The trademarks of the products mentioned in this manual are held by the companies that
produce them.
INFICON® is a registered trademark of INFICON.
SWAGELOK® is a registered trademark of Swagelok Co.
Tygon® is a registered trademark of Saint-Gobain Performance Plastics.
Teflon® and Tedlar® are registered trademarks of Dupont.
PEEK™ is a trademark of Victrex plc.
Fischer Connectors® is a registered trademark of Fischer Connectors SA.
All other brand and product names are trademarks or registered trademarks of their respective companies.
Disclaimer
The information contained in this manual is believed to be accurate and reliable. However, INFICON assumes
no responsibility for its use and shall not be liable for any special, incidental, or consequential damages related
to the use of this product.
Due to our continuous improvement program, specifications are subject to change without notice.
While photos are believed to be accurate and reliable, slight variations in equipment or software may occur.
INFICON warrants that the products sold by it are delivered free from any
defect in materials, workmanship and construction, and meet the products'
specifications set forth by INFICON.
INFICON warrants the products for one (1) year from the date of shipping
invoice of the products to the customer. The warranty excludes carrier gas,
GC columns, concentrator tubes, and all other items deemed by INFICON as
consumables. In the event the customer finds any defective products which do
not meet the aforesaid warranty, it shall give notice to that effect to INFICON.
The customer will return defective systems, accessories and parts to be
repaired to INFICON or INFICON contracted suppliers after obtaining a Return
Material Authorization (RMA) from INFICON Service Department.
INFICON liability under this warranty is limited to such products as are
returned, transportation prepaid, to INFICON plant no later than thirty (30)
days after the expiration of the warranty coverage and are found by INFICON
examination to have failed because of defective workmanship. At INFICON
election, it may either repair and return the product, or furnish a replacement
product, with transportation paid by INFICON in either case.
This warranty is made and accepted in lieu of all other warranties, express or
implied, whether of merchantability or of fitness for a particular purpose or
otherwise, as buyer's exclusive remedy for any defects in the product sold
hereunder. All other obligations and liabilities of INFICON, whether in contract
or tort (including negligence) or otherwise, are expressly excluded. In no event
shall INFICON be liable for any costs, expenses or damages, whether direct
or indirect, on any claim of defective product, in excess of the price paid by the
buyer for the products plus return transportation charges prepaid.
No warranty is made by INFICON for any INFICON product which has been
installed, used or operated contrary to INFICON written instruction manual or
which has been subject to misuse, negligence or accident, or has been
repaired or altered by anyone other than INFICON or which has been used in
a manner or for a purpose for which the product was not designed.
The CMS5000 Monitoring System provides online water or air monitoring for the
detection and analysis of VOCs. The programmable sample collection system
allows for on-site, rapid analysis of current air or water conditions without the need
for pre-treatment or filtration.
CMS5000 Operating Manual
Chapter 1
Introduction
Due to U.S. Nuclear Regulatory Commission regulations,
the CMS5000 oven, which contains a sealed radioactive
source, may not be repaired by unauthorized personnel.
INFICON will provide the maintenance, repair,
replacement and disposal of the radioactive source, as
well as any part of the detector.
For water analysis, VOCs are purged from the water flowing through the water
vessel. Argon will bubble into the water, the gas bubbles will rise through the water
and collect at the top of the collection tube. As the bubbles rise, a portion of the
VOCs will pass from the water phase to the gas phase — this is known as
"partitioning". The ratio of the VOC concentration in the water phase, VOC
the concentration in the gas phase, VOC
equation [1].
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Each compound will partition according to its solubility in water, its vapor pressure,
the specific water sampling matrix and the temperature. The quantity of VOCs
detected is dependent on the partition coefficient. In general, highly polar
compounds are more readily detected than less polar compounds.
A permeation tube that contains toluene is used as a check standard to ensure
proper system calibration and verify sample integrity. It will compensate for normal
fluctuations in the column, the concentrator and detector sensitivity. The lifetime of
the permeation tube is approximately 8 years.
After collection, the VOCs from the air or water samples are drawn into the
CMS5000 with the internal pump and adsorbed by the concentrator. The VOCs are
then desorbed into the column of the gas chromatograph by heating the
concentrator and reversing the carrier gas flow.
, is the partition coefficient. See
gas
water,
to
[1]
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CMS5000 Operating Manual
1.2 Gas Chromatograph
The gas chromatograph (GC) performs a time separation of the sample
compounds. The separation order is primarily based on increasing compound
boiling point.
Argon is used as the carrier gas to transport analytes through a 100%
dimethylpolysiloxane, 0.32 mm id, 30 M, 4.0 µm (or equivalent) column. The inside
of the column is coated with a thin layer of material known as the stationary phase.
The stationary phase selectively attracts components in a sample mixture. The
mixture of sample compounds in the argon gas, also known as the mobile phase,
interact with the chemicals of the stationary phase. The chemicals which spend the
least time partitioned in the column will elute (exit) off the column first.
The time taken by an individual compound to travel into the system until the
compound elutes from the column is referred to as the retention time (RT). If the
GC conditions remain constant, the same compound will elute from the column at
nearly the same retention time for each injection.
The performance of the column is affected by temperature, therefore, the column
is housed in a temperature controlled oven. The oven is programmed to increase
the temperature gradually (called ramping) to improve compound separation while
decreasing analysis time. As the temperature increases, the compounds with the
lowest boiling points will elute first with the standard non-polar phase coated
column installed.
A chromatogram of eluting organic gases from the gas chromatograph is plotted as
a function of time from the injection the compound mixture. The chromatogram
depicts the separation of the various compounds from each other by the action of
the gas chromatograph, as described above.
1.3 Micro Argon Ionization Detector (MAID)
The Micro Argon Ionization Detector (MAID) is sensitive to organic compounds
having an ionization potential of 11.7 eV or lower, which includes halomethanes,
haloethanes, carbon tetrachloride and 1,1,1-trichloroethane. The CMS5000 can
detect these compounds, as well as other hydrocarbons, to parts-per trillion (PPT)
levels.
