.MAN.
pH
Sensors
Recorder
Distributor
Computer
Hand Held Communicator
Output/supply
Input
2 , 5 or 10 m
Safety Barrier PH202S only
CURRENT OUTPUT
ref
pH/ORP temp.
Installation and wiring 3-4
IM 12B6C3-E-E
3-5 Installation and wiring
3-3-3. Installation in: Hazardous Area-Non-Incendive
The EXA PH202S-N may be installed in a Category 3/ Zone 2/ Div.2 area without the use of safety barriers. Maximum permissible supply voltage 31.5V
3-3-4. Liquid earth
In all circumstances, the sensor side of the measuring loop must be grounded to the measuring liquid. The EXA PH202S uses advanced differential high impedance input circuits. This technique calls for a grounding to the liquid. In addition to that the sensor checking circuits also use the liquid earth for measurement of impedance of the sensors. All Yokogawa fittings have provisions for this connection. It is usually called liquid earth in all our manuals. A separate connection should be made to the terminal numbered 14 in all cases to get a proper and stable measuring loop.
3-3-5. Access to terminal and cable entry
1. To access terminals remove the front cover of the EXA PH202S by releasing the 4 captive screws.
2. Thread the sensor cables into the connection space and connect the cables to the terminals as indicated in the wiring diagram. Make sure all connections are firm and do not touch each other.
3. Screw the gland securely and tighten it to keep out moisture. DO NOT use a wrench to tighten the nut.
4. The optional hose connection is used to guide the cables coming from an immersion fitting through a protective plastic tubing to the transmitter.
3-4. Wiring of power supply
3-4-1. General precautions
Do not activate the power supply yet. First make sure that the DC-power supply is according to the specifications given.
DO NOT USE ALTERNATING CURRENT OR MAINS POWER SUPPLY! !
The cable leading to the distributor (power supply) or safety barrier transports power to and output signal from the transmitter. Use a two conductor shielded cable with a size of at least 1.25 mm
2
and an outside diameter of 7 to 12 mm. The cable gland supplied with the instrument accepts these diameters. The maximum length of the cable is 2000 metre, or 1500 metres when using the communications. This ensures the minimum operating voltage for the instrument.
Grounding:
• If the transmitter is mounted on a grounded surface (e.g. a metal frame fixed in the soil) the shield of the
2-wire cable may NOT be connected to ground at the distributor.
• If the transmitter is mounted on a non-conducting surface (e.g. a brick wall) it is recommended to ground
the shield of the 2-wire cable at the distributor end.
WARNING
IM 12B6C3-E-E
3-4-2. Connection of the power supply
The terminal strip is accessed as was described in §3-2-1. Use the left-hand gland to insert the supply/ output cable to the transmitter. Connect the supply to the terminals marked +, - and G as is indicated in figures 3-8 and 3-9.
3-4-3. Switching the instrument on
After all connections are made and checked, the power can be switched on from the distributor. Observe the correct activation of the instrument at the display. If for any reason the display does not indicate a value, consult the trouble shooting section.
Red
ref
pH/ORP
temp.
Green
Yellow
Colour code
rd bl
rd bl bk wt
= = = =
red blue black white
11 12 14 17 13
15 16HIGH I
MPLOW IMP
TEMP LE INPUT 2 INPUT
1
rd bl
SINGLE ELECTRODES
CONNECTION DIAGRAM FOR SENSORS
Blue
Combi pH/Ref
Comb
i
Orp/Re
f
temp.
Green
Colour code
COMBINED ELECTRODES
rd
bk
11 12 14 17 13
15 16HIGH I
MPLOW IMP
TEMP LE INPUT 2 INPUT
1
wtbl
bl
rd
bk
bl rd
rd bl bk wt
= = = =
red blue black white
12B6C3-06
CONNECTION DIAGRAM FOR SENSOR
link
link
Fig. 3-7. Connection diagrams
ORP/Ref
Installation and wiring 3-6
IM 12B6C3-E-E
3-7 Installation and wiring
3-5. Wiring the sensor system
3-5-1. Impedance measurement jumper settings
NOTE: It is important to decide first which application and which settings are appropriate for the installation. This decision is best made before the jumpers are installed, because the cables will rest beside the jumpers in their installed positions.
Table 3-1. Impedance measuring jumpers
Figure no. Jumper Settings Jumper Settings Application & Sensor Connections
Input #1 Input #2
1 High Impedance Low Impedance Normal pH sensors Glass sensor on Input #1 Reference sensor on Input #2
2 High Impedance High Impedance Special electrodes using 2 glass sensors (e.g. Pfaudler 18)
3 Low Impedance High Impedance ORP (pH compensated) and/or rH metal sensor on Input #1 pH glass (as reference) on Input #2
4 Low Impedance Low Impedance ORP (Redox measurement) metal sensor on Input #1 Normal reference on Input #2
For convenience insulated jumper links are provided. Ordinary wire links can also be used, and are just as effective.
The following four jumper figure illustrations (figure 3-8) show the jumper positions related to the figure numbers in the above table.
11 12 14 17 13 15 16
HIGH IMPLOW IMP
HART SUPPLY TEMP LE
INPUT 2
INPUT 1
11 12 14 17 13 15 16
HIGH IMP
LOW IMP
HART SUPPLY TEMP LE INPUT 2 INPUT 1
11 12 14 17 13 15 16
HIGH IMP
LOW IMP
HART SUPPLY TEMP LE
INPUT 2
INPUT
1
11 12 14 17 13 15 16
HIGH IMP
LOW IMP
HART SUPPLY TEMP LE
INPUT 2 INPUT 1
1
2
3
4
Fig. 3-8. Jumper positions
IM 12B6C3-E-E
Figure 3-9. Terminal identification labels
3-6. Sensor wiring
Refer to figure 3-10, which includes drawings that outline sensor wiring.
The EXA analyzers can be used with a wide range of commercially available sensor types, both from Yokogawa and other manufacturers. The sensor systems from Yokogawa fall into two categories; the ones that use a fixed cable and the ones with separate cables.
To connect sensors with fixed cables, simply match the terminal numbers in the instrument with the identification numbers in the instrument on the cable ends.
The separate sensors and cables are not numbered, but instead use a color-coding system. The electrodes have a colored band incorporated in the label on the connection cap:
Red for measuring electrodes (both pH and ORP)
Yellow for reference electrodes
Blue for combined sensors with both measuring and reference elements in the same body
Green for temperature sensors
The recommended procedure is to color-code each end of the cables to match the sensors with the color strips provided with each cable. This provides a quick way to identify the ends of the cables belonging to a particular sensor when they are installed. (The procedure for fixing the identification labels is described in detail in the instruction sheet provided with the cable.)
11 12 14 17 13 15 16
HIGH IMPLOW IMP
HART SUPPLY TEMP LE INPUT 2 INPUT 1
Installation and wiring 3-8
3-9 Installation and wiring
IM 12B6C3-E-E
3-6-1. Connection cable
There are two types of connection cable, one for single sensors and one for combined sensors. The former is a coaxial cable and has only two connections.
Red to measuring element
Blue to screen (shield)
The latter is a triaxial cable with three connections, (it has an extra white wire termination) these wires are connected:
Red to measuring element
Blue to reference
White to screen (shield)
To connect the other sensor systems, follow the general pattern of the terminal connections as listed below: 11 & 12 Temperature compensation resistor input 13 Input no. 2 (normally the reference element) 17 Screen (shield) for input no. 2 14 Liquid earth (solution ground) connection 15 Input no. 1 (normally the measuring element) 16 Screen (shield) for input no. 1
Figure 3-10a. Sensor wiring
*
*
*
*
12B6B3-03/1
12B6B3-03/3
*
*
*
12B6B3-03/2
pH transmitter
Green
Yellow
Red
Cable markers
11 Temperature 12 Temperature 13 Reference 14 Solution ground 15 Glass (measure) 16 Shield 17 Shield
Red
Blue
Red
Black Red
Blue Blue
11 Temperature 12 Temperature 13 Reference 14 Solution ground 15 Glass (measure) 16 Shield 17 Shield
11 Temperature 12 Temperature 13 Reference 14 Solution ground 15 Glass (measure) 16 Shield 17
11 Temperature 12 Temperature 13 Reference 14 Solution ground 15 Glass (measure) 16 Shield 17 Shield
Combined pH/ref sensors
Cable markers
Red
Blue Blue Black
Red White
Green
Blue
FU20/FU25 4-in one sensor
Note: Connect cables to similarly marked terminals: 11 to 11, 12 to 12, etc.
Retractable sensor assembly PR20
(Also PD20, PF20 & PS20)
NOTE: Connect cables to similarly marked terminals: 11 to 11, 12 to 12, etc.
IM 12B6C3-E-E
Installation and wiring 3-10
Figure 3-10b. Sensor wiring
3-6-2. Sensor cable connection with special grommet
In order to seal multiple sensor cables into EXA, a special grommet is provided that is designed to accommodate one, two or three sensor cables (5 mm dia.) plus a liquid earth cable (2.5 mm dia.). In the pack with the grommet are blanking pieces to close any unused holes. When correctly assembled, the grommet maintains the IP65 (NEMA 4X) rating of the EXA PH202 housing.
Refer to figure 3-5 to assemble the grommet connections:
1. First remove the nut and standard rubber seal from the selected gland
2. Discard the seal. This will be replaced later by the special grommet
3. Thread the cables through the nut and the gland
4. Connect the cables to their designated terminals
5. Arrange the cables to avoid tangles and insert the grommet between the gland and the nut
6. The grommet is split to permit the cables to be mounted after connection. (This also ensures even length adjustment.)
7. Ensure that any unused holes are filled with the blanking pieces
8. Tighten the nut to form a firm seal. (Hand-tight is sufficient.)
NOTE: The special gland is intended to be used to seal the multiple cables from the Yokogawa flow fittings such as FF20 and FP20. The designated cables are WU20 sensor cables, which are approximately 5 mm (0.2 “) in diameter, and 82895002 liquid earth cables, which are approximately 2.5 mm (0.1 “) in diameter.
For sensor systems using a single cable, like the FU20 (FU25) and the PR20, PD20, PF20 and PS20, the standard gland will accommodate the cable adequately. Single cables between approximately 7 mm and 12 mm (0.28 “ and 0.47 “) can be sealed properly with these glands.
*
*
*
12B6B3-09 Separate electrodes ORP/REF Electrode
*
*
12B6B3-08
Combined ORP/pH Electrode
Separate electrodes
ORP/REF electrode
Red
Yellow
Cable markers
11 Temperature 12 Temperature 13 Reference 14 Solution ground 15 Metal (measure) 16 Shield 17 Shield
Red
Black
Red
Blue Blue
11 Temperature 12 Temperature 13 Reference 14 Solution ground(ORP) 15 pH 16 Shield 17
ORP/rH wiring
Note: ORP and or rH setting in service
code 02.
11 Temperature 12 Temperature 13 Reference 14 Solution ground 15 Metal (measure) 16 Shield 17 Shield
Blue
Blue
Red
White
Cable markers
Combined ORP/pH electrode
Notes
1. A temperature sensor maybe connected to 11 & 12, for temperature indication.
2. See section 5-3-1 for impedance checking of glass reference sensors.
IM 12B6C3-E-E
3-11 Installation and wiring
3-6-3. Sensor cable connections using junction box (BA10) and extension cable (WF10)
Where a convenient installation is not possible using the standard cables between sensors and converter, a junction box and extension cable may be used. The Yokogawa BA10 junction box and the WF10 extension cable should be used. These items are manufactured to a very high standard and are necessary to ensure that the specifications of the system are not compromised. The total cable length should not exceed 50 metres (e.g. 5 m fixed cable and 45 m extension cable). In the case of systems using dual high impedance sensors (e.g. Pfaudler 18), then the cable length is restricted to 20 metres (fixed cable only, no extension with WF10).
