This user’s manual describes the specications, installation, operation, maintenance, and
troubleshooting for Model FC500G Free Available Chlorine Analyzer. Read this manual
thoroughly to understand the contents before operating the equipment.
n Notes on Hardware
l Appearance and Accessories
Check the following when you receive the product:
• Appearance
• Standard accessories
Contact our sales representative or your local distributor if the product’s coating has come o, it
has been damaged, or there is shortage of required accessories.
l Model and Sux Codes
The name plate on the product contains the model and sux codes. Compare them with those in
the general specication to make sure the product is the correct one. If you have any questions,
contact our sales representative or your local distributor.
Safety, Protection, and Modication of the Product
n
• In order to protect the system controlled by the product and the product itself and ensure
safe operation, observe the safety precautions described in this user’s manual. We assume
no liability for safety if users fail to observe these instructions when operating the product.
• If this instrument is used in a manner not specified in this user’s manual, the protection
provided by this instrument may be impaired.
• Be sure to use the spare parts approved by Yokogawa Electric Corporation (hereafter simply
referred to as YOKOGAWA) when replacing parts or consumables.
• Modication of the product is strictly prohibited.
Signal Words
n
The following words are used in this manual.
CAUTION
This symbol gives information essential for understanding the operations and functions.
NOTE
This symbol indicates information that complements the present topic.
Notes on Handling User’s Manuals
n
• Please hand over the user’s manuals to your end users so that they can keep the user’s
manuals on hand for convenient reference.
• Please read the information thoroughly before using the product.
• The purpose of these user’s manuals is not to warrant that the product is well suited to any
particular purpose but rather to describe the functional details of the product.
• No part of the user’s manuals may be transferred or reproduced without prior written
consent from YOKOGAWA.
• YOKOGAWA reserves the right to make improvements in the user’s manuals and product at
any time, without notice or obligation.
• If you have any questions, or you nd mistakes or omissions in the user’s manuals, please
contact our sales representative or your local distributor.
Warning and Disclaimer
n
The product is provided on an “as is” basis. YOKOGAWA shall have neither liability nor
responsibility to any person or entity with respect to any direct or indirect loss or damage arising
from using the product or any defect of the product that YOKOGAWA can not predict in advance.
n Trademark Acknowledgments
• EXA FC is a trademark of Yokogawa Electric Corporation.
• All other company and product names mentioned in this user’s manual are trademarks or
registered trademarks of their respective companies.
• We do not use TM or ® mark to indicate those trademarks or registered trademarks in this
user’s manual.
IM 12F5A2-01E
After-sales Warranty
n Do not modify the product.
n During the warranty period, for repair under warranty consult the local sales
representative or service oce. Yokogawa will replace or repair any damaged
parts. Before consulting for repair under warranty, provide us with the model
name and serial number and a description of the problem. Any diagrams or
data explaining the problem would also be appreciated.
l If we replace the product with a new one, we won’t provide you with a repair report.
l Yokogawa warrants the product for the period stated in the pre-purchase quotation
Yokogawa shall conduct dened warranty service based on its standard. When the
customer site is located outside of the service area, a fee for dispatching the maintenance
engineer will be charged to the customer.
n In the following cases, customer will be charged repair fee regardless of
warranty period.
• Failure of components which are out of scope of warranty stated in instruction manual.
• Failure caused by usage of software, hardware or auxiliary equipment, which Yokogawa
Electric did not supply.
• Failure due to improper or insucient maintenance by user.
• Failure due to modication, misuse or outside-of-specications operation which Yokogawa
does not authorize.
• Failure due to power supply (voltage, frequency) being outside specications or abnormal.
• Failure caused by any usage out of scope of recommended usage.
• Any damage from re, earthquake, storms and oods, lightning, disturbances, riots, warfare,
radiation and other natural changes.
iii
n Yokogawa does not warrant conformance with the specic application at the
user site. Yokogawa will not bear direct/indirect responsibility for damage due
to a specic application.
n Yokogawa Electric will not bear responsibility when the user congures the
product into systems or resells the product.
n Maintenance service and supplying repair parts will be covered for ve years
after the production ends. For repair for this product, please contact the
nearest sales oce described in this instruction manual.
IM 12F5A2-01E
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Model FC500G
Free Available Chlorine Analyzer
(Non-Reagent Type)
8.2.6 Brush and Slip Ring (Part number: K9332JX, K9332JZ) .................. 8-2
Customer Maintenance Parts List .......................................... CMPL 12F5A2-01E
Revision Information ...............................................................................................i
IM 12F5A2-01E
<1. OVERVIEW>
1. OVERVIEW
Model FC500G Free Available Chlorine Analyzer (Non-Reagent Type) is used for continuous
measurement of free available chlorine in tap water distribution. This analyzer consists of a
detector and a converter as shown in Figure 1.1.
This chapter describes the FC500G free available chlorine analyzer specications and its
measuring principle.
Detector
Converter
1-1
Figure 1.1 Appearance of Model FC500G Free Available Chlorine Analyzer
IM 12F5A2-01E
<1. OVERVIEW>
1-2
1.1 Standard Specications
Measured Object: Free available chlorine contained in tap water
Measuring System: Polarographic method using rotating electrode
Measuring Ranges: 0 to 1 / 0 to 2 / 0 to 3 mg/L (Model FC500G-1)
0 to 5 / 0 to 10 mg/L (Model FC500G-5) (Air purge is necessary.)
Indication: Digital (3 1/2 LCD)
Output Signal: 4 to 20 mA DC (Load resistance: Maximum 500 Ω)
Operating pH Range of Sample Solution:
pH 6.5 to 7.5: For measured liquids whose pH exceeds the above limits,
error increases (refer to the following gure).