The MAID uses argon as a carrier gas. When argon flows over a nickel-63 (Ni-63)
source, argon atoms are energized to an excited, metastable state, while other
argon atoms are ionized. The excitation energy of argon is approximately 11.7 eV.
Ar
Ar* (Energized to excited state)
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When an organic molecule (R) enters the detector, it collides with the metastable
WARNING
argon (Ar*). During this collision, energy is released to the organic molecule. Since
the ionization potential of most organic compounds is less than 11.7 eV, the
metastable argon atoms will ionize them, producing positive ions and electrons.
The reaction is illustrated as follows:
Ar* + R
Ar + R + e
High voltage applied across the detector produces a current, which is amplified and
measured to produce a chromatogram.
1.4 Radioactive Source
The MAID in the CMS5000 contains a radioactive isotope in a solid form of Ni-63,
with an activity level of up to 2.4 millicuries. The half-life of Ni-63 is approximately
96 years. The source of the radioactivity is sealed within a stainless steel cylinder
which is located within the detector cavity. Per New York State radioactive materials
license regulations, a wipe test is required for the Ni-63 source every 36 months.
The first test is completed at the factory prior to shipment.
CMS5000 Operating Manual
-
No repair of the detector cell should be performed by the
user. If the detector cell does not exhibit an electronic
signal, the isotope may require replacement. Contact
INFICON for repair or replacement of the detector cell.
The State of New York Department of Labor, Division of Safety and Health and the
United States Nuclear Regulatory Commission under either a Specific License or a
General License authorizes possession and use of the radioactive source in the
instrument. A copy of the terms and requirements of a General Licensee (section
12 NYCRR, part 38:41, table 3, item b) accompanied INFICON transfer of this
instrument. The safety requirements of the Specific License or General License are
designed to protect the user and the public from unnecessary prolonged exposure
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to radiation. Following these requirements is imperative.
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CMS5000 Operating Manual
WARNING
WARNING - Risk Of Electric Shock
CAUTION
1.5 Definition of Note, Hint, Danger, Warning
and Caution Paragraphs
NOTE: This is a note paragraph. Notes provide additional information about the
current topic.
HINT: This is a hint paragraph. Hints provide insight into product usage
This is a Warning paragraph. It warns of actions that may
cause physical injury.
This Warning paragraph warns of the presence of
electrical voltages which may cause physical injury.
This is a Caution paragraph. It cautions against actions
which may damage the instrument or lead to the loss of
data.
CMS5000 Training CD . . . . . . . . . . . 074-5020-G1
3.3 CMS5000 Diagram
930-469-G4 (230 V China)
930-469-P2 (230 V European)
930-469-G3 (230 V UK)
3 - 2
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3.4 Mounting Instructions
CAUTION
WARNING
Installation of the CMS5000 must be performed by an
INFICON authorized technician.
The CMS5000 Monitoring System is heavy. Use proper
saftey procedures and PPE when mounting the unit.
NOTE: After the CMS5000 has been powered on, the system should only be
operated with the door closed to ensure stability of heated internal
components
The CMS5000 Monitoring System requires mounting as well as some minor
assembly. The four mounting brackets included in the ship kit need to be attached
to the four corners on the back of the unit. Position the bracket on the analytical
module by lining up the openings in the bracket and on the unit. Place the washer
over the lag bolt and using a socket wrench, screw in the lag bolt until tight (see
page 5 of the instructions included with the hardware). See Figure 3-1.
CMS5000 Operating Manual
NOTE: The nuts included with the lag bolts are not needed to mount the brackets
to the unit.
Figure 3-1 Attaching the Mounting Brackets
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Structural mounting hardware is not included. It is the responsibility of the user to
ensure that proper mounting hardware is used to support the weight of the
CMS5000, and (if the CMS5000 is to be used for continual online water monitoring)
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CMS5000 Operating Manual
the filled sampling vessel. The CMS5000 weighs 55.1 lbs. (25 kg). All plumbing to
and from the sampling vessel should be supported independently of the analytical
module, as the system design will not support any additional weight.
For air monitoring, the CMS5000 should be mounted in an optimal location for
collecting air samples of interest. Care should be exercised to avoid locations
affected by air currents from heating or cooling systems, doors, windows or
structural openings.
To ensure proper operation when utilizing the CMS5000 for continuous water
monitoring, it is necessary to determine optimal mounting height and unit
placement to accommodate both the water intake as well as allow for clearance for
the sample collection tube when attaching and removing the sampling vessel.
Allow a minimum of a 15” (38.1 cm) clearance below the mounted sampling vessel
for vessel removal. Verify that the CMS5000 is level when mounted and that the
slope is less than five percent. See Figure 3-2.
Figure 3-2 Dimensions for Mounting the CMS5000
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CMS5000 Operating Manual
3.5 Water Monitoring Assembly Instructions
If not using the CMS5000 for water monitoring, skip to section 3.8 on page 3-8.
The temperature sensor, or RTD, will be unfastened and taped to the bottom of the
CMS5000 for shipment. Remove the tape, guide the excess wire back into the
CMS5000, and screw the stainless steel nut into the port nearest to the beige
sample collection tube mounting bracket located on the bottom of the CMS5000.
The Swagelok® fitting should be tightened 1/4 turn past finger tight using a 7/16”
open end wrench. See Figure 3-3.
Figure 3-3 Attaching the Temperature Sensor
The PEEK purge tube (found in the ship kit) is attached to the middle port in the
beige sample collection tube mounting bracket. See Figure 3-4.
Figure 3-4 Attaching the PEEK Purge Tube
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CMS5000 Operating Manual
Install the collection tube o-ring into the beige sample collection tube mounting
bracket. Screw the clear acrylic sample collection tube from the ship kit into the
beige sample collection tube mounting bracket located on the bottom of the
CMS5000 until finger tight. Do not over tighten. See Figure 3-5 and Figure 3-6.
