Thank you for purchasing the WE440 Phosphate Analyzer.
This Instructor’s Manual contains all essential information for the user to make full use of WE440.
Please read the following respective documents before installing and using the WE440.
The related documents are listed as follows.
General Specications
ContentsDocument numberNote
Model WE440 Phosphate AnalyzerGS 12Y18A04-01ENOnline manual
“EN” in the document number is the language code.
User’s Manual
ContentsDocument numberNote
WE410, WE420, WE430, WE440
WET CHEMISTRY ANALYZER
Safety Precautions and Protection of Environment
Model WE440 Phosphate AnalyzerIM 12Y18A04-01ENOnline manual (This manual)
“EN” in the document number is the language code.
An exclusive User’s Manual might be attached to the products whose sux codes or option
codes contain the code “Z” (made to customers’ specications). Please read it along with this
manual.
IM 12Y18A00-01EN
i
Attached to the product
(printed manual)
You can download the latest documents from our website. Scan QR code.
• Please provide the user’s manuals to your end users so that they can keep the user’s
manuals for convenient reference.
• Please read the information thoroughly before using the product.
• The purpose of these user’s manuals is not to warrant that the product is well suited to any
particular purpose but rather to describe the functional details of the product.
• No part of the user’s manuals may be transferred or reproduced without prior written
consent from YOKOGAWA.
• YOKOGAWA reserves the right to make improvements in the user’s manuals and product at
any time, without notice or obligation.
• If you have any questions, or you nd mistakes or omissions in the user’s manuals, please
contact our sales representative or your local distributor.
n Drawing Conventions
Some drawings may be partially emphasized, simplied, or omitted, for the convenience of
description.
Some screen images depicted in the user’s manual may have dierent display positions or
character types (e.g., the upper / lower case). Also note that some of the images contained in this
user’s manual are display examples.
ii
n Trademark Acknowledgments
• All other company and product names mentioned in this user’s manual are trademarks or
registered trademarks of their respective companies.
• We do not use TM or ® mark to indicate those trademarks or registered trademarks in this
user’s manual.
IM 12Y18A04-01EN1st Edition : Oct. 04, 2019-00
u Safety Precautions
n Safety, Protection, and Modication of the Product
• In order to protect the system controlled by the product and the product itself and ensure
safe operation, observe the safety precautions described in this user’s manual. We assume
no liability for safety if users fail to observe these instructions when operating the product.
• If this instrument is used in a manner not specied in this user’s manual, the protection
provided by this instrument may be impaired.
• If any protection or safety circuit is required for the system controlled by the product or for
the product itself, prepare it separately.
• Be sure to use the spare parts approved by Yokogawa Electric Corporation (hereafter
simply referred to as YOKOGAWA) when replacing parts or consumables.
• Modication of the product is strictly prohibited.
• The following safety symbols are used on the product as well as in this manual.
WARNING
This symbol indicates that an operator must follow the instructions laid out in this manual in order
to avoid the risks, for the human body, of injury, electric shock, or fatalities. The manual describes
what special care the operator must take to avoid such risks.
iii
CAUTION
This symbol indicates that the operator must refer to the instructions in this manual in order to
prevent the instrument (hardware) or software from being damaged, or a system failure from
occurring.
CAUTION
This symbol gives information essential for understanding the operations and functions.
NOTE
This symbol indicates information that complements the present topic.
This symbol indicates Protective Ground Terminal.
n Warning and Disclaimer
The product is provided on an “as is” basis. YOKOGAWA shall have neither liability nor
responsibility to any person or entity with respect to any direct or indirect loss or damage arising
from using the product or any defect of the product that YOKOGAWA can not predict in advance.
IM 12Y18A04-01EN1st Edition : Oct. 04, 2019-00
u CE marking products
n Authorized Representative in EEA
The Authorized Representative for this product in EEA is Yokogawa Europe B.V. (Euroweg 2,
3825 HD Amersfoort, The Netherlands).
n Identication Tag
This manual and the identication tag attached on packing box are essential parts of the product.
Keep them together in a safe place for future reference.
n Users
This product is designed to be used by a person with specialized knowledge.
n How to dispose the batteries:
This is an explanation about the EU Battery Directive. This directive is only valid in the EU.
