Fig. 1-1: Structure of the IQ SENSORNET operating manual
The IQ SENSORNET operating manual has a modular structure like the
ENSORNET system itself. It consists of a system operating manual
IQ S
and the operating manuals of all the components used.
Please file this component operating manual into the ring binder of the
system operating manual.
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P 700 IQ
1.2Metrological basics
PhosphateThe salts of the phosphoric acid are called phosphate. With simple
phosphoric acid (orthophosphoric acid, H
3-
(anion PO
).
4
Measuring methodThe P 700 IQ phosphate analyzer measures the concentration of
orthophosphate in an aqueous solution with the aid of the vanadate
molybdate method (yellow method).
The reagent contains an aqueous solution of ammonium metavanadate NH
addition of sulfuric acid H
and ammonium heptamolybdate (NH4)6Mo7O24 with an
4VO3
. In an acidic environment, the chemical
2SO4
reaction takes place according to the following molecular formula:
) this is orthophosphate
3PO4
PO
3-
+ 2 VO
4
-
+ 10 MoO
3
2-
+ 20 H+ → [PV2Mo10O40]5- + 10 H2O
4
The originally pale yellow reagent will turn a deep yellow. The change
of absorbance is photometrically measured at a wavelength of 420 nm.
From this, the concentration of orthophosphate is calculated.
Citation formsPhosphate concentration is quoted in milligrams per liter (mg/l). This
value can either refer to all orthophosphate ions or only to the phosphorus atom included. The values can be converted as follows:
• 1 mg P = 3.066 mg PO4
• 1 mg PO4 = 0.3261 mg P
Concentration values referring to the phosphorus atom are indicated by
the addition PO4-P (citation form).
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P 700 IQ
2
1
3
4
5
6789
Instrument designFig. 1-2, 9 shows the mains components of the P 700 IQ.
1.3Product description
1.3.1 Overview
The P 700 IQ analyzer is designed for online measurements of the
orthophosphate concentration (PO4) in aqueous samples, especially
for phosphorus elimination in waste water treatment plants. Measurement takes place photometrically, at adjustable intervals.
Fig. 1-2: Main components of the P 700 IQ
1 Power supply unit for the photometer unit
2IQSENSORNET interface MIQ/WCA 232
3 Photometer unit P700IQ-PO4
4 Power supply box
5 Filtration pump (instrument option)
6 Overflow vessel
7 Cleaning solution
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8 Standard solution
9 Reagent
P 700 IQ
15 V DC
RS 232
Analyzer P 700 IQ
P700IQ-PO4
Photometer unit
(Options)
(Option “P“)
H1
Line voltage
input
P
F
H2
IQ Sensor Net (data + power)
e.g. SN 12500005
e.g. SN 13030003
Power supply box
PS15V
e.g. SN 12500258
MIQ/WCA 232
IQ Sensor Net
interface
Overload protection
Line filter
On/Off
Power supply unit
e.g. SN 12500258
Climate kit
(option “O“)
Outputs
Legend:
P Filtration pump
H1 Heat tracing for feed line
H2 Heat tracing for permeate return line
F
Power supply and
communication
Fig. 1-3, 10 shows the power supply and communication interfaces
of the P 700 IQ.
Fig. 1-3: Block diagram P 700 IQ
OperationThe P 700 IQ is operated with a terminal on the IQ SENSORNET. It is
connected to the IQ S
ENSORNET through the MIQ/WCA 232 interface.
For more ease of use while maintenance activities are being carried out
on the open analyzer, a mobile terminal can be docked onto the lid of
the MIQ/WCA 232. The MIQ/WCA 232 interface is supplied with power
by the IQ S
ENSORNET.
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P 700 IQ
V8
2
NO
3
NC
V7
V11
VK6
VK5
Currentless path, filled
1
C
V8V7
V11
VK6
VK5
Cleaning
solution
Standard
solution
Reagent
solution
Blue
Orange
Green
Optical block
Valve block
SampleOutlet
Peristaltic
pump
P700IQ-PO4
Information on IQ SENSORNET terminals is given in the relevant IQ S
ENSORNET system operating manual.
