YSI 5000 User Manual

YSI Model 5000 YSI Model 5100
Dissolved Oxygen Temperature
Operations Manual
1. General Description..............................................................................................................................1
2. Specifications........................................................................................................................................3
3. Quick Start.............................................................................................................................................5
4. Controls .................................................................................................................................................6
4.1 Front Panel...................................................................................................................................................... 6
4.2 Software Flow Chart....................................................................................................................................... 7
4.3 Rear Panel....................................................................................................................................................... 9
5. Setup....................................................................................................................................................11
5.1 Display Setup................................................................................................................................................ 12
5.2 Report Setup ................................................................................................................................................. 14
5.3 Autostable Setup........................................................................................................................................... 16
5.4 System Setup................................................................................................................................................. 17
6. Calibration ...........................................................................................................................................19
6.1 Dissolved Oxygen Calibration...................................................................................................................... 19
Auto Cal........................................................................................................................................................ 20
DO Cal (manual)........................................................................................................................................... 21
Barometer ..................................................................................................................................................... 22
Salinity.......................................................................................................................................................... 23
6.2 Zero Calibration............................................................................................................................................ 24
7. Operation.............................................................................................................................................26
7.1 Main Mode ................................................................................................................................................... 26
Making Measurements .................................................................................................................................. 26
Store.............................................................................................................................................................. 27
Review.......................................................................................................................................................... 28
Send .............................................................................................................................................................. 30
7.2 Application Mode ......................................................................................................................................... 32
OUR.............................................................................................................................................................. 32
SOUR............................................................................................................................................................ 37
Remote.......................................................................................................................................................... 42
8. Diagnostics..........................................................................................................................................44
History .......................................................................................................................................................... 45
Sensor ........................................................................................................................................................... 46
Reset Ps......................................................................................................................................................... 47
9. Principles of Operation.......................................................................................................................48
10. Understanding Dissolved Oxygen Error Factors......................................................................49
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11. Maintenance..................................................................................................................................52
Batteries........................................................................................................................................................ 52
12. Troubleshooting...........................................................................................................................54
Error Messages ............................................................................................................................................. 54
13. Warranty & Repair ........................................................................................................................56
Cleaning Instructions .................................................................................................................................... 57
Packing Instructions...................................................................................................................................... 58
14. Required Notice............................................................................................................................59
15. Accessories and Replacement Parts..........................................................................................60
16. Appendix A - Oxygen Solubility Table........................................................................................61
17. Appendix B - Pressures and Altitudes.......................................................................................63
18. Appendix C - Conversion Factors...............................................................................................64
19. Appendix D - Remote Command Language...............................................................................65
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1. General Description
Model 5000 Features
The Model 5000 is a microprocessor based, menu-driven, dissolved oxygen meter designed to perform laboratory measurement of dissolved oxygen and Biochemical Oxygen Demand (BOD). The instrument’s menu system makes it simple to use.
The Model 5000 has a new case design which facilitates laboratory measurement. The angled profile makes these instruments both functional and attractive. A large graphical display provides on-screen menus, and large data fields for ease of operation and readability. The angle and position of the keypad make operation of the 5000 comfortable. The tactile and audio response from each key stroke give you the confidence that every command has been received.
The Model 5000 is compatible with all existing YSI dissolved oxygen probes when used with the YSI Model 5011 adapter. The new YSI Model 5010 self-stirring BOD Probe allows you to operate the probe from the instrument’s power supply, eliminating the need for a separate power cable for the probe.
Internal memory for storing up to 100 sets of data, and an RS232 port allow you to upload data
from the Model 5000 directly to your computer. Or you can use your Model 5000 with YSI BOD
Analyst software. Model 5000 Features & Benefits
Feature Benefit
1. Menu driven operation for ease of use Ease of use -- little need for instruction manual.
2. Compatible with all existing YSI probes No need to re-invest in probes. (5011 adapter required)
3. Large graphic liquid crystal display Easy to read.
4. Internal memory for 100 data points No need to write down readings.
5. Auto stabilization feature You are alerted when stable DO reading is reached.
6. Compatible with YSI BOD Analyst Software Software does all the BOD calculations -- no chance for
math errors.
7. User upgradable internal software No fear that an instrument purchased today will be out of date tomorrow.
8. RS232 interface Computer uploads to spreadsheets eliminates transcription errors, & increases regulatory confidence.
9. 8-pin DIN connector which allows the instrument to
power the YSI 5010 self-stirring BOD probe
10. Computer interface control Allows you to control the functions of the instrument
11. Audio & tactile keypad response Affirmation of successful key strokes reduces errors and
12. Real-time clock For recalling or downloading data, this is essential.
No power supply needed for the DO probe which means one less cable to clutter your work space.
from a computer.
uncertainty.