Batteries are included in this product. Batteries incorporated into this product cannot be removed
by yourself. Dispose them together with this product.
iv
When you dispose this product in the EU, contact your local Yokogawa Europe B.V.oce.
Do not dispose them as domestic household waste.
Battery type: Manganese dioxide lithium battery
Notice: The symbol (see above) means they shall be sorted out and collected as ordained in the
EU Battery Directive.
IM 12Y18A04-01EN1st Edition : Oct. 04, 2019-00
Model WE440
Phosphate Analyzer
IM 12Y18A04-01EN 1st Edition
CONTENTS
u Introduction ....................................................................................................i
u Safety Precautions ......................................................................................iii
u CE marking products ..................................................................................iv
1. General Information ................................................................................. 1-1
8.6 Stand-By Mode and Extended Shutdown ...................................................... 8-7
9. Standby and On-Demand Modes ........................................................... 9-1
Revision Record .......................................................................................................i
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Blank Page
<1. General Information>
1. General Information
The YOKOGAWA WE400 series analyzers are compact wet-chemistry analysis systems,
designed for the continuous on-line analysis of water in several applications across many
industries.
The WE440 Phosphate Analyzer uses the colorimetric detection method that relies on specic
reagents that are added to the sample to produce a reacted color compound.
The intensity of the color determines the concentration in reference to a known reacted standard.
The colored compound absorbs energy at a specic wavelength in accordance with the Beer-
Lambert Law.
The instrument uses Light Emitting Diodes (LEDs) that emit light at a narrow bandwidth selected
for the specic application.
The phosphate analysis method uses the blue LED.
n Unpacking the Instrument
Remove the analyzer from its shipping carton and inspect it for damage.
Do not destroy the shipping container during unpacking so that you can save it for possible future
use.
1-1
NOTE
The analyzer may be shipped with a translucent protective cover on the LCD. Carefully peel o
this translucent layer and discard it.
WARNING
DO NOT APPLY ELECTRICAL POWER TO VISIBLY DAMAGED COMPONENTS, AS INJURY
OR FURTHER EQUIPMENT DAMAGE MAY OCCUR.
1.1 Startup Procedure
This section describes the necessary steps to begin using the WE440 Phosphate Analyzer. Refer
to Chapter 2 for instructions on mounting the analyzer, making the plumbing connections, and
connecting electrical power. More details can be found in subsequent chapters.
Once the analyzer is securely mounted in a xed location, wired to electrical power, wired to
communications, (if necessary) and plumbed to process water, perform the following instrument
startup procedure:
1. Power on instrument.
2. To allow longer lifetime of unit, the pump-head tubing are not fully engaged when the unit is
shipped. Refer to Plumbing Connections section.
a. Reset tubes in pumps heads.
Note: This step must be repeated for all pump heads.
i. Remove tape.
ii. Slide tube retainer into place along keyway.
iii. Install tubing cover by squeezing both sides, and sliding into grooves.
3. Install reagents. Very carefully match reagent numbers and colors in their proper order.
Refer to “2.2.2 Installing the Reagents” section.
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<1. General Information>
NOTE
• It is recommended to wear latex gloves whenever handling or changing reagents.
• Turn the reagent cap clockwise while holding bottle vertical and level.
• Inspect the tubes to be sure none have been pinched.
4. Prime the tubing. (See Installing Peristaltic Pump Head Tubing section for more details.)
a. Press Menu.
b. Select Services.
c. Select Prime Fluidics.
d. Select Prime All.
Note: This procedure will run automatically and take approximately 10 minutes per cycle.
5. Refer to Chapter 3 for more details on startup and operation. Once the above four steps
have been completed, (4. a, b, c, d) press Run. Allow the unit to operate overnight or for at
least 12 hours, to become stabilized in the local environment.
6. For additional information on WE440 Phosphate Process Analyzer Operation, refer to
Chapter 3.
Additional details can be found in the following sections:
“3.6 Instrument Operation Modes”
“4. Analyzer Hardware Conguration and Calibration”
“5. Calibration of the Instrument for Measurement Analysis”
“6. Menu Overview”
“7. Terms Denition”
“8. Maintenance Schedule”
1-2
RGTSTD
REAGENT STANDARD
DRAIN
Figure 1.1 Reagent bottle numbers in proper order
SAMPLE (INLET)
SAMPLE (RETURN)
SAMPLE CHAMBER
SAMPLE
SMP
SAMPLE CHAMBER
WITH FLOAT SENSOR
1.2 General Product Description
This user manual provides the information necessary to obtain the maximum benets from the
WE440 Phosphate Analyzer. All operating instructions, functional descriptions, illustrations, and
other relevant information are contained in this manual.