Figure 3-5 Attaching the sample collection tube
Figure 3-6 Attached Sample Tube
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CMS5000 Operating Manual
3.6 Attaching the Water Sampling Vessel
NOTE: If you are not using the CMS5000 for water monitoring, skip sections
section 3.6 and section 3.7.
The optional sampling vessel mounts to the bottom of the CMS5000 using the wing
nuts supplied in the sampling source kit. See Figure 3-7.
Figure 3-7 Optional Sampling Vessel
Attach the sampling vessel to the CMS5000 by aligning the screws with the four
openings on the flange of the sampling vessel. Hold the vessel against the
mounting screw standoffs and screw on the wing nuts to hold the sampling vessel
in place. See Figure 3-8.
Figure 3-8 Attaching the Sampling Vessel
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The function of the standoffs is to provide spacing between the CMS5000 and the
vessel to allow water overflow to prevent water from entering the analytical module.
See Figure 3-9.
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CMS5000 Operating Manual
Standoffs
Wingnuts
Figure 3-9 Standoffs for Overflow
3.7 Connecting the Water Supply
If not using the CMS5000 for water monitoring, skip this section.
It is the responsibility of the integrator to configure any and all plumbing. Care
should be taken to support the weight of all plumbing hoses and hardware
independently of the CMS5000.
3.8 Air Monitoring Assembly Instructions
The CMS5000 easily converts to a continuous Air Monitoring System via two
configurations. The first configuration, designed for ambient air sampling, requires
the user to replace the water collection tube with a air collection tube with attached
filter. The filter at the opening of the collection tube prevents large particulates in
the sampling environment from entering the system.The second configuration is
designed for in-line air sampling. This configuration is more complex.
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3.8.1 Ambient Air Sampling
Ambient air sampling requires only the Air Sampling Tube (Figure 3-10). See
Figure 3-10.
Figure 3-10 CMS5000 Air Sampling Tube
Attach the Air Sampling Tube. See Figure 3-11.
CMS5000 Operating Manual
Figure 3-11 CMS5000 with Air Sampling Tube Attached
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CMS5000 Operating Manual
Center Port
Air Monitoring
Sample Inlet Line
Configuration
3.8.2 Air Line Sampling
Preparing the CMS5000 is more intensive for this type of sampling. First, attach a
sampling inlet line with a 1/8" compression fitting (with ferrule). In the example, the
purge line is removed from the center port (Figure 3-12) and moved to the right port
to become the Sample Inlet Line (Figure 3-13).
Figure 3-12 Purge Line in Position for Water Sampling
Figure 3-13 Sample Inlet Line in Postition for Air Sampling
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CMS5000 Operating Manual
CAUTION
Sample
Compression
Fitting
Sample Inlet
Exhaust Line
Detector
Exhaust
If switching from air line sampling to water sampling,
carefully move the purge tube back to the proper inlet.
Placing the sample inlet line in the wrong port will allow
water to be drawn into the CMS5000 and will cause
severe damage to the unit.
The pressure of the sample in the air line must be greater than exhaust of the
CMS5000 but no more than 1 atm. This will prevent any back pressure from
re-entering the sample path and collecting more sample than necessary onto the
concentrator. Sample flow is directional, and when the pressure changes the flow
also changes. The exhaust line is attached to the exhaust port via a compression
fitting (see Figure 3-14). The exhaust line should have at least the same internal
diameter as the sample inlet.
Figure 3-14 Exhaust Line Attached
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An example of air line sampling setup is shown in Figure 3-15.
Figure 3-15 Example Air Line Sampling Setup
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CMS5000 Operating Manual
3.9 Connecting the Argon Supply
It is the responsibility of the user to provide the argon supply. An ultra high purity
source of argon (99.99999%) is required for optimal operation of the MAID. The
included regulator is preset at the factory to the required pressure (90 psi). Connect
the argon supply to the CMS5000 using the included Teflon argon supply line and
the quick connect valve. The fitting for the quick connect is located on the left side
of the mounted analytical module. See Figure 3-16.
Figure 3-16 Connecting the Argon Supply to the CMS5000
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3.10 Connecting the Power Supply
Power Supply
Connect the 4 pin Fischer Connector® from the power supply to the 4 pin
receptacle near the rear of the upper right side of the CMS5000. Connect the plug
end of the power supply to electrical outlet. The CMS5000 will power on
automatically. The CMS5000 does not have an “on” switch. See Figure 3-17.
Figure 3-17 Connecting the Power Supply
CMS5000 Operating Manual
NOTE: The CMS5000 contains an onboard permeation tube for internal
calibration. The permeation tube is designed to continually emit toluene at
a particular rate. During shipments, power outages, or prolonged periods
of time when the CMS5000 is powered off, the permeation tube will
continue to emit toluene, thus causing a buildup of toluene within the
CMS5000. This is normal and expected. To compensate for this buildup, it
is necessary to run the CMS5000 with an argon purge for a period of
approximately 24 hours to allow the permeation tube to equilibrate. The
permeation tube is considered to be equilibrated when a stable response
for toluene is observed from consecutive runs of the check standard
calibration method. See Chapter 5, Software Setup for information on
calibrating the check standard.
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CMS5000 Operating Manual
Ethernet
I/O
3.11 Communication Configuration
Select the desired communication configuration from the selections below.
3.11.1 Ethernet
The Ethernet port used to connect the CMS5000 to a PC or network is located on
the upper right side of the CMS5000, next to the wireless antenna. Plug the end of
the Ethernet cable with the water tight cap into the CMS5000 and plug the other
end into a PC or network. See Figure 3-18.
