YOKOGAWA SC200 Instruction Manual

Page 1
Instruction Manual
Model SC200 2-wire Conductivity or Resistivity transmitter
IM 12D7B2-E-H
4th edition
Page 2
FAILHOLD
MEASURE CAL DISPLAY HOLD
YES
NO
ENT
OUTPUT
SET HOLD TEMP. SERVICE
*
NO MODEYES
>
ENT>
MODE
mS/cm M/cm
k/cm µS/cm
.
ADJUSTMENT KEYS
: Choose digit
for adjustment
: Adjust digit (to decrease
pass through zero)
ENT: Enter new value
MEASURE VALUE DISPLAY
MESSAGE DISPLAY
KEY PROMPT FLAGS
SELECTION KEYS YES: Accept
setting
NO: change to
new setting
L
L
SELECT MODE MEASURE/MAINTENANCE
Can be used to escape program at any time
SELECT MODE MEASURE/COMMISSIONING
OUTPUT HOLD FLAG
MANUALLY SET TEMPERATURE COMPENSATION FLAG
FAIL FLAG
MENU POINTER FLAGS
MENU FOR MAINTENANCE FUNCTIONS see chapter 5
MENU FOR COMMISSIONING FUNCTIONS see chapter 4
Note: First digit changes from 1,-1,- to blank.
TEMP.MAN
Page 3
IM 12D7B2-E-H
1. INTRODUCTION
1-1. Application.................................................................1
1-2. Required components for
conductivity measurement .........................................1
1-3. Identification...............................................................2
2. TECHNICAL SPECIFICATIONS .........................................2
2-1. General technical specification...................................2
2-2. Functional description................................................3
3. INSTALLATION AND WIRING............................................4
3-1. Installation and dimensions ........................................4
3-1-1. Installation site.................................................4
3-1-2. Mounting methods ..........................................4
3-2. Wiring of sensors .......................................................6
3-2-1. General precautions ........................................6
3-2-2. Additional precautions for installations in
hazardous areas..............................................6
3-2-3. Grounding the liquid ........................................6
3-2-4. Access to terminal and cable entry..................6
3-2-5. Connecting diagram for sensors......................7
3-3. Wiring of power supply...............................................8
3-3-1. General precautions ........................................8
3-3-2. Additional precautions for installation
in hazardous areas ..........................................8
3-3-3. Access to terminal and cable entry..................8
3-3-4. Power on ........................................................8
4. COMMISSIONING.............................................................11
4-1. Operations overview ................................................11
4-2. Output range adjustment ............OUTPUT ..............12
4-3. Set up Hold function ...................SET HOLD ...........14
4-4. Temperature compensation ........TEMPERATURE...16
4-5. Sensor selection and diagnostics` ............................18
5. MAINTENANCE.................................................................20
5-1. Calibration...................................CAL......................20
5-2. Selecting a value to display .........DISPLAY..............22
5-3. Use of the hold function ..............HOLD...................24
6. TROUBLE SHOOTING......................................................26
6-1. Introduction .............................................................26
6-6. Error messages and explanation ..............................27
7. SERVICE (Mode) ...............................................................28
7-1. Introduction .............................................................28
7-2. Access to service settings........................................29
7-3. Temperature sensors and units................................30
7-4. Reference temperature ............................................30
7-5. Output code selection..............................................30
7-6. Output table for non-linear range .............................31
7-7. Cell constant adjustment..........................................31
7-8. Auto return function .................................................31
7-9. Measuring principle..................................................32
7-10. Temperature sensor adjustment...............................32
7-11. Signalling of fail condition.........................................32
7-12. Temperature compensation coefficient adjustment ..33 7-13. Percent by weight indication on second
display line ...............................................................34
7-14. Polarisation check....................................................34
7-15. Passcode protection by three digit code..................35
7-16. Restore default setting .............................................35
7-17. Non linear ranges.....................................................36
CONTENTS
Page 4
8. CLASSIFICATION .............................................................36
8-1. Cenelec ...................................................................36
8-2. FM...........................................................................37
9.
CHANGE FROM CONDUCTIVITY TO
RESISTIVITY MEASUREMENT .............
............................38
9-1. How to change from conductivity to resistivity
measurement...........................................................38
9-2. Resistivity measurement ..........................................38
9-3. Maintenance of the transmitter.................................38
10. SOFTWARE VERSION 3.0
COMPARED TO VERSIONS 1 AND 2 ............................39
10-1. Cell constant............................................................39
10-2. Matrix compensation ...............................................39
10-3. Matrix temperature-compensation range .................40
10-4. Matrix data...............................................................40
10-5. Selection between “soft” or “hard” Fail situations .....41
10-6. Selection between yes or no E6 Fail-message .........41
10-7. Matrix examples.......................................................42
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1
1. INTRODUCTION
1-1. Application
The EXA SC200 transmitter is a 2-wire con­ductivity instrument intended to be used in industrial installations in the field. For easy maintenance and operation it should be located close to the sensors. The cable length is limited to 10 metre. It is powered from a remote low voltage DC power supply through the 2-wire connec­tion. The EXA SC200 is compatible with most commercial available conductivity sensors and fitting systems. The instrument is available in two versions:
- A general purpose version for use in safe areas.
- An intrinsically safe version for use in hazardous areas. The instrument can then be installed in Zone 1 with the sensors in Zone 0 or Zone 1.
The micro-processor is used in this instru­ment for continuous loop diagnostics, flexi­ble on site commissioning and fine tuning by advanced functions.
In general a conductivity loop can be set up for different purposes:
- To be part of a total process control sys­tem.
- To indicate dangerous limits of a process.
- To monitor product quality.
1-2. Required components for
conductivity measurement
A. a conductivity sensor ( also called con-
ductivity cell) with integral temperature sensor Ni-100 or Pt-1000.
B. a fitting for the above sensor with acces-
sories.
C. a signal cable with or without extension
boxes etc.
D. the EXA SC200 2-wire transmitter with
universal mounting accessory for wall, pipe or panel mounting.
E. a DC power supply (nominal 24 V DC)
with cabling and optional zener barriers or an intrinsic safe power supply.
F. peripherals: e.g. strip-chart recorder,
panel indicator, PID-controller
1-3. Identification
The instrument has an identification label, which is fixed to the front plate. This serves as a reference for the full model code, power supply voltage and serial num­ber. This label also carries authorised marks to certify compliance with the current regu­latory norms.
