ALTANA Haze-Gloss User Manual [en, de, fr, it]

Additives & Instruments
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Measure what you see.
Manual Betriebsanleitung
Modo d’emploi
Istruzioni d’uso
Gardner
haze-gloss
Gardener
Version: 2.6 Copyright 1990
haze-gloss Reectometer
Cat. No. AG-4601
haze-gloss Reektometer
Best.-Nr. AG-4601
haze-gloss Brillancemètre
o
N
Ref. AG-4601
haze-gloss
228 012 718 EDFI 0811
Riettometro
No di cat. AG-4601
Gardner
haze-gloss
Gardener
Version: 2.6 Copyright 1990
haze-gloss Reectometer
Cat.No. AG-4601
Table of Contents
 1. SafetyInformation  2.SystemDescription  3.Start-Up  4.Operation  5.Calibration  6.SettingtheInstrumentParameters   SETUPMenu  7.PracticalMeasuringHints  8.MeasurementSeriesandStatistic  9.InternationalSpecications 10.InterfaceDescription 11.TechnicalData 12.SourcesofErrors 13.OrderingGuide
TechnicalDataareSubjecttoAlterations.
Power Switch Line Voltage Selector Switch Fuses
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Version: 2.6 Copyright 1990
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RS 232 Footswitch Power Cord
Control Panel LCD Display
Sample Support Table
Hand Lever to Lower the Sample Support Table
Footswitch for Motorized Sample Support Table
!
1. Safety Information
Before switching on the unit, make sure the voltage setting on the unit matches the voltage of your power outlet. The unit must be plugged into a grounded outlet. Do not eliminate the ground protection by using an ungrounded extension cord.
Warning!
Any break in the ground conductor either inside or outside the unit, or any loosening of the ground connection, may make the unit hazardous to operate. Never break the ground connection intentionally!
Attention!
For USA use only: Detachable Power Supply Cord - Listed, type SVT or SJT, 18 AWG. Terminates in parallel blade grounding type plug 125 V, 15 A configuration.
any power source. Any adjustments, maintenance or repairs that must unavoidably be performed with the power on and the unit open should be left to qualified personnel familiar with the possible hazards. Capacitors inside the unit may still carry a charge even after the unit has been disconnected from the power source. Be sure that all replacement fuses are of the specified type and size. Never resort to using reconditioned fuses or short-circuiting.
Defects and Extreme Usage
If safe operation can no longer be presumed, shut down the unit and secure it against unintended operation. The unit must be presumed unsafe to operate:
• if it shows visible damage
Adjustments, Replacement of Parts, Maintenance and Repairs:
Removing covers or components, except where this can be done without tools, may expose live parts. Connection terminals may also be live. Before replacing parts or performing any adjustment, maintenance or repair for which the unit must be opened, make sure the unit is disconnected from
• if it no longer operates
• if it has been stored for long periods under adverse conditions
• after harsh treatment during shipping
2. System Description
The haze-gloss reectometer is a stationary instrument designed to measure specular gloss and reection haze on paint coatings, plastics, binders, pigments, and metal surfaces (mirror reection).
The sample surface is illuminated at a dened angle and the reected light is measured photoelectrically. Selection of the appropriate angle of illumination (geometry) is dependent on the specic gloss level of the sample surface: matt, medium, or high gloss. (For the application of these measuring ranges, see Chapter 6, Practical Measuring Hints.) Advanced electronic engineering in the development and production of haze-gloss provides a performance level, ease of operation and high accuracy at a level not previously achieved.
• Three geometries: 20°, 60° and 85° Mirror reection on metal surfaces, Reection haze
motorized and controlled using a footswitch
• Illuminated target for accurate sample positioning
• Easy-to-read control panel and microprocessor controlled operation
• High accuracy and long-term stability due to reference beam principle
• No warm-up time, immediate opera­ tion, long-term calibration (≥ every two months)
• Internal statistic mode and storage
• Interface for data transfer and control via PC
• Display can be selected to be English, German, French, Spanish, or Italian
The haze-gloss measuring unit con­forms with the standards ISO 2813,
ASTM D 523 and DIN 67 530.
