Metrohm TitrIC pro II User Manual

p

n

eana

aareconconMesyspar

n

esofide

dsta

m

a

n

a

d

H

o

m

u

a

h

t

s

o

I

u

y

n

t

r

p

e

u

d

m

p

n

o

e

o

C

e

c

o

m

d

e

o

a

c

s

p

u

n

I

e

t

u

t

o

e

d

m

h

s

I

2.

12.22.32.42.52.6

4.

14.24.3

15.25.3

16.26.26.26.26.26.26.26.36.36.36.3

n

p

d

o

c

o

w

n

e

o

a

e

o

a

e

i

h

w

C

t

T

:

r

t

n

o

A

plicatio

I

stallati

Th

TitrIC pro lysis of w

titr

tion, and ion

determine

ductivity, p

centrations trohm instru tem at any ameters.

alytical seq

A

1.

The sample anion and c

2.

The sample flow-throug Afterwards values) are

Th

whole pro

tware: The u ntification int

is

one by Mag

rting titration

tia

oTM is done

data is concl

All M

gIC Net.

Bulleti

on ins

II system is ter samples

chromatogra

in a ve

, acid ca

f the individu

ents can b

time and

ence

is transferre

tion analysis

is transferre

cell to deter

emperature,

determined i

cedure is c

er enters th

MagIC Net

C Net. MagI

analysis, res

via RS232.

ded in a joint

354

ruction

used for th

using dire phy. The foll y short ti

acity and,

al anions an

incorporate

sed to det

to the two C

.

into an exter

ine the cond

H and acid c

the external

ntrolled by sample po

nly. All sam

Net Comm

pectively tran

report contai

of Titr

fully autom

t measurem

wing parame e: temperat in parallel,

cations. Fur

in the exis

rmine additi

mpact ICs fo

al cell via th

uctivity.

pacity (p an

ell.

the MagIC ition and sa le liquid hand

nication suc

sfer of result

ing all result

C pro

atic

ent,

ers

re, the her

ting

nal

r

m

Net

ple

ling

as

to

by

I

Ta

ble of conte

1.

Delivery

-delivere

-Optional

Installati

2.

. 815 Rob

. Titrando

. Conduct

. 881 Com

. Dosino h

3.

Cable co

Tubing c

4.

. External

. Installati

. Overvie

5.

Miscella

5.

. Membra

. Stirrer ....

. Electrod

6.

Software

6.

. Installati

ts:

ackage: .......

with TitrIC p

accessories:

n ..................

tic USB Sam

2.905.0010) .

meter (2.856

pact IC pro –

lder (6.2057.

nections ......

nnections .....

ell ................

n of the 50 m

of all the tub

eous .............

e Pumps of t

.....................

s ...................

.....................

n of the soft

.....................

ro II package

.....................

ple Processo

.....................

.0010) ...........

Anion – MCS

Cation (2.881

210) .............

.....................

L Dosing Uni

ing connectio

.....................

e 815 ..........

.....................

are ...............

.....................

....................

.....................

XL (1T/2P) ..

.....................

(2.881.0030)

.0010) ..........

.....................

....................

s .................

.....................

.... 3

.... 4

... 5

.... 5

.... 6

.... 7

.... 8

. Configur

.1. Devices .

.2. Solution .

.3. Swing H

.4. Lift positi

Fig

.: TitrIC pro II s

stem setup

.5. Needle ri

.6. Methods

. Configur

.1. Devices .

.2. Solution .

.3. Electrod

tion of MagI

.....................

ad configura

ns ................

nse position ..

.....................

tion of tiamo

.....................

s ...................

Net .............

.....................

ion ................

.....................

..................

.....................

Page 1

.... 8

.... 9

f 14

Application Bulletin 354

Installation Instruction of TitrIC pro II

6.3.4. Methods .................................................................... 9

6.4. Setup of RS232 communication between MagIC Net

and tiamo

TM

............................................................ 10

7. Complete Analysis with TitrIC ................................. 10

9 TitrIC pro – Combo Kit Dilution ............................... 11

9.1 Delivery package .................................................... 11

9.2 Installation .............................................................. 11

9.3 Dosino .................................................................... 11

9.4 Transfer Tubing ...................................................... 11

9.5 External Dilution Vessel .......................................... 11

9.6 Analysis .................................................................. 11

9 TitrIC pro – Combo Kit Partial Loop ........................ 13

9.1 Delivery package .................................................... 13

9.2 Installation .............................................................. 13

9.3 Rinsing station ........................................................ 13

9.4 MiPT Dosino ........................................................... 13

9.5 Analysis .................................................................. 13

Page 2 of 14

Application Bulletin 354

Installation Instruction of TitrIC pro II

1. Delivery package:

-delivered with TitrIC pro II package:

No. Article no. Article designation

IC

1 2.881.0010 881 Compact IC pro - Cation

1 2.881.0030 881 Compact IC pro - Anion - MCS

2 2.850.9010 IC Conductivity Detector

Sample processor

1 2.815.0020 815 Robotic USB Sample Processor

XL (1T/2P)

1 2.786.0040 Swing Head

1 6.1462.040 Robotic Arm with transfer head for

786 Swing Head, right swinging

1 6.2833.020 Needle holder 1/8 in. With tubing

connection M6

1 6.1835.050 PEEK sample aspiration tube (1.58

mm ID)

1 6.2629.000 Screw nut to needle holder IC

Conductometry

2.856.0010 856 Conductivity Module

1 6.0915.100 Five-ring conductivity measuring cell,

c = 0.7 cm-1, with Pt 1000

1 6.2151.000 Cable USB A - mini-DIN 8P (R)

1 6.2763.000 Flow through cell for 60915100

p and m value titration (pH measurment)

1 2.905.0010 905 Titrando

1 6.0277.300 iAquatrode plus with Pt 1000

1 6.2151.000 Cable USB A – mini-DIN 8P

1 6.2307.230 Buffer solutions pH 4, 7 and 9

1 6.2325.000 Phit kit

Liquid Handling

2 2.800.0010 800 Dosino

1 6.3032.220 807 Dosing Unit, glass, 20 mL

1 6.3032.250 807 Dosing Unit, glass, 50 mL

1 6.2057.210 Holder Dosino for IC Instruments

1 6.1608.030 Glass bottle GL45 1L (round)

1 6.1808.280 Adapter Dosino Port 4 / M6

1 6.1618.020 Thread adapter S 40 to GL45

2 6.2744.080 Coupling M6-UNF 10/32 (Dosing Unit

– IC screw)