MODEL
SERIAL NO.
SUPPLY
Page 6
2. SPECIFICATIONS
2-1. General specifications
A. Intrinsic safety (model SC200S only)
- BASEEFA : Certified by and meets the requirements of EEx [ia] ib IIC T4 of CENELEC Certificate No.: 89C2379.
- FM : For IS CL1, DIV1, GP ABCD T3B for TA-30 to 70˚C T4 for TA-30 to 40˚C Approval report: J.I. 1Y1A7.AX
- CSA : For Ex[ia] Class 1, Div. 1, Groups C and D, T4A Approval file: LR 102851-1
B. Indicating range : 0.055µS/cm to 2000 mS/cm at 25˚C
reference temperature with cell-con­stants between 0.01 to 10 cm
-1
C. Transmission signal : 4 - 20 mA DC; maximum load.550 . D. Transmission range : User programmable to any range within
the indicating range with a maximum of 60% zero suppression. A user programmable output table can be set up in 21 steps.
E. Power supply
- Model SC200G : 17 to 40 V DC, dependent on load.
- Model SC200S :
17 to 31,5 V DC, powered from a certified zener barrier or isolated power supply
F. Climatic condition
- Ambient temperature : -10 to +55 ˚C(10 to 130°F)
- Storage temperature : -30 to +70 ˚C (-20 to 160°F)
- Relative humidity : 10 to 90%
- Weather protection : Rain and dust-tight to IP65 (NEMA 4X)
- Interference protection : EMI Class B RFI less than 2% at 5 V/m for 20 MHz to 1 GHz.
G. Display method : Custom liquid crystal display.
- Main display : 31/2digit, 12.5 mm high.
- Message display : 6 alphanumeric characters, 7 mm.
- Special fields : Flags for status indication. : Units: µS/cm, mS/cm. : Key prompts: YES, NO, ^, >, ENT
H. Keys : 6 keys operated through the flexible win-
dow with tactile feedback and one hid­den key behind the front cover.
I. Housing
- Body material : Cast aluminium with chemical resistant
coating.
- Window : Flexible poly carbonat.
- Colours used : Moss green/ off-white.
- Cable glands : Polyamide
- Cable entries : Two glands PG 16 (
1
/2” NPT adapter for US Model). Hose connection optional.
- Terminals : For maximum 2.5mm
2
cable (cable
finishings preferred).
- Earth connection : For external ground.
J. Mounting possibilities
- Bracket mounting : Two M6 bolts, 9 mm length. Wall, or pipe mounting by the optional mounting kit, panel mounting by self tap­ping screws.
K. Shipping details
- Dimensions : 162 x 178 x 115 mm (6.5 x 7 x 4.5”)
- Package : 290 x 225 x 170 mm (11.5 x 8.9 x 6.7”)
- Weight : approx. 2,5 kg (5 Ibs)
L. Safety and security
- Data protection : Non volatile memory(EEPROM).
- Data backup : All data is stored 3 times.
- Interference test : according to IEC 801.
- Power down : no effect, reset to measurement.
- Operation : All 3 levels can be protected with a 3 digit passcode.
2
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3
2-2. Functional description
The EXA SC200 is a real time micro-control­ler operated conductivity-analyzing system. It uses a dedicated micro-controller to con­trol all function necessary in such a system. The input and output functions are concen­trated in the analogue section of the instru­ment. Even these functions are operated through special interfaces designed to give a minimum of interference problems to the digital functions. A separation of function is strictly executed. By using very low power components it is possible to make a complete micro-compu­ter system work on less than 4 mA current. By using an EEPROM for essential informa­tion the operating parameters are fixed in memory without the need for batteries. The supply-voltage is stabilized by regulators to the internal supply system. Any voltage between 17 and 40 Volt is acceptable. The user-interface is limited to a basic set of 6 keys accessible through the flexible win­dow cover. The software is designed with the user in mind. It uses a simple 3 layer set-up to communicate with the operator by giving messages on the second line of the display area and indicating which keys are to be pressed in the display too.
The keys are scanned continuously and the actions are taken immediately. An extensive system of checking values and parameters is implemented.
The EXA SC200 operates just like a normal 2-wire instrument but with additional func­tions. These extra functions are possible by using a micro-controller at the heart of the system.
- Continuous sensor polarisation checking during measurement.
- Automatic optimisation of measuring pulse frequency and reference voltage.
- Accurate temperature compensation by non liner NaCI algorithm.
- Simple output range adaptation making it a versatile instrument.
- A HOLD-function for the current output signal.
- Selection of temperature sensors.
- Passcode protection.
Additionally YOKOGAWA designed the in­strument in such a way that an intrinsically safe version is available with the same featu­res and specifications. In fact the instrument is only adapted slightly to fulfil the require­ments of CENELEC.
The instrument comes in 2 versions only:
-A general purpose model.
-An intrinsically safe model.
This makes it easy to set up the instrument on site and valuable for large scale exchan­ges or emergency operations.
Page 8
3. INSTALLATION AND WIRING
3-1. Installation and dimensions 3-1-1. Installation site
As the transmitter is a rain-tight type, it can be installed outdoors as well as indoors. It should, however, be installed as close as possible to the sensors avoiding long cable lengths between sensors and transmitter. The certified version can be installed in Zone
1. Select an installation site where:
- mechanical vibrations and shocks are neg­ligible;
- no relay/power switches are in the direct environment;
- the transmitter is not mounted in direct sunlight and severe weather conditions;
- maintenance activities are possible (no corrosive atmospheres).
The ambient temperature and humidity should be the limits of the specifications.
3-1-2. Mounting methods
The EXA SC200 transmitter has universal mounting possibilities:
- panel mounting using selftapping screws;
- surface mounting on a plate (by bolts from the back);
- wall mounting on a bracket (e.g. thick brick wall);
- pipe mounting using a bracket on a hori­zontal or vertical pipe (maximum diameter 50 mm);
Panel-mounting Surface mounting
Cut-out dimensions for panelmounting Dimensions
4
2 x M6 (bolts)
Unit: mm (inch)
162 (6.4)
115 (4.5)
77
180 (7)
30 (1.2)
Unit: mm (inch)
min. 203 (8)
min. 229 (9)
172 (6.77)
154(6.06)
30 (1.18)
2x ø4
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5
Universal pipe/wall mounting
Wall mounting
Pipe mounting
(vertical)
Pipe mounting
(horizontal)
2" I.D. pipe
2" I.D. pipe
115
200
70
4x ø10
2x ø6.6
56
77
Page 10
3-2-4. Access to terminal and cable
entry
1. To access terminals remove the front cover of the EXA SC200 by releasing the 4 captive screws.
2. Pull the sensor cable into connection space and connected the wires to the terminals as indicated by the numbers on the wires. Make sure all connections are firm and do not touch each other.