1
Model 5100 Features
The YSI Model 5100 has all of the same functionality of the Model 5000 and much more.
The YSI Model 5100 is a state-of-the-art, microprocessor-based, dissolved oxygen instrument with many automated and application specific features.
The YSI 5100 DO instrument contains built-in application software for the calculation of Oxygen Uptake Rate (OUR) and Specific Oxygen Uptake Rate (SOUR). These application features simplify compliance with USEPA 503 regulations for vector attraction and provide useful tools for plant operation decisions.
For laboratories with larger volumes, the Model 5100 offers an optional bar code reader and
BOD Analyst software capability. These tools greatly reduce the labor required for processing
BODs and calculating BOD values. The RS232 serial port makes it easy to capture data electronically.
The model 5000 and 5100 software can be upgraded easily using your computer. When YSI upgrades these instruments, you’ll be able to get a floppy disk from YSI and simply upgrade the software in a few minutes.
Calibration of the Model 5100 has been greatly simplified when compared to other dissolved oxygen instruments. With its internal barometer, the Model 5100 is able to automatically compensate for changes in barometric pressure so there is no need for charts, altitude information or external barometric pressure information. The 5100 also has a membrane integrity feature which will notify you when the membrane needs to be changed.
Model 5100 Features & Benefits
The Model 5100 has all the same functionality as the Model 5000, but with these additional features:
Additional Feature Benefit
1. Built-in application software for OUR/ SOUR Easy compliance with USEPA 503 regulations.
2. Internal barometer No need to consult external barometer and perform manual barometric pressure compensation.
3. Automated calibration Saves time and extra steps of manual calibration.
4. Bar-code capability No need to manually type or write the bottle number on your bench sheet.
5. Port for computer keyboard For some applications, using a keyboard for data entry will be faster than using the instrument keypad.
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2. Specifications
Oxygen Measurement
Ranges: mg/L: 0.0 to 60.0 mg/L % air saturation: 0.0 to 600.0% air saturation mbar: 0 to 1500 Accuracy: mg/L: ±0.1% plus 1 Least Significant Digit (LSD) % air saturation: ±0.1% plus 1 LSD mbar: ±±±±1% plus 1 LSD Resolution: mg/L: 0.1%, or 0.01 mg/L , whichever is greater % air saturation: 0.1% air saturation mbar: 1 mbar
Temperature Measurement
Range: -5.0 to +50.0°C Accuracy: ±0.1°C Resolution: 0.01°C
Barometric Pressure Measurement
Range: 450 to 825 mmHg (600 to 1100 mbar) Accuracy: ±1% plus 1 LSD within ±10°C ambient temperature from calibration point Resolution: 1 mmHg
Temperature Compensation
The mg/L mode is automatically temperature-compensated to an accuracy of ±1% of DO readings between 0 and 5°C, and to an accuracy of ±0.6% of readings between 5 and 45°C.
The % air saturation mode is automatically temperature-compensated to an accuracy of ±0.5% of calibration values between 0 and 5°C, and to an accuracy of ±0.3% of values between 5 and 45°C.
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Salinity Compensation
Range: 0.0 to 40.0 ppt Accuracy: ±.02 mg/L
Operating Environment
0 to 45°C, 10 to 90% relative humidity, non-condensing
Water Resistance
The Model 5000 and 5100 are designed exclusively for indoor use and are NOT waterproof.
Power
The Model 5000 & 5100 are powered by an AC adapter or 4 C-size alkaline batteries. A new set of alkaline batteries will power the selected instrument for approximately 30 hours (not including stirring).
Size and Weight
22.9 by 24.1 by 11.2 cm; 1.1 kg (with batteries)
9 by 9.5 by 4.4 inches; 2.6 pounds (with batteries)
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3. Quick Start
When you unpack your new Model 5000 or 5100 there are several things you’ll want to do to set the instrument up.
1. Inspect the product to assure that it has not been damaged during shipment.
2. Check the packing list to make sure you have received everything you should have.
3. Install the batteries (see 11. Maintenance, Batteries).
4. Plug the power supply into its mating connector on the back of the meter (see 4.3 Rear Panel).
5. Prepare the DO probe, as discussed in the Probe Operations Manual, and plug it into the connector on the back of the instrument.