3.11.2 I/O
The multi-pin I/O cable receptacle is located on the right side of the CMS5000 next
to the power supply receptacle. Plug the multi-pin Fischer Connector from the I/O
cable into the CMS5000 and configure the other end of the cable as desired. See
Figure 3-18.
Figure 3-18 Connecting the Ethernet and I/O
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Setting Up Laptop Communication
4.1 Introduction
Communication must be established between the CMS5000 and the PC in order
to run analysis and review data from the laptop. It is necessary to use the laptop to
calibrate the CMS5000 methods and setup software parameters.
4.1.1 Setting Up Laptop Communications
NOTE: Setting up communication is an Advanced User function. To change the
access level, see section 11.2.5.1, Set Access Level, on page 11-18.
1Open CMS IQ Software. From the System drop-down menu, select
Properties. See Figure 4-1.
Figure 4-1 Selecting Properties from the System Drop-down Menu
CMS5000 Operating Manual
Chapter 4
2Click the CMS5000 List button. See Figure 4-2.
Figure 4-2 CMS5000 List Button
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CMS5000 Operating Manual
3Enter the IP Address for the CMS5000 into the Enter New CMS5000 Name or
IP Address. (The IP Address can be found on the Front Panel of the CMS5000
by touching STAT Scroll down using the DOWN key to select NET.) See section
6.4, NET Option, on page 6-2. An example of an IP address is 10.210.50.116.
Click Add. See Figure 4-3.
Figure 4-3 Add CMS5000
4The newly added CMS5000 will be displayed in the CMS5000 List.
Double-click OK.
Figure 4-4 Closing the CMS5000/TCP Window
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CMS5000 Operating Manual
5Press OK on the System Properties Window.
Figure 4-5 Closing the System Properties Window
6The newly added CMS5000 icon will now be displayed at the bottom of the
System Setup Screen. If the CMS5000 is displayed without an "X", as in Figure
4-6, communication has been established.
Figure 4-6 Newly Added CMS5000
6aIf the CMS5000 is overlaid with a red "X", the CMS5000 is not properly
communicating with the Laptop. If the CMS5000 icon is overlaid with a blue "X",
communication has not been fully established. See Figure 4-8 and Figure 4-8.
Figure 4-7 CMS5000 Not Properly Communicating with the Laptop
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Figure 4-8 Communication Has Not Been Established Between CMS5000 and Laptop
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CMS5000 Operating Manual
NOTE: If a communication error has occurred, which is indicated by an "X",
contact the system administrator or integrator. If not available, follow the
instructions in Configuring the CMS5000 for Laptop Communications, see
section 4.1.2.
4.1.2 Configuring the CMS5000 for Laptop Communications
1Touch the STAT key on the front panel of the CMS5000 to display the STATUS
page. See Figure 4-9.
Figure 4-9 STATKey
2Use the DOWN keyto highlight NET andtouch SEL. See Figure 4-10.
Figure 4-10 Accessing NET Screen
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CMS5000 Operating Manual
3Each CMS5000 will have a unique IP address. An example of an IP address is
10.210.50.107. The subnet mask is also displayed on the NET page. An
example of a subnet mask is 255.252.0.0. See Figure 4-11.
Figure 4-11 NET Page
4On the PC, click the Windows Explorer Start button. See Figure 4-12.
Figure 4-12 Start
4aMouse over Settings and click Network Connections. See Figure 4-13.
Figure 4-13 Network Connections
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CMS5000 Operating Manual
5Double-click on the desired connection. Choose Local Area Connection to
connect with an Ethernet cable. Choose Wireless Connection to connect
wirelessly.
Figure 4-14 Select Connection
6The Connection Status window will open. Click Properties. See Figure 4-15.
Figure 4-15 Local Area Connection Status Window
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CMS5000 Operating Manual
7In the General tab, scroll down and highlight Internet Protocol (TCP/IP), click
Properties. See Figure 4-16.
Figure 4-16 Selecting Internet Protocol (TCP/IP)
8Select Use the following IP address. Enter the first number of the IP address
into the first slot. For example, if the IP address is 10.210.50.107, enter 10 into
the first slot. Refer to Step 2 on page 16-3 to find the IP address on the
CMS5000. See Figure 4-17.
Figure 4-17 Entering First Number of IP Address
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CMS5000 Operating Manual
9For the second number of the IP address, enter 210 if connecting with the
cable, or 209 if connecting with the wireless radio, into the second slot. See
Figure 4-18.
Figure 4-18 Entering Second Number of IP Address
10For the third number of the IP address, add 128 (the maximum total number is
255) to the number in the IP address. In this example, adding 128 to 50 equals
178, so 178 is entered into the third slot. See Figure 4-19.
NOTE: If the total third number is greater than 255, add 5 to the original third
number.
Figure 4-19 Entering Third Number of IP Address
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CMS5000 Operating Manual
11The fourth number of the IP address is entered into the fourth slot without
modification. Therefore, in this example, 50 would be entered into the fourth
slot. See Figure 4-20.
Figure 4-20 Entering Fourth Number of IP Address
12Press OK in the Internet Protocol Properties window to close. See Figure
4-21.
Figure 4-21 Closing the Internet Protocol Properties Window
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CMS5000 Operating Manual
13Communication between the CMS5000 and the Laptop is now established as
indicated by the absence of an "X" over the CMS5000 Sensor in the System
Setup Screen. See Figure 4-22.
Figure 4-22 Active CMS5000 Sensor Icon
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5.1 Software Setup
Prior to running continuous analyses, CMS5000 methods require calibration. This
chapter provides instructions for calibrating the Check Standard method, the Water
Purge method, and the Air Purge method.
Various software parameters will need to be established in order to operate the
CMS5000 and retrieve data. This includes entering startup and input methods,
setting up the FTP server(s) and if desired, sequencing methods.
5.2 Calibrating the Check Standard
1Run the check standard method, CMS5000 Ck Std. See Chapter 7, Operation
for information on running a method.