3. Screw the gland securely and tighten it to keep out moisture. DO NOT use a wrench to tighten the nut.
4. A hose connection can be used to guide the cables coming from an immersion fit­ting through a protective plastic tubing to the transmitter. This adaptor has to be bought separately.
3-2. Wiring of sensors
3-2-1. General precautions
Generally, transmission of signals from the conductivity sensor is at a low voltage and high impedance level. Thus care must be taken to avoid interference. Before connecting the sensor cable to the transmitter make sure the next conditions are met:
- the sensor cable is not to be mounted in tracks together with high voltage and or power switching cables;
- use only the standard conductivity cable with a maximum length of 10 metre;
- mount the transmitter within the distance of the cable.
NOTE: The outside earth terminal should be con­nected to site ground by a large area con­ductor (e.g. a flat earth strip) for best protec­tion against interference.
3-2-2. Additional precautions for instal-
lations in hazardous areas
Make sure that the total of capacitancesand inductances connected to the input termi­nals of the EXA SC200 do not exceed the limits given in the certificate.This sets a limit to the cable and extensions used.
The intrinsic safe version of the EXA SC200 instrument can be erected in Zone 1.
The sensors can be installed in Zone 0 or Zone 1 if a safety barrier according to the limits given in the system certificate is used.
3-2-3. Grounding the liquid
In all circumstances, the sensor side of the measuring loop is grounded to the measu­ring liquid through one of the electrode con­tacts in the conductivity cell. The supply and output signal are isolated to avoid uninten­tional ground loops.
6
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7
Range selection
3-2-5. Connecting diagram for sensors
2-Electrode system 4-Electrode system
TEMPERATURE SENSOR
TEMPERATURE SENSOR
CEL
C= 10/cm
C= 1/cm
C= 0.1/cm
C= 0.01/cm
CEL
e.g. Use cable WU40/LH... Max. recommended length 10 m Use Cells SC41 or SC42
Range selection
* Use of 4-electrode
cell recommended
e.g. Use cable WU40/LH... Max. recommended length 10 m. Use Cells SC49
1 µS/cm 1 mS/cm 1 S/cm 1 µS/cm 1 mS/cm 1 S/cm
C= 10/cm
C= 1/cm
*
*
Page 12
3-3. Wiring of power supply 3-3-1. General precautions
Do not activate the power supply yet.First make sure that the DC-power supply is according to the specifications given. WARNING: DO NOT USE ALTERNATING CURRENT OR MAINS POWER SUPPLY! ! The cable leading to the distributor (power supply) or safety barrier transports power to and output signal from the transmitter. Use a two conductor shielded cable with a size of at least 1.25 mm2and an outside diame­ter of 9 to 15 mm. The cable gland supplied with the instrument accepts these diame­ters. The maximum length of the cable is 2000 metre. This ensures the minimum ope­rating voltage for the instrument.
3-3-2. Additional precautions for
installation in hazardous areas
1. Ensure that the total of capacitances
and inductances connected to the termi­nals of the EXA SC200 do not exceed the limits given in the certificate of the safety barrier or distributor.
2. The cable used should preferably have a
BLUE colour or marking on the outside.
3. Grounding:
• If the transmitter is mounted on a grounded surface (e.g. a metal frame fixed in the soil) the shield of the 2-wire cable may NOT be connected to ground at the distributor.
• If the transmitter is mounted on a non­conducting surface (e.g. a brick wall) it is recommended to ground the shield of the 2-wire cable at the distributor end.
4. Installation for EEx ia (sensors in Zone 0
or 1):
Generally, the distributor with input/output isolation has no external earth connection.If there is an earth connection on the distribu­tor and the external connection of the trans­mitter is connected to ”protective” earth, the shield of the 2-wire cable may NOT be con­nected to ”protective” earth at the distributor too.
3-3-3. Access to terminal and cable
entry
The terminal strip is accessed by removing the cover from the transmitter as was des­cribed in § 3-2-4. Use the left-hand gland to insert the 2-wire cable to the transmitter. Connect the supply to the terminals marked +, - and G as is indicated in the figures on pages 9 & 10.
3-3-4. Power on
After all connections are made and chec­ked, the power can be switched on from the distributor. Observe the correct activation of the instrument at the display.If for any rea­son the display does not indicate a value, consult the trouble shooting section.
8
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9
Wiring diagrams for power supply
General purpose design
Conductivity transmitter EXA SC200G
NOTE: The outside earth terminal should be connected to site ground by a large area conductor (e.g. a flat earth strip) for best protection against interference.
Sensor
Distributor
Output Supply
Dependance of load to supply voltage
1200
1000
800
600
400
200
0
1718 20 24 40
Ohm
550
Supply voltage (V)
Load resistance ()
Page 14
Wiring diagrams for hazardous areas
10
Intrinsically safe design (CELENEC standard EEX ib [ia] IIC T4) Conductivity transmitter EXA SC200S
EEx ib
certified safety
barrier
Distributor
Output
Sensor
Elektronic current Limiting barrier Vmax: 31.5 V lmax : 35 mA Pmax: 0.66 W
Zener barrier with resistor Vmax: 28 V lmax : 93.3 mA Pmax: 0.66 W
Protective earth
Safe area
Protective earth
Hazardous area Supply
Zone 0 of 1 Zone 1
Eex ib
Certified distributor with
input/output
isolation
Output
Sensor
Shunt zener­barrier or supply unit or isolated repeater Vmax: 22 V Imax : 85 mA
Protective earth
Safe areaHazardous area
Supply
Zone 0 of 1 Zone 1
Intrinsically safe design (CELENEC standard EEX ib [ia] IIC T4) Conductivity transmitter EXA SC200S
Page 15
11
4. COMMISSIONING
4-1. Operations overview
MAINTENANCE Operation by keys through the closed cover
CAL
DISPLAY
HOLD
Calibration
Show or fix additional values
Switching hold function on/off
5-1
5-2
5-3
Adjusting the output range
Activating the hold function
Temperature compensation
4-2
4-3
4-4
Fine tuning the performance 7
OUTPUT
SET HOLD
TEMPERATURE
SERVICE
COMMISSIONING Operation by *-key when cover is removed
SERVICE Operation by coded entry from commissioning
Routine Use Chapter
Note: All levels can be protected by a 3 digit passcode. See §7-15.