1 6.2744.070 Pressure screw made of PEEK,

short, 5x

1 6.1808.010 Coupling piece 2 x M6 outer threads

1 6.1808.060 T Connector M6

Connection tubings

1 6.1805.060 Connection tubing FEP, L = 60 cm, 2

x M6 thread

2 6.1805.110 Connection tubing FEP, L = 80 cm, 2

x M6 thread

1 6.1805.030 Connection tubing FEP, L = 150 cm,

2 x M6 thread

External cell

1 2.802.0020 802 Rod Stirrer

1 6.2001.070 Stand support for 804

1 6.1414.060 Titration vessel lid micro ECO

1 6.1415.250 Titration vessel / 50-150 mL

5 6.2730.030 Stopper with nipple and O-ring

1 6.2730.080 Screw nipple M16/NS14

1 6.2730.020 Septum stopper

3 6.2730.060 Screw nipple for electrodes

1 6.1543.170 Aspiration tip M8

1 6.2709.090 Stopper (12 mm)

1 6.1543.210 3-way stopper with antidiffusion valve

Software

1 6.6056.231 Tiamo 2.3 light CD: 1 Licence

1 6.6059.232 MagIC Net 2.3 Professional CD: 1

Licence

RS232 Communcation MagIC - Tiamo

1 6.2134.040 Connecting cable RS-232 to IMP-PC

(DBp)

2 6.2148.050 USB/RS-232 Converter for 900

Touch Control / Ti-Touch

-Optional accessories:

1 6.2041.xxx Sample rack made of PVC

1 6.1432.xxx Sample beaker

1 6.2324.000 Conductivity standard (100 µS/cm)

1 6.2301.060 Conductivity standard (12.88 mS)

1 6.2307.230 Buffer solutions 3 x 10 x 30mL of pH

4 / 7 / 9

1 6.2065.000 Stacking frame for 846 Dosing

Interface, 856 Conductivity Module,867 pH Module

1 6.2041.800 Sample rack 100* 75 ml

1 6.2041.810 Sample rack 34* 150 ml

1 6.2041.820 Sample rack 28* 250 ml

1 6.2041.840 Sample rack 59* 120 ml

Page 3 of 14

Application Bulletin 354

Installation Instruction of TitrIC pro II

1 6.1432.210 Sample beaker 75 mL made of glass

(for 6.2041.800)

1 6.1432.320 Sample beaker 250 mL made of

glass (for 6.2041.820)

1 6.1453.250 Sample beaker 250 mL made of

polypropylene (for 6.2041.820)

1 6.1459.300 Sample beaker 120 mL made of

polypropylene (250 pieces) (for

6.2041.840)

1 6.1006.510

Metrosep A Supp 5 - 100/4.0

1 6.1006.520 Metrosep A Supp 5 - 150/4.0

1 6.1006.500 Metrosep A Supp 4/5 Guard/4.0

1

6.1030.410 Metrosep A Supp 15 – 100/4.0

6.1030.420 Metrosep A Supp 15 – 150/4.0

1 6.1030.500 Metrosep A Supp 15 Guard/4.0

1 6.1050.410 Metrosep C 4 – 100/4.0

1 6.1050.420 Metrosep C 4 – 150/4.0

1 6.1050.500 Metrosep C 4 Guard/4.0

1 2.849.1030 849 Level Control for Inline Eluent

Preparation

2. Installation

The following is a detailed description of the TitrIC pro II installation.

We strongly recommend that the individual steps are carried out in the order given below!

2.1. 815 Robotic USB Sample Processor XL (1T/2P)

The sample processor is placed at the side at which it is most easily accessible. Please note that the following procedure refers exclusively to the version in which the sample processor is located at the left-hand side of the IC system.

 On the left-hand side of the 815 Robotic USB Sample

Processor XL, attach the stand support (6.2001.070) for the external titration vessel.

 Mount the Swing Head (2.786.0040) onto the 815 (see

installation instructions).

 Do not screw the robotic arm (6.1462.040) onto the

Swing Head!

 The Sample Rack supplied is screwed onto the 815.

 In the vicinity of the 815 the two canisters (standard

equipment of 815) are placed on the floor: One 10 L canister is used as a waste container, the second one as a reservoir for deionized (DI) water used for rinsing the external cell.

 From the smaller opening of the canisters containing DI

water, an M8 PTFE tubing connection of suitable length is led to the connection box made of white plastic of membrane pump 1 / tower 1 and connected.

 From the front opening of the waste canister an M8

PTFE tubing connection of suitable length is led directly to membrane pump 2 / tower 1 (black plastic) and connected.

A more detailed description is given in the instructions for use of the 815 Robotic USB Sample Processor XL.

2.2. Titrando (2.905.0010)

Directly to the right of the 815 Robotic USB Sample Processor, place the Titrando with a bottle of titration solution (0.1 mol/L HCl will be connected to the 20 mL Dosing Unit and 800 Dosino).

2.3. Conductometer (2.856.0010)

The 856 Conductometer is placed directly at the left of the Titrando. For detailed information about the usage check the Instructions of Use of the 856.

Before measurement it is recommended to carry out the calibration of the cell constant in the flow-through cell of this setup. For further information consult the Installation Instructions of the 856 Conductometer.

Page 4 of 14

a

h

sThe

3

e

rinssw

ethe

t

m

e

p

o

h

e

o

C

U

o

d

C

o

n

e

o

c

t

e

M

/

e

f

n

v

o

r

3

s

r

o

T

h

r

o

0

2

p

s

e

r

(

B

C

(

n

t

e

5

(

m

e

n

M

m

.

e

d

o

n

f

5

e

n

f

o

d

c

o

f

o

n

e

a

b

5

e

0

e

a

m

e

w

i

AIn

eope

ascr

g

1

u

p

0

n

e

s

c

s

d

s

e

r

e

s

e

r

w

s

e

r

w

.

D

t

e

.

p

2

t

a

n

8

h

6

n

8

h

6

e

n

8

h

6

t

.

o

h

o

h

d

o

e

p

m

e

w

p

m

e

w

n

p

m

e

p

n

1

-

s

n

t

o

g

a

pplication Bulle

stallation Instr

in 354

ction of TitrIC

ro II

2.4. 881 C

Pl

ce the 881 C

to

the right of t

installed. Pl

be

mpact IC pro

Co

2.5. 881 C

ce the 881

Pl rig

t of the 881

ins

trument can

tructions for

In

2.6. Dosin

Dosino hol

sid

e of the 881

032.250) D

(6. lat

r stage.

