jenway 3505 Operating Manual

350 550/REV A/03-03
Model 3505
pH/mV/Temperature Meter
Operating Manual
SAFETY
Please read this information carefully prior to installing or using this equipment.
2. It is essential that both operating and service personnel employ a safe system of work, in addition to the detailed instructions specified in this manual.
3. References should always be made to the Health & Safety data supplied with any chemicals used. Generally accepted laboratory procedures for safe handling of chemicals should be employed.
4. If it is suspected that safety protection has been impaired in any way, the unit must be made inoperative and secured against any intended operation. The fault condition should immediately be reported to the appropriate servicing authority.
350 550/REV A/03-03
Model 3505
pH/mV/Temperature Meter
Operating Manual
Contents
Section 1 Introduction
Instrument Description 1.1 Instrument Specifications 1.2
Section 2 Installation
Unpacking 2.1 Installation 2.2
Displays/Controls 2.3 Inputs/Outputs 2.4
Section 3 Operation
Theory of pH Measurement 3.1 pH Measurement 3.2 Preparation of Buffer Solution 3.3 Solution Temperature Values 3.4 Good Practice Guidelines 3.5 pH Calibration Using Buffers 3.6 Performing Measurements 3.7
Section 4 Maintenance
General 4.1 Cleaning/Re-conditioning Combination Electrodes 4.2
Section 5 Optional Accessories
Optional Accessories 5.1 Spares 5.2
Section 6 Troubleshooting & Functional Checks
Troubleshooting 6.1 Functional Checks 6.2
EC Declaration of Conformity
350 550/REV A/03-03
Section 1
Introduction
1.1 Instrument Description
The Model 3505 is a general purpose, laboratory pH/mV meter that uses rotary controls for mode selection, pH calibration and manual temperature adjustment. Automatic Temperature Compensation can be achieved by use of the ATC probe, which will enable the user to perform temperature measurements within the range of 0 to 100°C.
The Model 3505 has a liquid crystal display and is battery operated. The use of an optional power supply permits the unit to be operated from the a.c. mains supply.
1.2 Instrument Specifications
Range Resolution
-2.00 to 16.00pH 0.01pH
-1999 to +1999mV 1mV
Accuracy: pH: ±0.02pH
Millivolts: ±1mV Temperature: ±0.5°C
Input Impedance: >1012ohms
Temperature Compensation: Manual: -10 to 105°C 0.1°C
Automatic: 0 to 100°C 0.1°C
Calibration: Manual Display: 25mm LCD Power: 9V Battery (MN1604, PP3 or equivalent) Outputs: Analogue buffered electrode potential Size: 250(L) x 210(W) x 55(D)mm Weight: 850g
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Section 2
Installation
2.1 Unpacking
Remove the Model 3505 from the packaging and ensure the following items are included:
1. Model 3505 pH/mV/Temperature meter
2. Epoxy bodied combination pH electrode (924 001)
3. ATC probe (027 500)
4. Electrode holder
5. 4, 7 and 10pH buffer sachets
6. BNC shorting plug (009 146)
7. Battery (PP3)
8. Condensed operating instructions (350 551)
9. Instruction manual (350 550)
Any shortages or damage should be reported immediately to the Manufacturer or your local Distributor.
2.2 Installation
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The Model 3505 is supplied ready to use. Connect the ATC (if required) and the pH electrode to the rear panel Temp and pH sockets.
The electrode stand requires minimal assembly (refer to the diagram below).
Fig. 2.2.1 - Electrode Holder Assembly
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2.3 Displays/Controls
Fig. 2.3.1 - Displays/Controls
1. Display Provides direct readout of pH, millivolts, temperature of samples and standards and low battery indication.
2. Function Used for selection of mode of operation.
Switch Off - power off.
pH - pH measurement based on last calibration (the adjustment controls have no function). pH Cal - pH display based on settings of the adjustment controls for buffer and slope. °C - displays the measured temperature if an ATC probe is connected, or the manually adjusted temperature (set by the Slope/Manual temperature control). mV - displays the electrode potential in mV.
3. Buffer Used to balance out the electrode offset between the pH measurement cell and reference. This should be set with the electrode immersed in pH7 buffer. This control adjusts the electrode effect between -60mV to +60mV.
4. Slope Used to compensate for the variable sensitivity of pH electrodes. As the electrodes age their sensitivity decreases and this control is used to compensate for this. This control adjusts the slope between 75% and 125% of Nernst.
5. Manual Temp When the °C mode is selected (without the ATC probe connected) this control allows the compensation temperature to be set on the display. This control becomes inoperative during use of the ATC probe. The display will show the measured temperature if an ATC probe is connected, or the manually adjusted temperature (set by the Slope/ Manual Temp control).
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