Page 16
Remove cover by releasing 4 screws. Display will show * 0% Display will show *100%
12
4-2. Output range adjustment
1. Access output 2. Adjust low span value 3. Adjust high span value
OUTPUT SET HOLD TEMPERATURE SERVICE
YES
NO
YES
NO
MODE
.
*
OUTPUT SET HOLD TEMP. SERVICE
ENT
µS/cm
ENT
OUTPUT SET HOLD TEMP. SERVICE
ENT
mS/cm
ENT
Access commissioning menu
Adjust value for low span Select digit to adjust or decimal point and units
Adjust digit
Confirm adjusted value
ENT
L
*
Return to measurement
select output function Select OUTPUT
YES
NOTE: If the output is commissioned to be via a table this whole item will be skipped! Default is a linear range.
L
Adjust value for high span Select digit to adjust or decimal point units
Adjust digit
Confirm adjusted value
ENT
L
L
MODE
ESCAPE TO MEASURE can be used at any stage to abort operation. WARNING: If the HOLD function is activated the instrument returns with the question HOLD (flashing); answer YES or NO or MODE again to return to measurement.
MODE
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13
1. What is the output range?
The display will always show the full range of the instrument from 0-2000 mS/cm. Maximum resolution is assured by autorang­ing, where the position of the decimal point and the measuring units (microSiemens/­milliSiemens) are moved to best fit the actu­al value.
For control or recording the current output can be ranged to a specific part of the total measuring span. When selecting the measuring range care must be taken to use the appropriate conductivity cell. For any given cell constant there is a defined range of operation which should not be exceeded.
From the factory the instrument has a linear output range 0-1 mS/cm in combination with a cell constant C=0.1 cm
-1
.
Other linear ranges can be programmed in this routine. It is also possible to program non linear output ranges for specific applica­tions. These are programmed in the service level, see sections 7-5 and 7-6.
2. Programming a linear output range
A linear output range is programmed by entering two values:
- 0% the conductivity at the start of the output range which corresponds to 4 mA
- 100% the conductivity at the end of the output range which corresponds to 20 mA.
When programming a range which does not start at zero conductivity, take care to respect the minimum value corresponding to 60% of the maximum value.
3. Example
The EXA SC200 has an output table which can be programmed to give any non-linear output characteristic. Activation of this table is described in §7-5. Once the table is acti­vated the linear OUTPUT routine will no lon­ger have any effect and will not be accessi­ble in the commissioning menu. Programming of the 21 step table is descri­bed in § 7-6.
Non-linear outputs are commonly used for measurements in pure water where high resolution is required over a small range combined with trend indication over a larger range. Common forms of output for these applications are given in §7-17. The non-linear output can also be used to follow a concentration curve for a specific product. Care must be taken to ensure that the temperature compensation is also set up for the measured fluid under representa­tive conditions. It should also be noted that conductivity measurements are not specific, so it can be influenced by impurities present or changes in the fluid composition.
4. Other possibilities
Programming a percent by weight indication on the second display line §7-13
4-2. Output range adjustment
Page 18
14
*
HOLD = Set HOLD function Display shows actual status.
*H.OFF = HOLD not active *H.ON = HOLD activated
Displa`y shows current setting
4-3. Set up HOLD function
1. Access HOLD routine 2. Activate HOLD function 3. Adjust value to hold
OUTPUT SET HOLD TEMPERATURE SERVICE
YES
NO
YES
NO
MODE
.
*
OUTPUT SET HOLD TEMPERATURE SERVICE
YES
NO
YES
NO
MODE
.
*
OUTPUT SET HOLD TEMP. SERVICE
ENT
ENT
HOLD
.
Access commissioning menu
SELECT choice
*
Select SET HOLD Move pointer to SET HOLD
NO
YES
Activate (de-activate) HOLD Change setting
Conform setting
NO
YES
Select HOLD fixed or last Change selection
Confirm selection
NO
YES
*H.FIX = Hold fixed value *H.LST = Hold last value
Adjust fixed value Select digit to adjust
Adjust value of digit
Accept value
Return to measurement
ENT
L
L
MODE
ESCAPE TO MEASURE can be used at any stage to abort operation. WARNING: If the HOLD function is activated the instrument returns with the question HOLD (flashing); answer YES or NO or MODE again to return to measurement.
MODE
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15
1. What is HOLD?
HOLD is a function freezing the output sig­nal temporary, during normal maintenance, preventing all sorts of alarming situations to occur. Two possibilities are generally used:
a .Keeping the output at the LAST value just
before the start of maintenance. This can only be used when a recorder is connec­ted.
b. Keep the output at a preset FIXED value
which will not cause any of the alarms to go off or any controlling action to be taken. This is the preferred situation when dealing with Conductivity-control sys­tems.
2. How does it work?
The HOLD-function has to be activated from the *-menu before it can be used.
The EXA SC200 will keep the output frozen during the following events:
- Access to the *-menu.
- Access to the calibration mode.
- Switching it from the MODE-menu.
HOLD is signalled in the display by a special field.
The operator is prompted to switch HOLD on or off before returning to normal mea­surement.
3. Example
In a storage tank the concentration of sodi­um hydroxide (caustic soda) has to be kept at 5% . The mixing process is controlled by a conductivity transmitter and electro-mag­netic valves. During maintenance of the conductivity cell or the transmitter the HOLD function is acti­vated to keep the mixing process from was­ting precious chemicals to the sewer. The HOLD function is set for a fixed output so that the dosing valves will not be activa­ted.
4. Time out
Hold will be de-activated after 20 minutes if no key is pressed. To cancel this function see 7-8.
4-3. Set up HOLD function
Page 20
ESCAPE TO MEASURE can be used at any stage to abort operation. WARNING: If the HOLD function is activated the instrument returns with the question HOLD (flashing); answer YES or NO or MODE again to return to measurement.