1.3.2 Photometer unit
Fig. 1-4, 11 shows the hydraulic system of the P700IQ-PO4
photometer unit.
Fig. 1-4: Hydraulic system
ba76133e0109/201311
Fig. 1-5, 12 shows the photometer unit installed.
1
3
4
5
2
7
6
P 700 IQ
Fig. 1-5: Photometer unit without plastic cover
1 Controller housing
2 Status LED
3 Optical block
4 Joint connection cable for supply voltage and communication
5 Overflow vessel
6 Valve block with inlet and outlet tubes
7 Peristaltic pump
How it functionsThe photometer unit is supplied with d.c. voltage by the PS15V power
pack and operated by a controller (1). It communicates with the
ENSORNET through the MIQ/WCA 232 interface.
IQ S
In conjunction with the peristaltic pump (7), the valve block (6) controls
the movement of the liquids (sample, reagent, standard solution, cleaning solution).
The photometer unit draws the sample from the overflow vessel (5). Filtrated sample continuously flows through the overflow vessel. Thus the
sample is constantly available and free of air bubbles. The filtration unit
(available as an accessory) in conjunction with the filtration pump
(instrument option "P“) provides an optimally prepared sample.
The absorbance of the reaction mixture is measured in the optical block
(3). The optical block has an LED as the light source and photo diodes
as a detector. After the measurement, the liquid is removed from the
optical block.
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P 700 IQ
P 700 IQ-(P)X123
12 3
Options
1.3.3 Status LED
The status LED on the controller enclosure indicates the current operating condition:
LEDMeaning
OffNo power supply
greenThe P700IQ-PO4 photometer unit is ready for operation
and waiting for the next action.
redThe photometer unit is performing an action.
Tab. 1-1: Conditions of the status LED
1.3.4 Instrument options
The P 700 IQ analyzer is available with different options. The options
installed are quoted in the type designation on the name plate:
Fig. 1-6: Structure of the type designation
Option
1PWith filtration pump
2IWithout climate kit (“Indoor“)
3115Input voltage 115 V AC
Identification /
value
(without)Without filtration pump
OWith climate kit (“Outdoor“)
Option
Filtration pump
(instrument option “P“)
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Tab. 1-2: Explanation of the option identifiers in the type designation
The filtration pump is optimally adjusted to the sample filtration available as an accessory.
P 700 IQ
1
2
4
5
6
3
7
Fig. 1-7, 14 shows the filtration pump in the P 700 IQ analyzer.
Climate kit
(instrument option “O“)
Fig. 1-7: Filtration pump
1 Control panel with pump frequency indication
2 Intake tube of the sample filtration (accessory, see section 1.3.6,
3 Connection tube
4 Overflow vessel
5 Outlet of the overflow vessel
6 Return tube (accessory, see section 1.3.5,
7 Manometer
15)
15)
The filtration pump continuously draws sample through the intake tube
(2) and pumps it into the overflow vessel (4) through the connection
tube (3). The flow rate can be set on the control panel (1). On the intake
side, a manometer (7) is installed for low pressure measurement.
For sample preparation, a sample filtration device (available as an
accessory) can be connected upstream.
The climate kit includes an electrical circulating air heating, two housing
ventilators and three temperature regulators. The temperature regulators switch on the heating or ventilators if the temperature is less than
+15 °C or more than 40 °C. Thus the analyzer with the door closed is
suitable for all-season operation in the open. The climate kit is automatically active when the switch on the power supply box is in the ON position.
Where there is a chance of frost, the intake tube and return
14ba76133e0109/2013
tube must be provided with a heat tracing.
P 700 IQ
2
1
3
6
5
4
1.3.5 Return tube (accessory)
The return tube directs out of the analyzer housing the overflowing
sample from the overflow vessel and the waste solution from the photometer unit. Return tubes with heat tracing are available for frost protection.