3.

Cable con

Fi

st all the

truments. B

itched off.

Controll

Conduct Process

2x USB

Compac

Controll

Connect

(transfer injection Anion –

Connect

(0.1 mol

Controll

USB 2 o

4.

Tubing co

4.1. Exter

numbers gi

Th

drawing bel

In

he next step

co

ponents a

(6.

1414.060):

small 6.27

Th ar

screwed loo

in

osition when

(2.881

mpact IC p

.0030)

ompact IC pr

e Titrando. ase consult t instruments.

mpact IC p

ompact IC p Compact IC

already be se for the C

o holder (6.2

der (6.2057.

ompact IC

sing Unit is

ections

power cabl

oth the inst

r cable USB

ometer to US

r.

able (6.2151

IC pro to P

r cable USB

r, do not co

the MSB cab

to external ti

valves) to th

MCS at MSB

the MSB cab

L HCl) to 90

r cable USB

the 815 Sa

nections

al cell

en here ( ,

w.

the external

e inserted

0.030 stopp ely into ope

the buret tips

o – Anion –

– Anion –

he IC instru

e Instruction

o – Cation (2

o –Cation (2

pro – Anion

installed. Pl

mpact IC pro

57.210)

10) is place ro – Anion –

crewed ont

s are co

uments and

6.2151.000)

1 of the 81

.020) from th , do not con

6.2151.000) nect!

le from Dosin ration cell an

881 Compa

1

le from Dosin MSB 1

6.2151.000) ple Process

...) and “ope

cell is prepar

in the titr

rs (with the

ings 1, 2, 3,

, etc. are ins

CS

CS (2.881.0

ent can alre

s for Use for

.881.0010)

881.0010) to – MCS. Th

ase consult instruments.

on the left

MCS; the 50

this holder

nected to

the PC re

rom 856 Sample

two 881 ect!

rom PC to 81

800, 50 mL

to the IC

t IC pro –

800, 20 mL

rom 905 to

r

ing 1”, ... ref

d. The follo

tion vessel

lack rubber r

and 7 and fi

rted.

30)

ady

the

the IC the

top mL

t a

the

ain

5

r to

ing

lid

ing) xed

A

eptum stop

e 6.2730.08

Th

ning 9 and

op

nings 4, 8 a

Th

e titration v

2001.070) u

(6.

ght with the

he

nd support i

st

ew.

Fi

.: Numbers an

(6.

414.060)

The rin

This op

The rin

This is

The rin

The 3-

is insert the dist pump 1 connect

815).

(6.1543 20 mL with the cm, sup Further connect (6.1805

er (6.2730.0 screw nippl

the 6.2730

d 6.

ssel lid is a ing opening

lamping ring mounted on

connections o

ing nozzle (6.

d into openi ibutor (6.180 / tower 1 of t

on (6.1805.0

ning remains

ing nozzle (6.

d into openi ibutor (6.180 / tower 1 of t

on (6.1805.0

here the pH

ing nozzle (6.

d into openi ibutor (6.180 / tower 1 of t

on (6.1805.0

ay stopper wi

210) is put in

osing Unit (0 FEP-tubing c

lied with the

he port 1 of t

d with an FE 110, 80 cm) t

0) is put int e M16/NS14 .060 screw

ttached to t

10. It is fixe and the horiz

the 815 with

n the titration v

2740.020, su

g 1, which is .170) to the

e 815 with th

0, supplied

empty.

2740.020, su

g 3, which is .170) to the

e 815 with th

0, supplied

lectrode is i

2740.020, su

g 5, which is .170) to the

e 815 with th

0, 60 cm, su

th antidiffusio

o opening 6. 1 mol/L HCl)

onnection (6.

807) to the 3 e 50 mL Do

P-tubing con

o the 3-way s

the openin is screwed

nipple M16

e stand sup

at the requ

ntal brace of the socket h

ssel lid

plied with 81

connected vi

embrane FEP-tubing

ith 815).

plied with 81

connected vi

embrane FEP-tubing

ith 815).

serted.

plied with 81

connected vi

embrane FEP-tubing plied with

valve Port 1 of the is connected

805.100, 40

way stopper.

ing Unit is

ection opper.

6. into into

port

ired

the

ead

5)

Page 5

f 14

Application Bulletin 354

Installation Instruction of TitrIC pro II

The PTFE aspiration tip (6.1543.170, M8) is

inserted in opening 7, which is connected via the distributor (6.1808.170) to the membrane pump 2 / tower 1 of the 815 with the M8-PTFE-tubing connection (6.1805.510, 60 cm).

This opening is not used. It can be closed with a

stopper (6.2709.090)

After the screw nipple (6.2730.080) has been screwed into opening 9, the 802 Rod Stirrer (2.802.0020) is pushed through it and connected to the tower 1 stirrer connection of the 815 Robotic USB Sample Processor.

4.2. Installation of the 50 mL Dosing Unit

6.5620.000

Luer: Port 4

Port 3

6.1805.030

Port 1

M6: Port 2

6.2744.080

6.2744.070

6.1803.020

6.1805.110

Fig.: Connections on the bottom of the 50 mL Dosing Units

 Port 1 is used for transferring the sample to the

external titration vessel using FEP-tubing 6.1805.110 (80 cm, supplied by the 815 Sample Processor)

 Port 2 is used for aspirating the sample via conductivity

flow through cell which is connected to the titration arm. The FEP-tubing 6.1805.110 is used here (80 cm, again supplied by the 815 Sample Processor).

 Port 3 is used by for sample transfer to the IC system.

The transition from M6 to the IC screw size (1/16 in.) is achieved with the 6.2744.080 adapter. A PTFE-capillary (0.75 mm ID) is used to aspirate the sample from the T piece at the swing arm through the anion injection valve into the 50 mL Dosino. At the T piece the adapter M6 thread to UNF 10/32 (6.2744.080) is used.

 Port 4 requires a coupling between Luer and M6

(6.1808.280): This port is used for emptying the Dosing

Unit into the waste canister. Herefore the FEP-tubing (6.1805.030) with 150 cm length is used.

Once the tubing connections have been made, the Dosing Unit is attached to the Dosino holder (6.2057.210) with the thread adapter 6.1618.020.

4.3. Overview of all the tubing connections

The three 60 cm FEP-tubing connections

(6.1850.060, supplied with the 815) are used to connect the membrane pump 1 / tower 1 of the 815 and the three rinsing nozzles (6.2740.020, supplied with 815) to the openings 1,3, and 5 of the external cell (see chapter 4.1).