16
TEMP = Temperature compensation function NaCl = Automatic temperature compensation The setting of the temperature coefficient is done
by adjusting a conductivity value, at process tem­perature, to the conductivity value that was meas­ured at reference temperature
4-4.Temperature compensation
1. Access temperature compensation routine
2. Select automatic NaCl temperature compensation
3 Select temperature coefficient
compensation
OUTPUT SET HOLD TEMPERATURE SERVICE
YES
NO
YES
NO
MODE
*
OUTPUT SET HOLD TEMPERATURE SERVICE
YES
NO
YES
NO
MODE
*
OUTPUT SET HOLD TEMP. SERVICE
ENT
ENT
TEMP. MAN
.
.
mS/cm
Access the maintenance menu
Select temperature compensation function
*
Select temperature compensation routine Move pointer to TEMP
NO
YES
Select automatic compensation Change displayed selection
Confirm selection
NO
YES
NOTE:
1. If NaCl is chosen the temperature compensa-
tion will be according to NaCI solutions.
2. If *NaCl and *T.C. do not appear, this indicates
that Matrix compensation is selected in service code 13.
Adjustment of the conductivity value Select digit to adjust
Adjust manual temperature
Confirm adjusted value
ENT
L
L
Error E2 indicates that the temperature coefficient is less than-10%/°C or more than +10%/°C.
NOTE: Direct setting of the compensation factor is possible. Refer to §7-12.
MODE
Page 21
17
1. Why is temperature compensation necessary?
The conductivity of a solution is very strong­ly influenced by temperature. Typically for every 1°C change in temperature the solu­tion conductivity will change by approxima­tely 2%.
The effect of temperature varies from one­solution to another and is determined by several factors: solution composition,con­centration and temperature range. In very pure water the temperature influence increa­ses dramatically with increasing purety to approximately 6%/°C.
A coefficient (a) is used to express the amount of temperature influence in % chan­ge in conductivity/°C. In almost all applications this temperature influence must be compensated before the conductivity reading can be interpreted as a measure of concentration or purity.
2. Automatic temperature compensa­tion with EXA SC200
From the factory EXA SC200 instruments are calibrated with a general temperature­compensation function based on a sodium­chloride salt solution. This is suitable for many applications and is compatible with the compensation functions of typical labo­ratory or portable instruments.
As conductivity decreases into the range of pure water the instrument will follow the non-linear compensation function of neutral NaCl solutions. In the high conductivity region the effect of temperature decreases and the compensation factor is decreased too. In these extreme regions the tempera­ture compensation factor is calculated with a square equation.
A temperature compensation factor is de­rived from the following equation:
α
= Temperature compensation factor (in
%/°C) T = Measured temperature (°C) Kt= Conductivity at T T
ref
= Reference temperature (25°C)
K
ref
= Conductivity at T
ref
3. Manual setting of temperature com­pensation with EXA SC200
If the general compensation function is found to be inaccurate for the sample in question, the instrument can be set manual­ly for a linear factor on site to match the application.
The procedure is as follows:
1. Take a representative sample of the pro­cess liquid during operation.
2. Heat or cool this sample to the reference temperature of the instrument (usually 25°C). Note: see §7-4.
3. Measure the conductivity of the solution with the SC200 and note the reading of the display.
4. Bring the sample to the typical process temperature. (Check the temperature with the display routine.)
5. Adjust the reading of the display to the previously noted value at the reference temperature.
6. Check that the temperature compensa­tion factor has been changed (from the display routine).
7. Insert the conductivity cell into the pro­cess again
4. Other possibilities
Manual temperature coefficient §7-12.
4-4. Temperature compensation
Kt- K
ref
x 100
α=
X
T - T
ref
x K
ref
Page 22
4-5. Sensor selection and diagnostics
4-5-1. General remarks
The EXA SC200 continuous sensor diagnos­tics can lead to the indication of faults due to the fouling of the connected sensor. The fault will be indicated with a signal field on the display and (if activated) by a 22 mA sig­nal. The selection of the correct conductivity cell with the suitable cell constant is explai­ned in the next section.
4-5-2. Selecting a conductivity cell
First select the range limits for the EXA in­strument. For conductivity values below 1 µS/cm the only choice is a cell with cellconstant 0.01 cm-1. From 1 µs/cm up to 10 mS/cm a cell­with cellconstant 0.1 cm-1can be used. A cellconstant of 1 cm-1is used between 10 µS/cm up to 100 mS/cm. The cell with cell­constant 10 cm-1is used from 100 µS/cm to 1 S/cm. All these values refer to the actual measured values at the operating tempera­ture. Above 20 mS/cm with C=1 cm-1and 200 mS/cm with C=10 cm-14-electrode cells are advised.
Yokogawa delivers cells from a choice of chemically resistant materials like stainless steel, epoxy resin, PTFE and PVDF.
The cell determines the principle used to measure the conductivity: there is a distinc­tion between 2-electrodes and 4-electrodes cells. The selection of 2 or 4 electrode measuring principle is from the service level §7-9.
4-5-3. Selecting a different cell-con­stant
The EXA SC200 can be programmed to ac­cept any cell with a cell-constant between
0.01 and 50/cm. The adjustment of the cell­constant must be executed from the service level §7-7.
4-5-4. Integral temperature sensor
The factory setting for the temperature sen­sor is a Pt-1000 element. To get a different temperature setting the service level setting at § 7-4 is used. A separate temperature sensor can be con­nected, if no integral temperature element is present in the conductivity cell. Choose a Ni-100, NTC or Pt-1000 sensor to get the correct temperature reading.
4-5-5. Sensor diagnostics and related-
error messages
The check for polarisation of the electrodes is only working correctly when the cell-con­stant has been chosen to match the measu­ring range. The check is automatically switched off when the 4-electrode measu­ring principle is selected. The check can manually be switched on or off: refer to
§7-14. The factory setting for the polarisa­tion check is off.
18
Page 23
19
Page 24
20
CALIB = Calibration
START = Start calibration CAL.END = End of calibration session
5. MAINTENANCE 5-1. Calibration
1. Access calibration routine 2. Adjust value 3. End calibration
MEASURE CAL DISPLAY. HOLD
YES
NO
YES
NO
MODE
µS/cm
MODE
.
MEASURE CAL DISPLAY. HOLD
YES
NO
ENT
µS/cm
MODE
MEASURE CAL DISPLAY. HOLD
YES
NO
YES
NO
MODE
µS/cm
MODE
.