Sample Solution:
Temperature: 0 to 40°C (temperature compensation range 5 to 35°C).
Pressure: 1 to 30 kPa (for without VALVE)
1 to 150 kPa (with VALVE)
Flow Rate: 0.1 to 2.5 L/min (at tank inlet)
Conductivity: 100 to 300 μS/cm
SS (Suspended Solid): 10 mg/L or less
Air Purging (for only 0 to 5 / 0 to 10 mg/L Range)
Supply Air Pressure: About 50 to 140 kPa
Air Consumption: About 5 L/min
0 to 1 / 0 to 2 / 0 to 3 mg/L Switchable
0 to 5 / 0 to 10 mg/L Switchable
100 V ±10%, 50/60 Hz
110 V ±10%, 50/60 Hz
200 V ±10%, 50/60 Hz
220 V ±10%, 50/60 Hz
Without Valve
With Valve
IM 12F5A2-01E
<1. OVERVIEW>
1.3 External Dimensions
(1) With Inlet Valve (FC500G-¨¨¨1-E)
1-5
105131
52.5
Approx.150
Wiring inlet
3-Ø23 holes
Converter
4-Ø8.5 holes
for mounting
(U-bolt on bracket)
Approx.250
240
Cap
100
128.548
302226
22
5.5
Cable gland
space
Maintenance
17.5
52.5
70
(22)
22 22
108
0.50
mg/l
70
21
Outlet
Ø12 Nipple
2-inch pipe (Ø60.5)
265
(209)56
76
Cap
17.3
13.7
Outlet
Maintenance spaceMaintenance space
Approx.160
Mounting bracket
2.8
49.2
35
33.4
Inlet
Drain cock
Approx.
Driving
Box
Tub
150
space
Maintenance
295
310
154
50
Approx.
space
Maintenance
Purge air inlet
1/4-18 NPT
(for only FC500G-5-E)
Insert
Drain cock
Unit: mm
(48)(154)
Inlet
Ø6/Ø4 Union
(2) Without Inlet Valve (FC500G-¨¨¨0-E)
17.3
92
Maintenance spaceMaintenance space
Approx.160
2.8
49.2
35
33.4
Inlet
Drain cock
Driving
Box
Tub
10
Approx.150
Wiring inlet
3-Ø23 holes
Converter
100
128.5
3022
22
Cable gland
space
Approx.250
Maintenance
240
Cap
2-Ø8.5 holes
for mounting
22 22
0.50
(22)
Outlet
mg/l
Outlet
Ø12 Nipple
260
76
Cap
146.5(5.5)108
13.7
150
Approx.
17830
295
154
50
Approx.
space
Maintenance
Purge air inlet
1/4-18 NPT
(for only FC500G-5-E)
space
Maintenance
Insert
Drain cock
Unit: mm
75
4
Inlet
Ø6/Ø4 Union
Figure 1.4 Model FC500G Free Available Chlorine Analyzer External Dimensions
IM 12F5A2-01E
<1. OVERVIEW>
1-6
1.4 Measuring Principle
The FC500G free available chlorine analyzer (non-reagent type) is used for measuring
concentration of free available chlorine present in sample water, such as chlorine (Cl2)
hypochlorous acid (HClO), and hypochlorite ion (ClO-).
The measuring principle of this analyzer is analysis determination using the rotating electrode
polarographic method. Free available chlorine concentration is determined by measuring the
current (diusion current) which ows when free available chlorine is subjected to electrolytic
reduction by applying a voltage (applied voltage) between the indicator electrode (rotating
electrode) and the counter electrode. The applied voltage is set in a region where concentration
polarization occurs (plateau region) in polarography. In the plateau region, the diusion current
does not change even if the applied voltage changes.
In measurement practice, since the plateau region changes with free available chlorine
concentration, the applied voltage is compensated so that measurement can always be
performed in the plateau region. Also, since the diusion current is aected by the sample water
temperature, temperature is compensated using a temperature sensor (Pt1000Ω) incorporated in
the counter electrode.
Figure 1.5 shows the block diagram for the FC500G free available chlorine analyzer (nonreagent type) operation. The analyzer determines the free available chlorine concentration by
applying an applied voltage corresponding to the diusion current between the indicator and
counter electrodes and by applying temperature compensation to the diusion current.
First stage
amplifier
Applied voltage
compensating
pulse circuiut
Drain
Measuring
tank
Temperature
signal
Free available
chlorine
detecting circuit
Temperature
compensation
circuit
PWM circuit
isolator
Free available
chlorine/
conductivity
display
Voltage-current
conversion
circuit
Sample
water
Indicator
electrode
Diffusion current
Applied voltage
Counter
electrode
(Pt 1000Ω)
Figure 1.5 Block Diagram for FC500G Free Available Chlorine Analyzer Operation
4 to 20 mA DC
output
F1-5.ai
IM 12F5A2-01E
<2. COMPONENT NAMES AND FUNCTIONS>
2. COMPONENTS AND FUNCTIONS
2.1 Detector
Teflon (PTFE) ring
2-1
Beads case
Measuring tank
Electrode assembly
Measuring tank
Indicator electrode
(rotating elecrtrode)
Glass beads
Polishes the totating indicator
electrode to hold indicator
electrode in a clean state.
Cell motor
A motor for rotaing the
indicator electrode at a
constant speed.
Air purge piping connection port
(for FC500G-5)
Sample inlet
Counter electrode
(Pt1000Ω sensor
incorporated)
Indicator electrode
(rotating elecrtrode)
Drain cock
If loosened, this cock drains the
liquid in the measuring tank.