Order information referring to accessories is given in
chapter 5.2 Consumables, accessories, replacement parts,
65.
1.3.6 Sample filtration device (accessory)
To separate the particles in the sample, the FM filter membrane module
is available as an accessory. It is connected to the analyzer with a suction line. The filtered sample is drawn by the filtration pump in the analyzer (instrument option "P“).
The FM filter membrane module consists of a separable housing and
two membrane inserts. With the aid of the M 1.5 attachment for filtration, the FM filter membrane module can be immersed in the measuring
medium and can be adjusted in height. To clean the membrane inserts,
the filter membrane module can be pulled out along a guide rail with a
chain.
The suction line consists of a suction tube in a robust sleeve tube. Suction lines are available in different lengths and, as frost protection, with
heat tracing.
Fig. 1-8, 15 shows an application example in a sedimentation tank.
Fig. 1-8: Sample filtration device (installed)
1 Chain (scope of delivery: Attachment for filtration M 1.5)
2 Guide rail (scope of delivery: Attachment for filtration M 1.5)
ba76133e0109/201315
3 Height adjustable slide (scope of delivery: Suction line)
4 Suction line (scope of delivery: Suction line)
5 Sleeve tube (scope of delivery: Suction line)
6 Filter membrane module FM with membrane insert
P 700 IQ
Order information referring to accessories is given in
chapter 5.2 Consumables, accessories, replacement parts,
65.
1.4Name plates
The following components have name plates:
ComponentPlace of the name plate
Total analyzerIn the right-hand bottom edge on
the inside of the housing door
ENSORNET interface
IQ S
MIQ/WCA 232
Photometer unit P700IQ-PO4On the left side of the controller
Power supply unit for the PS15V
photometer unit
Tab. 1-3: Name plates
Keep the series numbers on the name plates ready for any
service requests.
On the right side of the
MIQ/WCA 232
housing of the photometer unit
On the right side of the PS15V
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P 700 IQ
2.Safety instructions
2.1Safety information
2.1.1 Hazard warnings in this operating manual
The hazard warnings are defined for the following levels of danger:
WARNING
WARNING indicates a possibly dangerous situation that
can cause death or serious injuries if the safety instruction is not followed.
CAUTION
CAUTION indicates a possibly dangerous situation that
can cause slight or medium injuries if the safety instruction is not followed.
ATTENTION
ATTENTION indicates a situation where goods might be
damaged if the actions mentioned are not taken.
2.1.2 Safety information on the product
Note all labels, information signs and safety symbols on the product.
2.1.3 Labels on the chemical containers
Note the labeling on the chemical containers, especially the hazard and
safety information.
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P 700 IQ
2.1.4 Safety datasheets of the chemicals
Safety datasheets provide security relevant information on hazardous
materials and mixtures. Carefully read the safety datasheets and follow
all instructions. We recommend storing all datasheets in one folder.
2.2Safe operation
2.2.1 Authorized use
The authorized use of the P 700 IQ phosphate analyzer comprises its
use as a sensor in the IQ S
of the analyzer according to the instructions and technical specifications given in this operating manual is authorized (see chapter 7. Technical data, 99). Any other use is considered unauthorized.
ENSORNET. Only the operation and running
2.2.2 Requirements for safe operation
Note the following points for safe operation:
• The product may only be operated according to the authorized use
specified above.
• The product may only be supplied with power by the energy sources
mentioned in this operating manual.
• The product may only be operated under the environmental conditions mentioned in this operating manual.
• The product or its components may only be opened if this is required
for installation and maintenance work and described in the operating
manual.
2.2.3 Unauthorized use
The product must not be put into operation if:
• it is visibly damaged (e.g. after being transported)
• it was stored under adverse conditions for a lengthy period of time
(storing conditions, see chapter 7 Technical data)
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P 700 IQ
2.3Personal protective equipment (PPE)
The PPE includes clothing and other equipment that is used to protect
you against risks at your place of work. You must always wear your
PPE while doing dangerous jobs to avoid injuries or damage to your
health.