Access maintenance mode
Select calibration
Select manual calibration Move pointer to display
NO
YES
End calibration End calibration and return to measurement
Continue routine to calibrate second point (repeat step 2)
YES
NO
MODE
Conform start of adjustment
YES
Select digit to adjust
Adjust value
Conform adjusted value
ENT
L
L
Adjust process value to previously determined value (e.g. from hand-held conductivity-meter)
Error E3 indicates that the calibration value is deviating more than 20% from the originally meas­ured value.
ESCAPE TO MEASURE can be used at any stage to abort operation. WARNING: If the HOLD function is activated the instrument returns with the question HOLD (flashing); answer YES or NO or MODE again to return to measurement.
MODE
Page 25
21
1. When is calibration necessary?
Calibration of conductivity instruments is not normally required since conductivity cells are manufactured within controlled tolerances and do not alter in use.
If the cell has been severely fouled or sub­ject to abrasion (possibly during cleaning) it may be necessary to calibrate.
Alternatively calibration may be carried out with a simulator to check the electronics only.
2. How is calibration done?
Calibration is carried out by measuring a solution which has a known conductivity and adjusting the instrument to show the correct conductivity value.
Calibration solutions can be made up in the laboratory. A solution of salt is made with precise concentration. Temperature is stabi­lised to the reference temperature of the in­strument (usually 25°C). The conductivity of the solution is taken from tables.
Alternatively the instrument may be calibra­ted in an unspecified solution against a standard instrument. Here care should be taken to make measurement at the refe­rence temperature since differences in the type of temperature compensation of the instruments may cause an error.
3. Typical calibration solutions
The table below shows typical conductivity values for solutions which may be made up in the laboratory.
Table for NaCI at 25°C
5-1. Calibration
% weight mg/kg Conductivity
00.001 10 021.40 µS/cm
00.003 30 064.00 µS/cm
00.005 50 106.00 µS/cm
00.01 100 210.00 µS/cm
00.03 300 617.00 µS/cm
00.05 500 001.03 mS/cm
00.1 1000 001.99 mS/cm
00.3 3000 005.69 mS/cm
00.5 5000 009.48 mS/cm 01 10000 017.60 mS/cm 03 30000 048.60 mS/cm 05 50000 081.00 mS/cm
10 100000 140.00 mS/cm
Page 26
ESCAPE TO MEASURE can be used at any stage to abort operation. WARNING: If the HOLD function is activated the instrument returns with the question HOLD (flashing); answer YES or NO or MODE again to return to measurement.
22
5-2. Selecting a value to display
DISP = DISPLAY routine
The second line of the display will show the possi­bilities
The second line of the display will show the possi­bilities
1. Access display routine 2. Read data 3. Reprogram data display
MEASURE CAL DISPLAY. HOLD
YES
NO
YES
NO
MODE
MODE
MEASURE CAL DISPLAY. HOLD
YES
NO
YES
NO
MODE
MODE
.
MEASURE CAL DISPLAY. HOLD
YES
NO
YES
NO
MODE
MODE
.
Access maintenance mode
Select Display routine
Select display Move pointer to DISPLAY
NO
YES
Read data To read values only
Parameter Unit
- Temperature ˚C/˚F
- Output signall mA
- % by weight % C.C - Cell constant cm-1 T.R. - Reference
temperature ˚C/˚F NaCl/jjj - Temperature T.C Compensation coefficient
standard/manual
%/˚C
REL - software release
Return to measure
NO
MODE
Reprogram data display Move to desired value for display
Parameter Unit
- Temperature ˚C/˚F
- Output signal mA
- % by weight %
C.C - Cell constant cm
-1
T.R. - Reference
temperature ˚C/˚F NaCl/jjj - Temperature T.C Compensation coefficient
standard/manual
%/˚C
REL - software release
To select a value for permanent dis­play during measurement
NO
YES
MODE
MODE
Page 27
23
1. What is the display routine?
The second line in the display is intended to be used to:
- Show actual status
- Show messages
- Show errors
When delivered from the factory the EXASC200 shows the temperature on the second line. You can make the instrument show a diffe­rent parameter on the second line by selec­ting it from the list at right.
2. What can you read?
Temperature is an actual value. Output is an actual value. Percent by weight is an actual value. Cell constant is programmed. Reference temperature is programmed. NaCl or temperature coefficient is program­med.
The choice of temperature units is done from the Service level.
Error messages have priority over other messages.
Note: Percent by weight is only visible when activated from the service level §7-13.
3. Example
To check the value of the output signal (4...20 mA) it is displayed on the second line.
Measuring range 0...100 µS/cm Output signal 4...20 mA
Process value 60 µS/cm Output value 13.6 mA
When the second line is changed to display output the current signal is visible all the time.
Whenever HOLD is activated the value on the display is frozen to the programmed value (using the FIXED setting). Pressing MODE will take you back to measuring and the temperature will show again.
5-2. Selecting a value to display
Page 28
ESCAPE TO MEASURE can be used at any stage to abort operation. WARNING: If the HOLD function is activated the instrument returns with the question HOLD (flashing); answer YES or NO or MODE again to return to measurement.
24
5-3. Use of HOLD function
HOLD = HOLD output function
Display will blink HOLD and YES/NO
1. Access hold 2. Switch hold on/off
MEASURE CAL DISPLAY. HOLD
YES
NO
YES
NO
MODE
MODE
MEASURE CAL DISPLAY. HOLD
YES
NO
YES
NO
MODE
MODE
HOLD
Access maintenance mode
Select HOLD function
Move pointer to HOLD
Select HOLD function Select HOLD
NO
NO
Switch hold OFF
Switch hold ON
NO
YES
MODE
NOTE: This function can only be used if activated during commissioning (see chapter 4-3).
HOLD in left top of display is switched
MODE
Page 29
25
1. What is HOLD?
Hold is a function which freezes the output signal temporarily, it is normally used during maintenance when the cell is removed from the measured solution to prevent unwanted controller reaction.
The HOLD function must be commissioned from the programming menu before it can be switched on or off. See commissioning the hold function for more details.
Note: AUTO RETURN will switch off HOLD after 20 minutes, see § 7-8.
2. How does it work?
From this level the HOLD function can only be switched ON or OFF. HOLD is switched on when you press YES when HOLD and YES/NO are blinking. When you press NO hold will be switched off A flag is kept in memory and an indication is made in the upper left corner of the display field.