Figure 2.1 Component Names and Functions of the Detector
F2-1.ai
IM 12F5A2-01E
<2. COMPONENT NAMES AND FUNCTIONS>
2-2
2.2 Converter
Figure 2.2 shows the converter component names and their functions.
Figure 2.2 is a gure with the cover removed. Measuring range selection should be performed in
this state.
Converter cover
Display (liquid crystal)
Measuring range
setting switch
Sets a measuring
range.
Measuring range
selecting jumper
Applied voltage
compemsation/fixation
selection jumper
Fastener
The terminal cover
should be attached
or detached with
this fastener grip
pulled out.
Terminal cover
MEAS / CHECK selection switch
For converter checking,
select CHECK position.
mg/l
POWER
MEAS.
CHECK
SPAN
+
ME RE T1
-
G
T2
ON
OFF
L2
L1
G
C2
G
SG
C1
FUSE
1A
Zero calibrator
Operated when
zero is to be
calibrated.
(To be operated
with the
terminal cover
removed.)
Power supply
voltage selection
jumper
Power switch
Fuse
External wiring
connection terminals
Span calibrator
Operated when span
is to be calibrated.
Figure 2.2 Converter Component Names and Their Functions
NOTE
The measuring range selection jumper and the power supply voltage selection jumper are
shipped with these set based on the desired specications.
The specications cannot be changed by jumper selection.
IM 12F5A2-01E
<3. INSTALLATION, PIPING, AND WIRING>
3-1
3.
INSTALLATION, PIPING, AND WIRING
This chapter describes procedures for the FC500G free available chlorine analyzer installation,
piping, and wiring.
3.1 Installation
3.1.1 Location
Install the FC500G free available chlorine analyzer (non-reagent type) in a location which meets
the following conditions:
● Free from rain water such as an indoor location or in a cabinet
● Low vibration
● No exposure to direct sunshine
● Little dust
● Absence of corrosive gas
● Easy maintenance
Figure 3.1 shows maintenance spaces.
Approx.150
265
Maintenance spaceMaintenance space
Approx.160
Unit: mm
154
50
space
Approx.
Maintenance
space
Approx.250
Maintenance
0.50
mg/l
240
Figure 3.1 Maintenance Spaces for the FC500G Free Available Chlorine Analyzer
150
Approx.
310
space
Maintenance
IM 12F5A2-01E
<3. INSTALLATION, PIPING, AND WIRING>
3-2
3.1.2 Mounting
Mount the FC500G free available chlorine analyzer (non-reagent type) on a wall surface. For
mounting holes, see section 1.3.
3.2 Piping
3.2.1 Sample Water Piping
Connect a 6 mm OD X 4 mm ID polyethylene tube to the sample water inlet. Set the sample
water pressure at the sample water inlet to 1 to 30 kPa (ow rate: 0.1 to 2.5 l/min).
Note: If a sample water inlet valve is used, set the pressure at the valve inlet to 10 to 150 kPa.
Connect a hose of 12 mm lD to the sample outlet. Make piping so that no drain stagnates in the
hose.
3.2.2 Air Purge Piping
Make the air purge piping only when the FC500G-5 free available chlorine analyzer is used.
The air purge piping connecting port (1/8 NPT female) is located at the electrode assembly.
Exercise care in piping because the electrode assembly must be removed in implementing
inspection or maintenance (see Figure 3.2).
Electrode
assembly
Measuring
tank
Detector
Pressure regulator
6 mm OD X 4 mm ID
polyyethylene tube
Figure 3.2 Air Purge Piping
Inspection or
maintenance
Air supply
IM 12F5A2-01E
<3. INSTALLATION, PIPING, AND WIRING>
3.3 Wiring
Make wiring for power supply and output signal. Figure 3.3 shows the symbols on the converter
terminals and the types of wiring to be connected.
Terminal board TM1 (M4 screw)
TM1
+
- GG L1 L2ME RE T1 T2 SG G C1 C2
3-3
500Ω or less
4 to 20 mA DC
output
Note: Make grounding to earth (grounding resistance 100 Ω or less).
Figure 3.3 Symbols on the Converter Terminals and the Types of Wiring to be Connected
Ground
to earth
(Exclusively used cable: already wired)
Power
supply
Detector signal
F3-3.ai
3.3.1 Wiring for Power Supply and Grounding
Use a three-conductor cable of 9 to 12 mm OD, each conductor having a cross section of 1 mm2
or more.
Make grounding to earth (grounding resistance 100 Ω or less).
3.3.2 Analog Output Wiring
Use a two-conductor shielded cable of 9 to 12 mm OD, each conductor having cross section of
0.5 mm2 or more. The shield should be connected to terminal ‘‘G”.
IM 12F5A2-01E
Blank Page
<4. OPERATION>
F4-1.ai
4. OPERATION
This chapter chiey describes the preliminary work to be performed prior to putting into operation.
4.1 Preparation for Operation
4.1.1 Inspection of Piping and Wiring Status
Conrm that wiring and piping are made properly.
4.1.2 Fill with Glass Beads for Electrode Polishing
Put glass beads (accessories) for cleaning the indicator (rotating) electrode into the beads case
in the measuring tank in the following procedure:
(1) As shown in Figure 4.1, mount the electrode assembly to the holding stud. The electrode
assembly is xed to the measuring tank assembly using two screws.
In doing this, exercise care so that the indicator (rotating) electrode and the counter
electrode are not struck by the measuring tank. Also, do not touch the surface of the
indicator electrode with the ngers.
In maintenance position
4-1
Electrode
assembly
Measuring
tank
Fixing screws
(2 pcs.)
Holding stud
Figure 4.1 Removal of Electrode Assembly
(2) Remove the beads case from the measuring tank. The new glass beads are normally lled
up to the bottommost notch of the beads case when the indicator electrode is inserted.