The following table shows the PPE that is required while dealing with
dangerous chemicals such as when exchanging the chemical containers. More information is given on the label of the chemical containers
and the relevant safety datasheets.
Personal protective equipmentTypical examples
Protective clothing with long sleeves
Protective goggles
Chemical resistant gloves
Tab. 2-1: Personal protective equipment
It is the duty of the operator to provide all users with the
required PPE. The PPE must fulfill the national standards
and laws.
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P 700 IQ
20ba76133e0109/2013
P 700 IQ
3.Commissioning
3.1IQ SENSORNET system requirements
Software statuses of the
controller and terminal
components
The operation of the P 700 IQ requires the following software versions
in the IQ S
MIQ/MC2Controller software:Version 3.39 or higher
MIQ/TC 2020 XTTerminal software:Version 3.39 or higher
ENSORNET:
3.2Scope of delivery
3.2.1 P 700 IQ scope of delivery
The following parts are included in the scope of delivery of the
P 700 IQ:
• Housing with mounted and wired installations including instrument
options
• Key for outer housing door
• Switch cabinet key for interior door
• Screwdriver for MIQ/WCA 232
• Mounting aid for pump tube
• Chemicals tray
• Lid set for chemicals
• Operating manual
Check whether the scope of delivery is complete before starting the
installation.
The power line is not included in the scope of delivery.
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P 700 IQ
3.2.2 Accessories required in addition
Depending on the application, the following additional accessories are
required or recommended for operation. We explicitly recommend
using original YSI accessories:
Mounting accessoriesEnsure the safe fastening at the mounting location. The following vari-
ants are available:
• Rail mount RM
• Wall mount WM
• Stand mount SM
Chemicals• Reagent solution RE 2.5
Sample preparation
(filtration)
• Cleaning solution CL 1.0
• Standard solutions ST ... (depending on measuring range and cali-
bration procedures)
• Filter membrane module FM
• Attachment for filtration M 1.5 for filter membrane module FM, also
available with extension M-EXT 1.5
• Suction line SL ... (different lengths up to 20 m, with and without heat
tracing)
• Return tube RL ... (different lengths up to 20 m, with and without
heat tracing)
Order information referring to accessories is given in
chapter 5.2 Consumables, accessories, replacement parts,
65.
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P 700 IQ
3.3Installation
3.3.1 General installation instructions
This section describes the installation of the P 700 IQ with
various especially designed accessories. We assume that
the operator uses these accessories. In this section, the
individual scopes of delivery are not distinguished so the
comprehensibility of the instructions is not affected.
Pay attention to the following points during installation:
• Installation in the open should be done while the weather is frost-
free.
• Due to its weight, the analyzer always has to be carried by two
people (housing door upward, both people grasp the housing at the
upper C rail and at the housing bottom on the side of the door).
• The analyzer may only be fastened on a wall or fixture with the aid
of the two rails (enclosure upright).
Main stepsInstallation of the P 700 IQ includes the following main steps:
1Installing the housing.
See section 3.3.2, 24.
2Installing the FM filter membrane module and the
M 1.5 attachment for filtration.
See section 3.3.3, 35.
3Inserting the connections into the housing.
See section 3.3.4, 36.
4Connecting the IQ S
See section 3.3.5.1, 39.
5Connecting the power line and heat tracing lines.
See section 3.3.5.2, 40.
6Connecting the liquid containers.
See section 3.3.5.3, 42.
ENSORNET cable.
ba76133e0109/201323
Assembling the stand
1
2
(2 x)
3
mount
P 700 IQ
3.3.2 Installing the housing
The housing of the P 700 IQ can be installed in the following ways:
• On the SM stand mount. See section 3.3.2.1 Installation on the SM
stand mount, 24.
• On a rail. See section 3.3.2.2 Installation on a rail, 29.