17 Overall Screen
11
12
12
13
14
14 16
15
13
14141615
17
11
17
11 Red
12 Blue
15 Core 16 Screen White Co-axial cable
13 Core 14 Screen
Brown Co-axial Cable
14 (screen)
17 (overall screen)
12 (blue)
11
(red)
13 (core
)
16 (screen
)
15 (core)
Co-axial cable
(white)
Co-axial cable
(brown)
WF10 Cable
EXA
pH TRANSMITTER / CONVERTER
11
12
13
14
15
16
17
11
12
13
14
15
16
17
Fig. 3-11. Connection of WF10 extension cable and BA10/BP10 junction box
NOTE: See page 3-12 for termination for WF10 cable in combination with EXA pH.
3-6-4. Connection VP type sensor
> Connect ions norm al
p
H
A-15 B-13 C­D-14 E-11 F-12 S-3 or 63
pH
ref
LE
temp
> Connections differential pH
A-15 B-14 C-13 D-17 E-11 F-12 S-3 or 63
pH
pH ref
LE
temp
IM 12B6C3-E-E
Installation and wiring 3-12
Extension cable may be purchased in bulk quantities, cut to length. Then it is necessary to terminate the cable as shown below.
Termination procedure for WF10 cable.
1. Slide 3 cm of heat shrink tube (9 x 1.5) over the cable end to be terminated.
2. Strip 9 cm of the outer (black) insulating material, taking care not to cut or damage internal cores.
3 cm
heat shrink
9 cm
remove insulation
Fig. 3-12a.
3. Remove loose copper screening, and cut off the cotton packing threads as short as possible.
4. Strip insulation from the last 3 cm of the brown, and the white coaxial cores.
3 cm
cotton threads
Fig. 3-12b.
5. Extract the coaxial cores from the braid, and trim off the black (low-noise) screening material as short as possible.
6. Insulate the overall screen and the 2 coaxial screens with suitable plastic tubing.
7. Strip and terminate all ends with suitable (crimp) terminals and identify with numbers as shown.
11 12
13
15
16 17
14
Fig. 3-12c.
8. Finally shrink the overall heat shrink tube into position.
IM 12B6C3-E-E
4-1 Operation
4. OPERATION; DISPLAY FUNCTIONS AND SETTING
4-1. Operator interface
This section provides an overview of the operation of the EXA operator interface. The basic procedures for obtaining access to the three levels of operation are described briefly. For a step-by-step guide to data entry, refer to the relevant section of this user’s manual. Figure 4-1 shows the EXA operator interface.
LEVEL 1: Maintenance
These functions are accessible by pushbutton through a flexible front cover window. The functions make up the normal day-to-day operations that an operator may be required to complete. Adjustment of the display and routine calibration are among the features accessible in this way. (See table 4-1).
LEVEL 2: Commissioning
A second menu is exposed when the EXA front cover is removed and the display board is revealed. Users gain access to this menu by pressing the button marked
*
in the lower right of the display board. This menu is used to set such values as the output ranges and hold features. It also gives access to the service menu. (See table 4-1).
LEVEL 3: Service
For more advanced configuration selections, press the button marked
*
, then press “NO” repeatedly until you reach SERVICE. Now push the “YES” button. Selecting and entering “Service Code” numbers in the commissioning menu provide access to the more advanced functions. An explanation of the Service Codes is listed in chapter 5 and an overview table is shown in chapter 10.
Table 4-1. Operations overview
Routine Function Chapter Maintenance AUT CA• Calibration with programmed buffer solutions 6 MAN CAL Calibration with other buffer solutions 6 SAMPLE Grab sample calibration 6 DISPLAY Read auxiliary data or set message display 4 MAN.IMP Manual start of impedance check 5 TEMP Select automatic or manual compensation 5 HOLD Switch hold on/off (when activated) 5 Commissioning RANGE Adjust the output range 5 SET HOLD Activate the hold function 5 Service SERVICE Fine tune the specialized functions of the 5 (Access to coded entries converter from the commissioning level)
NOTE: All three levels may be separately protected by a password. See Service Code 52 in chapter 5 Service Code table for details on setting passwords.
mA
IM 12B6C3-E-E
Operation 4-2
Figure 4-1. PH202 operator interface
4-2. Explanation of operating keys MODE key This key toggles between the measuring and maintenance modes. Press once to obtain
access to the maintenance function menu.
AUTO CAL MAN CAL DISPLAY SETPOINT WASH MAN.IMP TEMPERATURE HOLD Press again to return to the measuring mode (press twice when hold is activated)
YES/NO keys These are used to select choices from the menu.
YES is used to accept a menu selection.
NO is used to reject a selection, or to move ahead to the next option.
DATA ENTRY keys
( )
is used as a “cursor” key. Each press on this key moves the cursor or flashing digit
one place to the right. This is used to select the digit to be changed when entering numerical data.
is used to change the value of a selected digit. Each press on this key increases the
value by one unit. The value can not be decreased, so in order to obtain a lower value, increase past nine to zero, then increase to the required number.
When the required value has been set using the > & ^ keys, press ENT to confirm the
data entry. Please note that the EXA does not register any change of data until the ENT key is pressed.
* key This is the commissioning mode key. It is used to obtain access to the commissioning
menu. This can only be done with the cover removed or opened. Once this button has
been used to initiate the commissioning menu, follow the prompts and use the other keys
as described above.
OUTPUT SET HOLD
SERVICE
ENT
HOLD FAIL
YES NO
ENT
MAN.CAL
DISP LAY
HOLD
NO MODEYES
YOKOGAWA
MODE
TEMP
AUT.CA L
TEMP.MAN.
pH
mV
MEA SURE
12B6C3-13
FRONT EXA PH20
2
WASH
Output hold flag
Manual temperature compensation flag
Fail flag
Menu pointer flags
Commissioning function menu
Commissioning mode access key
Measure/Maintenance mode key
Broken line indicates area that can be seen through front cover
Adjustment keys > : Choose digit to
adjust ^ : Adjust digit ENT : Confirm change
Selection keys YES : Accept setting NO : Change setting
Key prompt flags
Message display
Main display
Units
IM 12B6C3-E-E
4-3 Operation
4-3. Setting passcodes
4-3-1. Passcode protection
In Service Code 52, EXA users can set passcode protection for each one of the three operating levels, or for any one or two of the three levels. This procedure should be completed after the initial commissioning (setup) of the instrument. The passcodes should then be recorded safely for future reference.
When passcodes have been set, the following additional steps are introduced to the configuration and programming operations:
Maintenance
Press MODE key. The display shows 000 and *PASS* Enter a 3-digit passcode as set in Service Code 52 to obtain access to the Maintenance Mode
Commissioning
Press
*
key. The display shows 000 and *PASS*
Enter a 3-digit passcode as set in Service Code 52 to obtain access to the Commissioning Mode.
Service
From the commissioning menu, select *Service by pressing YES key. The display shows 000 and *PASS* Enter a 3-digit passcode as set in Service Code 52 to obtain access to the Service Mode.
NOTE: See Service Code 52 for the setting of passcodes.
4-4. Display examples
The following pages show the sequence of button presses and screens displayed when working in some standard configurations.
More or less options will be made available by the configuration of some service codes. For instance the impedance measurement screens do not appear when impedance checking is switched off in service codes 03 and 04.
mA
IM 12B6C3-E-E
Operation 4-4
NO
YES
pH
pH
pH
YES
pH
YES
NO
pH
pH
pH
YES
(See Temp menu
Chapter 5)
YES NO
TEMP.
MODE
NO
YES
YES
NO
NO
NO
(See Auto calibration Chapter 6)
(See Manual calibration
Chapter 6)
YES
NO
YES NO
YES NO
MEASURE
MAN.CA
L
DISPLA
Y
HOLD
TEMP.
AUT.CA
L
MAN.CA
L
DISPLA
Y
AUT.CA
L
MAN.CA
L
(See Sample calibration Chapter 6)
pH
pH
pH
pH
pH
pH
NO
NO
Offset (as. pot. or zero point)
Efficiency
(slope)
Press YES to fix
the selected second
line of display
YES
NO
YES
NO
DISPLAY
NO
NO
NO
NO
Display Access
Impedance of input
1
Impedance of input
2
Process temperatur
e
Software release number
YES
YES
NO
YES
NO
YES
NO
YES
NO
DISPLAY
DISPLA
Y
DISPLA
Y
DISPLAY
NO
YES
(See Manual Impedanc
e
check Chapter 5)
NO
OUTPUT SET HOLD
SERVICE
ENT
FAIL
YES NO
ENT
MAN.CAL
DISPLAY
HOLD
NO MODEYES
YOKOGAWA
MODE
TEMP
AUT.CAL
TEMP.MAN.
pH
mV
MEASURE
DISPLAY
4-5. Display functions
4-5-1. Display functions pH (default)
IM 12B6C3-E-E
4-5 Operation
pH
pH
pH
NO
pH
pH
YES
NO
YES
NO
TEMP.
HOLD
NO
YES
YES
See Temp Menu chapter
5
See Hold Menu chapter
5
DATE
pH
pH
pH
TIME
CAL -1
VALU
E
Service Code 01 Set for pH
. Service Code 02 Set for ORP on parameter 2.
DISPLAY
DISPLA
Y
DISPLA
Y
DISPLA
Y
DISPLA
Y
"Logbook Scrolling"
Logbook data is availabl
e
only in instruments with
"PIN" for advanced function
The display can give informatio
n
about calibrations performe
d
with date and time.
The example below show
s
Asymmetry Potential
.
Scrolling of Data is also
available on Slope.
As Pot ORP
Impedance Input
1
Impedance Input 2
When these function
s
are enabled in Servic
e
Codes.
Measurin
g
Mod
e
As Po
t
Display
2
pH
YES
NO
DISPLAY
DISPLAY
DISPLA
Y
NO
NO
YES
NO
YES
NO
pH
pH
YES
DISPLAY
DISPLAY
DISPLAY
DISPLAY
DISPLA
Y
DISPLA
Y
YES
NO
NO
NO
NO
NO
NO
pH
NO
MODE
NO
NO
YES
YES
YES
YES
YES
YES
YES
NO
NO
NO
NO
pH
pH
pH
pH
YES
NO
YES
NO
YES
NO
YES
NO
pH
pH
pH
pH
pH
pH
MAN.CAL
MEASURE
MAN.CA
L
DISPLA
Y
HOLD
TEMP.
AUT.CA
L
AUT.CAL
DISPLAY
YES
NO
YES
NO
YES
NO
YES
NO
YES
NO
YES NO
ENT
YES NO
ENT
YES NO
ENT
YES NO
ENT
YES NO
ENT
NO
NO
YES
pH
NO
YES
See Man. Imp. Check chapter
5
Back to
the Top
YES
NO
4-5-2. Display functions pH (ORP)
mA
mA
IM 12B6C3-E-E
Operation 4-6
4-5-3. Display functions pH (rH)
pH
YES
NO
DISPLAY
TEMP.