The 60 cm M8-PTFE-tubing connection

(6.1805.510) is used to connect the membrane pump 2 / tower 1 of the 815 and the M8-PTFEaspiration tip (6.1543.170) to the opening 7 of the external cell (see chapter 4.1).

The Robotic Arm (6.1462.040) is equipped with a

PEEK aspiration tube (6.1835.050). The aspiration tube can be mounted using the screw nut (6.2629.000) and the needle holder (1/8 in with tubing connection M6, 6.2833.020). The coupling piece with two outer M6 connections (6.1808.010) is used to connect the needle to the T Connector M6 (6.1808.060).

Two 80-cm-FEP-tubing connections (6.1850.110)

are used to connect the T piece (6.1808.060) at the robotic arm with the flow-through cell (6.2763.000) for the conductivity measurement and the flow-through cell with the 50 mL Dosino at Port

2. The third 80-cm-FEP-tubing (6.1850.110, supplied with the 815) is used to connect the 50 mL Dosino Port 1 to the external titration vessel at the left of the 815

The 40-cm-FEP-tubing connection (6.1805.100,

supplied with the Dosing Unit) is used to connect port 1 of the 20 mL Dosing Unit (0.1 mol/L HCl) with the 3-way stopper in the external cell (opening 6 in chapter 4.1)

The 150-cm-FEP-tubing connection (6.1805.030)

is used to connect port 4 of the 50 mL Dosing Unit to the 10 L PE waste canister (6.1621.000, supplied with the 815).

Suitable lengths of the 0.97 mm PTFE capillary

(6.1803.020, supplied with the 881) are used to connect port 3 of the 50 mL Dosing Unit (using the screws 6.2744.080 and 6.2744.070) and the injection valves of the 881 Compact IC pro

Page 6 of 14

Application Bulletin 354

Installation Instruction of TitrIC pro II

instruments. The injection valves are connected in series and finally connected to the T-piece (6.1808.060) at the robotic arm (using the screws

6.2744.080 and 6.2744.070). In this setup and methods the following sequential arrangement was implemented: T-piece – anion injection valve – cation injection valve – 50 mL Dosino.

5. Miscellaneous

5.1. Membrane Pumps of the 815

The membrane pump 1 at tower 1 is used to supply the DI water for rinsing of the external vessel; the membrane pump 2 is used to empty the external vessel.

Connect the membrane pump 2/tower 1 to the left connector of the Distributor leading to the M8 aspiration tip for emptying the external vessel. The upper part of the membrane pump 2 is connected to the waste canister.

The upper part of membrane pump 1 is connected to the right connector of the Distributor leading to the three M6 rinsing nozzles to rinse the external vessel. The lower part of the membrane pump 1 is connected to the DI-water canister.

5.2. Stirrer

The 802 Rod Stirrer is inserted through opening 9 of the external cell, and connected to the tower 1 of the 815. The propeller (6.1909.050) is pushed on from below.

 Length of the aspiration tips in the external cell

 Clamp the titration vessel to the titration vessel lid.

 The M8 aspiration tip in opening 7 must reach right to

the base of the titration vessel, as this is the only way to ensure that the external cell is cleaned properly.

 The 3-way stopper with antidiffusion valve in opening 6

should reach the middle of the titration vessel.

5.3. Electrodes

 The pH electrode (iAquatrode Plus with Pt 1000;

6.0277.300) is inserted into opening 4. The cable is connected with the 854 iConnect (provided with the

905) to the 905 Titrando at the rear on measuring input

1.

 If the electrode is not used for some time then it should

be returned to its holder and kept in the storage solution (6.2323.000).

 The electrode has to be filled up regularly with the

electrolyte solution (6.2308.020).

 Conductivity cell (6.0915.100): The measuring cell

cable is connected to the opening marked ‘

Cond. Cell’ of

the 856 Conductometer. The measuring cell is inserted into the flow-through cell (6.2763.000). The flowthrough cell itself is mounted on the rod of the stand support (6.2001.070).

Page 7 of 14

S

w

t

agenconaut

eMa

s

3

r

d

o

2

r

d

g

2

f

t

N

D

a

u

e

q

S

D

e

t

o

s

o

p

i

o

v

M

2

h

P

w

a

o

e

s

v

u

5

n

h

c

g

o

)

r

c

e

r

t

o

a

–

d

s

u

g

a

r

d

c

a

h

c

e

c

N

c

b

d

a

AIn

oDo

DPD

D

g

n

m

o

d

o

l

g

o

eGo

s

i

e

u

g

e

n

S

r

o

h

a

n

r

I

L

n

g

o

n

e

N

p

d

t

c

e

A

a

n

a

H

>

k

c

r

m

p

c

d

t

8

c

0

t

w

d

S

o

n

o

u

o

e

w

U

w

,

T

w

g

i

k

6.

Software

6.1. Install



tiamo

standard di be accepte Metrohm.c



MagIC Net

standard di be accepte

Restart win



closed.

6.2. Confi



The Controll

B cables (6.

U to

an USB inter

fe

seconds.

‘

au

omatic installa



Start MagIC

6.2.1.

nnected USB

Co

gIC Net is st

M

erated req

figuration. K

omatically re

on

<Yes>

.

TM

2.

er cable (6.

ation of the

– installation

ectories prop

. Please dow

m/com home

.3 – installat

ectories prop

.

ows and lea

uration of

151.020) of t ace on the

The driver

ion of the soft

et

evices

devices are

rted. After c est the d

ep the propo

uested to sa

oftware

(tiamoTM CD

sed by the p

nload the pat

age.

on (MagIC N

sed by the p

e MagIC Net

agIC Net

151.000) of e two 881 ar C one after

installation f

are

’ for all.

utomatically

nfirmation of

vices are ed device n

e solutions

: All the ogram shoul h 1 from the

t CD): All the ogram shoul

and tiamoTM

he 815 and

now conne

he other. W

llows: click

recognized w the automati

stored in

mes. The us

accept and

the ted it a

on

hen

ally

the r is lick

pplication Bulle

stallation Instr

w the tubin

N

sing unit und

osing Port

rep/Empty

osing Port 1

osing Port 2

F

ill Port

S

pecial Port

Fi

.: Configuratio

U

der ‘

Configu

Sa

ple Process

‘

T

wer 1’

mi

dle of the

‘

C

nfiguration’

va

ues:

6.2.3.