CMS5000 Operating Manual
Chapter 5
Software Setup
NOTE: The onboard toluene permeation tube is considered to be equilibrated
when a stable response for toluene is observed. Consecutive runs of
the check standard method may need to be run until the toluene
response is stable.
2The finished run will look similar to the chromatogram shown in Figure 5-1.
Figure 5-1 Check Standard Method Run
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3When the method has finished running, open CMS IQ on the PC.
Figure 5-2 CMS IQ
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CMS5000 Operating Manual
4Click on the Calibrate button on the top toolbar. See Figure 5-3.
Figure 5-3 Calibrate Button
5Double-click to select the desired method. See Figure 5-4.
Figure 5-4 Selecting Method for Calibration
6A screen similar to Figure 5-5 will be displayed.
Figure 5-5 Calibrate Screen
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CMS5000 Operating Manual
NOTE: To change the selected method, use the top Browse button in the
Method section on the left hand side of the screen. See Figure 5-6.
Figure 5-6 Browse Button
7Click the Browse button in the Data Files section to enter a data file. See
Figure 5-7.
Figure 5-7 Data File Browse Button
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CMS5000 Operating Manual
8Select the data file generated from the method run in step 1. To locate the file,
first select the data folder for the method. Then, select the individual data file.
See Figure 5-8 and Figure 5-9.
Figure 5-8 Method Data Folder
Figure 5-9 Individual Data File
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CMS5000 Operating Manual
9Verify that toluene is the only component in the library. See Figure 5-10.
Figure 5-10 Is Check Std Library Box
NOTE: If the Methods Differ message is displayed, verify that the differing
parameters are acceptable and click Yes. If the parameters are not
acceptable, run a calibration sample with the exact method selected in
the Method box and use that data file. See Figure 5-11.
Figure 5-11 Methods Differ Message
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inconsistent. This message is displayed because units for the data files have
yet to be selected. Click OK to continue. See Figure 5-12.
Figure 5-12 Inconsistent Data Files
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10A message will be displayed stating that the units between the data files are
CMS5000 Operating Manual
11The data file will be loaded into the Data Files list. See Figure 5-13.
NOTE: Only one file should be loaded into this list.
Figure 5-13 Data File List
12Check the Reset Library box. Checking this box will reset the calibration curve
by deleting all points currently contained in the library. See Figure 5-14.
Figure 5-14 Reset Library
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CMS5000 Operating Manual
13In the Conc/Factor column, set the concentration to 1. See Figure 5-15.
Figure 5-15 Conc/Factor Column
14Check the Selection box to process this data file. See Figure 5-16.
Figure 5-16 Selection Box
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CMS5000 Operating Manual
15Underneath Peak Search, verify that Search is selected. Click on Start to run
the calibration. See Figure 5-17.
Figure 5-17 Running Calibration
16Click on the Analytes in File tab to view the area counts for the data file.
Ensure that an area count is displayed for the analyte. Then, save the method
by clicking Save. See Figure 5-18.
Figure 5-18 Analytes in File Tab
17The check standard calibration is now complete.
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CMS5000 Operating Manual
5.3 Calibrating the Water or Air Purge Methods
1Both CMS5000 Water Purge and Air Purge methods requires calibration at
initial startup. Susbsequent calibrations may be performed as necessary.
NOTE: In the CMS5000 Water Purge method, the actual water temperature is
recorded during calibration-the CMS IQ software uses the Beta Value
to automatically compensate for the water sample temperature
fluctuations.
2Refer to section 16.2, Using the Calibrate Function, and follow steps 1-11 to
prepare and run standards for the calibration.
NOTE: The water temperature of the calibration standards needs to be
uniform when creating water calibration methods.
3Verify that the retention times of the analytes in the standard with the highest
concentration correspond to the retention times in the library template
associated with the method.
3aTo select a peak, follow the instructions in section 12.8, How to Access the
Scan Cursor, on page 12-25. See Figure 5-19.
Figure 5-19 Selecting a Peak
4The actual retention times should be within +/- 0.5 seconds of the library
retention times
5Refer to section 16.2, Using the Calibrate Function, and follow steps 22-23.
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6Refer to section 16.2, Using the Calibrate Function, and follow steps 27-37.
7Perform an initial calibration verification of the CMS5000 Water Purge method
by running the calibration standard at a concentration within the limits of the
calibration curve. See Chapter 7, Operation, for information on running a
method.
8Refer to section 16.3.6, View Reports, to access the report of the calibration
verification standard. Verify that the reported concentration is within 30% of the
actual concentration.
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CMS5000 Operating Manual
5.4 FTP Connection
Up to three FTP servers, each with its own unique IP address, user name and
password, can be configured to upload data files and can be enabled or disabled
independently. If a FTP server is enabled, the CMS5000 will maintain a queue on
which to upload data files. After each run, the CMS5000 will upload the files onto
the queues. If the CMS5000 cannot connect or login to an FTP server, the data file
will be stored in the queue until another data file is ready to be uploaded. At this
point, the CMS5000 will attempt to upload both the new and the previous data file.
If there is a loss of power, the data files will continue to be stored in the queues.
However, if a data file is deleted by a user prior to uploading, the CMS5000 will not
transfer the file to the FTP server. The CMS5000 also has an option to clear the
files in the queue if the data is no longer desired.
1Verify that the PC will connect to the FTP server. If the PC can connect to both
the FTP server and the CMS5000, it can be configured to upload data files.
2To verify the connection, first open Internet Explorer. See Figure 5-20.
Figure 5-20 FTP Server
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3Type in the FTP address of the server using the following format: "ftp://<ip
address>". See Figure 5-21.
Figure 5-21 FTP Server
4Enter the Username and Password of the ftp server. Click Log On. See Figure
5-22.
Figure 5-22 Entering Username and Password
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5When the PC connects to the FTP site, the screen will look similar to the one
that is displayed in Figure 5-23. Once the connection has been verified, this
screen can be closed by clicking the "X" button.