HOLD
NO
YES
YES
NO
YES NO
See Hold Menu Chapter
5
See Temp Menu Chapter
5
YES
NO
pH
pH
MAN.CAL
NO
NO
YES
pH
MEASURE
MAN.CA
L
DISPLA
Y
HOLD
TEMP
.
AUT.CAL
NO
YES
AUT.CAL
NO
MODE
DISPLAY
NO
DISPLAY
DISPLAY
DISPLAY
mV
DISPLAY
DISPLAY
DISPLAY
DISPLAY
DISPLAY
NO
NO
NO
NO
NO
NO
mV
As Pot ORP
Impedance
Input
1
Impedance
Input
2
Softwar
e
Releas
e
Version
NO
Slope
pH Senso
r
As Po
t
pH Senso
r
YES
NO
YES
NO
YES
NO
YES
NO
YES
NO
YES
NO
pH
pH
pH
pH
pH
pH
NO
YES
NO
rH Display
Curren
t
Outpu
t
YES
NO
pH
pH
12B6B3-22
See Auto Cal Chapter
6
See Man Ca
l
Chapter 6
See Man Cal Chapter
6
YES
YES NO
YES NO
YES
YES
YES
pH
pH
pH
pH
Service Code 01 Set for pH. Service Code 02 Set to rH
on parameter 2.
NO
Temp Display
NO
NO
YES
pH
NO
YES
See Man. Imp.
check Chapter 5
mA
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IM 12B6C3-E-E
5-1 Parameter setting
5. PARAMETER SETTING
5-1. Maintenance mode
Standard operation of the EXA instrument involves use of the maintenance (or operating) mode to set up some of the parameters.
Access to the maintenance mode is available via the six keys that can be pressed through the flexible window in the instrument cover. Press the MODE-key once to enter this dialog mode. NOTE: At this stage the user will be prompted for pass code where this has been previously set up in service code 52 in chapter 5.
Automatic calibration See “calibration” section 6.
Manual calibration See “calibration” section 6.
Sample calibration See “calibration” section 6.
Display setting See “operation” section 4.
Manual impedance check See “parameter setting” §5-1-4 and §5-3-5 code 51.
Temperature Set automatic or manual compensation and adjust manual reading (when
pH is set in section 5 service code 01). See adjustment procedure in
§5-1-1. Set automatic reading (when ORP is set in Section 5, service code 01). See adjustment procedure §5-1-2.
Hold Manually switch on/off HOLD (when enabled in commissioning menu
section). See adjustment procedure in §5-1-3.
mA
IM 12B6C3-E-E
Parameter setting 5-2
5-1-1. Manual temperature selection and adjustment
pH selected in service code 01.
TEMP.MAN.
ENT
12B6C3-23
NO
YES
pH
AUT.CAL
YES
NO
pH
TEMP.
pH
OUTPUT SET HOLD
SERVICE
ENT
FAIL
NO MODEYES
YOKOGAWA
MODE
Measure
MODE
NO
NO
NO
NO
YES
NO
YES
pH
NO
YES
pH
NO
YES
(pH Selected in Service Code 01)
Use
keys to
adjust and enter manual temperature settin
g
IM 12B6C3-E-E
5-3 Parameter setting
5-1-2. Process temperature measuring in ORP mode
ORP selected in service code 01.
MODE
mV
OUTPUT SET HOLD
SERVICE
ENT
NO MODEYES
YOKOGAWA
MEASURE
12B6C3-24
NO
YES
mV
MAN.CAL
YES NO
TEMP.
mV
MODE
NO
NO
NO
YES
NO
YES
mV
NO
YES
mV
NO
YES
MEASURE
YES
NO
mV
YES
5.2 Process Temperature Measuring in ORP mode.
(ORP selected in Code 01)
Display return to measuring mode with temperature reading.
IM 12B6C3-E-E
Parameter setting 5-4
5-1-3. Manual activation of HOLD
MODE
pH
OUTPUT SET HOLD
SERVICE
ENT
NO MODEYES
YOKOGAWA
M E A S U R E
12B6C3-25
pH
AUT.CAL
YES
NO
pH
MODE
NO
NO
NO
YES
NO
YES
pH
pH
HOLD
YES
NO
5.3 Manual Activation of Hold.
Note: The HOLD feature must first be activated in the commissioning mode section 5.2.
2
YES
NO
MEASURE
NO
YES
pH
NO
YES
NO
HOLD
mA
IM 12B6C3-E-E
5-5 Parameter setting
5-1-4. Manual impedance check
12B6C3-36
NO
YES
pH
AUT.CAL
YES
NO
pH
MODE
NO
NO
NO
NO
YES
pH
YES
NO
NO
YES
pH
5-1-4. Manual Impedance Check
Return to measuring
mode after updating
impedance chec
k
Note: The manual impedance start is available when the sensor impedanc
e measurement is enabled in Service Code 3 and 4. This enables the impedance data to be updated immediately after a maintenance event (e.g. replacing an
electrode).
YES
MODE
pH
OUTPUT SET HOLD
SERVICE
ENT
NO MODEYES
YOKOGAWA
MEASURE
IM 12B6C3-E-E
Parameter setting 5-6
5-2. Commissioning mode
In order to obtain peak performance from the EXA, you must set it up for each custom application.
Output range mA output is set as default to 0 - 14 pH.
For enhanced resolution in more stable measuring processes, it may be desirable
to select 5 - 10 pH range, for example. Service codes 31 and 35 can be used to choose output function on mA output.
Hold The EXA transmitter has the ability to “hold” the output during maintenance
periods. This parameter should be set up to hold the last measured value, or a fixed value to suit the process.
Service This selection provides access to the service menu.
What follows are pictorial descriptions of typical frontplate pushbutton sequences for each parameter setting function. By following the simple YES/NO prompts and arrow keys, users can navigate through the process of setting range, hold and service functions.
mA
mA
IM 12B6C3-E-E
5-7 Parameter setting
5-2-1. Output range
NO
NO
NO
pH
pH
pH
pH
pH
pH
pH
pH
OUTPUT SET HOLD
SERVICE
ENT
MAN.CAL DISPL AY
HOLD
NO MODEYES
YOKOGAWA
MODE
TEMP
AUT.CAL
MEA SURE
Output Range
12B6C3-26
YES
ENT
YES
NO
pH
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
YES
NO
YES
NO
YES
NO
YES
Note: When rH or ORP is enabled in codes 02 and 31, the output range is set in a similar way to pH
.
mA
IM 12B6C3-E-E
Parameter setting 5-8
5-2-2. Hold
YES
NO
YES
NO
YES
NO
YES
NO
NO
12B6C3-27
YES
YES
NO
YES
NO
YES
NO
YES
NO
YES
YES
NO
Hold
HOLD active last measured
value.
HOLD deactivated, retur
n
to commissioning menu.
HOLD
YES
HOLD
pH
OUTPUT SET HOLD
SERVICE
ENT
MAN.CAL DISPL AY
HOLD
NO MODEYES
YOKOGAWA
MODE
TEMP
AUT.CAL
MEA SURE
YES
NO
NO
NO
mA
IM 12B6C3-E-E
5-9 Parameter setting
YES
NO
ENT
HOLD
HOLD value set, return to commissioning menu
.
HOLD
ENT
HOLD
ENT
HOLD
ENT
YES
Set HOLD "fixed value" for mA1
.
Set HOLD “fixed value” for mA Output
IM 12B6C3-E-E
Parameter setting 5-10
5-2-3. Service
ENT
YES
NO
YES
NO
YES
NO
NO
NO
NO
12B6C3-29
Service
ENT
ENT
ENT
YES
ENT
ENT
Example: Service Code 01
Select main parameter
for pH
for ORP
With the
>, ,ENT keys
>
ENT
pH
OUTPUT SET HOLD
SERVICE
ENT
MAN.CAL DISPLA Y
HOLD
NO MODEYES
YOKOGAWA
MODE
TEMP
AUT.CA
L
MEA SURE
Wait screen is displayed briefly before returning to commissionning menu
.
Wait screen is displayed briefly before returning to commissioning menu.
mA
mA
IM 12B6C3-E-E
5-3-1. Parameter specific functions
Code 1 pH/ORP Choose the main measuring parameter. The option of the ORP input is used with
an inert metal electrode as measuring sensor which gives a reading directly in millivolts. This signal can then be interpreted to give information about the oxidation state of the process solution, and derived information like the absence of a compound (like Cyanide for example which is destroyed in oxidizing solutions).
Code 2 PRM.2 Enable the use of a second measuring parameter simultaneously with pH (the
main parameter). With the correct sensor (e.g FU20), ORP measurement is possible as parameter 2 With the same sensor, rH measurement is possible as parameter 2, this is calculated from pH and ORP and is a value which gives the oxidizing power of the solution while compensating for the effect of pH.
This function is particularly useful for applications where both the pH and
oxidation-reduction potential of the process need to be known. The availability of both measurements in a single system is convenient.
Note that in both cases a suitable sensor combination is needed to make this
possible. The Yokogawa FU20 (4-in-1) sensor can be used for this purpose, or a combination of individual sensors. Contact your local Yokogawa sales office for advice regarding applications and sensor selection.
Code 3 & 4 Z1.CHK & The EXA PH202 has an impedance check capable of monitoring the impedance Z2.CHK of all sorts of sensor systems. In order to “fine tune” this diagnostic tool it is
necessary to set it up to match the sensors used. The default settings give a good setup for a conventional system comprising pH glass sensor and a reference electrode, either as individual electrodes or as a combination style sensor. The impedance limits will need to be adjusted to get the best from systems using heavy duty, or fast response electrodes.
The impedance measuring system has a very wide span requirement. As it can
measure in k and also in G (109) there are hardware switches to set high range (1M to 2 G) or low range (1k to 1M) measuring. As a default the system is set to measure high impedances on input 1 (the one normally used for the pH glass sensor input) and low impedances on input 2 (the one normally used for the reference input). Examples of where these settings need to be changed from the default, are Pfaudler enamel sensors which need two high impedance settings, and Platinum sensors with a standard reference, which need two low impedance settings.
The temperature compensation of the impedance measurement is for conven-
tional pH glass sensors. When other sensors are used, switch this feature off.
Code 5 CAL.CK The calibration checking feature, when enabled, gives security against entering
wrong calibration data. For example when aged sensors are due for replacement, the EXA flags an error message and prevents a calibration being completed where the subsequent measurement can only exhibit errors and drift.
Limits are set for the maximum permissible Asymmetry potential, and Slope.
5-11 Parameter setting
Parameter setting 5-12
Code Display Function Function detai• X Y Z Default values
Parameter specific functions
01 *PH.ORP Select main parameter pH 0
ORP 1
02 *PRM.2 Enable 2nd parameter Off 0 0 Off
ORP 1
rH 2
03 *Z1.CHK Impedance check 1 Low 0 1.1.1
High 1 High
Temp comp off 0
Temp comp on 1 On
Imp check off 0
Imp check on 1 On
*Z.L.x
Low impedance limit Press NO to step through choice of units, 1 M
x = None, K, M or G press YES to select units, then use the
>, ^ ENT keys to set the value
*Z.H.x High impedance limit Press NO to step through choice of units, 1 G
press YES to select units, then use the
>, ^ ENT keys to set the value
04 *Z2.CHK Low 0 0.0.1 Low
High 1
Temp comp off 0 Off
Temp comp on 1
Imp check off 0
Imp check on 1 On
*Z.L.x Low impedance limit Press NO to step through choice of units, 100
x = None, K, M or G press YES to select units, then use the
>, ^ ENT keys to set the value
*Z.H.x High impedance limit Press NO to step through choice of units, 200 k
press YES to select units, then use the
>, ^ ENT keys to set the value
05 *CAL.CK Calibration check Asymmetry check off 0 1.1
Asymmetry check on 1 On
Slope check off 0
Slope check on 1 On
06-09 Not used
IM 12B6C3-E-E
IM 12B6C3-E-E
5-13 Parameter setting
5-3-2. Temperature compensation and measuring functions.