• Sample pressing device allows for a rapid change of samples, sample support table optionally
3. Start-Up
Important Notes
Please read this information before you operate the instrument:
The haze-gloss system does not require a special room for measuring. As with every electronic equipment, however, it is important to observe the usual operating conditions.
Please avoid:
• excessive oscillations and vibrations
• extreme ambient temperatures
• temperature shocks
• air humidity 85%, splash water
• caustic and explosive chemicals, aggressive vapors, and gases
• extreme electromagnetic fields
The instrument housing is resistent to a number of solvents. However, resis­tance to all chemicals can not be ensured. For this reason, use a soft moist cloth for cleaning. In the case of severe contamination, some alcohol or suds may also be used. If your haze-gloss should experience a malfunction, we ask that you do not attempt to repair the unit yourself. Our Customer Service will be glad to help you as quickly as possible.
• extreme electrostatic discharge
• penetration of foreign matter in the measuring aperture
Installation
Always disconnect the instrument from
Power Switch
Jack for Power Cord
Voltage Selector Fuses
the mains supply before you plug-in or unplug the various connectors!
Unpack the instrument and check for any possibility of shipping damage (visual inspection). Before initial operation, check if the delivery is
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Install the unit at its place of destination.
Check the position of the voltage selector switch on the back panel and, if
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RS 232 Interface
Footswitch
necessary, set the switch to your power requirements as follows: Remove the plastic cover next to the mains cord jack. Then plug-in the plastic cover so that the triangular marking on the power switch housing and the required voltage range indication coincide.
With the unit being still disconnected, plug the power cord into the shockproof socket. In the case of motorized units: connect the footswitch.
If required, plug the PC connection cable into the RS 232 jack.
8
SELF-DIAGNOSTIC
STATUS
Gardner
Version: 2. Copyright 1990
Switch on the unit using the power switch on the rear panel.
Logotype and copyright message appear in the display.
Lamp Lamp Lamp Lower Lower
The haze-gloss performs a self­diagnostic test.
Note
Motorized units also test the downward movement, provided that no sample is inserted.
20°: 60°: 85°: 4 cm: 7 cm:
ok ok ok ok ok
Haze Compens.: Lower: Autom. Meas.: Target:
The status of the set parameters appears in the display.
ok 4 cm on on
REFLECTOMETER
20° : 60° : 85° : Haze: 20° Cust. spec: 60° Cust. spec: 85° Cust. spec:
ASTM
99.2
93.3
90.1 457 2000 1000 300
STATUS
Stored Values: 20° : 60° : 85° : Haze: 20°& 60°: 60°& 85°:
n= 520 n= 82 n= 0 n= 571 n= 101 n= 0
20°
36.7
60°
73.2
The stored calibration values appear on the display. Display of customized calibration values requires prior definition (see Chapter 5).
The number of stored readings appears on the display.
After completion of self-diagnostic test and display of status, the instrument immediately goes to the last mode activated before the unit was disconnected and is now ready for operation.
Before you start measuring, the haze-gloss has to be calibrated (see
Chapter 5).
4. Operation
haze 20° 60° 85°
20° + 60° auto-range 60° + 85°
Select the desired geometry or the auto-range function (see Chapter 6, Practical Measuring Hints).
Lower the sample support table using the hand lever, or the footswitch in the case of a motorized table.
Insert sample, test surface facing up.
Check the sample for possible surface defects (e.g. scratches, fingerprints). The illuminated target marks the sample port position (see SET UP Menu: Target)
Release hand lever or footswitch respectively. Now the support table moves the sample towards the sample port.
The measurement is started automati­cally but can also be started manually by pressing the operate key. (see SET UP Menu: Measure autom.)
The measured values and the corre­sponding geometry/measuring mode appear in the display.
5. Calibration
Calibration of the haze-gloss is seldom necessary due to state of the art technology and a reference beam principle. We recommend a calibration interval of 2 months.
SET UP OPERATION
Cursor: SET UP Change: OPERATE
Calibration is also recommended
• if the ambient temperature differs extremely from the normal room temperature.
• if "Please Recalibrate" appears on the display. (The unit automatically de­ tects lamp aging by 4 %)
Continue: SET UP
Calibration Procedure
• Call SET UP Menu
set up
SET UP MENU Haze Compens.:
on Calibration Measure autom: Target: Lower: Decimal Point: Escape:
on
on
4cm
on
SAMPLE
• Select Calibration
set up
operate
Note Make sure that the glass standard is clean and has no scratches!