Descriptions of the system hardware and user-interface software (the control panel) are included,
as an overview of the analytical techniques employed in the analyzer. Step-by-step instructions
guide you through all operating procedures and eld programming.
The analyzer is designed for easy operation. Each analyzer in this family runs in a fully
automated mode for routine, day-to-day water analysis.
The need for operator interaction is minimal. Accordingly, the information required by the routine
operator of this analyzer is modest, and that information is provided in Chapter 3 Startup and
Operation, of this manual.
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<1. General Information>
Important standard analyzer capabilities include:
• Sampling the process stream automatically.
• Calculating concentration of your sample and reporting it in units of concentration.
• Recalibrating automatically at preprogrammed intervals to compensate for any changes in
captured sample volume, pump ow rates and reagent composition.
• Cleaning automatically (when programmed) at user-specied intervals to prevent
precipitation build-up, coating of the optics or bacterial/fungal growth.
The analyzer brings colorimetric laboratory precision to the real world of unattended process
analyzing. It is designed for long life under continuous, rigorous use.
The WE400 series analyzers are designed for accommodating several applications. Each
application requires a specic conguration in hardware and software that is set at the factory.
This analyzer model is intended to use for clean water applications such as power plant water
analysis only, suspended solids must be less than 60 microns.
1.2.1 User Interface
n General Description
The user-interface consists of a keypad and a graphical LCD display. The keypad is located
to the right of the display. The “F1-F4” function keys (soft-keys) take on dierent meanings
depending on the menu selection. The column on the left of the soft-keys labels the keys with
their appropriate functions.
1-3
Keys
RUN: starts the analysis
STOP: stops the current functioning of the instrument.
+ , -: allows for navigation between pages
ENTER: conrms selections made in the menus
MENU: accesses the menus, Pressing the MENU key displays the instrument’s Main
Menu. System parameters can be congured from the Main Menu.
soft-keys (in appropriate menus):
additional navigations for left / right or up / down cursor movement.
LCD display
the date, analysis label, time, navigational menus, current user, instrument-working mode,
current status of the instrument and the soft-key labels.
Application name field
Data field Cursor
06/06/19
Display field Time field
PHOSPHATE
MAIN MENU
+SETUP
+MEASUREMENT
+VIEW DATA AND ALARMS
+SERVICES
Function keys assignment
Function keysOperational keys
02:20 PM
Figure 1.2
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<1. General Information>
l Display Fields
1. DATE FIELD shows the current date.
2. CURSOR indicates current selection.
3. APPLICATION NAME FIELD shows instrument name tag.
4. TIME FIELD shows present time.
5. DISPLAY FIELD shows menus / measurements.
6. INFO eld shows information / instructions to navigate.
7. USER eld shows current user name.
8. MODE eld shows whether the instrument is working in Auto, Manual or Run mode.
9. STATUS eld shows current working status of the instrument.
10. FUNCTIONAL KEYS ASSIGNMENT FIELD shows the functions allotted to the functional
keys.
11. FUNCTION KEYS select functions.
12. OPERATIONAL KEYS are meant for operation of the instrument.
l Symbols used
Escape (Cancel/Back)Cursor
Logged out (Locked)Logged in
Scroll UpScroll Down
1-4
PrintDelete
Scroll LeftScroll right
AcceptReject
1.2.2 Menus Display
A “+” before a menu item denotes that the item has multiple options.
Keys
UP/DOWN arrow: scrolls up or down through options
ENTER: shows details of the options
MENU: shifts to Main Menu. Parameters can be congured from the Main Menu
NOTE
The analyzer may be shipped with a translucent protective cover on the LCD. Carefully peel o
this translucent layer and discard it.
1.2.3 Measurement Mode Display
In measurement mode, the instrument displays current and previous readings, units, date and
time. The measurement results can be displayed as large size fonts or normal size fonts. F1 key
will toggle between large and normal fonts.
