Brookfield UL Adapter Enhanced User Manual

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B R O O K F I
E L D E N G I N E E R I N G L A B O R AT O R I E S , I N C .
 Comm erce B oule va rd • M i dd le bo r o , MA 0  46 US A
ISO9001 CERTIFIED
T
E L
A X
5 0 8 - 9 46 - 6 6 
w w w . b r o o k f i e l d e n g i n e e r i n g . c o m
Bosto n • Chicag o • London • Stuttg art • Guan gzhou
Enhanced UL Adapter
PIVOT CUP, BR-3 (PART OF LAB VISCOMETER)
ULA-E SPINDLE WITH COUPLING NUT, YULA-15E -304 SS YULA-15EZ-316 SS
MOUNTING CHANNEL, ULA-10E
MOUNTING SCREW, HT-99
CLAMPING KNOB, ULA-05EY
TUBE END CAP, ULA-34
(NOT REQ’D WITH ULA-31EYZ SAMPLE CHAMBER)
SAMPLE CHAMBER, ULA-31EY
(304 s/s, open tube)
ULA-31EYZ
(316s/s, closed tube)
CLAMPING COLLAR, ULA-02E
WATER JACKET with MOUNTING COLLAR, ULA-49EAY
CONICAL PORTION OF SHAFT
PIN
Assembly & Operating Instructions
No. M06-084
The Enhanced UL Adapter, shown in Figure 1, is a kit consisting of a spindle with coupling nut attached, sample chamber, mounting channel, and water jacket with mounting collar. It is available in two versions: (1) with type 304 stainless steel suitable for most general purpose applications; (2) with type 316 stainless steel for use with corrosive/acidic applications. All versions are shipped with the water jacket (ULA-49EAY) mounted on the sample chamber.
The type 304 s/s UL Adapter (Part No. ULA-EY) may be used either as an “open tube” or “closed tube” system. In the “open tube” method, the water jacket (ULA-49EAY) must be removed, allowing measurement in a beaker or other suitable vessel. In the “closed tube” method, the sample is poured into the sample chamber with tube end cap installed, which may be temperature controlled by direct immersion into a water bath or with the use of the water jacket connected to a circulating water bath. The 316 s/s UL Adapter (Part No. ULA-EZY) has a closed
sample chamber with solid bottom and cannot be used as an open tube conguration.
The Enhanced UL Adapter may be ordered without the water jacket (Part No ULA-E). Check your sales order to
verify that you have received the correct conguration for your Enhanced UL Adapter.
Figure 1: Enhanced UL Adapter Assembly
Brookeld Engineering Laboratories Inc. -  - Operating Instructions M06-084-A0507
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Assembly & Operation
CLAMPING COLLAR
CLAMPING KNOB
IMMERSION GROOVE
END CAP GROOVE
1. Attach the mounting channel to the viscometer by threading the upper mounting screw into the viscometer pivot cup. Do not overtighten. The end of the mounting channel with the pin must be at the bottom, as shown in Figure 1.
2. Open Tube Operation (#304 stainless steel)
The water jacket (ULA-49EAY) must be removed when the “open tube” method is used. This allows
measurement in a beaker or other container. The sample chamber must be inserted into the clamping collar
before immersion in sample uid. The top of the sample chamber should be ush with the top edge of the
clamping collar.
The clamping collar connects to the mounting channel as shown in Figure 1. The spindle with coupling nut
can be attached to the viscometer beforehand for easy handling. Observe the immersion groove located on the outside of the sample chamber as shown in Figure 2.
3. Closed Tube Operation with Water Jacket The UL Adapter may be used with the ULA-49EAY water jacket and a circulating water bath by connecting
the water jacket to the bath inlet and outlet ports (Figure 3). The tube end cap (ULA-34) is snapped over the bottom end of the sample chamber before the sample is added. Be sure that it is securely seated in the groove. Fill with 16 mL of sample uid. Insert the clamping collar into the mounting collar as shown in Figure 1. Insert the sample chamber upwards into the water jacket and clamping collar. When fully inserted, secure the sample chamber by tightening the clamping knob. Insert the spindle into the chamber. Attach the clamping collar to the mounting channel. Connect the spindle coupling to the viscometer; note left hand
thread. Conrm that the uid level in the sample chamber covers the conical portion of the spindle shaft.