, set t

in 354

ction of TitrIC

lengths an

r ‘

Edit/Proper

LH Titration Sa

Port

Dosing Port 1

Port 1

Port 3

Port 2

Port 4

table of the 50

wing Head

ation’

doubl

r XL 1’

e ‘

xial dist

window u

nd

<Yes>

ro II

ports are

ties…/ Dosing

mple

Length

-

80.0 cm

150.0 cm

160.0 cm

150.0 cm

mL dosing uni

onfiguration

-click on ‘

und

r ‘

nce’

der ‘

nd then en

Devices’

to 196.

Swing

efined for

unit’

as follo

Diameter

-

2.0 mm

0.7 mm

2.0 mm

15 Robotic

,

lick on the e

mm and in

Head’

er the follo

click

ach

s:

SB

ntry

the

on

ing

6.2.2.

Th

solution to

ke sure the

to

MSB 1 of the

wit

h the method

cribed below

de

 At th

‘

Solutio

enter and ‘

Fig

.: Configuration

olution

be used m

osino of the

Anion 881. I s provided, t .

left click

ns’

double-

he followin

C

ncentration’

table for soluti

st be define 0 mL Dosing

order to en

e solution m

on ‘

Confi

lick on the

data unde

:

ns

in MagIC

unit is conne

ure compati

st be name

uration’

, un

ppropriate

‘

Solution n

et. ted ility as

der

nd

me’

Fi

.: Configuratio

C

nfirm the ent

to

Rack

then

nsfer arm (6.

tra H

ad at ‘

to the ‘Manu

To

wer 1’ and

ition’ to defi

po (cl

ck on

 Shift p

 Work p

A

special positi

pared metho

pr

‘

tower 1

6.2.4.

<Confi

positio

sampl

6.2.5.

of the Swing

ies with

nitialize Rac

<OK

1462.040) is

’

.

ift positions

l’ operation

use the ent

e suitable va

ure>

each tim

sition

(approx. 30

sition

(approx. 158

eedle rinse

on of the ra

s, the used

ead at tower 1

>

and open t

’

. Wait a fe

now mounte

lick on ‘815 ies ‘Rack p

lues for the f

e):

for cha

mm)

for aspi

mm)

osition

k is used f

position is n

e properties

seconds.

onto the S

ample Chan

sition’ and

llowing posit

ging the rac

ating of the

r rinsing. In

mber 59. On

go

he

ing

er / ‘Lift ons

the

Page 8

f 14

cbeaThe

p

a

e

o

e

rfam

m

ncon

t

0

h

M

o

n

d

i

_

o

m

v

_

e

m

e

n

r

h

e

a

g

a

g

s

D

t

u

e

q

t

i

o

n

c

o

a

e

o

h

m

s

a

n

e

s

v

o

t

o

d

f

n

o

m

h

m

s

o

e

h

t

a

–

m

b

d

e

s

p

t

f

b

g

h

c

e

c

AIn

rthewitdes

g

oDo

DPD

D

g

u

S

o

d

w

l

n

t

n

g

e

n

E

e

y

w

u

M

c

m

s

e

t

g

p

t

n

h

e

d

t

h

e

r

<

m

i

t

s

g

d

o

M

t

s

o

d

t

n

i

d

a

b

d

t

s

t

o

M

d

b

d

h

e

w

c

r

e

a

n

ra

k 6.2041.84

ker filled wit

6.2.6.

following m

Ne

t:



TitrIC pro II:

Depending carried out:

Value 1 = 1 ion chromat Value 1 = 2 a calibratio Value 1 = 3



This metho method in t



TitrIC pro II

for calibrati used in co

II_ conducti



TitrIC pro II

used to det used in tia

tiamoTM m

Im

ort: Click o

Me

hod manage

rel

ted to TitrIC

th

methods in t

N

te!

Alt

rations of th

pe

son at the

iliar with Ma



Shut down M

6.3. Confi



tiamoTM 2.3 i

6.3.1.

Co

nnected USB

oTM is star

tia

ge

erated req

figuration. K

au

omatically re

on

<Yes>

.

this refers

ultrapure wa

ethods

ethods (.imet

This method

n the value

complete a

ography.

only an ion

)

only a titrati

is used in c

amoTM.

conductivity c

n of the cond

bination with

ity calibration

titer determin

rmine the tit o. It has to b thod

TitrIC pr

Method

… / Edit / I

at t

pro II from th

e folder exa

se methods dministrator

IC Net

gIC Net

uration of ti

started now.

evices

devices are ed. After co

est the d

ep the propo

uested to sa

o the last p ter is placed

files) are pr

s the standar f

Value 1

the

alysis includi

hromatograp

n analysis

mbination wit

alibration:

Thi uctivity sens the tiamoTM .

tion of HCl:

T

r of the 0.1 m

used in com

II_titer deter

e left, then

mport

… Imp

e MagIC Net

ple/TitrIC of

hould only b level and w

moTM

utomatically

firmation of

vices are ed device n

e solutions

sition. A sa here.

vided for Ma

method.

ollowing will

g titration an

hy analysis (

h the

TitrIC pr

s method is u r. It has to be

ethod

TitrIC

is method is

ol/L HCl solut

ination with

ination of HC

elect under

F

rt the meth CD. You will the CD.

carried out

o is thorou

recognized w

he automati

stored in

mes. The us

accept and

ple

gIC

e

.g.

o II

sed

ro

ion

he

l

.

ile /

ods find

y a

hly

hen

ally

the r is lick

pplication Bulle

stallation Instr

Th

e solution to

su

e the Dosin MSB 1 port

h the metho

cribed belo



At the left c under ‘Titra appropriate under ‘

6.3.2.

in 354

ction of TitrIC

olution

e used mus of the 20 m of the 905. I

s provided, t .

ick on ‘Config

ts/Solutions’

(empty) entri

Solu

ion name’

ro II

be defined i

L Dosing uni

order to en e solution m

uration’, then double-click

s and enter t

an

‘

Concentrati

n tiamoTM.

is connecte ure compati

ust be name

at the top rig

n the

he following

n’

:

ake

to ility as

t

Fi

.: Configuratio

N

w the tubin sing unit und

osing Port

rep/Empty

osing Port 1

osing Port 2

F

ill Port

S

pecial Port

Fi

.: Configuratio



pH electrod

‘iAquatrode

<Ok>

Conductivit



on ‘

Edit/Ne

name’ Cond

information

e following

Th

TM

:

mo

tia

TitrIC pro II:



It does the results to M

TitrIC pro II

6.3.3.

.