Code 10 T.SENS Selection of the temperature compensation sensor. The default selection is
the Pt1000 Ohm sensor, which gives excellent precision with the two wire connections used. The other options give the flexibility to use a very wide range of other pH sensors.
Code 11 T.UNIT Celsius or Fahrenheit temperature scales can be selected to suit user preference.
Code 12 T.ADJ With the process temperature sensor at a stable known temperature, the
temperature reading is adjusted in the main display to correspond. The calibration is a zero adjustment to allow for the cable resistance, which will obviously vary with length.
The normal method is to immerse the sensor in a vessel with water in it, measure
the temperature with an accurate thermometer, and adjust the reading for agreement.
Code 13 T.COMP Process compensation automatically allows for changes in the pH or ORP of the
process with temperature. The characteristic of each process will be different, and the user should determine if this feature is to be activated, and what compensation figure to choose.
The compensation is given in pH per 10 °C or mV per 10 ºC.
Example: For pure water with an alkali dose, (e.g. boiler feed water) a coefficient
of approx. 0.35pH can be expected. However, applications vary and a simple test will determine what if any coefficient is suitable for the process.
IM 12B6C3-E-E
Parameter setting 5-14
Code Display Function Function detai• X Y Z Default values
Temperature measuring and compensation functions
10 *T.SENS Temperature sensor Pt1000 0 0 Pt1000
Pt100 1
3kBalco 2
5k1 3
8k55 4
350 5
6k8 6
PTC10k 7
11 *T.UNIT Display in °C or °F °C 0 0 °C
°F 1
12 *T.ADJ Calibrate temperature Adjust to allow for cable resistance None
13 *T.COMP Set temp comp Compensation for process changes off 0 0 Off
Compensation for process changes on 1
*T.COEF Adjust process TC Set for TC in pH per 10 °C -0.00 pH per
10 °C
14-19 Not used
IM 12B6C3-E-E
5-15 Parameter setting
5-3-3. Calibration functions
Code 20
t.SEC & These functions are used to determine the stability level demanded by the EXA as
pH acceptance criteria for the automatic calibration. The default settings give a good
calibration for general purpose electrode systems with a fast response. Where heavy duty electrodes are used, or when low temperatures are concerned, these values should be adjusted.
When adjusting these settings, the longer the time interval and the smaller the
pH change, the more stable will be the reading. However, it is important to bear in mind that the time taken to reach stability is an exponential function, and too ambitious a setting will cause the instrument to wait for a very long time before accepting a calibration.
Code 21 AS.LOW & Limit values for the drift of an electrode system before an error is signalled when AS.HI a calibration is done. These default values should be adjusted to suit the
application, this will be especially important with enamel or Antimony probes. In case in SC 27 the Asymmetry Potential is disabled and the Zero Point is used,
SC 21 is used for entering the limits of the Zero Point. ZR.LOW & Limit values for zeropoint, if enabled in Code 27. ZR.HI
Code 22 SL.LOW & Limit values for acceptable slope (sensitivity) calibrations. SL.HI
Code 23 ITP, SLOPE Values can be entered directly in this section. These data can be provided by the & ASPOT manufacturer of the probe, or by the users laboratory etc. They are determined
independently of the measuring loop.
NOTE: it is not necessary to enter this data in most cases as the EXA
automatically does this while performing a calibration. The feature is used in the case of special electrode systems and where calibration in the process environment is not possible.
Code 24, Buffer tables The following buffer calibration tables are programmed into the EXA. They are the 25, & 26 primary buffer standards according to NIST (formerly NBS) and various other
national standards. We strongly recommend the use of these buffer solutions as
they give the best buffer capacity, reliability and accuracy when calibrating.
Table 5-1.
pH 4 pH 7 pH 9 pH 4 pH 7 pH 9
0 °C 4.00 6.98 9.46 45 °C 4.05 6.83 9.04 5 °C 4.00 6.95 9.40 50 °C 4.06 6.83 9.01 10 °C 4.00 6.92 9.33 55 °C 4.08 6.83 8.99 15 °C 4.00 6.90 9.28 60 °C 4.09 6.84 8.96 20 °C 4.00 6.88 9.23 65 °C 4.11 6.84 8.94 25 °C 4.01 6.87 9.18 70 °C 4.13 6.85 8.92 30 °C 4.02 6.85 9.14 75 °C 4.15 6.85 8.90 35 °C 4.02 6.84 9.10 80 °C 4.16 6.86 8.89 40 °C 4.04 6.84 9.07
These tables may be adjusted in the case that the user wishes to use other
calibration solutions. The “name” of the buffer can be changed at the *BUF.ID
prompt. The other values can then be adjusted in sequence.
Code 27 Zero Point As an alternative to Asymmetry Potential, the Zero point can be used to define
and calibrate the EXA pH unit.
Note that this method conforms to the DIN standard for instruments
No. IEC 746-2.
IM 12B6C3-E-E
Parameter setting 5-16
Code Display Function Function detai• X Y Z Default values
Calibration functions
20 *
t.SEC Stability check time 5 sec.
*PH Stability check pH 0.02 pH
21 *AS.LOW As Pot low limit -120 mV
(As Pot) *AS.HI As Pot high limit 120 mV
21 *ZR.LOW Zero Point low limit 5.00 pH
(Zero) *ZR.HI Zero Point high limit 9.00 pH
22 *SL.LOW Slope low limit 70 %
*SL.HI Slope high limit 110 %
23 *ITP Set ITP Preset calibration data from manufacturer 7.00 pH
(pH) *SLOPE Set slope or from laboratory determinations. 100 %
*ASP.1D Set As Pot For the main parameter 0.0 mV
Press YES to confirm 0.1 mV resolution,
then set value with >, ^, ENT keys.
Press NO to change to *ASP.
*ASP Set As Pot For the main parameter
Press YES to confirm 1 mV resolution,
then set value with >, ^, ENT keys.
*ASPmV Set As Pot ORP For parameter 2 (when activated in
service code 02)
23 *ASP.1D Set As Pot (ORP) For the main parameter
(ORP) Press YES to confirm 0.1 mV resolution,
then set value with >, ^, ENT keys.
Press NO to change to *ASP.
*ASP Set As Pot For the main parameter
Press YES to confirm 1 mV resolution,
then set value with >, ^, ENT keys.
24 *BUF.ID Buffer table 4 Buffer tables to NIST (formerly NBS)
25 *BUF.ID Buffer table 7 (see section 10 for table details)
26 *BUF.ID Buffer table 9 User adjustable for special requirements
27 *ZERO.P Enable zero point in Disable zero point (enable As Pot) 0 0 Disabled
pH units Enable zero point (disable As Pot) 1
28-29 Not used
pH
mV
ITP
As pot
0 mV
0 ºC
10 ºC
25 ºC
12B6B3-12
ASYMMETRY POTENTIAL
mV
500
0
- 200 14
pH
ITP
Zero Point
0
7
Fig. 5-1.
IM 12B6C3-E-E
5-17 Parameter setting
5-3-4. mA output functions
Code 31 OUTP.F When pH is set in code 1 as the main parameter, the output functions may
be set as follows:­ pH pH (table) Parameter 2 (ORP or rH as set in code 02) When ORP is set in code 1 as the main parameter, the output functions
may be set to: ORP ORP (table)
Code 32 BURN Diagnostic error messages can signal a problem by sending the output
signals upscale or downscale (21 mA or 3.9 mA)*. This is called upscale or
downscale burnout, from the analogy with thermocouple failure signalling
of a burned-out or open circuit sensor. The pulse burnout setting gives a
21 mA signal for the first 30 seconds of an alarm condition. After the
“pulse” the signal returns to normal. This allows a latching alarm unit to
record the error. In the case of the EXA the diagnostics are extensive and
cover the whole range of possible sensor faults.
* Only when the HART communication is disabled the downscale output
signal is 3.6 mA. When HART communication is enabled the output signal
is 3.9 mA.
Code 35 TABLE The table function allows the configuration of an output curve by 21 steps (intervals of 5%). The following example shows how the table may be configured to linearise
the output with a mA curve.
Table 5-2.
4-20 mA 4-20 mA 0% 4.0 mA 50% 12.0 mA 5% 4.8 mA 55% 12.8 mA 10% 5.6 mA 60% 13.6 mA 15% 6.4 mA 65% 14.4 mA 20% 7.2 mA 70% 15.2 mA 25% 8.0 mA 75% 16.0 mA 30% 8.8 mA 80% 16.8 mA 35% 9.6 mA 85% 17.6 mA 40% 10.4 mA 90% 18.4 mA 45% 11.2 mA 95% 19.2 mA 100% 20.0 mA
mA
IM 12B6C3-E-E
Parameter setting 5-18
Code Display Function Function detai• X Y Z Default values
mA Outputs
30 Not used 31 *OUTP.F mA output functions pH 0 0 Code 01 set for pH pH (table) 1 Parameter 2 (with suitable sensor(s), 2 and when enabled in code 02) 32 *BURN Burn function No burnout 0 0 No Burn. Burnout downscale 1 Burnout upscale 2 Pulse burnout 3 33, 34 Not used 35 *TABLE Output table for mA *0% Linearisation table for mA1 in 5% steps. *5% The measured value is set in the main *10% display using the >, ^, ENT keys, for ... each of the 5% interval steps. ... Where a value is not known, that value may *90% be skipped, and a linear interpolation will *100% take place. 36-39 Not used
mA
IM 12B6C3-E-E
5-19 Parameter setting
5-3-5. User interface
Code 50 *RET. When Auto return is enabled, the converter reverts to the measuring mode from
anywhere in the configuration menus, when no button is pressed during the set time interval of 10 minutes.
Code 51 *MODE The manual impedance check (on demand) can be setup for operation in the
maintenance mode. (Through the closed front cover).
Code 52 *PASS Passcodes can be set on any or all of the access levels, to restrict access to the
instrument configuration.
Code 53 *Err.4.1 Error message configuration. Two different types of failure mode can be set.
Hard fail gives a steady FAIL flag in the display, A Fail signal is transmitted on the
outputs when enabled in code 32.
Soft fail gives a flashing FAIL flag in the display. The call for maintenance is
a good example of where a SOFT fail is useful. A warning that the regular maintenance is due, should not be used to shut down the whole measurement.
Code 54 Not used
Code 55 *CALL.M Call for maintenance is a trigger to signal that the system has been in service for
longer than the set time without calibration. The user can set up to 250 days as a routine service interval.
Code 56 *DISP The display resolution can be set to either 0.01pH or 0.1pH. Not applicable to the
ORP (mV) display.