CAUTION: The spindle, sample chamber, and cap (if used) should be clean before use. The cap material
Brookeld Engineering Laboratories Inc. -  - Operating Instructions M06-084-A0507
Figure 2: Sample Tube Immersion
Chamber Shown is #304 Stainless Steel
is low density polyethylene. Replace when damaged or loose.
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Fluid Recommended Recommended Note Temperature Fluid Tubing
-10°C to 15°C TC-FLUID 2
1
ULA-45
R, 2
Do Not Use Gum Rubber Tubing With This Fluid
15°C to 65°C Water Gum Rubber or Fluran
R
65°C to 100°C TC-FLUID 3
3
ULA-45 R Do Not Use Gum
Rubber Tubing With This Fluid
Table 1
R
Fluran is a Registered Trademark of Norton Co.
1. Use only laboratory grade ethylene glycol. Do not use automobile anti- freeze which contains materials that can damage the equipment.
2. Fluran tubing (5/16" ID) and clamps are offered in a kit, part # ULA-45A.
3. Do not use high viscosity oil. Recommended is 50 centipoise.
TEMPERATURE BATH
BATH OUTLET
BATH INLET
VISCOMETER
PIVOT CUP
(on Viscometer)
WATER JACKET OUTLET
WATER JACKET INLET
T
UBE END CAP, ULA-34
SAMPLE CHAMBER
MOUNTING COLLAR
KNOB
Figure 3: ULA-49EAY Water Jacket Connections
4. Level the viscometer. General operating procedures for making viscosity measurements are described in the viscometer operating instruction manual.
5. UL Adapter spindle factors are shown on page 4. The factor is used to calculate viscosity when using Dial
Reading Viscometers. All Brookeld digital model Viscometers and Rheometers calculate the viscosity value
automatically. The spindle entry code for the UL Adapter is 00.
Notes
Maximum recommended viscosity for measurement with the UL Adapter is 2000 cP (mPa•s). If viscosity exceeds 2000 cP, the material being measured may be too viscous to immerse the spindle into the sample chamber; damage to internal parts of the viscometer may result.
For tubing and uid recommendations when using a Constant Temperature Bath, refer to the table below:
Brookeld Engineering Laboratories Inc. -  - Operating Instructions M06-084-A0507
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UL Adapter Factors
SP E CI ALI STS I N T HE
ME AS UR EM EN T AN D
CONTROL OF VISCOSITY
T
EL
508-946-600 or 800-68-89 FAX 50 8-9 4 6 -6 6 
www. b r o o k f i e l d e ngine e r i n g . c o m
BROOKFIELD ENGINEERING LABORATORIES, INC.
 Commerce Boulevard, Mi ddleboro, MA 0 46-0 USA
TYPE I
TYPE II
TYPE III
Threaded
Hole
The factor is used to calculate viscosity in units of centipoise (cP) or milli Pascal seconds (mPa•s) when using Dial Reading or Model DV-I Viscometers. The Viscometer Dial Reading/DisplayValue x Factor = cP (mPa•s). Factors are built-in for Digital Models DV-E, DV-I+, DV-I Prime, DV-II+ (all versions), and DV-III (all versions) — no calculations required.
LV Models
RV-HA-HB Models
Shear Shear Factor Speed Rate Speed Rate (RPM) (sec-1) Factor (RPM) (sec-1) RV HA HB
60.0 73.38 0.1 100.0 122.30 0.64 1.28 5.12
30.0 36.69 0.2 50.0 61.15 1.28 2.56 10.24
12.0 14.68 0.5 20.0 24.46 3.20 6.40 25.60
6.0 7.34 1.0 10.0 12.23 6.40 12.80
3.0 3.67 2.0 5.0 6.12 12.80 25.60
1.5 1.83 4.0 4.0 4.89 16.00
0.6 0.73 10.0 2.5 3.06 25.60
0.3 0.37 20.0 2.0 2.45
1.0 1.22
0.5 0.61
Shear Rate Constant = RPM x .
When an older dial reading visco­meter is used, the viscometer pivot cup may need to be replaced with the current design. If your viscometer has a Type I or Type II pivot cup, the cup should be replaced with a Type
III cup. Contact Brookeld or your Brookeld agent for information.
Brookeld Engineering Laboratories Inc. - 4 - Operating Instructions M06-084-A0507
Figure 4: Pivot Cup Compatibility
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