Figure 5-23 FTP Site
6Open CMS IQ which is located on the desktop. See Figure 5-24.
Figure 5-24 CMS IQ Icon
7Click the Status icon. See Figure 5-25.
Figure 5-25 Status Icon
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8Click on the Data Settings tab. See Figure 5-26.
Figure 5-26 Data Settings Tab
9Click on the Configure FTP Settings button. See Figure 5-27.
Figure 5-27 Configure FTP Settings
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10Enable the number of FTP servers to upload by checking the Enable FTP
boxes. Note that FTP1 is enabled as default. Up to three FTP servers can be
uploaded. See Figure 5-28.
Figure 5-28 FTP Config Window
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11Enter in the FTP server information including FTP Server IP address,
username, and password. Also enter the Connection Timeout (the amount of
time the CMS5000 will wait for a response from the FTP site), the Upload
Timeout (the allotted time for a single file to upload), and the # of Upload
Retries (the number of times the CMS5000 will attempt to communicate with
the FTP server if the Upload Timeout is reached).
NOTE: The State will be indicated as Standby mode . When the CMS5000 is
actively transmitting data to the FTP server, the State will indicate
Running. See Figure 5-29.
Figure 5-29 Entering FTP Server Information
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12Click on the Network Settings button. See Figure 5-30.
Figure 5-30 Network Settings
13To locate the Network Gateway, click on the start button on the desktop. See
Figure 5-31.
Figure 5-31 Start Button
14Select Run... from the menu. See Figure 5-32.
Figure 5-32 Run
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15The Run window will be displayed. See Figure 5-33.
Figure 5-33 Run Window
16Type in cmd and click OK. See Figure 5-34.
Figure 5-34 CMD
17At command prompts on the PC, enter route PRINT to verify the default
Network Gateway setting. See Figure 5-35.
Figure 5-35 route PRINT
18The default gateway will be displayed. See Figure 5-36.
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Figure 5-36 Default Gateway
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19Enter in the Network Gateway settings. See Figure 5-37 and Figure 5-38.
Figure 5-37 Network Gateway Settings
Figure 5-38 Entering Network Gateway Settings
20The number at the bottom of the screen should match the Network Gateway
setting in CMS IQ. If not, re-enter the Network Gateway setting displayed on
the PC into CMS IQ. See Figure 5-39.
Figure 5-39 Matching Gateway Settings
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21Accept the Network Gateway settings by clicking OK. See Figure 5-40.
Figure 5-40 Accepting Network Gateway Settings
CMS5000 Operating Manual
22Accept the FTP Server settings by clicking OK. See Figure 5-41.
Figure 5-41 FTP Server Settings
23Click OK to exit the Properties screen. See Figure 5-42.
Figure 5-42 Exiting the Properties Screen
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24FTP site is now setup and communicating.
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CMS5000 Operating Manual
5.5 System Integration
The current system I/O integration allows only input commands. This includes the
selection and start of a method created in the CMS IQ software. See section 5.6,
Setting Startup Methods, for details on how to input methods. For more advanced
integration details, please contact INFICON.
5.6 Setting Startup Methods
The CMS5000 can be operated automatically. In the Parameters tab, a Startup
Method, a method that will automatically run when powering on the system, can
be selected. Additionally, a method sequence can be selected as a startup method.
See section 5.8 on page 5-25 for information on creating a method sequence.
1Double-click the Status icon, which is located on the System Setup screen of
CMS IQ. See Figure 5-43.
Figure 5-43 Status Icon
2Click on the Parameters tab. See Figure 5-44.
Figure 5-44 Parameters Tab
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3Click on the Browse button for the startup method. See Figure 5-45.
Figure 5-45 Browse Button
4Double-click on the desired method from the method folder or highlight the
method and click OK. See Figure 5-46.
Figure 5-46 Choosing Startup Method
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5The chosen method will be displayed. See Figure 5-47.
Figure 5-47 Startup Method
6To clear the startup method, click on Clear Startup Method. See Figure 5-48.
Figure 5-48 Clear Startup Method
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5.7 Input Methods
In the Input/Output tab, up to four input methods can be selected. An input method
will begin when a relay contact, which has been integrated into the water/air control
system, triggers its start. Also, a method sequence can be selected as an input
method. See section 5.8 on page 5-25 for information on creating a method
sequence.
1To enter input methods, click the appropriate Browse button. See Figure 5-49.
Figure 5-49 Input Browse Buttons
CMS5000 Operating Manual
2Double-click on the desired method from the method folder. See Figure 5-50.
Figure 5-50 Choosing Input Method
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3The selected input method will appear in the Input 1 Method field. To clear the
input method, click the Browse button for the desired method.
See Figure 5-51.
Figure 5-51 Clearing Input Method
4Click X without selecting a method. See Figure 5-52.
Figure 5-52 Clicking "X"
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5The method will be cleared from the selected input method line.
See Figure 5-53.
Figure 5-53 Method Cleared
5.8 Method Sequence
CMS5000 Operating Manual
A series of methods can be selected to run at timed intervals, which includes
consecutive runs. Once the series has been started, it can run unattended and
unprompted until the sequence has finished. Follow the instructions below to
create a method sequence.
1From the CMS IQ Setup screen, double-click the Method Editor icon.
See Figure 5-54.
Figure 5-54 Method Editor Icon
2The Edit Method window will be displayed. Click on Method Sequence.
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See Figure 5-55.
Figure 5-55 Edit Method Window
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CMS5000 Operating Manual
3In the Method Name box, type in a name for the method sequence or use the
name provided. Verify that the file extension for the method name is .xmth.
See Figure 5-56.
Figure 5-56 Method Name Box
4Click the Method Sequence (...) button. See 4.
Figure 5-57 Adding Method File
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5A list of methods will be displayed. Double-click the desired method for
sequencing. See Figure 5-58.