Routine
• Call Calibration Routine
GLOSS CALIBRATION
Measure High-Gloss
--> OPERATE
Escape:
SAMPLE
Move down the sample support table using the hand lever and insert black high-gloss standard. If your haze-gloss is equipped with a motorized sample table you can alternatively use the footswitch.
GLOSS CALIBRATION
20° Calibration ok
90.2
60° Calibration ok
93.3
85° Calibration ok
99.1
The calibration cycle for the single angle geometries is now performed automatically.
HAZE CALIBRATION
Measure Haze Tile
--> OPERATE
HAZE CALIBRATION
Haze cal. ok 457
CUSTOM SPEC. CALIB. MIRROR MODE 20°: Val.: not defined 60°: Val.: 1000 85°: Val.: not defined
Escape:
SAMPLE
Haze Calibration
Insert white haze tile.
The haze standard must be clean and free of scratches.
• Press the operate key
operate
Note
The value indicated on the haze standard has been reduced by the luminance factor (see Chapter 6, Haze Compensation).
Calibration is completed.
• Go into the measuring mode by pressing the
sample/ statistic
Important!
Only use standards supplied with the instrument. These have been calibrated against officially tested standards and correspond to ASTM D 523 or DIN 67 530. Should a standard be damaged or lost, the haze-gloss has to be recalibrated with new standards by our service engineers as the values of your original standards are memo-rized in the instrument.
sample/statistic key.
Escape:
SAMPLE
Customer-specified Calibration
For mirror reflection measurements you can calibrate the instrument using your company's own standards and define specific reflectometer values. All future measurements will then be related to these values.
• Call the SET UP Menu and select "Change Cal.
set up
operate
Value" (2nd page of menu)
• press the operate key to define "Custom Cal."
• Select desired geometry
CUSTOM SPEC. CALIB. Calib. Value 20°
* * * 1 2 3 0 * * *
Change Value: Confirm: Escape:
SETUP OPERATE SAMPLE
CUSTOM SPEC. CALIB.
Measure Custom Tile 20° : 1000
--> OPERATE
Escape:
SAMPLE
Note
If you define very high standard values, limit errors might occur during the measurement as the numerical range is limited to 500 gloss units. In this case, 4 stars will be displayed instead of the reflectometer value.
• Set reflectometer value:
• Press the set up key to change the number above
set up
operate
the arrow, cycling from
0 - 9.
• Confirm the selected number using the operate key. The arrow jumps to the next number.
• Measure mirror reflection standard.
operate
haze-gloss calibration is performed against your
own standard.
6. Setting the Instrument Parameters SET UP Menu
SET UP OPERATION
Cursor: SET UP Change: OPERATE
Continue: SET UP
In the SET UP Menu the instrument parameters are set and the calibration routine is called.
• Call the SET UP Menu. Operating instructions
set up
set up
set up
appear on the display.
• Press the set up key again to call the first SET UP page
• Select the individual functions by repeatedly pressing the set up key.
SET UP MENU Haze Compens.:
on Calibration Measure autom: Target: Lower: Decimal Point: Escape:
on
on
4cm
on
SAMPLE
The selected function is marked by a filled rectangle (cursor).
SET UP MENU Country D,US,F,I,E Mirror Mode:
on
Change Cal. Value:
Custom. Cal.: Escape:
on SAMPLE
• Call or change the
operate
sample/ statistic
selected function.
• Leave the SET UP Menu
Description of the Individual Functions:
Haze Compensation
(Compensation of the luminance factor) The light scattered diffusely by the sample is detected by a special aperture and can be subtracted from the haze values. The brighter the sample, the more important becomes this haze effect. (e.g. with white enamel) In the mode "Haze Compens.: off" haze values are displayed with the indication "nc." = not compensated. Pigmented samples such as paints or plastics should always be measured with "Compensation on" since the sample luminosity affects the haze value.
Calibration
Call the calibration routine (see Chapter 5)
Automatic Measurement
When raising the sample support table a measurement is taken automatically, thus minimizing keystrokes.