The HOLD function only influences the out­put signal, no other functions are influenced.
The operator is prompted to switch HOLD on or off after having performed a mainte­nance function.
3. Example
During the transfer of cleaning liquid into a batch reactor with a conductivity-control system, the HOLD function is switched ON to prevent the controlling instruments from running wild. After cleaning has ceased and the new batch has been started HOLD is switched OFF again and conductivity control resu­mes.
5-3. Use of HOLD function
Page 30
6-1. Introduction
The EXA SC200 microprocessor based conductivity analyser continuously monitors the condition of all key components of the measuring system to ensure that measure­ment is dependable. If a fault is detected this is immediately signalled. Errors are shown on the display with a code. The following table shows the errors which can be detected and gives information to help locate the fault or identify the error. Faults detected whilst the instrument is on line can also be signalled by a (temporary) high output signal (22 mA).
6-2. Self diagnostics of the conductivity
cell
During measurement the instrument adjusts the measuring frequency to give the best conditions for the actual value being meas­ured. At low conductivity there is risk of error due to capacitive effects in the cable and cell. These are reduced by using a low measuring frequency. At high conductivity these capacitive effects become negliable and errors are more likely to be caused by polarisation or fouling of the cell. These errors are reduced by increasing the measu­ring frequency.
At all values the instrument checks the sig­nal from the cell to search for distortion which is typical of capacitive or polarisation errors. If there is a problem with the installa­tion or the cell becomes fouled this will trig­ger an error message on the display possi­bly accompanied by a fault signal through a (temporary) high output current (22 mA).
6-3. Self diagnostics of the temperature
sensor
The temperature sensor, which is normally built into the conductivity cell, is checked to detect damage or faulty connections.
NOTE: A temperature fault may be caused by incorrect programming of the temperature element!
6-4. Self diagnostics of the electronics
The microprocessor operation is checked by a watchdog which initiates an electronic reset if the normal function suffers severe interference. During reset the instrument checks the program and all stored data. If a fault is then detected an alarm is given.
6-5. Checking during operation
Whenever the instrument is being program­med or calibrated, data is checked and an error is shown when appropriate. Should this occur the new data is rejected and the instrument continues to work with the previous settings.
26
6. TROUBLE SHOOTING
Page 31
27
6-6. Error messages and explanation
Code Error description Possible cause Suggested remedy
E1* Faulty signal from conductivity cell Polarisation Check cell is correct for range
Cell is fouled Clean cell
E2 Wrong temperature coefficient during Incorrect data entered Repeat temperature calibration
calibration
E3 Calibration out of limits Calibration value deviates more than Check cell, connections or reference
20%
E5* Conductivity too high Measurement is out of range Check cell range, reprogram range E6* Conductivity too low Measurement is out of range Check cell range, reprogram range
E7* Temperature too high Wrong temperature sensor selected Program sensor type
Fault in connections Check connections
E8* Temperature too low Wrong temperature sensor selected Program sensor type
Fault in connections Check connections
E10* EEPROM write failure Fault in electronics Call yourYOKOGAWA service
organisation
E15 Temperature correction Fault in cable or wrong Check connections or program
outside limits (> 5) temperature sensor selected correct sensor type
E17 Output span too small 0% range value set too high Program value <60% of high range E18 Output table makes no sense Table changes from ascending to Check programming of table
descending or vice versa
E19 Programmed value not accepted Values not acceptable Reprogram with new values E20* Data lost Data, including initial setting, lost Call your YOKOGAWA service
organisation
* These errors will trigger the FAIL-status.
Page 32
7. SERVICE MODE
7-1. Introduction
Generally speaking their is no necessity to adjust the settings of the service section All parameters are pre-programmed to values (so-called defaults) enabling you to start working immediately.
The advanced functions available through this section are only needed in some speci­fic applications. This fine-tuning of the in­strument gives a superior performance over conventional 2-wire instruments.
If a function has to be adjusted it is called up with the code mentioned. Having selected the code then give you the possibility to either activate or adjust the values for this function. After this you will return to the entry point to make other adjustments or go back to the measuring status.
If errors are made during the programming process, these will be indicated, no action will be taken and you can start the program­ming again.
28
Code Routine Use Chapter
01 Temperature sensors and units Select sensor type 7-3
Select °C or °F 02 Reference temperature Adjust value 7-4 03 Output table or linear Select which to use 7-5 04 Program output table Set values in table 7-6 05 Cell constant Adjust cell-constant 7-7 +10-1 06 Auto return function Switch on or off 7-8 07 Measuring principle Select 2 or 4 electrode 7-9 08 Temperature adjust Correct cable error 7-10 09 Signal errors or output Switch on or off 7-11 10 Temperature compensation factor Adjust factor 7-12 11 %-indication on second Switch on or off and 7-13
display line Set values 12 Polarisation check Switch on or off 7-14 13 Matrix compensation Select 5x5 matrix compensation 10-2 14 Matrix temperature Set temperatures for user matrix 10-3
compensation range 15-19 Matrix data Set data for user matrix 10-4 20 “Soft”/“hard” fail situation Select “soft” or “hard” fail 10-5
message per fail code 21 E6-fail message Switch on or off 10-6 33 Passcode activation Protecting levels 7-15 55 Restore defaults Erase values 7-16
Page 33
29
ESCAPE TO MEASURE can be used at any stage to abort operation. WARNING: If the HOLD function is activated the instrument returns with the question HOLD (flashing); answer YES or NO or MODE again to return to measurement.
7-2. Access to service settings
*SERV = Service settings
Display will show *CODE Display shows current setting
Values adjusted access to individual routine description
1. Access service 2. Enter code to select required function
3. Adjust setting (see individual routines)
OUTPUT SET HOLD TEMPERATURE SERVICE
YES
NO
YES
NO
MODE
*
OUTPUT SET HOLD TEMP. SERVICE
ENT
ENT
OUTPUT SET HOLD TEMP. SERVICE
ENT
ENT
.
.