Figure 5-58 Selecting Method to Sequence
6The selected method will be displayed in the method sequence list. See Figure
5-59.
Figure 5-59 Selected Method
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7In the Start Run column, choose either Run Button or Immediately for each
method. This selection determines how each method in the run is started. See
Figure 5-60.
NOTE: If the Run Button option is selected, the run button will have to be
pressed each time. If Immediately is selected, the method will
automatically commence.
Figure 5-60 Start Column Selection
8In the End Run column, choose Sleep for or Sleep until for each method. See
Figure 5-61.
NOTE: The Sleep for option is used to enter a time period, such as one hour.
The Sleepuntil option is for a specific time, such as one o’clock.
Figure 5-61 Sleep Column
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9In the End Run column, enter the desired time for the next method to start or
the length of time to sleep before the next method starts. See Figure 5-62.
NOTE: Enter 0:00:00 to run the next method as soon as the previous one has
finished.
Figure 5-62 Time Column
10Repeat steps 4-9 to add additional methods for sequencing. Alternately,
right-click anywhere in the windowand select Duplicate Row. See Figure 5-63.
Figure 5-63 Duplicate Row
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11When the desired sequence has been entered, the user can either enter a
number up to repeat the sequence a set number of times (Number of
Iterations, see Figure 5-64), or run a continuous loop of the sequence without stopping (Run Continuously, see Figure 5-65).
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CMS5000 Operating Manual
NOTE: When using Run Continuously, the Number of Iterations option is
grayed out. See Figure 5-65.
Figure 5-64 Number of Iterations
Figure 5-65 Run Continuously
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12Click Save when all the desired methods have been entered. See Figure 5-66.
Figure 5-66 Saving the Method Sequence
13Save the method sequence to the desired location. Click OK. See Figure 5-67.
Figure 5-67 Save Method Sequence
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6.1 Introduction
The STAT button provides real time data regarding various system parameters.
These parameters include the SYS (system) option, the TIME (time) option, the NET (network) option, the STAT (status) option and the FIRM (firmware) option.
6.2 SYS Option
The first option, SYS, provides system information including the Hostname, Serial
Num (Number), Ver sion number, Built on (build date), Free Disk space, and the
Startup method. The Hostname is used for PC communication, and the Serial
Num is the serial number of the unit that is used for identification. Version displays
the version of CMS5000 software that is loaded onto the system. The date and time
that the software was released is located in the Built on field. Free Disk is the
amount of free disk space available for data storage and the last entry is the
Startup which is the method that will automatically run when turning on the unit.
See Figure 6-1. Navigate through the SYS options by using the UP and DOWN
buttons.
CMS5000 Operating Manual
Chapter 6
Status Button
Figure 6-1 SYS Option
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CMS5000 Operating Manual
IP Address
Subnet Mask
6.3 TIME Option
The TIME option gives Date, Time (in a 24 hour format) and Time Zone
information. This option is used to timestamp the data files. See Figure 5-2. If the
time is incorrect, see section 9.3, Set Date, Time and Time Zone, on page 9-3 for
instructions.
Figure 6-2 TIME Option
6.4 NET Option
The NET option displays the IP Address, Subnet Mask, and the User Host. The
IP address and subnet mask can be used to set up communication between a
CMS5000 and a PC. This communication will allow for data to be transferred from
the CMS5000 to the PC for analysis and storage. The User Host is the laptop that
is communicating with CMS5000. See Figure 6-3.
Figure 6-3 NET Option
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6.5 STAT Option
The STAT option displays temperature information and carrier gas pressure. This
includes the current temperatures and the setpoint temperatures of the Regulator
Heater, Check Standard, Valve Oven, Column, Detector (MAID), and the Argon
Supply pressure. The state of the heaters will be shown, as well, with ctrl
indicating that the heaters are within 2 degrees of their setpoint. The temperature
of the water sample and the temperature of the card cage, which holds the boards
of the unit, are located beneath the temperatures of the heated components. The
pressure of the argon carrier gas is the last listing on the screen. See Figure 6-4.
NOTE: If the argon pressure is 380 kPa or less, a low-pressure warning will
Figure 6-4 STAT Option
CMS5000 Operating Manual
appear. When the pressure drops to 350 kPa, a low pressure error
message will be displayed.
6.6 FIRM Option
The FIRM option displays the firmware version for the gas chromatograph (GC)
and the front panel (FP). See Figure 6-5.
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Figure 6-5 FIRM Option
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7.1 Introduction
The CMS5000 can be programmed to operate uninterrupted or at timed intervals,
either through remote operation or through the front panel. Following a method run,
analysis results can be uploaded onto an FTP site allowing for data review at an
off-site location. The results are also stored directly onto the hard drive of the
CMS5000 unit.
The CMS5000 will commence sampling the air sample or the headspace above the
water sample at the beginning of the method run. The results will be shown on the
front panel during the run. If accessing data from a remote location, the results will
be available immediately following the method run.
7.2 Default Methods
Default methods are included with the CMS5000. The CMS5000 Ck Std method
verifies that the retention time and the response of the internal calibration standard
is within range. The CMS5000 Water Purge method detects specifically selected
VOCs during water monitoring. The CMS5000Air Purge method detects
specifically selected VOCs during air monitoring.
CMS5000 Operating Manual
Chapter 7
Operation
7.3 System Calibration Standard
A toluene filled permeation tube is used to calibrate the CMS5000 system and has
a life span of approximately eight years. The software will use this calibration to
automatically compensate for normal fluctuations in detector sensitivity.
7.4 Operating the CMS5000 using the Front Panel
1Touch ESC until the CMS5000 Main Menu is displayed. See Figure 7-1.
Figure 7-1 Main Menu
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CMS5000 Operating Manual
2Run Method will be highlighted. Touch SEL. See Figure 7-2.