IM 12B6C3-E-E
Parameter setting 5-20
Code Display Function Function detai• X Y Z Default values
User interface
50 *RET Auto return Auto return to measuring mode Off 0 Auto return to measuring mode On 1 1 On 51 *MODE Mode setup Manual impedance check Off 0 0 Off Manual impedance check On 1 52 *PASS Passcode Maintenance passcode Off 0 0.0.0 Off Note # = 0 - 9, where Maintenance passcode On # 0 = no passcode Commissioning passcode Off 0 Off 1=111, 2=333, 3=777 Commissioning passcode On # 4=888, 5=123, 6=957 Service passcode Off 0 Off 7=331, 8=546, 9=847 Service passcode On # 53 *Err.4.1 Error setting Impedance low (input 1) Soft fai• 0 Impedance low (input 1) Hard fai• 1 1 Hard *Err.5.1 Impedance high (input 1) Soft fai• 0 Impedance high (input 1) Hard fai• 1 1 Hard *Err.4.2 Impedance low (input 2) Soft fai• 0 Impedance low (input 2) Hard fai• 1 1 Hard *Err.5.2 Impedance high (input 2) Soft fai• 0 Impedance high (input 2) Hard fai• 1 1 Hard *Err.07 Temperature too high Soft fai• 0 Temperature too high Hard fai• 1 1 Hard *Err.08 Temperature too low Soft fai• 0 Temperature too low Hard fai• 1 1 Hard *Err.09 pH out of range Soft fai• 0 pH out of range Hard fai• 1 1 Hard *Err.11 Wash recovery check Soft fai• 0 0 Soft Wash recovery check Hard fai• 1 *Err.16 Call for maintenance Soft fai• 0 0 Soft Call for maintenance Hard fai• 1 54 Not used 55 *CALL.M Call for maintenance Set time limit for calibration Off 0 0 Off Set time limit for calibration On 1 56 *DISP Display resolution Set pH decimal display 0.1 pH 0 Set pH decimal display 0.01pH 1 1 0.01 pH 57-59 Not used
IM 12B6C3-E-E
5-21 Parameter setting
5-3-6. Communication setup
Code 60 *COMM. The settings should be adjusted to suit the communicating device connected to
the output. The communication can be set to HART or to PH201
*
B distributor
(for Japanese market only)
*ADDR. For the Yokogawa PC202 software package, the default settings match the
software as shipped.
Code 61 *HOUR The clock/calendar for the logbook is set for current date and time as reference. *MINUT *SECND *YEAR *MONTH *DAY
Code 62 *ERASE
Erase logbook function to clear the recorded data for a fresh start. This may be desirable when re-commissioning an instrument that has been out of service for a while.
5-3-7. General
Code 70 *LOAD The load defaults code allows the instrument to be returned to the default set up
with a single operation. This can be useful when wanting to change from one application to another.
Code 79 *CUST.D Load customer defaults. This code allows the instrument to be returned to the factory default set, except that buffer tables (code 24,25,26) are unchanged.
5-3-8. Test and setup mode
Code 80 *TEST The test mode is used to confirm the instrument setup. It is based on the factory
setup procedure and can be used to check the QIC (factory generated test certificate). To use this test feature it is necessary to have the detail provided only in the QIS (Quality Inspection Standard) or the Service manual.
NOTE: attempting to change data in service code, 80 and above without the proper instructions and
equipment, can result in corruption of the instrument setup, and will impair the performance of the unit.
mA
mA
IM 12B6C3-E-E
Parameter setting 5-22
Code Display Function Function detai• X Y Z Default values
Communication
60 *COMM. Communication Set communication Off 0 1.0 On Set communication On 1 write enable 0 write write protect 1 enable Set communication PH201*B 2 Without half time check 0 With half time check 1 *ADDR. Network address Set address 00 to 15 00 61 *HOUR Clock setup Adjust to current date and time using *MINUT >, ^ and ENT keys *SECND *YEAR *MONTH *DAY 62 *ERASE Erase logbook Press YES to clear logbook data 63-69 Not used
Code Display Function Function detai• X Y Z Default values
General
70 *LOAD Load defaults Reset configuration to default values 71-78 Not used 79 *CUST.D Load Customer Reset configuration to default values Defaults except buffer tables
Code Display Function Function detai• X Y Z Default values
Test and setup mode
80 *TEST Test and setup Built in test functions as detailed in QIS and Service Manual
mA
mA
IM 12B6C3-E-E
5-3-9. Notes for guidance in the use of service coded settings
5-23 Parameter setting
IM 12B6C3-E-E
Calibration 6-1
6. CALIBRATION
The EXA PH202 can be calibrated in three distinct ways.
6-1. Automatic calibration
This method uses internally programmed buffer tables, (from Service Codes 24, 25 and 26), to calculate the buffer value at the actual temperature during the calibration. In addition, the stability of the reading is automatically calculated, and when the reading has stabilized fully automatic adjustments of slope and asymmetry are made. This eliminates the question of how long the operator should allow prior to adjustment. A menu driven prompt system conducts the operator through the simple, foolproof routine.
Default settings for the buffer solutions are the standard NIST (formerly NBS) recognised solutions “4”, “7” and “9”. These are known as primary buffers. They have a much better buffer capacity than the “commercial” or adjusted buffers. Yokogawa strongly recommends the use of these buffers to provide the best pH calibration.
6-2. Manual calibration
In this method, the operator decides on the actual value to enter. Manual calibration is most often used for single-point adjustment of the asymmetry potential, by comparison method.
Manual calibration can also be used to perform a full 2-point calibration with solutions other than the NIST buffers that are listed in the calibration tables. In this case, the solutions are applied sequentially as in the AUT CAL method, but the user determines the adjustment of reading and stability.
NOTE: During manual calibration the temperature coefficient is still active. This means that the readings are referred to 25 °C. This makes grab sample calibration easy and accurate. However, if the manual calibration technique is used for buffer calibration, the temperature coefficient must be set to zero in maintenance mode in the “TEMP” routine (see chapter 5).
6-3. Sample calibration
The operator activates the “SAMPLE” calibration routine, at the same time as taking a representative process sample. After determining the pH of this sample by independent methods, (in the lab for example) the reading can be adjusted. While the sample is being analyzed, EXA holds the sample data in memory, while continuing to control and read pH normally.
6-4. Data entry
In special circumstances, users can directly enter the calibration data in the service code menu (see chapter
5). This is appropriate where the manufacturer provides calibration data for each probe (as with the Pfaudler sensors) or where electrodes are laboratory calibrated for subsequent installation on the plant. Service Code 23 allows the values of ITP, asymmetry potential (or zero point) and slope to be entered.
IM 12B6C3-E-E
6-2 Calibration
pH
pH
YES NO
YES NO
YES
NO
pH
YES NO
pH
NO
pH
YES
Press YES for single point (As Pot) adjustment
.
Press
NO to proceed to calibrate Slope.
The instruments waits for the reading to stabilize
.
(The pH display flashes
) When reading Is stable, the CAL END messag
e
appears.
Transfer to second buffer (pH4) and press YES
.
After briefly displaying WAIT, the display
returns to the normal readout.
The display now flashes th
e pH value. The instrument waits for the reading to stabilize
.
NO
YES
pH
NO
YES
pH
YES
pH
ENT
MAN.CAL
DISPLA Y
HOLD
NO MODEYES
YOKOGAWA
MODE
TEMP
AUT.CAL
MEAS URE
12B6C3-30
NO
YES
pH
Automatic Calibration Press the MODE key. AUT.CAL appears in the display, and the
YES/N
O key prompt flags flash. Press YES.
NEW.SNS: Display flashes YES/N
O
answer YES if new sensor fitted or
NO if not.
Care! YES resets logbook calibration data.
Insert the sensors in pH 7 buffer solution
.
Press YES to start calibration
.
NO
Note: To start calibration with another solution, press NO to cycle through the other options. "CAL 7"
NO "CAL 4" NO "CAL 9" NO
"CAL 7"
YES
When the reading is stable, the CAL END message appears. Press YES
.
After briefly displaying WAIT, the display returns to the normal readout
.
6-5. Calibration procedures
6-5-1. Automatic calibration
IM 12B6C3-E-E
Calibration 6-3
pH
HOLD
NO
YES
pH
YES
pH
HOLD
YES NO
pH
HOLD
pH
HOLD
HOLD
pH
NO
YES
12B6C3-31
NO
YES
pH
HOLD
pH
YES
NO
HOLD
pH
pH
HOLD
NO
YES
NO
YES
NO
YES
NO
YES
Automatic Calibration With Hold Active
Note: To start calibration with another solution, press NO to cycle through the other options. "CAL 7"
NO "CAL 4" NO "CAL 9" NO
"CAL 7"
The single
­point calibration is now complete. put sensors back in the process an
d
press NO
to switch off HOLD and return to measuring mode
.
Transfer to pH 4 buffer and press YES
.
The instrument then waits for the reading to stabilise. (The pH display flashes).
When the reading is stable, the CAL EN
D
message appears. Press YES
.
WAIT flashes briefly then HOLD
The calibration is now complete. Put the sensors back in the process and press
NO to turn off HOLD and return to the measuring mode.
NO
Press YES for single point (As Pot) adjustment. Press NO to proceed to calibrate Slope.
The instruments waits fo
r the reading to stabilise. (The pH display flashes
) When reading Is stable, the CAL END message appears.
YES
Press the MODE key. AUT.CAL appears in the display, and the
YES/N
O key prompt flags flash. Press YES.
NEW.SNS: Display flashes YES/N
O
answer YES if new sensor fitted or NO if not.
Care! YES resets logbook calibration data.
Insert the sensors in pH 7 buffer solution.
Press YES
to start calibration.
pH
ENT
MAN.CAL DISPLA
Y
HOLD
NO MODEYES
YOKOGAWA
MODE
TEMP
AUT.CA
L
MEAS URE
6-5-2. Automatic calibration with HOLD active
mA
IM 12B6C3-E-E
6-4 Calibration
pH
NO
YES
pH
NO
YES
YES
NO
YES
pH
YES
pH
pH
NO
YES
ENT
pH
pH
pH
pH
NO
YES
Put sensors in buffer solution. Press YES
.
Set the value using the
>, , ENT key.
Select the flashing digit with the
> key.
Increase its value by pressing th
e key.
When the correct value is displayed, press ENT to enter the change
.
>
>
12B6C3-32
pH
NO
YES
Manual Calibration. (2nd parameter calibration) Press the MODE key. The legend AUT.CAL appears,
and the YES/NO key prompt flags flash. Press NO
.
The display MAN.CAL appears.
Press YES to start calibration.
Press YES or NO at NEW.SNS prompt
.
YES
NO
For 2 point (As Pot and Slope)
Adjustment select second buf
fer
solution and adjust as for pH7 buf
fer.
NO
ENT
ENT
YES
WAIT is displayed briefly then EXA returns to measuring mode
.
pH
ENT
MAN.CAL DISPLA
Y
HOLD
NO MODEYES
YOKOGAWA
MODE
TEMP
AUT.CA
L
MEAS URE
6-5-3. Manual calibration (2nd parameter calibration)
IM 12B6C3-E-E
Calibration 6-5
IM 12B6C3-E-E
6-6 Calibration
pH
NO
YES
NO
YES
pH
pH
pH
NO
YES
12B6C3-34
pH
NO
YES
Sample Calibration.
Press the MODE key. The legend AUT.CAL appears, and the YES/NO
key prompt flags flash. Press NO
.
The display MAN.CAL appears.
Press NO.SAMPLE appears
YES
Press to start calibration
.
NO
YES
NO
YES
Press YES at the same time as taking sample for analysis.