NOTE
In AUTO mode, the user can navigate between dierent menus even though the instrument is
performing a measurement or a calibration.
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<1. General Information>
POWER AND
I/O SIGNALS
CONNECTIONS
REACTION CELL
AIR VENT
SAMPLE &
STANDARD PUMP
REAGENT
PUMP
SAMPLE &
STANDARD VALVE
SAMPLE (BACK) N.C.
STANDARD (FRONT) N.O.
RGTSTD
RGT
REACTION CELL
ASSEMBLY
1-5
REAGENT STANDARD
DRAIN
SAMPLE (INLET)
SAMPLE (RETURN)
SAMPLE CHAMBER
SAMPLE
SMP
SAMPLE CHAMBER
WITH FLOAT SENSOR
Figure 1.3 WE440 Phosphate Analyzer PO4 layout
WARNING
• Handling chemical samples, standards, and reagents can be dangerous.
• Review the necessary Material Safety Data Sheets and become familiar with all safety
procedures before handling any chemicals.
CAUTION
REAGENT BOTTLES MUST BE KEPT TIGHTLY CLOSED.
Observe all health and safety procedures for handling chemicals. Wash any spillage with Distilled
water.
Allow enclosure to vent any trapped fumes before servicing.
Air purge of enclosure is recommended.
EMPTY ALL REAGENTS BEFORE SHUTTING UNIT DOWN.
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<1. General Information>
1.2.4 Analysis Reaction Principle
The colorimetric method is based on the reaction of reagents with the sample to produce a
color. This color is measured and compared to a standard color, which proportionally denes its
concentration.
The color compound, which is the reacted mixture of the sample with the reagents, absorbs
energy at a specic wavelength in accordance to Beer-Lambert Law.
1.2.5 Fluids Storage
Store all reagents and standards in a dark place at room temperature.
1.2.6 Calibration Standard
Standard part # 229510, the calibration standard required for this application is a 10 ppm
solution. Each calibration cycle consumes approximately 50 mL. Each bottle contains enough
standard solution for approximately 20 calibrations.
1.2.7 Reagents Required
The analyzer requires one reagent, and one standard solution. All bottles are housed in the
uidics enclosure compartment.
For proper operation: Ensure that the reagents are correctly installed, the analyzer tubing is
correctly routed in the pumps and that the analyzer drain tube is connected to an atmospheric
drain. All of the reagents and standard vent tubes need to exhaust to the outside of the enclosure,
to minimize the trapping of any vapors inside the enclosure.
1. Connect sample to the analyzer and ensure that it is owing through the sample chamber
by observing the ow from the sample return line.
2. Turn the power ON to the instrument. After the booting sequence (this may take several
minutes), press STOP and then MENU key.
3. Select SERVICES MENU option and then PRIME FLUIDICS → AUTO PRIME → ENTER.
1-6
The instrument will go through a priming sequence of all the available solution to the analyzer.
Follow the startup procedure described in Chapter 3. You may repeat the AUTO PRIME
sequence as necessary to purge out any trapped bubbles in the lines.
1.2.8 Reagent Consumption
The phosphate method requires one reagent. The reagent usage depends on the frequency of
analysis. Typically 0.23 mL of the reagent is used per analysis cycle.
Based on 4 analyses per hour, the 1 Liter reagent should last approximately 45 days.
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<2. Installation>
2. Installation
The instrument is designed for general-duty, indoor installations. The electronics enclosure
environmental rating is NEMA 12 and the Fluidics enclosure is a NEMA 4X berglass with a clear
door window.
The WE440 Phosphate Analyzer should be installed in a well-ventilated location, with ambient
temperature between 5°C and 45°C (41°F to 113°F); and relative humidity not to exceed 90%
at 40°C. The area must be free from dust, corrosive gases, vibration and shocks; sheltered from
direct sunlight, and shielded from dripping water. Power should be instrument grade with over
voltage protection, and a provision for disconnecting power.
2.1 Mounting the Instrument
The instrument case is designed for wall or panel mounting.
• Use four #10 screws or equivalent for proper support.
• Refer to Figure 2.1 and Figure 2.2 for dimensions (in mm and inches).
• Make sure that the wall that you choose can support the weight of the instrument
(approximately 20 kg or 44 lbs.) See Figure 2.1.