Taking care that glass beads do not drop from the beads case. Mount the beads case so
that its slits face the counter electrode.
Slits
Beads case
Counter electrode
(reference electrode)
Glass beads
Rubber packing
Figure 4.2 Amount of Glass Beads to be Put into the Beads Case
The bottommost notch
of the beads case
Indicator electrode
(rotating electrode)
Beads case
Glass beads
F4-2.ai
IM 12F5A2-01E
<4. OPERATION>
4-2
(3) Return the electrode assembly to the measuring tank and tightly secure it using the xing
screws.
4.1.3 Measuring Range Setting
Select the measuring range using the setting switch. Set it as shown in Table 4.1. Operate the
setting switch using a small at blade screwdriver.
Table 4.1 Switch Setting Corresponding to Measuring Range
Model
FC500G-1
FC500G-5
1 2 3 4
ON
OFF
S3
Measuring
range
0 to 1 mg/l
0 to 2 mg/l
0 to 3 mg/l
0 to 5 mg/l
0 to 10 mg/l
J5 jumper
see Figure 4.5
DIP switch position
1234
ON
OFF
OFF
OFF
OFF
OFF
OFF
OFF
ON
OFF
OFF
ON
OFF
OFF
OFF
OFF
OFF
ON
OFF
ON
Figure 4.4 Measuring Range Setting Switch
IM 12F5A2-01E
<4. OPERATION>
NOTE
For the FC500G-1, measuring ranges of 0 to 5 and 0 to 10 mg/l cannot be used. For the
FC500G-5, measuring ranges of 0 to 1, 0 to 2, and 0 to 3 mg/l cannot be used.
4.1.4 Setting of “Applied Voltage Compensation/Applied
Voltage Fixation’’ Selection Jumper
The applied voltage can be xed to a denite value without applied voltage compensation. When
the applied voltage compensation/applied voltage xation transfer jumper shown in Figure 4.5 is
set to the side B (lower), the applied voltage is xed to the starting voltage value.
4-3
Side A
Applied voltage
compensation
J5
J5
Side B
Figure 4.5 “Applied Voltage Compensation/Applied Voltage Fixation” Selection Jumper
Applied voltage
fixation
J5
F4-5.ai
NOTE
If conductivity exceeds 300 μS/cm, applied voltage should be changed to xation.
IM 12F5A2-01E
<4. OPERATION>
4-4
4.2 Start-Up
4.2.1 Supplying Sample Water
<Sample inlet valve is not provided>
Conrm that the sample water pressure is within the range of 1 to 30 kPa and supply sample
water at the ow rate of 0.1 to 2.5 l/min. After supplying sample water, conrm that the sample
water level does not contact the top of the measuring tank.
<Sample inlet valve is provided>
First, fully close the sample inlet valve. Then, supply sample water at the pressure of 10 to 150
kPa. After supplying sample water, open the sample inlet valve so that the sample water ow rate
is 0.1 to 2.5 l/min.
4.2.2 Conrmation of “Power Supply Voltage” and
“Measuring Range” Selection Jumpers Setting Status
If power supply specication for the free available chlorine analyzer (non-reagent type) used is
the 100 V system, conrm that the “power supply voltage” selection jumper is set as shown in
Figure 4.6 (1).
If the power supply specication is the 200 V system, conrm that the jumper is set as shown in
Figure 4.6 (2).
If the FC500G-1 free available chlorine analyzer is used, conrm that the “measuring range”
selection jumper is set as shown in Figure 4.7 (1).
For the FC500G-5 free available chlorine analyzer, conrm that the jumper is set as shown in
Figure 4.7 (2).
(1)
FC500G-1
Side A
Measuring range
0 to 3 mg/l
4-5
(2)
FC500G-5
Figure 4.7 ‘‘Measuring Range” Selection Jumper
Side B
Measuring range
0 to 10 mg/l
4.2.3 Supplying Power
Arrange a power supply whose voltage and frequency conrm to the specications. Conrm that
the fuse holder cap in the converter is tight and then turn ON the power switch.
4.2.4 Operation Check
Conrm that a measured value is displayed in the display.
Also, visually conrm that there is no irregularity or signicant deection when the indicator
electrode revolves.
4.2.5 Calibration
Implement zero and span calibration referring to chapter 5.
4.3 Steady State Operation
There is no need for special action during analyzer operation except for executing inspection and
maintenance described in chapter 6. If a failure occurs, dispose of it referring to chapter 7.
IM 12F5A2-01E
Blank Page
<5. CALIBRATION>
5. CALIBRATION
Perform zero and span calibration when the analyzer is to be initially started up and also when
re-operated after prolonged shutdown.
During operation, perform span calibration periodically (approx. once a month). When span is to
be calibrated, rst polish the indicator electrode (see subsection 6.1.1) and then perform runningin operation for approx. one hour.
Zero calibration is virtually unnecessary during operation if it is performed once at start-up. However, merely conrm periodically that the zero point is correct during operation.
5.1 Zero Calibration
There are two methods for calibrating zero: the “open input circuit method” using which the
calibration is performed by pulling up the rotating and counter electrodes from the sample water
and the “chlorine-free water method” using water free from chlorine (e.g., water ltered through
activated carbon). Normally calibrate zero using the “open input circuit method”. However, if free
available chlorine of low concentration is always to be measured (e.g., approx. 0.1 mg/l), use the
“chlorine-free water method” for zero calibration.
5.1.1 Zero Calibration Procedure Using the Open Input
5-1
Circuit Method
(1) Remove the electrode assembly from the measuring tank with the indicator electrode ro-
tated and x it to the holding studs. (Remove the electrode assembly by loosening the two
xing screws.)