6.3.4.

table for titrant

lengths an

r ‘

Edit/Proper

HCl

Port

Dosing Port 1

Port 1

Port 3

Port 2

Port 4

table of the 20

lectrodes

: Under ‘

Plus’,

Con

check t

sensor: Und

/other sensor’

ctivity senso

and click on

ethods

methods (.

This method

omplete titra

gIC Net. It i

ethod in Ma

s/solutions

ports are

ties…/ Dosing

Length

-

40 cm

0 cm

25 cm

0 cm

mL dosing uni

figuration/Se

e informatio

er ‘

Configurat

and enter un

,

type in the

Ok>

.

met files)

is the standar

ion analysis used in com

gIC Net.

efined for

unit’

as follo

Diameter

-

2.0 mm

0.0 mm

2.0 mm

0.0 mm

sors’

click on

and click on

on/Sensors’

der ‘

Sensor

esired senso

re provided

method us

nd sends the

ination with

ach

s:

lick

for

d.

In tiamo it i the autorep to do a titra autorepeat

typically use

at mode. In

ion as soon

o to the Run

as a single ther words, i agIC require

window, righ

etermination

is always re

it. To set it i

-mouse-click

in

dy

to

and

Page 9

f 14

Application Bulletin 354

Installation Instruction of TitrIC pro II

select ‘Properties Run window’. Under Process select

Autorepeat determination’. Close the window with <Ok>.

‘

 TitrIC pro II_pH calibration manual: Here the iAquatrode

is taken out of the titration vessel and placed into the

TM

buffer solutions. Start this method only from tiamo

!

 TitrIC pro II_titer determination of HCl: This method is

used for the titer determination. It has to be used in combination with the MagIC Net method

II_titer determination of HCl



TitrIC pro II_conductivity calibration: This method is used

.

TitrIC pro

for calibration of the conductivity sensor. It has to be used in combination with the MagIC Net method

pro II_calibration conductivity

.

TitrIC

Import: Click on Method at the left, then select under File /

Method manager… / Edit / Import…

Import the methods related to TitrIC pro II also from the MagIC Net CD. You will find the methods in the folder example/TitrIC of the CD.

Note!

Alterations of these methods should only be carried out by a person at the administrator level and who is thoroughly

TM

familiar with tiamo

.

 Shut down tiamo

TM

6.4. Setup of RS232 communication between MagIC Net and tiamo

The communication, e.g. result transfer between MagIC Net and tiamoTM is done via RS232. MagIC Net is the master in this setup. To establish the communication follow the steps below:

Make sure MagIC Net and tiamo the PC has two built-in RS232 ports you can connect the RS232 cable (6.2134.040) directly between the two ports. If the PC does not have the built-in RS232 ports please connect two USB/RS232 Converters (6.2148.050) to two USB ports. You can e.g. use the USB hubs of the IC instrument, but it is recommendable to use the USB hubs of your computer, as they are more powerful. Then connect the two converters using the RS232 cable (6.2134.040). In the Device Manager of your Windows operating system check which two RS232 ports you are using.

Open the MagIC Net software. On the left click on

Configuration’, then in the devices window select

‘

TM

software are closed. If

‘

Edit/New/Miscellaneous’ and choose the RS 232 device.

Keep the proposed Device name and enter a random serial number. Go to the RS232 subsection and choose one of the used RS232 ports. Click on ‘ Close the window with

Connect’ and confirm with <Ok>.

<Ok>

Repeat the same steps in the tiamo

TM

software and choose

the second RS232 port.

7. Complete Analysis with TitrIC

As an example a short description of a complete analysis with TitrIC pro II is described here.

The whole procedure is controlled by the MagIC Net

TM

software which is the master software. In tiamo

, the

method TitrIC pro II is selected as a single determination. Start the determination in an autorepeat mode. To set it into autorepeat go to the Run window, right-mouse-click and select ‘

Autorepeat determination’. Close the window with <Ok>.

‘ Start the determination. Now tiamo

Properties Run window’. Under Process select

TM

is waiting for the start

signal from MagIC Net via RS232.

In the MagIC Net software select the method TitrIC pro II. Enter the required sample position, sample identification etc. into MagIC Net. For value 1 choose according to the list below:

 Value 1 = 1 a complete analysis including titration and

ion chromatography

 Value 1 = 2 only an ion chromatography analysis (e.g.

a calibration)

 Value 1 = 3 only a titration analysis

Start the determination in MagIC Net. All sample liquid handling is done by MagIC Net. At the right moment MagIC

TM

Net communicates to tiamo

via RS232 to do the titration analysis. Results are transferred back to MagIC Net and the rinsing steps of the titration equipment by MagIC Net initialized.

All data goes into the MagIC Net database and therefore one report can be generated.

Page 10 of 14

T

9

r

m

C

9

s

9

rThe

9

emo

nsecpiePT

9

e

ePro

u

eper

2

nThi

m

epro

m

C

e

c

0

3

l

t

s

e

o

s

f

a

e

o

i

a

y

n

o

S

m

p

t

d

p

f

l

e

l

T

c

s

g

I

s

1

e

u

)

M

g

e

t

o

t

V

w

o

c

C

c

w

s

e

u

h

e

m

h

g

8

r

t

n

m

u

p

s

a

o

8

)

t

e

F

h

e

t

o

c

s

w

p

u

U

T

e

m

n

s

m

M

v

p

n

a

m

a

AIn

econthe125

g

9

e

u

t

w

a

h

A

m

_

t

n

d

i

_

c

_

n

o

:

c

_

p

d

a

h

u

n

c

o

u

n

e

m

o

m

t

s

o

l

o

k

P

v

e

Val

n

p

t

m

y

f

e

T

a

r

a

b

N

o

n

e

b

C

d

e

a

L

e

pplication Bulle

stallation Instr

in 354

ction of TitrIC

ro II

9

itrIC pro –

.1 Deliv

Fo

the Dilution

ite

s:

N

umber Arti

I

Dilution

1

.2 Instal

A

short straigh

cribed here.

de

.3 Dosin

rt 4 of the Do

Po

h the FEP A

wit

sing Unit 10

Do

e water bottl

pu

Dosino is c

Sa

mple Proces

.4 Trans

Th

10 mL Tr

unted on th

tra

sfer tubing t

ond end of ce at the sw FE capillary

wh

ich is used b

.5 Exter

Th

External Dil

on

the right side

stirrer is c

Th

cessor on M

Us

e the 0.75

e/blue PVC

bl dil

tion vessel

inj

ction valve o

istaltic Pum

Co

nnect the de

744.040) to

(6. do

e with the

s gives the

pu

p channels

Th

external di

cessor, whic

re

oved. The

ombo Kit Di

ry package

setup with

le no. Arti

2.8

0.0010 Do

2.8

1.0010 Ma

6.5

38.000 Titr

ation

forward de

o

ino with the

spiration tub

mL) and mo

(6.1608.070

nnected to

or.

er Tubing

nsfer Tubin

tower (towe

port 1 of th

the transfer

ng arm. If c

nd the M6 U

TitrIC pro I s

al Dilution

ution vessel

of the 815 R

nnected to t

B 2.

m ID PTFE pump tubing via Peristalti f the anions I

the rinse

ector outlet the MSM rin

etector wast ossibility to or pumping t

ution vessel

h is easiest

xact position

ution

itrIC you n

le designatio

ino

netic Stirrer

C pro equip

cription of t

0 mL Dosin

(6.1829.010

nted directly

.