• Locate the instrument as close to the sampling point as practical to ensure complete purging
of the sample line during each cycle.
• Allow approximately 50 cm (20 in.) of clearance at the left side for door swing. Also allow
enough clearance on the right side for wiring conduit.
• Locate the analyzer height such that the display is at eye-level height for an operator,
allowing also for appropriate sample and drain connections.
162 (6.4)
70 (2.75)
406 (16)
304.8 (12.0)
Mounting holes 4-ø8.0 (0.313)
2-1
Unit: mm (inch)
AIR PURGE
152
(6)
698
(27.5)
330.3
(13.0)
VENT LINES
Figure 2.1 Mounting dimensions
DRAIN (3/8”)
41
(1.62)
SAMPLE RETURN (1/4”)
SAMPLE IN (1/4”)
132 (5.19)
25 (0.98)30 (1.18)
POWER IN
I/O SIGNALS
AIR VENT
674.6
(26.56)
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<2. Installation>
2-2
INSTALL HEIGHT TO
OPERATOR EYE LEVEL
FLOW DIRECTION
FILTERED AND OIL FREE
AIR PURGE SUPPLY LINE
FLOW DIRECTION
CONNECT TO
ATMOSPHERIC DRAIN
RGT
SAMPLE (BACK) N.C.
STANDARD (FRONT) N.O.
RGTSTD
REAGENT STANDARD
DRAIN
AC POWER
SAMPLE CHAMBER
SAMPLE
SAMPLE (INLET)
USER TO INSTALL A 40 to 60 MICRON
FILTER, SIZE IS BASED ON SAMPLE
CONDITION, SET FLOW RATE
BETWEEN : 50 TO 500 ML/MIN
SHUT-OFF
VALVE
AC MAINS
1
0
POWER CIRCUIT BREAKER
MUST BE CLEARLY IDENTIFIED
SAMPLE IN
PROCESS LINE
Figure 2.2 Typical external plumbing connections
NOTE
1. It is recommended that you install an external sample shut o valve to allow control while
accessing or service to the sample chamber.
2. Air purging of upper and lower enclosures is recommended.
3. Each analyzer MUST have its own drain tube vented to atmosphere.
4. The installation of a power circuit breaker is highly recommended.
2.2 Plumbing Connections
Sample inlet, sample return and drain connections are made on the bottom side of the
instrument. The sample inlet and sample return ttings on the bottom of analyzer require ¼” OD
(6 mm OD) exible tubing. The drain tting at the bottom of the analyzer requires ⅜” OD (9.6
mm OD) exible tubing. The air purge inlets require ¼” OD tubing. The air purge supply must be
ltered externally and free of oil and any other particulates.
WARNING
SAMPLE RETURN
The ⅜” (9.6 mm) DRAIN MUST BE VENTED TO ATMOSPHERE. The sample drain contains
analysis wastes, which include both sample and chemical reagents. Please check with local
authorities concerning proper disposal of waste from this product.
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<2. Installation>
NOTE
The enclosure drain produces no waste under normal use. However, in the event of spills or
leaks, some waste may be produced.
The analyzer is shipped with all of the internal tubing attached. Before starting up the instrument,
verify that the tubing lines are secured.
2-3
Figure 2.3 Internal tubing and tube routing interconnections
2.2.1 Installing Peristaltic Pump Head Tubing
Press the STOP key.
Disengage the U shape pressure plate of the pump head assembly by pressing with two ngers
and gently move upside as shown in Figure 2.4. Slide the tube tting retainers at each side.
Replace the old tube by sliding o the barbed tting. If necessary, clean the pump rollers.
Lubricate the tubing with pea-sized quantity of silicone oil which should be purchased separately.
Fit the new tube and replace in the pressure plate. Note that the pressure plate sides must click
properly in the pump head assembly and align on both sides.
Repeat above steps for all pumps.
You can test the pump under Diagnostics menu for proper operation:
MENU → SERVICES → DIAGNOSTICS → PUMPS & STIRRER
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<2. Installation>
2-4
Figure 2.4 Installing peristaltic pump head tubing - (Single channel)
2.2.2 Installing the Reagents
The analyzer reagent startup kit contains all the necessary reagent for the specic application.