It is not necessary to stop the sample water.
(2) After display of the free available chlorine concentration has stabilized, perform zero calibra-
tion. First, remove the terminal cover.
Next, slowly turn the zero calibrator (potentiometer) using the attached at blade screwdriv-
er to adjust display to zero.
(3) Mount the terminal cover. Return the electrode assembly to the measuring tank and tightly
x the assembly using the two xing screws.
5.1.2 Zero Calibration Procedure Using Chlorine-Free Water
Method
(1) Prepare two to three litre of chlorine-free water (prepared by adding 10 ml/l of pH 7 buer
solution and 50 mg/l of NaCl to puried water).
(2) Stop supply of sample water and wait until the sample water level in the measuring tank
decreases to below the sample water inlet. Then disengage the sample water inlet piping.
(3) Introduce the chlorine-free water into the measuring tank.
Connect a tube to the sample water inlet and pour the chlorine-free water contained in a
suitable vessel into the measuring tank by utilizing a head from the inlet. If a pump is used
for supply, use a ow rate of 100 ml/min or more.
(4) After the free available chlorine concentration display has stabilized, perform zero calibra-
tion. First, remove the terminal cover.
Next, slowly turn the zero calibrator (potentiometer) using an attached at blade screwdriver
to adjust display to zero.
(5) Mount the terminal cover. Also stop supply of the chlorine-free water.
After the solution level in the measuring tank decreases to below the sample water inlet,
remove the tube and restore the sample water piping connection.
Supply sample water.
IM 12F5A2-01E
<5. CALIBRATION>
5-2
5.2 Span Calibration
There are two span Calibration methods: “sampling method’’ using which calibration is performed
based on the manually analyzed free available chlorine concentration of sample water, and the
“standard solution method” which allows calibration using a standard calibration solution having a
free available chlorine concentration of approximately 80 % of the measuring range.
Calibrate the analyzer span using the “sampling method’’ unless the chlorine concentration of
sample water is near zero. (Span calibration can be performed without removing the terminal
cover).
Note: Before performing span calibration, conrm that the electrode does not remain exposed to
the air as after zero calibration, and the electrode rotates normally in the measuring tank.
5.2.1 Span Calibration Procedure Using the Sampling
Method
(1) Conrm that the free available chlorine concentration in the sample water is stable by ob-
serving displayed values.
(2) Sample the sample water by loosening the drain cock at the bottom of the measuring tank.
When sampling the sample water, exercise care so that the tip of the counter electrode is
not exposed to air above the level of the sample water.
(3) Quickly measure the free available chlorine concentration of the sampled sample water, us-
ing a manual analysis such as amperometric titration (AT method).
(4) Slowly turn the span calibrator (potentiometer) using the attached at blade screwdriver to
adjust display to the manually analyzed value.
5.2.2 Span Calibration Procedure Using Standard Solution
Method
(1) Prepare diluting solution which is obtained by adding 10 ml/l of pH 7 buer solution and 50
mg/l of NaCl to puried water (sample water can also be used instead of puried water).
(2) Prepare 2 to 3 liter of the standard solution conditioned to a free available chlorine concen-
tration of approximately 80 % of the measuring range. To obtain this solution, dilute commercially available sodium hypochlorite (NaClO) solution using the diluting solution prepared in
step (1).
(3) Stop supply of sample water and wait until the sample water level in the measuring tank
decreases to below the sample water inlet. Then disengage the sample water inlet piping.
(4) Introduce the standard solution into the measuring tank.
Connect a tube to the sample water inlet and pour the solution contained in a suitable vessel
into the measuring tank by utilizing a head from the inlet. If a pump is used for supply, use a
ow rate of 100 ml/min or more.
(5) After the free available chlorine concentration display has stabilized, loosen the drain cock
to sample the standard solution.
In sampling the solution, exercise care so that the tip of the counter electrode is not exposed
to air above the level of the solution.
IM 12F5A2-01E
(6) Quickly measure the free available chlorine concentration of the sampled sample water, us-
ing a manual analysis such as amperometric titration (AT method).
(7) Slowly turn the span calibrator (potentiometer) using the attached at blade screwdriver to
adjust display to the manually analyzed value.
(8) Stop supply of the standard solution.
After the solution level in the measuring tank decreases to below the sample water inlet,
remove the tube and restore the sample water piping connection.
Supply sample water.
<6. INSPECTION AND MAINTENANCE>
6. INSPECTION AND MAINTENANCE
To continue good operating status, perform inspections and maintenance as shown in Table 6.1.
Determine the implementation cycle in accordance with the individual operation conditions. Table
6.1 is a guide for the implementation cycle.
Table 6.1 Inspection and Maintenance Items and Implementation Cycle
Inspection and maintenance itemImplementation cycle
Indicator electrode polishingOnce/month
Glass beads cleaningOnce/three months
Measuring tank cleaningOnce/three months
Inspection or brush and slip ringOnce/three months
CalibrationOnce/month
Converter checkingOnce/month
Fuse replacementOnce/year
6.1 Mechanical System
6-1
6.1.1 Indicator Electrode Polishing
Indicator electrode contamination inuences the measured values. Accordingly, the indicator
electrode (rotating electrode) is always rotated to polish its surface using glass beads.
However, the surface very gradually becomes contaminated with time elapse. Thus, periodically
polish the electrode surface using a polisher (alumina).
Polish the electrode surface using the following procedure:
(1) Remove the converter cover and turn OFF the converter power switch.
(2) Remove the electrode assembly from the measuring tank and x it to the holding stud. It is
not necessary to stop the sample water.
(3) Remove the electrode assembly cover.