6. Depress the (on/off ) key (see 4.1 Front Panel).
7. Set the date and time (see 5.4 System Setup).
8. Calibrate the system in a known oxygen environment (see 6.1 Dissolved Oxygen Calibration).
You are now ready to make dissolved oxygen and temperature readings.
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4. Controls
4.1 Front Panel
The front panel of the instrument contains the display and keypad as shown below. The front panel display and controls of the 5000 and 5100 are identical.
Display
Power
ON/OFF
MODE Key
Soft-Keys
ENTER Key
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The 5000/5100 has two main operating modes, Main and Application. The current mode is displayed in the dark bar at the top right corner of the display. The following diagram shows the display while the instrument is in the Main mode.
Main
Mode
mg
8.15*
/L
24.38°C 11:33AM
STORE REVIEW SEND CALIBRATE
The bottom row of the display identifies the function of the four soft-keys which are located on the keypad below the display. The function of each of these keys changes with each mode.
The [Mode] key and soft-keys are used to navigate through the menus. The [Mode] key is used to cycle between the two main operating modes. Pressing a soft-key will bring up a new set of soft­key functions (menu). The [Mode] key is also used to backup through the menus to the top level.
4.2 Software Flow Chart
The following section shows the software flow chart for the 5000/5100. The two operating modes, Main and Application, are shown at the top with the soft-key functions that are accessed in each mode below them. Functions in shaded boxes are only available on the model 5100.
Soft-key functions
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5000/5100 Software Flow Chart
A
A
MAIN
Store
Review
Send
Calibrate
Recall
Send All
Clear
Delete All
uto Cal
DO Cal
Setup
Display
Size
Unit
Contrast
Last Digit
APPLICATION
OUR
Start
End
Send on/off
Setup
Review
Next Rec.
Modify
Send
Send
SOUR
Start
End
Send on/off
Setup
Report
SDF CDF
Range
Next
Stable
System
udio On/Off
Time/Date
Version
RS-232
Diagnostic
NOTE: Shaded boxes are only available on the model 5100
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Review
Next Rec.
Modify
Send
Send
Remote
Skip
Up
Down
Confirm
.
4.3 Rear Panel
The rear panel contains the connections for the power supply, probe, bar code reader, external computer keyboard and RS232 serial port as shown below. The bar code reader and external computer keyboard share the same socket and are only available on the model 5100.
Power Supply Connection
The power supply connection requires a 4.5 to 5.5 VDC power supply with at least 350 mA current (6.0 VDC 800 mA when using the YSI 5015 bar code reader).
Probe Connection
The connector for the probe is an 8-pin mini DIN connector and is marked with an arrow to show proper alignment. Be sure to align the arrows when plugging in the probe.
YSI 5000 series probes, such as the YSI 5010 BOD probe, will plug directly into the 5000/5100. If you have an older YSI 5700 or 5900 series probe, the YSI 5011 adapter will be required.
The YSI 5011 adapter has a mini-DIN connector at one end and a 5-pin MS connector and probe power connector at the other end. The 8-pin mini-DIN connector plugs into the 5000/5100 probe socket and the 5-pin MS connector plugs into a 5700 or 5900 series probe/cable. The power connector plugs into the matching connector on a self stirring BOD probe. This allows the 5000/5100 to power the BOD probe, eliminating the need for a separate probe power supply.
NOTE: Do NOT plug the 5011 adapter power connector into the 5000/5100 power supply
socket. Doing so will prevent the 5000/5100 from operating.
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Bar Code Reader Connection
The YSI 5015 bar code reader connects to this 6-pin mini DIN connector. The connector is marked with an arrow to show proper alignment. Be sure to align the arrows when plugging in
the YSI 5015 bar code reader (see 7.2 Application Mode, Remote, Bar Code Reader).
The bar code connector is also used for attaching an external computer keyboard. Using a
keyboard simplifies data entry when using the 5100 in the remote mode, such as with YSI BOD Analyst software (see 7.2 Application Mode, Remote).
RS232 Connection
The RS232 connection is a standard DB9 connector. See 7.2 Application Mode, Remote, System Setup for details.
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5. Setup
Before operating the 5000/5100 for the first time, you should set the instrument parameters. Once set, these parameters are maintained in memory. These parameters are discussed below.
From Main mode, press the [CALIBRATE] soft-key to enter the calibration menu. Notice that the dark bar in the top right corner of the display shows the current mode.
98.0 % 8.15
ppt
0.0
740
mg/L
mmHg
Calibrate
24.38°C 11:33AM
AUTO CAL DO CAL SETUP DIAGNOSTICS
Next, press the [SETUP] soft-key to enter the Setup menu. The bottom row of the display will show the following soft-key setup selections.