PH 202 now continues to measure/control, as before. SAMPLE flashes to indicate that data is stored waiting for input of analyze
d
value.
pH
ENT
MAN.CAL DISPLA
Y
HOLD
NO MODEYES
YOKOGAWA
MODE
TEMP
AUT.CA
L
MEAS URE
6-5-4. Sample calibration
IM 12B6C3-E-E
Calibration 6-7
pH
NO
YES
MAN.CAL
NO
YES
pH
MAN.CAL
YES
ENT
pH
MAN.CAL
pH
NO
YES
MAN.CAL
YES
pH
NO
YES
Set the value using the
>, , ENT key. Select the flashing digit with the > key. Increase its value by pressing the
key.
When the correct value is displayed, press EN
T to enter the change.
>
>
YES
pH
NO
YES
pH
MODE
NO
pH
When the laboratory analysis is completed the data is entered by first pressing MODE, then following the sequence belo
w
Note: Display show
s the value as at the time of taking the sample
.
ENT
Return to maintenance
menu
NO
NO
pH
NO
YES
YES
pH
NO
YES
pH
NO
YES
pH
NO
YES
YES
NO
NO
pH
NOYES
pH
YES
Note: Display shows
the value as at the time
of taking the sample.
NO
For first calibration of a new sensor
YES
or
NO
or
To calibrate
ORP or rH
NO
YES
or
Return to maintenance menu
IM 12B6C3-E-E
IM 12B6C3-E-E
Maintenance 7-1
7. MAINTENANCE
7-1. Periodic maintenance for the EXA transmitter
The transmitter requires very little periodic maintenance. The housing is sealed to IP65 (NEMA 4X) standards, and remains closed in normal operation. Users are required only to make sure the front window is kept clean in order to permit a clear view of the display and allow proper operation of the pushbuttons. If the window becomes soiled, clean it using a soft damp cloth or soft tissue. To deal with more stubborn stains, a neutral detergent may be used.
NOTE: Never used harsh chemicals or solvents. In the event that the window becomes heavily stained or scratched, refer to the parts list (Chapter 9) for replacement part numbers.
When you must open the front cover and/or glands, make sure that the seals are clean and correctly fitted when the unit is reassembled in order to maintain the housing’s weatherproof integrity against water and water vapor. The pH measurement uses high impedance sensors and may otherwise be prone to problems caused by exposure of the circuitry to condensation.
The EXA analyzer contains a logbook feature which needs a clock to provide the timings. The EXA instrument contains a lithium cell (battery) to support the clock function when the power is switched off. This cell needs to be replaced at 5 yearly intervals (or when discharged). Contact your nearest Yokogawa service centre for spare parts and instructions.
7-2. Periodic maintenance for the sensor system
NOTE: Maintenance advice listed here is intentionally general in nature. Sensor maintenance is highly application specific.
The sensor system must be kept clean to function well. This may require regular cleaning of the electrodes. (The effect of dirty electrodes will be to slow the system response and perhaps corrupt the measuring loop entirely). The frequency of cleaning and the method of cleaning will depend entirely on the process.
Where a refillable (flowing electrolyte) reference system is employed, make sure that the reservoir is kept topped up. The rate of electrolyte consumption will again be process dependent, so experience will show how often you must refill.
The periodic recalibration of the sensor system is necessary to ensure best accuracy. This takes into account the aging of the sensors, and the nonrecoverable changes that take place. These processes are slow, however. If frequent recalibration is needed, it is usually because the cleaning process is not effective, the calibration is not well executed or the pH readings are temperature dependent. Monthly calibrations should be sufficient for most applications.
If a film remains on the pH sensor after cleaning, or if the reference junction is partly plugged, then measuring errors can be interpreted as a need for recalibration. Because these changes are reversible with correct cleaning and/or proper selection or adjustment of the electrolyte flow through the junction, make sure that these items are correct before recalibrating the system.
IM 12B6C3-E-E
7-2 maintenance
7-3. Calibration procedures are described in step-by-step detail in chapter 6. However, follow these guidelines.
1. Before starting a calibration, make sure the electrode system is properly cleaned so that electrodes are fully functional. They must then be rinsed with clean water to avoid contamination of the calibration solution.
2. Always use fresh buffer solutions to avoid the possibility of introducing errors from contaminated or aged solutions. Buffers supplied as liquids have a limited shelf life, especially alkaline buffers which absorb CO2 from the air.
3. Yokogawa strongly recommends NIST (primary) buffer standards in order to ensure the best accuracy and best buffer capacity is available. Commercially adjusted buffers (e.g. 7.00, 9.00 or 10.00pH) are a compromise as a standard, and are often supplied without the temperature dependency curve. Their stability will be much worse than for NIST solutions.
NOTE: NIST (formerly NBS) buffers are available as consumable items from any Yokogawa sales office under the following part numbers: 6C232 4.01 pH at 25°C} 6C237 6.87 pH at 25°C} A box contains 5 packets of powder. Each makes a 200 ml solution. 6C236 9.18 pH at 25°C}
IM 12B6C3-E-E
Troubleshooting 8-1
8. TROUBLESHOOTING
The EXA is a microprocessor-based analyzer that performs continuous self-diagnostics to verify that it is working correctly. Error messages resulting from faults in the microprocessor systems itself are few. Incorrect programming by the user can be corrected according to the limits set in the following text.
In addition, the EXA also checks the electrodes to establish whether they are still functioning within specified limits. The transmitter checks the glass-electrode impedance for a low value to determine if it is broken or cracked, and for a high impedance to check for internal breakage or disconnection.
The reference system is prone to more faults than the glass electrode in general. The unit measures the impedance value and compares it to the programmed value in memory to determine acceptance during testing. A high impedance signals pollution or poisoning of the reference electrode diaphragm.
Also, the EXA checks the electrodes during calibration to determine if the reaction time is suitable for pH measurement. A specially timed check can be activated following each cleaning cycle. After calibration, the unit checks the calculated asymmetry potential and the slope to determine if they are still within limits specified by the software.
The slow shift of asymmetry potential could signal a poisoning of the reference electrode system by the process. The decrease of slope equals a decrease of sensitivity of the glass electrode or can show a coating buildup at the electrode.
The EXA makes a distinction among diagnostic findings. All errors are signaled by the FAIL flag in the display. Only faults in the measuring circuit can be set as HARD FAIL, with “Burn-up or Burn-down” signals on the mA output.
What follows is a brief outline of some of the EXA troubleshooting procedures, followed by a detailed table of error codes with possible causes and remedies.
NOTE: The diagnostic function of the EXA gives a variable time interval between impedance checks, up to 5 minutes. When trouble shooting, a manual impedance check can be initiated by following the procedure in section 5-1-6.
IM 12B6C3-E-E
8-2 Troubleshooting
8-1. Diagnostics
8-1-1. Off-line calibration checks
The EXA transmitter incorporates a diagnostic check of the asymmetry potential after a calibration has been completed. This is a valid check for both manual and automatic calibration routines.
The actual value can be called up from the DISPLAY routine in the maintenance menu. A large value often indicates poisoning or pollution of the reference system used. If the asymmetry potential exceeds programmable limits, the EXA generates an error (E2).
The EXA also performs diagnostics to check for the slope of the pH electrode after automatic calibration is completed. The actual value of the slope can be called up on the DISPLAY routine in the maintenance menu (SL). This value is an indication of the age of the electrode. If the value stays within the limits of 70 to 110 percent of the theoretical value (59.16 mV/pH at 25°C), it is accepted. Otherwise, the unit generates an error (E3).
Activation or deactivation of the asymmetry diagnostic check and slope check is made from the Service Codes. See Chapter 5 or Chapter 10 (Appendix).
8-1-2. On-line impedance checks
The EXA has a sophisticated impedance checking system. The sensors can be checked for their impedance over a very wide range, which makes the tool equally useful for glass, enamel, reference and metal (ORP) sensors. The measurement is temperature compensated for the characteristic of the pH glass sensor.
In order to measure accurately over such a wide range, it is necessary to split the range into two. This is done by a pair of jumper settings, high range and low range can be set on either input, making the system extremely flexible.
The following error message table gives a list of problems that are indicated when the high or low impedance limits are exceeded for a sensor. Such things as fouling, breakage and cable faults are readily detected. The non-immersion of the sensors in the process fluid is also signalled.
IM 12B6C3-E-E
Troubleshooting 8-3
Table 8-1. Error Codes
Code Error description Possible cause Suggested remedy
E0 Buffer solution temperature Buffer solution too hot or too cold Adjust buffer temperature outside the programmed range Check cabling E1 Measurement failed to stabilize . Sensors fouled Clean sensors during the calibration Sensors too slow (aged sensor) Replace sensors E2 Asymmetry potential too high. Sensors are aged or polluted Check buffer solution (Limits set in service code 22.) Mistake in calibration Recalibrate at pH7 Replace sensor E3 Slope (sensitivity) is outside limits. Measuring sensor aged Replace measuring sensor (Limits set in service code 23.) Poor insulation at the connector Replace or dry cables E4.1 Impedance of input 1 too low. Measuring sensor broken Replace measuring sensor (Limits set in service code 03.) Damaged or damp connections Replace or dry cable E4.2 Impedance of input 2 too low. Reference sensor broken Replace reference sensor (Limits set in service code 04.) Damaged connections Replace cables E5.1 Impedance of input 1 too high. Measuring sensor disconnected Check connections (Limits set in service code 03.) Sensors not immersed in process Check process Liquid earth disconnected Check connections E5.2 Impedance of input 2 too high. Reference sensor fouled Clean or replace sensor (Limits set in service code 04.) Liquid earth disconnected Check sensor immersion Insufficient electrolyte Check electrolyte reservoir E7 Temperature sensor open Process too hot or too cold Check process > 1400C (or <-100C for 8k55) Wrong temperature sensor setting Check sensor & setting Temperature sensor damaged Check connections E8 Temperature sensor shortened Process too cold or too hot Check process < -30 0C (or > 120 0C for 8k55) Wrong temperature sensor used Check sensor & setting Temperature sensor damaged Check connections E9 Measurement out of range (-2 to 16 pH) Sensors disconnected Check cabling Sensor wrongly connected Check cabling Sensor(s) defective Replace sensor(s) E10 EEPROM write failure Fault in electronics Try again, if unsuccessful contact Yokogawa E11 Wash recovery check error Measuring sensor aged Replace measuring sensor (if communication is set to pH201*B in code Sensor still coated after washing Check cleaning system
60) Defective wash system If needed adjust timings E12 ORP / rH outside of preset limits Sensors disconnected or wrongly Check cabling connected E14 No valid calibration data. Data lost after switching from Recalibrate pH to ORP E15 Cable resistance to temperature Cable resistance too high Use Pt1000 sensor exceeds limit value. Corroded contacts Clean and reterminate Wrong sensor programmed Reprogram E16 Call for maintenance interval time exceeded. System not maintained in Perform maintenance preset time period Reset interval E17 Output span too small < 1pH Incorrect configuration by user Reprogram E18 Table values make no sense E19 Programmed values outside acceptable limits Incorrect configuration by user Reprogram E20 All programmed data lost Fault in electronics Contact Yokogawa Very severe interference E21 Checksum error Software problem Contact Yokogawa E23 Zeropoint outside limits Sensors are aged or polluted Check buffer solution Mistake in calibration Recalibrate at pH7 Replace sensor
mA mA
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9-1 Spareparts
9. SPARE PARTS
Table 9-1. Itemized parts list
Item No. Description Part no.