(4) Insert an Allen wrench (accessories) into the hole on the side of the rotating shaft below the
drive belt and manually x the shaft. Remove the indicator electrode by turning it counterclockwise. Do not touch the rotating shaft brush, slip ring, or the indicator electrode surface.
(5) Apply polisher (alumina) attached as an accessory to a wet gauze and carefully polish the
electrode surface until all contamination is completely removed. After polishing, wash o the
polisher using clean water. Once the surface is clean, it will wet uniformly without repelling
water.
Electrode surface
Figure 6.1 Indicator (Rotating) Electrode
(6) Similar to electrode removal, insert an Allen wrench into the hole and manually x the
rotating shaft so that it does not turn. Fully screw in the indicator electrode (turn clockwise).
F6-1.ai
IM 12F5A2-01E
<6. INSPECTION AND MAINTENANCE>
6-2
CAUTION
Do not touch the rotating shaft brush, slip ring, or the indicator electrode surface.
(7) Mount the electrode assembly cover and restore the electrode assembly in the measuring
tank. Tightly secure the assembly using the two xing screws.
(8) Turn the converter power switch ON and conrm that the indicator electrode revolves
normally. Also conrm that the concentration display presents an approximately proper
value.
(9) Mount the converter cover.
In addition, after the electrode is polished, perform running-in operation for one hour or
longer. Then, calibrate span without fail.
Note: Polish the electrode surface (gold electrode) by following the instructions below when it has become corrugated or deformed
from the original shape (about 3 mm in diameter).
Polish the electrode surface with sandpaper (about #600) until the surface becomes nally rounded. Then, polish it with
sandpaper (about #2000), and lastly with polishing powder (alumina). Make sure the electrode surface is clean and then install
the indicator electrode. Reduce the amount of ceramic beads if the electrode has deformed greatly. The ceramic beads should
be lled up to 5 mm under the bottommost notch of the beads case when the indicator electrode is inserted.
6.1.2 Glass Beads and Measuring Tank Cleaning
If the glass beads are contaminated, cleaning eect deteriorates. Periodically clean the glass
beads and the measuring tank.
The procedure follows:
(1) Turn OFF the converter power switch. Stop sample water supply.
(2) Remove the two xing screws of the electrode assembly and secure the assembly to the
holding studs.
(3) Remove the beads case from the measuring tank with the rubber packing attached. In this
case, exercise care so as not to drop glass beads into the measuring tank.
(4) Clean the inside of the measuring tank using a brush with detergent on it. Use dilute
hydrochloric acid if manganese or iron adheres. Do not use organic solvent.
After cleaning, completely wash out the detergent (or acid) using clean water or sample
water.
(5) Move the glass beads to another vessel and clean them using dilute hydrochloric acid.
After that, completely wash out the acid using clean water or sample water. For the beads
case and rubber packing, remove dirt using detergent or dilute hydrochloric acid. After that,
completely wash out the detergent or acid using clean water or sample water.
(6) Set the beads case to the rubber packing and load the cleaned glass beads in the case.
If the beads have obviously become smaller in size (much smaller than a diameter of 1.7
to 2.3 mm), replace them with new ones. Glass beads are worn in long-term use, thereby
reducing the ability of polishing indicator electrode.
For optimum polishing, the new glass beads are normally lled up to the bottommost notch
of the beads case when the indicator electrode is inserted (See Figure 4.2). The polishing
ability cannot be recovered by replenishing the beads only by volume reduced by wear.
(7) Restore the beads case and rubber packing in the measuring tank.
(8) Restore the electrode assembly to the measuring tank and secure it using the two xing
screws.
(9) Supply sample water. Turn ON the converter power switch. Conrm that the indicator
electrode normally revolves and the concentration display presents approx. the proper
value. Finally, mount the converter cover.
The cleaning eect of the glass beads deteriorates owing to abrasion of the beads
themselves over prolonged use. Recommended practice is to replace the beads once or
twice a year.
IM 12F5A2-01E
<6. INSPECTION AND MAINTENANCE>
6.1.3 Brush and Slip Ring Checking
CAUTION
Do not touch the brush except when replacement is performed.
When the electrode assembly cover is removed for polishing the indicator electrode or for other
purposes, visually check the slip ring on the rotating shaft and the brush contacting the slip ring
for abrasion.
Further, measure resistance at the contact every six months. On revolving the indicator
electrode, measure the resistance between the brush-securing screws and the part of the
rotating shaft under the slip ring using a multi-meter. A resistance of 500 Ω or less is acceptable.
6-3
Deive shaft
Belt
Slip ring
Rotating shaft
Contact-pressure
adjusting screw
Electrode assembly
Clamp
Holder
Counter
(reference) electrode
Indicator
(rotating) electrode
Figure 6.2 Indicator (Rotating) Electrode
Pulleys
Brush
Base
Brush-securing screws
Lock screw
Gear head
Cell motor
F6-2.ai
If the resistance exceeds 500 Ω, clean the slip ring using an cotton applicator soaked with alcohol
with the indicator electrode rotated.
After cleaning, re-measure the resistance and conrm that the resistance is 500 Ω or less. If the
resistance does not decrease below 500 Ω or if abnormalities such as slip ring wear or brush
wear and bending are detected, the slip ring and/or the brush must be replaced.
The following is the replacement procedure: However, in principle, replacement should be
entrusted to Yokogawa service personnel.
(1) Turn OFF the converter power switch.
(2) Remove the electrode assembly cover. Remove the brush. The brush is secured using two
securing screws (one of them also serves for the wiring terminal).