Setup

mg
8.15*
/L
24.38°C 11:33AM
DISPLAY REPORT STABLE SYSTEM
These four selections are used to change the instrument setup.
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5.1 Display Setup
Press the [DISPLAY] soft-key to show the following menu.
Display
mg
8.15*
/L
24.38°C 11:33AM
SIZE UNITS CONTRAST LAST DIG.
The [SIZE] soft-key cycles among the two possible display arrangements for Main mode. One selection shows as many parameters as possible, the other shows Dissolved Oxygen in large type with temperature and time in small type. These different display arrangements are for Main mode only. The display will show all parameters in Calibration mode.
98.0% 8.15
ppt
0.0
740
mg/L
mmHg
Display
24.38°C 11:33AM
SIZE UNITS CONTRAST LAST DIG.
The [UNITS] soft-key brings you to the [UNITS] menu. Use the [UP] and [DOWN] soft-keys to change the measurement units. If you have selected the size to be large, only the DO units selected on the [UNITS] screen will be shown. When the size is set to small, both % and mg/L will be shown. The Date Format is also used to change from a 2 digit year to 4 digit year. The Sal – 78 scale give salinity in unitless values as the measurements are in reference to the conductivity of standard seawater at 15 °C. The HOUR units switch from a 12 to 24 hour day. Press the [MODE] key to return to the Display menu.
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[
[
[
[
[
[
]
DISPLAY UNIT SETUP D.O.
Barometer Salinity Temperature Date Format
UP DOWN NEXT
The [CONTRAST] soft-key allows the user to change the display contrast. The display contrast will change slightly each time the [UP] or [DOWN] soft-key is pressed.
The [LAST DIG.] soft-key allows the user to suppress the last digit of the DO reading. This function is only available when the large size display has been selected. The small size display will not be affected.
% ] in Hg ] Sal – 78 ] C ] MM/DD/YY ] HOUR
mg
8.2*
/L
Units
12H
Display
24.38°C 11:33AM
SIZE UNITS CONTRAST LAST DIG.
Press the [MODE] key to return to the Setup menu. If you wish to return to Main mode, press [MODE] two more times.
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[*]
[*]
[*]
[*]
[*]
[*]
[*]
]
5.2 Report Setup
From the Setup menu, press [REPORT] to display the following soft-keys.
[SDF] Space Delimited Format
SAMPLE ID # DO% DO mg/L
DATE TIME BAROMETER
TEMPERATURE [*] SALINITY
SEND Record from [ 0] to [99
SDF CDF RANGE NEXT
The display lists the parameters that can be included in the output string at the RS232 serial port, the default set has everything selected for inclusion.
You can select the report format that you wish to use by pressing the [SDF] or [CDF] soft-key. Select [SDF] for Space Delimited Format (standard text). If you are going to import the data to a spreadsheet, select [CDF] for Comma Delimited Format. The following are examples of each format:
Report
Space Delimited Format
SAMPLE ID mg/L % C ppt mmHg TIME DATE ID: 0 7.95 97.3 25.6 0.0 786 15:06:34 01/23/96 ID: 1 7.94 97.1 25.6 0.0 786 15:06:36 01/23/96 ID: 2 7.95 97.2 25.6 0.0 785 15:06:44 01/23/96
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[*]
[*]
[*]
[*]
[*]
[*]
[*]
Comma Delimited Format
"SAMPLE ID","mg/L","%","C","ppt","mmHg","TIME","DATE" "ID: 0", 7.95, 97.3,25.6, 0.0, 786,"15:06:34","01/23/96" "ID: 1", 7.94, 97.1,25.6, 0.0, 786,"15:06:36","01/23/96" "ID: 2", 7.95, 97.2,25.6, 0.0, 785,"15:06:44","01/23/96"
The asterisk character in front of each parameter indicates that the parameter will be included in the report. Press the [NEXT] soft-key to select the parameter that you want to change. Then press [ENTER] to turn the asterisk character on or off.
NOTE: After pressing [SDF] or [CDF] to choose the report format, press the [MODE] key to exit the Report menu. Do NOT press [ENTER] as this will change the currently selected parameter.
To return to Main mode, press [MODE] two more times.
The [RANGE] soft-key brings up the following soft-key menu.
[SDF] Space Delimited Format
SAMPLE ID # DO% DO mg/L
DATE TIME BAROMETER
Report
TEMPERATURE [*] SALINITY
SEND Record from [ 00] to [99]
UP DOWN DIGIT NEXT
Flashing Cursor
This menu allows specifying a specific range of memory locations for the report. The default range is 00 - 99 and empty locations will not be sent to a computer or serial printer.