1 Cover assembly including window, gasket and fixing screws K1542JZ 2 Window K1542JN 3a Internal works assembly (general purpose) K1544DA 3b Internal works assembly (intrinsically safe) K1544DD 4 Digital (display) board K1544DH 5a Analog (input) board (general purpose) K1544PL 5b Analog (input) board (intrinsically safe) K1544PE 6 Ribbon cable K1544PH 7 Eeprom + latest software pH202 K1544BK 8 Lithium cell (battery) K1543AJ 9 Terminals (block of 3) K1544PF 10 Terminals (block of 5) K1544PG 11 Housing K1542JL 12 Gland set (one gland including seal and backing nut) K1500AU 13 HART
®
modem for communications to PC K1544WM
Options
/U Pipe and wall mounting hardware K1542KW /H Hood for sun protection K1542KG /SCT Stainless steel tag plate K1544ST
10
9
4
5a(b)
11
12
2
13
7
8
6
1
3a (b)
Fig. 9-1. Exploded view
IM 12B6C3-E-E
Appendix 10-1
10. APPENDIX
10-1. User setting table
FUNCTION SETTING DEFAULTS USER SETTINGS
Parameter specific functions
01 *PH.ORP 0 pH 02 *PRM2 0 Off 03 *Z1.CHK 1.1.1 High range, TC on check on, 04 *Z2.CHK 0.0.1 Low range, TC off check off no TC 05 *CAL.CK 1.1 AP on, Slope on
Temperature functions
10 *T.SENS 0 Pt1000 11 *T.UNIT 0 °C 12 *T.ADJ None 13 *T.COMP 0 Off *T.COEF -0.00 pH/10°C
Calibration functions
20 *t.SEC 5 Sec *pH 0.02 pH 21 *AP.LOW -120 mV *AP.HI 120 mV 22 *SL.LOW 70 % *SL.HI 110 % 23 *ITP 7.00 pH *SLOPE 100.0 % *ASP.1D 0.0 mV *ASP.mV mV 24 *BUF.ID 4 NIST 4 25 *BUF.ID 7 NIST 7 26 *BUF.ID 9 NIST 9 27 *ZERO.P 0 disabled
mA outputs
31 *OUTP.F 0 pH (ORP) 32 *BURN 0 off 35 *TABLE 21 pt table see code 31
mA mA mA
IM 12B6C3-E-E
10-2 Appendix
FUNCTION SETTING DEFAULTS USER SETTINGS
User interface
50 *RET 1 on 51 *MODE 0 off 52 *PASS 0.0.0 all off 53 *Err.4.1 1 hard fail *Err.5.1 1 hard fail *Err.4.2 1 hard fail *Err.5.2 1 hard fail *Err.07 1 hard fail *Err.08 1 hard fail *Err.09 1 hard fail *Err.11 0 soft fail *Err.16 0 soft fail 55 *CALL.M 0 250 days 56 *DISP 1 0.01 pH
Communication
60 *COMM. 0.1 off/write prot. *ADDR. 00 00 61 *HOUR 62 *ERASE
General
70 *LOAD 79 *CUST.D
Test and setup mode
80 *TEST
mA
mA
IM 12B6C3-E-E
Appendix 10-3
10-2. Configuration checklist for PH202G
Standard Configuration Options Reference for
change
Measured Variable(s)
primary inputs pH, ORP and Temp pH range 0-14 pH any span within -2-16 pH “output” pH range linearized disabled 21 point table codes 31& 35 ORP range -500 to 500 mV spans up to 3000 mV between “output”
-1500 to 1500mV Temperature range -30-140°C Temperature unit Celsius Fahrenheit code 11 mA Outputs analog output 4- 20 mA for pH pH/ORP/(parameter 2) code 01, 02, 31 output linearization disabled pH/ORP codes 35 Communication digital interface disabled HART 60 communication software externa• HHC or PC202 contact factory variables on display pH/ORP and temp pH/ORP, parameter 2, mA output “display” SL, AP, Z1, Z2 etc. burn out disabled burn low (3.9)/ high (22) on mA output code 32 password protection disabled for maint/ comm./ serv leve• code 52 autoreturn return to measure in 10 min. enable or disable code 50 add. functions in MAINT disabled Impedance check start code 51 Diagnostics impedance checking active enable or disable code 03 & 04 check on calibration data active enable or disable code 05 check on stability 0.02 pH per 5 s choose stability leve• code 20 display calibration log. enabled with logbook diagnostics setup codes 03, 04 & 05 Compatibility pH or ORP glass sensor/metal electrode pH or ORP code 01 temperature sensor Pt 1000 Pt1000; Pt100, etc code 10 other sensors enamel sensors (Pfaudler) ITP & impedance check setup codes 23, 03 & 04 2nd parameter disabled pH & ORP/ pH &rH code 02 manual temp. comp. disabled disable or enable “temp” Special Features buffer table configuration NIST standard fully configurable codes 24, 25 & 26 temperature calibration none adjustment +/- 20 °C code 12 zero point calibration disabled disable or enable code 27 call for maintenance set time interval 1 - 250 days code 55 HOLD during maintenance hold last or hold fix “hold” process temp. compensation disabled set temperature coefficient code 13 logbook disabled 2 x 50 events code 61, 62
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IM 12B6C3-E-E
10-4 Appendix
10-3. Setup for sensor compatibility
10-3-1. General
The inputs of the EXA transmitter are freely programmable for ease of installation. Standard glass pH electrodes, Ag/AgCl reference electrodes and Pt100 and Pt1000 temperature sensors need no special programming. The EXA indicates a fault with a signal in the display field if there is a mismatch of sensors in the connection.
10-3-2. Selection of measurement and reference electrode
The EXA PH202 is preprogrammed to accept industry standard glass electrodes and reference electrodes. The unit initiates checks for asymmetry and slope during calibration. The on-line impedance checking function has been upgraded in this most recent EXA release.
The EXA is universally compatible with all types of electrodes, such as enamel and antimony. In such systems, however, the specific isothermal point of intersection (ITP), slope (pH/mV) and asymmetry potential can be set for the type of electrode.
10-3-3. Selecting a temperature sensor
The EXA PH202 reaches its highest accuracy when used with the Pt1000 temperature sensor. This element offers a 10-fold increase in resistance dependence over the Pt100 sensor. Choice of temperature sensor is made in the Service Codes found in Chapter 5 of this manual.
ITP
Most Yokogawa sensor systems use an Iso-thermal point (ITP) of pH7 and a zero point at pH7. This
is the default condition for which the transmitter is set. It is only necessary to consider this adjustment when installing a system with a different ITP. Antimony systems and Pfaudler probes are good examples of systems with different ITP values. Service code 23 is used. This also permits the setting of calibration data for precalibrated sensors.
Temperature sensor
The Pt 100U RTD sensor is now becoming the most commonly used for temperature compensation.
The transmitter accepts inputs from several different temperature sensors to suit most sensor systems. Service code 10-19 are used to set the temperature parameters and the process temperature coefficient.
Temperature calibration
For best accuracy, the temperature sensor should be calibrated to compensate for connection cable
errors. See Service code 12.
pH Calibration
Traditionally, users select buffer solutions to suit the chosen output range. This is merely a continuation
of the days of analog instruments that used indicators driven by the mA output. With digital technology, it is better to choose good buffer solutions and make an effective calibration than to use commercial (adjusted) buffers which may have round number values, but are less effective buffers with lower buffer capacity. It is for this reason that Yokogawa recommends that the NIST 4, 7 and 9 standard buffers be used to calibrate solutions. The temperature responses of these are pre-programmed into Service codes 24, 25, and 26 in the EXA PH202. Where other buffers are used with the semi-automatic calibration function, their temperature response should be programmed into the relevant code.
IM 12B6C3-E-E
Appendix 10-5
10-4. Setup for other functions
Current outputs
Transmission signals for the measured parameters and FAIL signals can be set up in service codes 30
to 39.
Diagnostic Checks
Impedance checks, response time and stability checks are all included in the PH202. In order to get
the best performance from each of these features, the converter should be fine tuned according to experience in the installation, and for the particular sensors selected. Service codes 3, 4, 5 & 20 all contribute to the diagnostics. Please note that the default settings provide an excellent starting point and provide most valuable information about the performance of the electrode system.
Communications
The proprietary HART (FSK) communication link allows remote configuration and data retrieval through
the PC202 communication package. This is an excellent tool for the maintenance engineer, quality engineer or plant manager. Service codes 60-69 are used to set up the communications.
Logbook
In combination with the communications link, a “logbook” is available to keep an electronic record of
events such as error messages, calibrations and programmed data changes. By reference to this log, users can easily evaluate diagnostic information to determine predictive maintenance schedules. For example, by monitoring the deterioration in the slope of the pH sensor, it can be changed before a failure (or process shutdown) occurs.
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IM 12B6C3-E-E
10-6 Appendix
10-5. Set up for Pfaudler Type 18 sensor
The PH202 is intended to measure with all sorts of pH sensors, including the Pfaudler Type 18 sensor. The Pfaudler design of dual membrane system uses two enamels of differing sensitivity. The first a pH sensitive membrane, and the second one that responds to Na
+
and K+ and acts as a reference.
The analyzer has dual high impedance inputs which measure perfectly even with very high impedance sensors. However, the impedance measuring system (diagnostics) needs to be set up for best performance.
10-5-1. General set up
1. Set impedance measuring hardware. This is done by the use of links on the terminals adjacent to the input terminals. For the Pfaudler system, this means that the terminals should have the links disconnected in order to set for HIGH/HIGH impedance measuring.
2. Set the impedance check in software. Use codes 03 & 04 to enable the measurement and set for high impedance and configure appropriate limits.
Code 03 set to 1.0.1 Iow limit 1 Megaohm high limit 1 Gigaohm Code 04 set to 1.0.1 Iowlimit 1 Megaohm high limit 1 Gigaohm
3. Set the temperature compensation sensor as 100 Ohm Platinum RTD with service code 10.
Code 10 set to 1 100 Ohms Pt.
The system will now respond properly to the Pfaudler type 18 sensor, and the other functions of the EXA analyzer will need to be set in the normal way to suit the use to which the loop is being put. Output ranges, control functions and alarms should all be set as described elsewhere in this manual.
10-5-2. Calibration set up
4. The alternative Zero point (calibration and display) according to IEC 746-2 may be enabled in service code 27, and set in the MAN.CAL routine. A value of 10.5 pH is a good starting point for the Pfaudler 18 sensor.
5. Where lab test data are available for the sensor, service code 23 can be used to set values for ITP & Slope (and As pot for parameter 2 when enabled).
(This method can be useful for the type 18 sensor, as it is not usual to perform regular calibrations on this system as with normal sensors. This is because the system may well respond differently, to ordinary buffers, than with the process solutions. The procedure is to determine the temperature response (ITP) and the sensitivity (Slope) of the sensor, and enter these values in code 23.)
Because this is a rather complex procedure, it is recommended instead to use the default settings of ITP = 7.00, and Slope = 100 %, and make a single point (MAN.CAL) calibration in the process at the working temperature, and at the normal operating (control setpoint) pH. This ensures that the desired control point will be measured accurately, even if there may be small deviations when there is a big deviation from the setpoint. This of course has no effect on the accuracy of a control loop. The special construction of the Pfaudler sensor ensures that there is practically no drift in the calibration. All that is necessary is to keep the sensor membranes clean. This is best done by cleaning with low pressure steam, which restores the original condition of the sensor, including the original calibration values.