(3) Remove both pulleys of the drive shaft (motor shaft) and the rotating shaft (indicator
electrode mounting shaft) together with the belt. Remove the drive shaft pulley by loosening
two set screws using an Allen wrench of nominal 1.5 mm (accessory). Remove the rotating
shaft pulley by loosening the screw at the tip of the shaft using a at blade screwdriver, with
an Allen wrench of nominal 2 mm (accessory) inserted in the hole of the rotating shaft for
preventing revolution.
(4) Draw out the slip ring from the rotating shaft and introduce a new slip ring.
IM 12F5A2-01E
<6. INSPECTION AND MAINTENANCE>
6-4
(5) Mount the two pulleys and the belt in the reverse procedure.
Note: If the belt is replaced, perform the procedure described in the following steps (6) and (7) without fail.
(6) Loosen the four mounting screws of the (acrylic) holder that secures the rotating shaft. Set a
spring balance to the hole under the rotating shaft slip ring and pull the shaft in the direction
of applying tension to the belt.
(7) Fix the holder. Tighten the holder-securing screws with a tension set at 0.4 kgf.
(8) Mount the brush. Fit the brush hole above the right brush-securing screw in with the
positioning pin on the mounting bracket and tighten the two brush-securing screws.
(Exercise care so as not to bend the brush tip.)
Conrm that the brush contactor contacts the slip ring and that the brush does not touch the
pulley. Adjust the contact-pressure of the brush contact or in the following procedure:
● Loosen the two securing screws of the brush-mounting bracket.
● Loosen the lock screw to the right of the contact-pressure adjusting screw.
● Move the brush-mounting bracket toward you to once separate the brush contactor from the
slip ring.
● Screw in the contact-pressure adjusting screw and then further screw in by three and a half
turns from the position where the brush contactor just contacts the slip ring. The contact of
the contactor to the slip ring should be judged by the resistance change on a multi-meter
connected between the brush and slip ring.
● Tighten the lock screw. Also tighten the brush-mounting bracket securing screws.
(9) Turn ON the converter power switch. Conrm that the driving and rotating shafts revolve
smoothly. Visually conrm that there is no irregularity at the contact part of the brush and the
slip ring.
(10) Measure the resistance value again between the brush and the slip ring and conrm that it is
500 Ω or less.
(11) Mount the electrode assembly cover.
(12) Conrm that the concentration displays present the proper values and then mount the
converter cover.
IM 12F5A2-01E
<6. INSPECTION AND MAINTENANCE>
6.2 Electrical System
6.2.1 Span Calibration
Perform span calibration at the rate of once every one or two weeks during the initial operation
start period and check the sensitivity changes owing to indicator electrode contamination or the
like to establish a reference for determining the calibration period. After the calibration period
is determined, perform span calibration in an appropriate interval using the above period as a
guide. When the indicator electrode is polished, perform span calibration without fail.
6.2.2 Converter Checking
Check the converter periodically.
The converter check function means to check the converter circuit operation.
Converter checks can be performed using switch operations. Placing the MEAS./CHECK
selector switch in the “CHECK” position transfers the converter input (current input and
temperature input) from connection to the detector to connection to the simulated input. When
the converter is normal, the free available chlorine concentration display indicates 0.90 to 1.10
mg/l regardless of the measuring range. In this case, the analog output is sent out in the range
shown in Table 6.2 corresponding to the measuring range setting.
6-5
Table 6.2 Analog Output in Checking
Measuring rangeOutput currentApproximate position
0 to 1 mg/l18.4 to 21.6 mAApprox. 100 % point of full scale
0 to 2 mg/l11.2 to 12.8 mAApprox. 50 % point of full scale
0 to 3 mg/l8.8 to 9.9 mAApprox. 33 % point of full scale
6.2.3 Fuse Replacement
For preventive maintenance, it is recommended to replace the power supply fuse once a year.
The fuse rating is 250 V, 1 A.
Power Supply Fuse
Figure 6.3 Power Supply Fuse
Cap
FUSE
Remove the cap by
turning it in the
direction of the arrow.
IM 12F5A2-01E
Blank Page
<7. TROUBLESHOOTING>
7. TROUBLESHOOTING
If any operation abnormality appears, take measures using the following procedures.
AbnormalitiesCauseCountermeasures
No indication1. The fuse is blown.
Indication shows
hunting.
Abnormal chlorine
concentration
displayed.
Abnormal analog
output
The indicator
electrode does
not revolve or
irregularly rotates.
Sample water
leakage
2. Converter connector poor contact
1. Poor contact in the indicator
(rotating) electrode mounting
position
1. Poor contact of the electrode
terminals with connecting
leadwires
2. Miss-wiring of leadwires to be
connected to electrode terminals
3. Poor continuity between the
indicator (rotating) electrode and
the contactor
4. Deterioration of RTD insulation
5. Sample water ow rate is out of
range (0.1 to 2.5 l/min).
6. Calibrated value deviation
7. Electrical circuit failure
1. The load resistance is larger than
500 Ω.
2. Electrical circuit failure
1. The belt is broken.
2. The motor fails.
3. The rotating shaft bearing has
corroded.
1. Drain cock is inadvertently not
closed.
2. Piping joint loosened.
1. Replace the fuse.
2. Once turn OFF power and re-engage the
relevant connector.
1. Coat conductive grease (auxiliary).
1. Correctly connect leadwires to the counter
electrode terminals (RE, T1, T2) and the
indicator electrode terminals (ME).
2. Check the leadwire symbols and correctly
connect the leadwires.
3. Clean the brush and the slip ring.
a. Adjust the brush contact pressure and
remove wear debris from the slip ring (see
subsection 8.2.6).
b. Replace the brush and slip ring (see sub-
section 6.1.3).
4. Disconnect leadwires to the counter electrode terminals T1 and T2, and check that
the resistance across terminals T1 and T2
is approx. 1 kΩ at room temperature and
the resistance across the terminals RE and
T1 (or T2) is 1 MΩ or more. If these are not
satised, replace the counter electrode.