• On a wall. See section 3.3.2.3 Installation on a wall, 33.
3.3.2.1Installation on the SM stand mount
Proceed as follows to install the housing on the stand mount:
Fig. 3-1: Mounting the ground pipes
1Press the plastic protective plugs (1) into both ends of the square
ground pipes (2).
2Mount the four height adjustable stand feet (3) on the square
ground pipes (2) using the enclosed M10 hexagon countersunk
head screws. Make sure to use the correct number of plain washers and nuts in the correct order according to Fig. 3-1, 24.
24ba76133e0109/2013
P 700 IQ
1
4
5
2
Fig. 3-2: Connecting the supporting pipes with the ground pipes
3Press the plastic protective plugs (1) into the upper ends of both
square supporting pipes (4).
4Using the triangular stabilizing sheets (5), connect both square
supporting pipes (4) with the preassembled ground pipes (2). To
do so, use a total of six M8 hexagon head screws with large M8
plain washers and locknuts as shown in Fig. 3-2, 25. Make
sure the two columns mirror each other after being mounted.
ba76133e0109/201325
P 700 IQ
67
Fig. 3-3: Connecting the supporting pipes with the cross pipes
5Connect both supporting pipes with each other using the two
square cross pipes (6). To do so, use the eight angle brackets (7)
and a total of twelve M8 hexagon head screws with plain washers
and locknuts.
Make sure that both triangular stabilizing sheets (5) are on
the inside.
6Mount the four retaining hooks (8) on the stand mount. To do so,
use a total of twelve M8 hexagon head screws with large M8 plain
washers and locknuts.
26ba76133e0109/2013
P 700 IQ
8
Positioning the stand
mount
Fig. 3-4: Mounting the retaining hooks
7Mount the four retaining hooks (8) on the stand mount. To do so,
use a total of eight M8 hexagon head screws with large M8 plain
washers and locknuts.
There are three pairs of holes each for the upper and lower
retaining hooks. Thus the analyzer can be mounted optimally at working level. Use the same relative positions for
each of the upper and lower hooks.
8Place the stand mount at the intended operating location.
9Adjust the four height adjustable stand feet so that the stand
mount stands straight.
ATTENTION
Always screw the four stand feet to the ground. With
installation at an open air test site, make sure that the
installation will also hold out against strong storms.
ba76133e0109/201327
Mounting the housing
10
9
11
P 700 IQ
Fig. 3-5: Mounting the housing
10Mount the housing by hooking the rails (9 and 10) fixed on its rear
side into the retaining hooks of the stand mount.
Fig. 3-6: Fixing the housing
11Fix the housing on both sides with the 4 mounting brackets (11)
so it cannot shift sideways. To do so, use a total of eight M8 hexagon head screws with small M8 plain washers and locknuts.
28ba76133e0109/2013
P 700 IQ
1
2
34
3.3.2.2Installation on a rail
For installation on a rail, the RM rail mount bracket is required.
ATTENTION
Make sure that the rail is sufficiently stable. With installation at an open air test site, make sure that the installation will also hold out against strong storms.
Assembling the bracketProceed as follows to install the housing on the rail:
Fig. 3-7: Connecting the supporting pipes with the cross pipes
1Press the plastic protective plugs (1) into the upper ends of both
square supporting pipes (2).
2Connect both supporting pipes with each other using the two
square cross pipes (6). To do so, use the eight angle brackets (7)
and a total of twelve short M8 hexagon head screws with large
plain washers and locknuts.
ba76133e0109/201329
P 700 IQ
5
Fig. 3-8: Mounting the retaining hooks
3Mount the four retaining hooks (5) on the rail mount. To do so,
use a total of eight short M8 hexagon head screws with small M8
plain washers and locknuts.
There are three pairs of holes each for the upper and lower
retaining hooks. Thus the analyzer can be mounted optimally at working level. Use the same relative positions for
each of the upper and lower hooks.
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