The display digit that has the flashing cursor below it is increased or decreased by pressing the [UP] or [DOWN] soft-key. If the [UP] or [DOWN] soft-key is held down, the digit will continue to change until the key is released. The [DIGIT] soft-key makes it easy to make large changes by selecting the digit you wish to change. Press the [NEXT] soft-key to change between the minimum and maximum parameter. When the desired number is obtained, pressing [ENTER] will accept the number and exit the RANGE sub-menu. The RANGE sub-menu can be left without making any changes by pressing the [MODE] key. Operation returns to the report setup menu.
To return to Main mode, press [MODE] three more times.
15
[
[
)
5.3 Autostable Setup
The autostable feature indicates when readings are stable by emitting a single beep and displaying an asterisk (*) to the right of the dissolved oxygen reading. The instrument uses criteria that you input to determine what a stable reading is. You select the maximum percent of change that may occur during a selected time duration. The default values are 10 seconds and
0.4% variation. The instrument will display an asterisk (*) only when these criteria are met.
mg
Stable reading indication
Main
8.20*
/L
24.38°C 11:33AM
STORE REVIEW SEND CALIBRATE
From the Setup menu, press the [STABLE] soft-key to display the following menu.
PARAMETERS
10] Time Duration (3-19) Seconds
0.4] DO % variation (0.0-1.9
UP DOWN DIGIT NEXT
This menu is used to change the autostable criteria. Press the [NEXT] soft-key to select between the time duration and the percent variation. Use the [DIGIT] soft-key to select the digit you wish to change by pressing [UP] or [DOWN]. When you have finished setting the parameters, press [ENTER] to confirm. The STABLE sub-menu can be left without making any changes by pressing the [MODE] key instead of [ENTER]. Operation returns to the setup menu.
Stable
If you wish to disable the autostable feature, set the DO% variation to 0.0.
To return to Main mode, press [MODE] two more times.
16
5.4 System Setup
From the Setup menu, press the [SYSTEM] soft-key to display the following menu.
mg
System
8.38*
/L
24.38°C 11:47AM
AUDIO off TIME / DATE VERSION RS232
The [AUDIO on/off] soft-key allows setting the beeper on or off. The key toggles between an [AUDIO off] soft-key and an [AUDIO on] soft-key. The present state of the beeper would be the OPPOSITE of the function shown on the soft-key. If the beeper is currently on, the soft-key shows “AUDIO off”; i.e., your alternate choice.
The [TIME/DATE] soft-key brings up the following menu to allow setting of the date and time.
Flashing Digit
Time/Date
09:58:04
01/20/96
UP DOWN DIGIT NEXT
Use the UP, DOWN, DIGIT and NEXT soft-keys to enter the time in 24-hour format. The display digit that is flashing is increased or decreased by pressing the [UP] or [DOWN] soft-key. If the [UP] or [DOWN] soft-key is held down, the digit will continue to change until the key is released. The [DIGIT] soft-key makes it easy to make large changes by selecting the digit you wish to change. After you have set the hour, press the [NEXT] soft-key to move to the next parameter, minutes. Repeat the process for the remaining parameters.
When you have finished entering the time and date, press [ENTER] to confirm and return to the system setup menu. The message at the bottom of the screen. The Time/Date sub-menu can be left without making any changes by pressing the [MODE] key instead of [ENTER]. Operation returns to the system setup menu.
“TIME SETTING SAVED” will be displayed on the message line
17
mg
System
8.38*
/L
24.38°C 9:59AM
TIME SETTING SAVED
AUDIO off TIME / DATE VERSION RS232
If you wish to return to Main mode, press [MODE] three times.
The [VERSION] soft-key displays the instrument software version on the message line of the display just above the soft-key descriptions.
The [RS232] soft-key displays the RS232 setup.
[ 2 ] BAUD RATE 19200
0. 4. 4800
1. 5. 2400
2. 19200 6. 1200
3. 9600
UP DOWN
RS232
Message
Select the baud rate by pressing the [UP] or [DOWN] soft-keys. The first two choices, 0 and 1, are not currently available.
The remaining RS232 parameters are fixed as follows:
Data Length: 8 bits Parity: None Stop Bits: 1
Press [ENTER] to confirm. The RS232 sub-menu can be left without making any changes by pressing the [MODE] key instead of [ENTER]. Operation returns to the system setup menu.
Press [MODE] to return to the previous menu, Setup. To return to Main mode, press [MODE] two more times.
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