5. Adjust the ow rate. (Adjust so that
sample water just overows the weir in the
measuring tank.)
6. Perform zero and span calibration.
7. Place the MEAS./CHECK selector switch
in CHECK position and check if the
display indicates 0.9 to1.1 mg/l. lf it is not
satised,contact Yokogawa.
1. Adjust the load resistance to 500 Ω or less.
2. Contact Yokogawa.
1. Replace the belt.
2. Replace the motor.
3. Replace the bearing.
1. Re-tighten the drain cock.
2. Re-tighten the piping joint ttings.
7-1
IM 12F5A2-01E
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<8. AUXILIARIES AND CONSUMABLES>
8. AUXILIARIES AND CONSUMABLES
8.1 Auxiliaries and Consumables List
Table 8.1 shows auxiliaries and consumables.
Table 8.1 Auxiliaries and Consumables
ItemPart numberRemarks
Indicator electrodeK9332MBRotating gold electrode
Counter electrodeK9332MKReference elctrode
Glass beadsK9332ZJ
Polishing powderK9088PE
BrushK9332JXPaired with slip ring
Slip ringK9332JZPaired with brush
GreaseK9044FX
Fuse (1 A)A1109EF250 V, 1 A
Washing indicator electrode
(2 bags)
Polishing Indicator electrode
alumina, 30 g
One bottle 3 ml, for continuity stabilization at
the base of indicator electrode
8-1
8.2 Auxiliaries and Consumables
8.2.1 Polisher (Part number: K9088PE)
This is used for polishing the indicator electrode surface.
8.2.2 Glass Beads (Part number: K9332ZJ)
The cleaning capability of glass beads in prolonged use deteriorates owing to abrasion. Normally,
replace the beads once or twice a year.
8.2.3 Indicator Electrode (Part number: K9332MB)
The electrode is gradually abraded by cleaning using glass beads. Generally, the electrode can
be used for around three or four years. However, it is recommended that one spare electrode
should be stored for unforeseen accident.
8.2.4 Grease (Part number: K9044FX)
The grease is applied to stabilize continuity at the mounting base part (screw connection) when
the indicator electrode is replaced. Apply the grease to the indicator electrode screw thread
referring to the procedure manual attached to the auxiliaries.
8.2.5 Counter Electrode (Part number: K9332MK)
Not subject to any abrasion, this electrode can be used for a prolonged period. However, it is
recommended to store one electrode as a spare.
IM 12F5A2-01E
<8. AUXILIARIES AND CONSUMABLES>
8-2
8.2.6 Brush and Slip Ring (Part number: K9332JX, K9332JZ)
Normally, two years are considered the replacement interval. Replacement of both items as a
pair should be performed.
CAUTION
Do not touch the brush except when replacement is performed.
l Procedures for adjusting the brush contact pressure and removing wear
debris from the slip ring
Wear debris generated from the sliding action of the slip ring and brush (generated largely at the
beginning), may enter between the slip ring and the brush, thereby temporarily increasing the
contact resistance. This may cause a drop in readings. When this phenomenon occurs, polish
and clean the surface of the slip ring to prevent the generation of wear debris and the ingress
of wear debris generated into a space between the slip ring and the brush, and furthermore
increase the contact pressure of the brush to the slip ring surface.
(1) Polishing and cleaning the surface of the slip ring
With the FC500G being powered, press sandpaper (#2000) on the rotating slip ring. Then,
press a cotton swab soaked in alcohol on the rotating slip ring to wipe o debris.
(2) Increasing the brush contact pressure
Turn o power to the FC500G. Loosen the lock screw next to the contact pressure adjusting
screw and then the 2 xing screws for the brush mounting bracket. Turn the contact
pressure adjusting screw in 1/2 turn.
Tighten the lock screws and bracket xing screws. Make sure that the brush does not come
in contact with the pulleys and does not come o the slip ring. Then turn on the power.
IM 12F5A2-01E
Customer
Maintenance
Parts List
Model FC500G
Free Available Chlorine Analyzer
( Non-Reagent Type)
l Title : Model FC500G Free Available Chlorine Analyzer (Non-Reagent Type)
l Manual No. : IM 12F5A2-01E
July 2018/5th Edition
Revision according to the suppliment
Added EMC(Australia and New Zealand) (p.1-2)
Note (p.6-2)
Revised description (p.3-3)
Aug. 2012/4th Edition Page layout changed
All page layout changed by the standard template; p.1-5, Deletion of conductivity measurement in
subsection 1.4 Measuring Principle; p.2-2, Deletion of some conductivity measurement description in
Figure 2.2; p.3-3, Deletion of subsection 3.3.3 Contact Output Wiring (this function doesn’t exist); p.42, Deletion of subsection 4.1.3 Setting of Display (Free Available Chlorine or Conductivity) Selection
Jumper; p.4-6, Deletion of subsection 4.3.1 “Out-of-Sample Detection” Contact Signal Output;
p.7-1, Deletion of “conductivity display shows abnormality”, and “Abnomal out-of sample detection”
in chapter 7. TROUBLESHOOTING table; p.8-1, Some revision of subsection 8.1 Auxiliaries and
Consumables List (P/N of fuse changed).
Oct. 2009/3rd Edition Editted by InDesign
Change the package of glass beads (p.1-3)
i
Apr. 2008/2nd Edition
Everything is reviewed.
Mar. 1993/1st Edition
Newly published.
Yokogawa Electric Corporation
2-9-32 Nakacho, Musashino-shi, Tokyo 180-8750, JAPAN
http://www.yokogawa.com/
IM 12F5A2-01E
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