Figure 7-2 Selecting Run Method
3Using the UP and DOWN keys, highlight the desired method. Touch SEL.
See Figure 7-3.
NOTE: Recent Methods will display the las methods run.
Figure 7-3 Highlighting Method
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CMS5000 Operating Manual
4The system will begin heating in preparation for the method selected.
See Figure 7-4.
Figure 7-4 Heaters
5Once the system is ready, a prompt to Press RUN to start method will be
displayed. Touch RUN. See Figure 7-5.
Figure 7-5 Press RUN to Start Method
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6While sample is being collected, the screen will display a Start Scanning in
message. See Figure 7-6.
Figure 7-6 Start Scanning Message
7A chromatogram will be displayed while the method is running. Figure 7-7
depicts a finished chromatogram.
Figure 7-7 Finished Chromatogram
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8To re-run the same method through the front panel, touch RUN. See Figure 7-8.
Figure 7-8 Run Button
9To return to the Main Menu, touch ESC. See Figure 7-9.
Figure 7-9 Returning to Main Menu
10To see the results of the run, touch SEL. See Figure 7-10.
Figure 7-10 Run Results
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11For information on reading reports, see Chapter 8, Review Data.
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8.1 Review Data
This option recalls data files for review. To access data files, follow the instructions
below.
1Return to the Main Menu by pressing ESC. See Figure 8-1.
Figure 8-1 Main Menu
CMS5000 Operating Manual
Chapter 8
Review Data
2Using the DOWN button, scroll to the second option Review Data and touch
SEL. See Figure 8-2.
Figure 8-2 Review Data
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2aAlternately, touch 2 followed by SEL. See Figure 8-3.
Figure 8-3 Review Data
3The data will be arranged in folders by method name. Select the desired folder
by scrolling through the list using the UP and DOWN buttons. Then, touch SEL.
See Figure 8-4.
Figure 8-4 Method Folders
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4Highlight the desired data file by using the UP and DOWN buttons. Then, touch
SEL. See Figure 8-5
NOTE: Files are named in the following format: method name_yearmonthday_
number of run for that date. Files will be in reverse chronological order with
the last data file at the top of the list. .
Figure 8-5 Selecting Data File
5The desired file will be displayed. See Figure 8-6.
Figure 8-6 Recalled Data File
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6Press SEL to retrieve results in a report format.
7The Summary report will be displayed. This report contains the information
about the method: the CAS number, the target (compound) name, the
predicted retention time, the actual retention time and the water temperature (if
running a water method). It also includes the date and time that the method was
run. Use the UP and DOWN buttons to view the full report. See Figure 8-7.
Figure 8-7 Summary Report
8To access the Quant (Quantitative) Report, touch 2 followed by SEL. This
report contains the predicted retention time, the actual retention time, the area
and the concentration. Use the UP and DOWN buttons to view the full report.
See Figure 8-8.
Figure 8-8 Quantitative Report
9Press ESC to return to the previous screen.
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9.1 Introduction
System is the third option on the Main Menu. This option will sets the date and time,
network addresses and language settings.
9.2 System Option
To select the System option, follow the instructions below.
1Touch ESC until the Main Menu is displayed. See Figure 9-1.
Figure 9-1 Main Menu
CMS5000 Operating Manual
Chapter 9
System Option
2Using the DOWN button, scroll until System is highlighted. See Figure 9-2.
Figure 9-2 System
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3Touch SEL. See Figure 9-3.
Figure 9-3 SEL Button
4Alternately, touch 3 followed by SEL. See Figure 9-4.
Figure 9-4 Using the Number Keys to Select System
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9.3 Set Date, Time and Time Zone
The first option is to set the date and time. The CMS5000 will use this setting to
timestamp the files.
1Scroll to Set Date and Time. Touch SEL. See Figure 9-5.
Figure 9-5 Set Date and Time
CMS5000 Operating Manual
2The Current Date and Time screen will be displayed. To change the date,
touch SEL when the Date is highlighted. See Figure 9-6.
Figure 9-6 Set Time
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3Use the number keys to enter the date. Use the STOP button to enter a
forward slash. See Figure 9-7.
Figure 9-7 Date and Time
4To save the date, touch SEL. See Figure 9-8.
Figure 9-8 Saving the Date
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5Upon saving, the system will return to the Current Date and Time screen.
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6To change the time, scroll to the Time option using the DOWN button.
See Figure 9-9.
Figure 9-9 Time Option
7Enter the time using the number keys. To enter a colon, touch STOP.
See Figure 9-10.
Figure 9-10 Set Time
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8To save, touch SEL. See Figure 9-11.
Figure 9-11 Saving the Time
9Upon saving, the system will return to the System screen. See Figure 9-12.
Figure 9-12 System Screen
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9.3.1 Set Network Info
The Set Network Info option allows the IP address to be changed on the
CMS5000.
1Using the DOWN button, scroll to Set Network Info. See Figure 9-13.
Figure 9-13 Set Network Info
CMS5000 Operating Manual
2Touch SEL. See Figure 9-14.
Figure 9-14
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3The IP address of the system will be displayed on the Network Addresses
page.
4If an additional or different IP address is desired, scroll to Add IP Address
using the DOWN button. Touch SEL. See Figure 9-15.
Figure 9-15 Add IP Address Option
5Using the number keys, enter in the new IP address. Use the STOP button to
enter in periods. See Figure 9-16.
Figure 9-16 Enter IP Address
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6To save, touch SEL. See Figure 9-17.
Figure 9-17 Enter IP Address
7The system will return to the Network Addresses screen. See Figure 9-18.
Figure 9-18 Network Addresses
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CMS5000 Operating Manual
9.3.2 Set Language
The Set Language option is used to change the choice of language on the front
panel.
1Using the DOWN button, scroll to Set Language. See Figure 9-19.
Figure 9-19 Set Language
2The Set Language screen will appear. See Figure 9-20.
Figure 9-20 Set Language
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