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Target
A target is automatically activated with the downward movement of the sample support table.
Lower
In the case of a motorized sample support table the downward movement can be set to 4 or 7 cm.
Decimal Point
The decimal point can be suppressed using the "decimal point off" function. Calculations in the statistic mode are always performed with the exact value.
Language US, D, F, I, E
Display can be selected to be English, German, French, Italian or Spanish.
7. Practical Measuring Hints
20°
Mirror Mode
off: If a gloss value exceeds
approx.190 the haze-gloss automatically goes to a lower channel and takes a new mea­surement.
on: If only high-gloss samples
(e.g. metals) have to be mea­sured, you will save time with the mirror mode.
Change Calibration Value
In this mode you can calibrate against your own mirror gloss standard with a defined reflectometer value. (See Chapter 5, Calibration)
Customer-specified Measurements
(Only displayed if defined) Calculation of reflectometer values related to a customer-specified mirror standard.
36.7
60°
73.2
Gloss Measuring
In accordance with DIN 67 530 the reflectometer value is related to a black glass standard with a refraction index of 1.567 (reflectometer value 100). Reflectometers are differentiated by the angle of illumination of the light source. In accordance with DIN 67 530 and ASTM D 523 the angles are set at 20°, 60° and 85°; each setting corresponds to a particular application:
• Semi-gloss surfaces are measured at an angle of 60°. Measurements should range between 10 and 70 gloss units.
• If highly reflective surfaces are measured using the 60° geometry and the measured value exceeds 70 units, the measurement should be repeated using the 20° geometry.
• Matt surfaces showing measured values of less than 10 units (using the 60° geometry), should be measured using the 85° geometry.
In order to obtain a better differentiation of the measured values, we recom­mend the 85° geometry in all cases in which the value measured at 60° is below 30 units. Application recommen­dations differ in the various standards. While the ASTM D 523 standard sets the upper limit for changing from 60° to 85° geometry at the value of 10 gloss untis, ISO 2813 sets this limit at 30 units. These limits should be regarded as recommendations.
surfaces, mirrors). In this mode the gloss values range up to:
2000 gloss units at 20° 1000 gloss untis at 60°
160 gloss units at 85° (calibration performed at the manufac­turer).
As mirror gloss measurements are often related to customers' standards, haze-gloss offers the possibility to calibrate against customer-specified standards (see Chapter 5, Calibration).
AUTO-RANGE
60°
20.7
85°
47.2
Note
• In the auto-range mode the 60/85° dual angle geometry is used for reflectometer values below 30; the 60° single angle geometry is used for reflectometer values between 30 and 70, and the 20°/60° dual angle geo­ metry is used for reflectometer values exceeding 70. (Reflectometer values always relate to 60°)
Mirror Reflection Measurements
The haze-gloss offers an extended measuring range, which allows for the measurement of samples with great reflecting power (polished metal
• It is not useful to take measurements on samples showing contaminations, scratches or other damages, unless you want to evaluate the degree of such defects by means of gloss measurement.
• Best results can only be obtained from plane surfaces.
• Since gloss properties are usually not constant over the complete sample surface, the reflectometer value should be determined on several different locations of the sample and the readings should be averaged.
• If a sample surface is structured, i.e. the gloss porperties are dependent on the measuring direction, it is recommended to report the structure characteristics and the angle of incidence or to calculate the mean value from readings taken in varying directions.
• Samples that have to be measured several times during a test (e.g. weathering samples) should be marked correspondingly in order to make sure that comparison measurements or check tests will be performed on the same location.
Haze nc.
13.7
20°
86.5
Haze Measuring
• press haze key
haze
If haze compensation: off was selected in the Set Up Menu, "nc." (= not compensated) appears in the upper left corner of the display.
In many cases, the reflectometer value does not suffice to describe the optical properties of a surface. In addition to color and gloss, reflection haze is of great importance.
Haze Measurement provides:
• better differentiation of optical properties for high gloss surfaces
• an indirect method to evaluate and characterize paint and raw material properties, such as
- degree of dispersion
- flocculation behavior
- wetting properties
- scratch resistance
- weathering tests
- optimization of paint formulae
• an indirect method to evaluate the manufacturing process of the surface.