SB 1 at the

with holde r 1). Connec 10 mL UPW

ubing is con nnected, re

NF 10/32 co

andard setu

essel

ith all acces

botic USB S he 815 Rob

apillary (6.1

(6.1826.020

Pump of

. To be abl

hannel has

ith a 2x UN

e channel. T

instead of

se one of th

e sample to

is mounted

when the ra

can be adju

ed the follo

n

ent for Dilutio

e dilution ki

Unit is equip , included in

on the 2 L

15 Robotic

(6.1562.130

one end of

Dosing Unit.

ected to th

ove the 0.75

pling connec

.

ories is mou

mple Proces

tic USB Sa

03.080) and

to connect he MSM to to use the

to be remo

10/32 cou

e rinsing is

ltra pure w

MSM perist

he loops.

nto the sa

k is tempor

ted by direc

ing

n

t is

ped

the ltra

SB

) is

the

he

Tmm tion

ted sor.

ple

the

SM

ed.

ling

ow

ter.

ltic

ple

rily

ting

needle into

th

trol (in the

swing head

mm.

Fi

.: Settings for t

.6

e following (.i

Th

N

t:



TitrIC pro II

method. De following wi

Value 1 = 1 ion chroma Value 1 = 2 a calibratio Value 1 = 3



This metho method in t



TitrIC pro II

is used for to be used i

TitrIC pro II



TitrIC pro II

method is u HCl solutio combinatio

determinati

Th

e following

tia

moTM:



TitrIC pro II It does the results to M TitrIC pro

he external indow manu

ngle is ~117

e 815 Robotic

naly

is

et files) met

dilution:

pending on th

l be carried o

complete a

ography.

only an ion

)

only a titrati

is used in c

amoTM.

dilution cond

alibration of t

n combinatio

calibration co

diution titer d

ed to deter used in tiam with the tia

n of HCl

methods (.

This method

omplete titra

gIC Net. It i

II

dilution

This

.

meth

ilution vesse

l). The appr

.2°. The wor

USB Sample

ods are pro

method is th

e value of

ut:

alysis includi

hromatogra

n analysis

mbination wi

ctivity calibra

he conductivi

with the tia

ductivit

termination o

.

ine the titer o

. It has to b

oTM method

met files)

is the standa ion analysis used in com

od in MagIC

with the ma

ximate valu

position is a

rocessor XL

ided for MagI

standard

ue 1

the

g titration an

hy analysis (

h

TitrIC pro II

ion:

This met

y sensor. It h

oTM method

HCl:

This

the 0.1 mol/

used in

itrIC pro II_tit

re provided

d method us

nd sends the

ination with

et.

ual

for

out

.g.

hod

s

r

for

d.

Page 11

f 14

Application Bulletin 354

Installation Instruction of TitrIC pro II

In tiamoTM it is typically used as a single determination in autorepeat mode. In other words, it is always ready to do a titration as soon MagIC requires it. To set it into autorepeat go to the Run window, right-mouse-click and

Properties Run window. Under Process select

select

Autorepeat determination. Close the window with <ok>.



TitrIC pro II_pH calibration manual: Here the iAquatrode

is taken out of the titration vessel and placed into the

TM

buffer solutions. Start this method only from tiamo



TitrIC pro II_titer determination of HCl: This method is

!

used for the titer determination. It has to be used in combination with the MagIC Net method

II_titer determination of HCl

TitrIC pro II_conductivity calibration: This method is used



.

TitrIC pro

for calibration of the conductivity sensor. It has to be used in combination with the MagIC Net method

pro II_calibration conductivity

.

TitrIC

With the TitrIC pro – Combo Kit Dilution following analysis can be carried out using the TitrIC pro II_dilution methods in

TM

MagIC respectively tiamo

:

The whole procedure is controlled by the MagIC Net software which is the master software. In tiamoTM the method TitrIC pro II_dilution is selected as a single determination. Start the determination in autorepeat mode. To set it into autorepeat go to the Run window, right-mouseclick and select

Autorepeat determination. Close the window with

select

<ok>. Start the determination. Now tiamo

Properties Run window. Under Process

TM

is waiting for the

start signal from MagIC Net via RS232.

In the MagIC Net software select the method

II_dilution

. Enter the required sample position, sample

TitrIC pro

identification etc. into MagIC Net. For value 1 choose according to the list below:

 Value 1 = 1 complete analysis including titration and

ion chromatography.

 Value 1 = 2 only an ion chromatography analysis (e.g.

a calibration)

 Value 1 = 3 only a titration analysis

With Value 1 = 1 a complete analysis is carried out. Depending on the entered dilution factor the following will be done:

Dilution Factor = 1:

Depending on the measured conductivity an appropriate dilution factor is automatically applied by MagIC Net. The calculation factor is calculated according to Time Program

No. 2. The finally used dilution factor is the integer of the conductivity divided by 250.

Dilution Factor >1:

If a dilution factor is known it can be directly entered into the sample table. It will be diluted accordingly. The conductivity measurement has no influence on the dilution in this case.

E.g. With Value 1 = 2 an ion chromatographic analysis will be carried out with the entered dilution factor. No dilution factor will be calculated.

Page 12 of 14

T

9

r

C

9

sdes

9

rthethetem

econappoutang

xpossta

9

e

sthe

e

C

e

t

86.5

l

n

a

c

o

e

r

t

o

t

h

D

a

1

j

e

o

s

a

w

r

o

i

r

h

a

r

e

m

o

j

e

r

t

p

w

a

n

l

1

t

m

c

n

0

T

e

o

k

d

n

m

a

6

r

s

e

p

AIn

o

9

e

u

m

e

c

m

A

i

_

o

t

n

d

i

_

c

a

_

e

m

c

m

i

a

t

g

e

A

d

_

e

n

m

p

)

M

e

o

n

c

o

i

e

w

v

e

t

h

m

i

t

s

g

h

M

d

n

s

a

n

g

C

o

t

f

n

p

t

s

T

y

H

t

a

b

s

t

r

n

e

p

t

o

u

c

a

o

b

d

e

r

h

i

e

d

n

k

d

e

M

9

itrIC pro –

.1 Deliv

Fo

the Partial

foll

owing items:

N

umber Ar

MiPT

I

1

.2 Instal

A

hort straight cribed here.