The reagent and calibration standard are supplied in ready-to-use bottles that can be replaced
directly onto the cap assemblies.
Follow the markings to install each solution into the respective feed line in the analyzer.
2.3 Connecting Power to the Analyzer
CAUTION
Only trained technical personnel should perform installation, electrical wiring and maintenance
of this product. Proper handling is required to avoid ESD (Electrostatic Discharge), as the
internal electronic components on the circuit boards can be damaged by static electricity. It is
recommended that before touching any electronic components, (such as printed circuit cards
and the components on them) you should discharge static electricity from your body. This
can be accomplished by touching an earth-grounded metal surface such as the chassis of an
instrument, metal conduit, or pipe.
The analyzer is equipped with a three terminal power connector strip located in the electronics
enclosure as shown in Figure 2.6.
IT IS HIGHLY RECOMMENDED THAT PROVISIONS FOR AN EXTERNAL CUSTOMERSUPPLIED POWER SWITCH OR BREAKER BOX (WITH COMPLETE CB SPECIFICATION),
CLEARLY MARKED FOR THE ANALYZER AND WITHIN REACH OF THE USER, BE
PROVIDED TO ALLOW REMOVING POWER DURING SERVICE.
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<2. Installation>
The analyzer has been designed to be hard-wired with provisions for the AC power lines to be
routed in conduit pipes connecting to the ¾” FNPT hubs located on the left side of the electronics
enclosure. See Figure 2.5.
When using line cords, use only certied power cords of 3 core, min 0.75 mm2 / 18 AWG, min.
temperature of 75°C, H05VV-F.
The power safety ground must be provided for proper operation.
BEFORE MAKING ANY CONNECTIONS:
• Make sure that the wires are not powered before connecting to the instrument.
• Disconnect any power previously connected to the relays.
• Connect the Phase Hot or L (line), Earth and Neutral to the terminal block. Note the location
of the fuse.
• Insert the wire into the terminal connector and make sure to tighten the screw.
• Route signal connections to the back hub, and power connections separately to the front
hub.
• All connections must conform to local safety standards.
2-5
Figure 2.5 Electrical wiring ports
Table 2.1 AC power terminal wire connections
Analyzer Terminal DestinationNorth America Wire ColorEuropean Wire Color
HOT or L ( Line)blackbrown
Protective Earth Ground (PG)greengreen with yellow tracer
Neutral (n)whiteblue
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<2. Installation>
AC POWER
CONNECTIONS
Figure 2.6 AC power connections
NOTE
When using a UL/CSA approved power cord, loop cord through clip retainer as shown in Figure
2.6 for proper strain relief.
2-6
CAUTION
The analyzer is intended for use only with single-phase power.
The analyzer is not equipped with a power switch, therefore a circuit breaking device such as
a circuit breaker should conform to local safety standards and must be tted before the nal
installation. The circuit breaker must be in close proximity to the analyzer and within reach of the
user, and must be marked clearly as the disconnection device for the analyzer.
ALL CONDUCTORS NEED TO HAVE MINIMUM INSULATION RATING OF 75°C.
2.3.1 Analog Outputs Connections
The analyzer is equipped with two isolated analog outputs. The analog outputs can be
programmed to be any one of the following: 0-20 mA or 4-20 mA or reverse acting i.e. 20 – 0
mA or 20 – 4 mA. The range is also programmable and can be scaled according to application
needs.
The outputs have a common isolation from the main system and can drive up to a 900 Ohms
load.
Please refer to Figure 2.7, and Table 2.1, for signal terminal connection detail.
2.3.2 Alarm Connections
The analyzer has ve level sensor inputs that accept a dry contact closure signal to indicate the
state of the level sensors. Input 5 is typically assigned for sample. The analyzer is equipped with
four relays that have voltage-free contacts. Two contacts: Normally Open (NO) and Normally
Closed (NC) with a Common (C). The relay contacts are rated for use at a maximum of 240 V
and 2 A.
The terminal connectors accept wire gauge up to 14 AWG.
The terminal strip is located at the bottom of the electronics cabinet (Figure 2.7).
Table 2.2 shows the connector order and terminal designation.
• Make sure no power is supplied to the instrument.
IM 12Y18A04-01EN1st Edition : Oct. 04, 2019-00
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