0
60
0
20
c
0
20
The Equation
The equation for reflection haze is: H = K x lg (linear haze value/20 + 1).
haze
a
0
60
b
In order to achieve a logarithmical haze value of 1000 at a linear value of 100 haze units, the constant k = 1285.1 is used.
0
85
a
For the measurement of reflection haze, 2 additional apertures c (width = 1.8°) are positioned on either side of the 20° specular gloss aperture. This allows for the measurement of the diffusely scattered light adjacent to the 20° specular angle.
85
Note
The reflection haze value is displayed logarithmically
• in order to correspond as close as possible with the visual perception of reflection haze by the human eye.
• in order to achieve a higher sensitivity in the case of low haze values. (The lower the haze value, the better the surface quality.)
0
8. Measurement Series and Statistic
20°
36.7
n=123 m=36.5 s= 1.3
20° m= 36.5 min= 32.8 max= 40.6
n= 123 s= 1.3 Vr= 3.6
60°
m=73.3
73.4
The statistic mode can be selected in every geometry. The AUTO-RANGE function can be used in the sample mode only.
sample/statistic key: Changing from individual
sample/ statistic
Key to the symbols: n = number of measurements m = mean value s = standard deviation
measurements to mea­ surement series.
s= 0.9
60° m= 73.3 min= 70.8 max= 75.7
Display of all statistical results
m mean value n number of measurements min minimum value max maximum value s standard deviation
n
i=1
(xi-x)
-
1
s=
/
n-1
v
coefficient of variance
r
vr =100 S/m (%)
s= 0.9 Vr= 1.2
2
S
Note
Measurement values in the statistic mode are stored and are protected when changing the geometry or using the sample mode. haze-gloss can store a series of up to 600 measurements per geometry. These data can be transferred to a PC via RS 232 interface. If the geometry is changed in the statistic mode, the values of the last measured series are displayed and the series can be continued if required. During a running measuring series in the statistic mode the calibration must not be changed (compensation, mirror gloss, customer-specified) since this would falsify the statistical results.
DELETE Delete last value
-->DELETE
Delete statistics
-->RESULT
Escape:
SAMPLE
delete key
delete
The counting variable n is reduced by 1. The last reading can only be deleted if no other function has been called after the last measurement.
results
deletes last reading.
results key deletes the complete measurement series of the set geometry.
9. International Specifications
DIN 67 530 Reflectometer as a means for gloss assessment of plane surfaces of paint coatings and plastics
ISO 2813 Paints and varnishes ­Measurement of specular gloss of nonmetallic paint films at 20°, 60° and 85°
ANSI/ASTM D 523 Standard Test Method for Specular Gloss
ASTM D 2457 Standard Test Method for Specular Gloss of Plastic Films
BS 3900 (Part D2 - D5) British Standard Methods of Test for Paints Gloss (Specular Reflection Value)
JIS Z 8741 Method of Measurement for Specular Glossiness
10. Interface Description
The haze-gloss is equipped with a serial interface (RS 232 C), which allows for data handling and control of the unit with a PC. A 9-pin SUB-D connector is mounted on the measuring unit for transfer purposes.
haze-gloss PC
1
5
Transfer Rate and Format
The serial asynchronous transfer of data is specified in the measuring unit and is performed according to the following format:
2400 baud, 8 data bits, no parity, 1 stop bit
Control Commands 'O' (ASCII) starts the on-line operation
(ONLINE appears on the display)
- the haze-gloss keyboard is blocked
- automatic measurement is started using the operating switch
3 TxD -------- RxD 3
6
2 RxD -------- TxD 2 7 RTS -------- CTS 5 8 CTS -------- RTS 4
9
5 ------ GND ------ 7
SET UP Status of haze-gloss is transferred to the computer: (1 byte each INTEGER)
- Current Mode: 0 = sample mode 1 = statistic mode
- Selected Geometry: 0 = haze 1 = 20° 2 = 60° 3 = 85° 5 = 20° & 60° 6 = auto-range 7 = 60° & 85°
- Current Downward Movement: 0 = lower 4 cm 1 = lower 7 cm
- Target Illumination: 0 = off 1 = on
- Decimal Point: 0 = display without decimal point 1 = display with decimal point
- Mirror Mode: 0 = off 1 = on
- Custom. Calibration: 0 = off 1 = on
- Compensation: 0 = off 1 = on
- Selected Language: 0 = German 1 = English 2 = French 3 = Italian 4 = Spanish
Operating the haze-gloss via PC (identical with function keys) All keys on the unit are blocked except for the operating switch (1 byte INTEGER)
Byte
0 haze key 1 20° key 2 60° key 3 85° key 5 20° + 60° key 6 auto-range key 7 60° + 85° key 9 sample/statistic key 10 results key 11 set up key 14 delete key 15 operate key
(or operating switch):
The readings of the last measurement are transferred to the PC (2 readings of 2 bytes each INTEGER multipied by 10, LSB, MSB). Using a single angle geometry, the second value is set to zero.