.3 Rinsi

Fo

this applicat inner comp sample pro

porarily rem

dir

cting the ne

trol (in the

roximately r

er one app

les in the se

2.

The work p ternal positi

(e

ition 2). A

tion to drain t

Fig

.: Settings for t

.4 MiPT

Th

transfer c

do

ino on port

881. This in

pi

ce on the ne

Po

rt 4 of the D

wit

h the FEP A

ombo Kit P

ry package

Loop setup

icle no. A

2.

00.0010 D

338.010 T

ation

forward desc

g station

ion, a stoppe

rtment. The

essor, whic ved. The ex dle into the

window man

lates to a sw

oximately rel

tings for the

sitions are 1

n 1) and 60

ube is fixed

e waste wat

e 815 Robotic

osino

pillary of 2

as well as ection valve

dle with a PE

sino with the

spiration tub

rtial Loop

ith TitrIC p

ticle designa

sino

trIC pro equi

ription of the

r is used to c insing station

is easiest ct position c

insing statio ual). The in ing head ang ates to ~11

xternal needl

20 mm for

for the angl at the botto r.

USB Sample P

L is conne n the anion i is further co

EK capillary

2 mL Dosing (6.1829.010

o you need

ion

ment for MiP

partial loop k

lose the outl

is mounted hen the rac

n be adjuste

with the ma

er compart

e of ~116.5°,

°. Define th e positions 1 he angle 11 e 111° (exte

of the rin

ocessor XL

ted both to

jection valv nected to th .5 mm i.d.

Unit is equip

, included in

the

it is

t of

nto

is by ual ent the

ese and

.5°

rnal

ing

the

on

T-

ped

the

pplication Bulle

stallation Instr

D

sing Unit 2

pu

e water bottl

Th

e Dosino is

pr

Anion instru

.5

Th

e following (.

N

t:



TitrIC pro II

Depending carried out:

in 354

ction of TitrIC

L) and mou

(6.1608.070

onnected to

ent.

naly

is

met files) m

MiPT:

n the value

This m

ro II

nted directly

).

SB 2 at the

thods are pr

thod is the s

f

Value 1

the

on the 2 L

881 Compa

vided for M

andard meth

ollowing will

ltra

t IC

gIC

d.

e

Value 1 = 1 ion chroma Value 1 = 2 a calibratio Value 1 = 3



This metho method in t



TitrIC pro II

used for cal be used in

pro II_calibr



TitrIC pro II

is used to d solution us with the tia

of HCl

complete a

ography.

only an ion

)

only a titrati

is used in c

amoTM.

MiPT conduct

ibration of th

ombination

tion conducti

MiPT titer det

termine the

d in tiamo. It

oTM method

.

alysis includi

hromatogra

n analysis

mbination wi

ivity calibratio

conductivity ith the tiamo

vit

.

rmination of

iter of the 0.1

has to be use

TitrIC pro II_ti

g titration an

hy analysis (

h

TitrIC pro II

:

This metho

ensor. It has

method

Cl:

Tit

This met

mol/L HCl

d in combinat

er determinat

.g.

d is

to

IC

od

ion

on

Th

e following

tia

moTM:



TitrIC pro II:

It does the results to M

TitrIC pro II

methods (.

This method

omplete titra

gIC Net. It i

ethod in Ma

met files)

is the standar

ion analysis used in com

gIC Net.

re provided

method us

nd sends the

ination with

for

d.

TM

In tiamo in autorepe to do a titra autorepeat



select

utorepeat

TitrIC pro II

is taken out buffer soluti



TitrIC pro II

used for th combinatio

II_titer deter

t is typically u

t mode. In ot

ion as soon

o to the Run

Prop

rties Run win

etermination

pH calibration

of the titratio

ns. Start thi

titer determin

titer determi

with the Ma

ination of H

sed as a sing

her words, it i

agIC require

window, righ

ow

. Under P

.

Close the wi

manual:

vessel and

method only

tion of HCl:

ation. It has IC Net meth

l

.

le determinati

always rea it. To set it i

-mouse-click ocess select dow with

Her

the iAquatro

laced into th

from tiamo

T

his method is o be used in

d

TitrIC pro

<o

T

on

y

to

and

>

.

e

!

Page 13

f 14

Application Bulletin 354

Installation Instruction of TitrIC pro II

 TitrIC pro II_conductivity calibration: This method is used

for calibration of the conductivity sensor. It has to be used in combination with the MagIC Net method

pro II_calibration conductivity

.

TitrIC

Import: Click on Method at the left (in MagIC Net and

tiamoTM), then select under File / Method manager… / Edit /

… Import the methods related to TitrIC pro II with the

Import

MiPT kit from the MagIC Net CD. You will find the methods in the folder example/TitrIC of the CD.

Note!

Alterations of these methods should only be carried out by a person at the administrator level and who is thoroughly

TM

familiar with tiamo

and MagIC Net

With the TitrIC pro – Combo Kit Partial Loop setup the following analysis can be carried out using the TitrIC pro II_MiPT methods in MagIC respectively tiamoTM:

The whole procedure is controlled by the MagIC Net

TM

software which is the master software. In tiamo method

TitrIC pro II_MiPT is selected as a single

the

determination. Start the determination in autorepeat mode. To set it into autorepeat go to the Run window, right-mouseclick and select

Properties Run window. Under Process

select Autorepeat determination. Close the window with

<ok>. Start the determination. Now tiamo

TM

is waiting for the

start signal from MagIC Net via RS232.

In the MagIC Net software select the method

. Enter the required sample position, sample

II_MiPT

TitrIC pro

identification etc. into MagIC Net. For value 1 choose according to the list below:

 Value 1 = 1 complete analysis including titration and

ion chromatography.

 Value 1 = 2 only an ion chromatography analysis (e.g.

a calibration)

 Value 1 = 3 only a titration analysis

Page 14 of 14

Metrohm TitrIC pro II User Manual

Specifications and Main Features

Frequently Asked Questions

User Manual