IM 12B6C3-E-E
Appendix 10-7
Display resolution Auto return Man. impedanc
e
Passcode
Hold on/off Hold type Hold valu
e
Manual temp valu
e
Manual temp
on/off
Temp. comp. Imp. chec
k
Imp. limits
Temp. comp Imp. chec
k
Buffer 4 name Buffer4 0º
C....80º C
Buffer 7 nam
e
Buffer7
0º C....80º C
Buffer9 nam
e
Buffer9
0º C....80º C
Maintenanc
e
Commissionin
g
Service
Process value Second process value Temperature % of output range
More
Status
Hold
Temp.Man
Logbook1 Logbook2
Ta
g
Unit
Device info
Param. Specific
Temp. Spec
Calibration Spec
.
Output function
Exa user interf
.
Manufacturer Distributor Model Meas. type etc.
etc.
Device setup
Primary value Analog outpu
t
Lower rangeval
.
Upper rangeval
.
Review
Stable time Stable pH
Zeropoint Aspot low limi
t
Aspot high limi
t
Slope low limi
t
Slope high limi
t
Buffer 4
Buffer
7
Buffer
9
table 0%.....
table 100%
Error 4.1.... Error 16
Timer on/off Reload valu
e
ON LINE MENU
Level 1 menu Level 2 menu Level 3 menu Level 4 menu Level 5 menu
Process variab.
Diag/Servic
e
Basic setup
Detailed Setu
p
Slope Aspot Aspot2 Imp1
Imp2
Date Descriptor Messag
e
Write protect
second
parameter
Impedance input1
Impedance input2
Calibration check Imp. limits Temp sensor Temp unit Temp comp. Temp coeff.
Stability
Aspo
t
Slop
e
ITP
Buffer
mA function Burn function
Table
Error programmin
g
Maintenance timer
Display
Slope value
10-6. Device Description (DD) menu structure
The Device Description (DD) is available from Yokogawa or the HART foundation. An example is shown below of the ON LINE menu structure. This manual makes no attempt to explain the operation of the Hand Held Communicator (HHC). For detailed operating instructions, refer to the HHC user’s manual and the on­line help structure.
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IM 12B6C3-E-E
10-8 Appendix
10-7. Field Change Order
Software changes of the PH202
10-7-1. Changes made by software release 1.1
- The hardware and software of the PH202 has been modified in order to make the instrument suitable for
8 temperature sensors.
- Software version 1.0 supports only the PCB suitable for 5 temp sensors.
- Software version 1.1 is prepared to handle both versions of transmitters (the 5 and 8 temperature sensor
PCB’s). The new release will recognize (auto detection) which version is used.
10-7-2. Changes made by software release 1.2
- In order to operate the PH202 in combination with the model 275 Hand-Held Communicator (HHC) from Fisher-Rosemount it is necessary that :
- the software of the PH202 is updated.
- the Model 275 is upgraded with the PH202-Device Description (DD).
- In case the instrument in programmed as pH device with second parameter rH-measurement enabled (Service code 02), the instrument returned with an inverted rH value. This calculation is now corrected in this software release.
- When MODE keypress during non-successful calibration (E0, E1, E2 ,E3), the error will be cleared instead of leaving the (soft) error active.
- In case a Sample is taken, the sample can be viewed. In this Sample view menu, the 2nd process value was the actual measured value instead of the wanted sample value. In this release, the sample value is shown correctly.
10-7-3. Changes made by software release 1.3
- Sample calibration did not work correctly in case the Temperature Coefficient (T.C.) is other than zero. -
The change in pH due to this T.C. was incorrectly interpreted as a direct aspot change.
- In case the passcode check was enabled, and an incorrect passcode was entered, this caused to stop functioning of the display and keyboard.
- Writing of instrument setting went wrong. Communication related update for handheld and PC202 operation. For PC202 operation with the PH202, this software version is necessary.
- In case manual temperature was enabled, any temperature error (E7, E8) was still displayed. the temperature errors should be cleared automatically in the case of a manual temperature value.
10-7-4. Changes made by software release 1.4
- A problem with Automatic Test Equipment during manufacturing was solved.
10-7-5. Changes made by software release 1.5
- The rH calculation was incorrect. There was a sign-error in the calculation formula. Also a 304mV offset voltage has been added in the calculation to make it right for a modern sensor. The rH calculation is correct now for a pH-sensor with a buffer solution of pH 7 and an Ag/AgCl/KCl reference system . The old calculation was based on a sensor with a buffer solution of pH 1 (with HCl reference system).
10-7-6. Changes made by software release 1.6
- Sensor check is switched OFF now during the start of CAL to prevent an unclear situation for the customer.
- Temperature errors were not switched OFF during MANTEMP.
- During INIT sometimes characters were missing in the messageline.
- During QIS the ORP measurement stops at 1220 mV. This has been changed so ORP can be measured up to 1500 mV. Also temperatures below -10 ºC were not shown correctly.
IM 12B6C3-E-E
Appendix 10-9
10-7-7. Changes made by software release 1.7
- Default * T.COEFF changed from 0.00 to -0.00.
- Error 5.1 occurs (instead of 4.1) if no sensor is connected.
- E12 can only occur if second process is ORP or rH.
10-7-8. Changes made by software release 1.8
- Communications with PH201
* B possible.
- Three new temperature sensors (DKK 350, 6K8 and NTC10K).
- Periodically unused errors are reset.
- Service 79 added for loading defaults excepts pH buffer tables.
- No longer PIN needed for communication and “logbook scrolling”.
10-7-9. Changes made by software release 1.9
- Enabling user to set Zero point limits in service code 21.
- mA table handling improved.
- Interpolation mA table improved.
- Communication with PH201
* B improved (WASH).
- High impedance limit raised to 2G (as described in IM).
10-7-10. Changes made by software release 2.0
- E20 is cleared after the programmed data was recovered.
10-7-11 Changes made by software release 3.0
- The maximum ORP span is set to 3000mV (was 2000mV) Communication is default set to enabled / write enabled
10-7-12 Changes made by software release 3.3
- The
NTC10k
was replaced by the
PTC10k.
10-7-13 Changes made by software release 3.4
- Updated internal tester identification range
.
10-7-14 Changes made by software release 3.5
- Fixed rare HART communication failure
.
10-7-15 Changes made by software release 3.6
- Solve problem with E4.1 / E5.1 impedance errors after loading all parameters from DCS
- Burn low value set to 3.6 mA, only selectable if HART-Communication is disabled
- Prevent incidental reset of the unit while loading default settings
- Prevent incidental communication problems with MH-02 PC-HART modem
10-7-15 Changes made by software release 3.7
- Implementation of Burn low in combination with HART changed.
IM 12B6C3-E-E
11-1 Test Certificate
Test EXA Series
Certificate Model PH202
Transmitter for pH / ORP
1. Introduction
This inspection procedure applies to the model PH202 converter. There is a serial number, unique to
the instrument, which is stored in non-volatile memory. Each time the converter is powered up, the serial number is shown in the display. An example is shown below, for details see the Users manual:
Unique Number
Line Number ATE (automatic test equipment no.) Month code Year code
2. General Inspection
Final testing begins with a visual inspection of the unit to ensure that all the relevant parts are present
and correctly fitted.
3. Safety Test
The (-) minus and the external ground terminal of the housing are connected to a Voltage generator
(100 VDC). The measured impedance value should be over 9.5 M.
Terminal 12 and the external ground terminal of the housing are connected to a Voltage generator
(500 VAC RMS) for 1 minute. The leakage current should remain below 8 mA.
4.1 Accuracy Testing
Our automated testing facility checks the accuracy of the dual high inputs of the instrument using a
calibrated variable resistor (decade resistor box) to simulate sensor mV’s.
4.2 Accuracy Testing of all supported temperature elements
Our automated testing facility checks the input accuracy of the instrument using a calibrated variable
resistor (decade resistor box) to simulate the resistance of all temperature elements.
11. Test Certificate
025
F70.00
IM 12B6C3-E-E
Test Certificate 11-2
4.3 Overall accuracy test
This test can be performed by the end-user to check the overall accuracy of the instrument. The data
specified on the Test certificate are results of the overall accuracy test performed during production and can be reproduced by performing similar tests with the following test equipment:
1. A variable resistor box 1 (resistor decade box) to simulate the temperate element. All tests are
performed simulating 25ºC (77 ºF).
1. A fixed resistor of 300
to simulate the mA-output load.
2. A millivolt source ranging from -1500 to +1500 mV with an accuracy of 0.1%.
2. A stabilised voltage supply unit : nominal 24 Volt DC
3. A current meter for DC currents up to 25 mA, resolution 1uA, accuracy 0.1%
3. A multimeter capable of measuring megohm ranges to check insulation impedance.
4. Screened cable to connect the input signals.
5. Single core flexible cable for liquid earth connection.
Connect the PH202 as shown in Figure 1. Set box 1 to simulate 25 ºC (1097,3
U for Pt1000)
Before starting the actual test, the PH202 and peripheral testing equipment has to be connected to the
power supply for at least 5 minutes, to assure the instrument is warmed up properly.
Figure 1. Connection diagram for the overall accuracy test
The tolerances specified relate to the performance of the PH202 with calibrated test equipment
under controlled test conditions (humidity, ambient temperature). Note that these accuracy’s are only reproducible when performed with similar test equipment under similar test conditions. Under other conditions, the accuracy and linearity of the test equipment will be different. The display may show values, which differ as much as 1% from those measured under controlled conditions.
4.4 Accuracy test mA output circuit
Our automated testing facility checks the output accuracy of the instrument with simulated
mA-output values.
IM 12B6C3-E-E
11-3 Test Certificate
IM 12B6C3-E-E
Glossary
GLOSSARY
pH (-log [H+] ) This is a logarithmic function of the Hydrogen ion activity (concentration).
This provides a quick indication of the acidic or alkaline behavior of a dilute solution. Normally measured on a scale of 0-14 pH where low numerical values are acidic (0 is approximately 1 Normal acid) and high numbers are alkaline (14 is approximately 1 Normal NaOH). The neutral point is pH 7.
Defined by Nernst in the following equation: E = Eo + RT/nF x Ln [H+]
E = measured potential R = gas constant T = absolute temperature n = valence F = Faraday number Ln = Napierian logarithm [H+] = activity of the Hydrogen ion Eo = Reference potential
ORP Oxidation reduction potential is a measure of oxidizing power of a solution.
The greater the milliVolt value with a negative polarity, the greater the oxidizing power. Reducing power is indicated by positive values of mV.
rH This is a composite value that indicates the oxidizing power of a solution
compensating for the influence of the acid or alkaline components. The scale is 0-55 rH, where oxidizing solutions provide the highest readings.
Asymmetry potential This is the difference between the isothermal point of intersection and the zero point.
Slope This is the sensitivity of the pH electrode (mV/pH) usually expressed as a % of the
theoretical value (Nernst).
ITP This is the isothermal point of intersection. This is the value in pH at which the
temperature response of the system is at a null point. In other words, the point of intersection of the temperature lines on a graph of millivolts vs pH. This point is critical to the correct operation of the temperature compensation circuitry.
Zero point This is the value of pH at which the electrode combination yields 0 mV as an output.
pH
mV
ITP
As pot
0 mV
0 ºC
10 ºC
25 ºC
12B6B3-12
ASYMMETRY POTENTIAL
mV
500
0
- 200 14
pH
ITP
Zero Point
0
7
IM 12B6C3-E-E Subject to change without notice
Printed in The Netherlands, 12-701 (A) I
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OKOGAWA
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Yokogawa has an extensive sales and distribution network. Please refer to the European website (www.yokogawa.com/eu) to contact your nearest representative.
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