‘P‘ Switch off ONLINE-operation, haze-gloss keys are released
‘Q‘ Transfer of statistical values of the required geometry to the computer
Computer code (1 byte INTEGER) for the selected geometry:
0 20° values, single angle geometry 1 60° values, single angle geometry 2 85° values, single angle geometry 3 20° values, dual angle geom. (20 & 60°) 4 60° values, dual angle geom. (20 & 60°) 5 60° values, dual angle geom. (60 & 85°) 6 85° values, dual angle geom. (60 & 85°) 7 haze values 8 20° values in haze mode
haze-gloss code/characters
4 byte index (number of values) 2 byte each INTEGER (multiplied by 10) reflectometer values
11. Technical Data
Measuring Geometries: 20° & haze, 60° , 85° Illuminated Area (mm/in.): 20° & haze 60° 85° ø 15 15 x 27 8 x 60 ø 0.6 0.6 x 1.0 0.3 x 2.4
Measuring Range: Gloss 0 - 2000 gloss units Haze 0 - 2500 gloss units Range change to mirror reection: automatic or preselectable
Display Resolution:
0.1 unit (range: 0-100 units) 1 unit (range: > 100 units)
Accuracy**: Gloss Repeatability ± 0.05 units* Reproducibility ± 0.3 units* Absolute Accuracy ± 1 unit Long-term Stability ± 0.2 units* (> 10000 measurements) Temperature Drift 0.02 units/°C*
Haze Repeatability ± 0.3 units* Reproducibility ± 2.0 units* Long-term Stability ± 0.3 units* (> 10000 measur.) Temperature Drift: 0.2 units/°C*
Measuring Time: 1.5 - 4 sec. (mode dependent)
Light Source: tungsten lamp (5 V / 190 mA)
Detector: silicon photocell V(Lambda) ltered
Display: LCD with back lighting
Statistics Memory: 9 x 600 meas. battery backed data protection for 10 years
Interface: RS 232 C for control and data evaluation via PC
Connections: RS 232 C 9-pin Sub-D footswitch 15-pin Sub-D
Power Supply: 115/230 V 50/60 Hz
Power Requirement: 50 VA
Fuses: 1 AT (230 V)
1.6 AT (115 V)
Temperature Range: Operation +10 to +40 °C Storage 0 - to 50 °C
Dimensions (cm): Width 33 cm / 13.0 in. Depth 40 cm / 15.7 in. Height 52 cm / 10.5 in.
Weight: 14,3 kg
Test Marks: DIN, GS-TÜV
Particularities: Display in
English, German, French, Spanish, and Italian
* Standard Deviation ** Related to a high gloss standard;
Haze values are related to values >10 haze units due to the logarithmic scaling.
Technical Data are subject to change without notice.
12. Sources of Errors
ERROR !
Cause
In the automatic measuring mode the measurement is started before the sample is moved close enough to the measuring aperture.
Remedy
Repeat measurement.
Memory full!
Please Recalibrate!
20° Lamp defect !
Delete: Escape:
DELETE SAMPLE
Cause
The storage capacity is exhausted (600 memory locations).
Remedy
If possible, transfer stored data to a PC.
Continue:
Cause
Lamp is defect.
Remedy
Replace the lamp.
OPERATE
Continue: Calibration:
SET UP OPERATE
Cause
Lamp aging or loss of stored calibration values.
Remedy
Re-calibrate.
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