Access commissioning menu
Select SERVICE
*
Select service function Move pointer to service
NO
YES
Enter access code to select routine Select digit to adjust
Adjust code for entry
Confirm choice
ENT
L
L
Adjust settings Select digit to adjust
Adjust value
Confirm adjusted value
ENT
L
L
Return to measure
MODE
MODE
Page 34
X.X
0. Temperature sensor = Pt-1000
1. Tempersture sensor = Ni-100
2. NTC sensor .0 Temperature displayed in ˚C
.1 Temperature displayed in ˚F
30
7-3. Temperature sensors and units
ACCESS-CODE: 01 (see § 7-2) DISPLAY : *T.CODE
Adjustment (X.X)
7-4. Reference temperature
ACCESS-CODE : 02 (see § 7-2) DISPLAY : *T.R. ˚C or *T.R. ˚F
Adjustment : Adjust the value for the
reference temperature used in the calculations. Normally this value will be 25˚C.
Explanation:
The code for the temperature units influen­ces the temperature indication on the dis­play only. Default value is ˚C. The indication here determines which tem­perature sensor is connected to the instru­ment. Check what sensor will be used in your plant and set the correct number for it. Default value is Pt-1000 for Yokogawa sen-
sors, type SC42-.....
Default: ˚C
Explanation:
All measured values are compensated for temperature to refer to comparable values at 25˚C. This temperature is easily produced at laboratory conditions and most literature data use this temperature. In exceptional cases it is possible to use a different refe­rence temperature in combination with a programmed temperature coefficient (e.g. Sulfuric acid measurement).
Default: 25˚C
7-5 Output code selection
ACCESS-CODE : 03 (see § 7-2 ) DISPLAY : *TABLE
Adjustment : 0=Linear range only
1=Output table with 20 steps
Explanation:
As a default a linear output is set and only 0% and 100% can be adjusted from the commissioning output function. When an output table is programmed by setting a 1, the table can be programmed at CODE 04. Otherwise CODE 04 will have no effect. See the entry at the next CODE.
Page 35
31
7-6. Output table for non-linear range
ACCESS-CODE : 04 (see §7-2) DISPLAY : 0% to 100%
Adjustment :
A 21 step table can be programmed from this entry ONLY IF it was set in the previous CODE 03. It is possible to set up a bi-linear, semi-logarith­mic or hyperbolic scale to cope with retro fitting on existing installations. Also linear output to con­centration related curves can be programmed.
Explanation:
First you will be presented with the question YES/NO to give the opportunity to skip valu­es from the table. To get a 10 step table you would skip every other value and only ans­wer YES to enter a value. The instrument uses interpolation between entered values. Press NO to skip values. Press YES to adjust value. Now adjust the value by pres­sing > and ^. The units can be adjusted as well as the decimal point position. Examples are mentioned in §7-17. Other possibilities: programming ”% by weight” indication on second display line: refer to §7-13.
Percentage of mA-output range versus percentage of conductivity range.
Examples: A = bilinear B = hyperbolic (2 decades) C = logarithmic (2 decades) D =linear
NOTE: Curves are not selectable, but can be pro­grammed from the tables at right.
Example of output tables
bi-lin = bi-lineair over 2 decades log 2 = logarithmic over 2 decades log 3 = logarithmic over 3 decades hyp 2 = hyperbolic over 2 decades hyp 3 = hyperbolic over 3 decades
NOTE: Multiply the values from the table with appropriate factors to get the end-scale value you want.
Special concentration tables can be pro­grammed by the user.
mA-output range
% of conductivity range
Output bi-lin log 2 log 3 hyp 2 hyp 3
0% 0.0 1.0 0.10 1.00 0.10 5% 1.0 1.3 0.14 1.20 0.27 10% 2.0 1.6 0.20 1.82 0.43 15% 3.0 2.0 0.28 1.90 0.61 20% 4.0 2.5 0.40 2.00 0.83 25% 5.0 3.2 0.56 3.75 1.10 30% 6.0 4.0 0.79 4.80 1.36 35% 7.0 5.0 1.12 5.92 1.68 40% 8.0 6.3 1.58 7.00 2.05 45% 9.0 7.9 2.24 8.31 2.49 50% 10.0 10.0 3.16 10.00 3.00 55% 20.0 12.6 4.47 11.85 3.66 60% 30.0 15.8 6.31 14.00 4.33 65% 40.0 20.0 8.91 16.65 5.22 70% 50.0 25.1 12.6 19.50 6.80 75% 60.0 31.6 17.8 23.80 8.25 80% 70.0 39.8 25.1 29.55 11.0 85% 80.0 50.1 35.5 36.70 14.8 90% 90.0 63.1 50.1 48.50 21.8 95% 100.0 79.4 70.8 68.60 36.5 100% 110.0 100.0 100.0 100.00 100.0
Page 36
X 0 OFF
1 ON
32
7-7. Cell constant adjustment
ACCESS-CODE : 05 (see §7-2) DISPLAY : *CELL.C
Adjustment : Adjust the value to the
cell-constant used with your instrument. Values between 0.01 and 50/cm can be program­med.
Explanation:
Every conductivity cell has a cell-constant, which can be indicated on the outside of the body. Sometimes the cell-constant can be indicated in the type-number of the sensor. Yokogawa produces several models with cell-constants of 0.01, 0. 1, 1 and 10/cm. For accurate measurements the cell-con­stant can be determined in a laboratory test.
Default: 0.1 cm
-l
7-8. Auto return function
ACCESS-CODE : 06 (see §7-2) DISPLAY : *RET
Adjustment: X
Explanation
As a safeguard against long maintenance jobs or inadvertently pushing a button it is possible to let the system return to its nor­mal function of measurement when no keys are pushed for 10 minutes.
Default: Auto return on
7-9. Measuring principle
ACCESS-CODE : 07 (see §7-2) DISPLAY :*4ELEC
Adjustment : Select the measuring
principle of the transmit­ter.
X 0 2-electrode principle
1 4-electrode principle
Automatic return to measure after 10 minutes.
Explanation:
Select the principle to cooperate with the measuring sensor. The conductivity cell determines which prin­ciple can be used. The 4-electrode principle is used for the high conductivity values in general.
Default: 2-electrode principle
Page 37
X.X 0 OFF 1 ON = 22 mA steady signal on
fault.
2 ON = 22 mA pulse during
30s at start of fault then normal output.
33
7-10. Temperature sensor adjustment
ACCESS-CODE :08 (see § 7-2) DISPLAY :*T.ADJ
Adjustment :Adjust the value of the
indicated temperature (°C/°F) to that of the actual temperature.
Explanation:
The temperature measurement is a two wire resistance measurement. In this kind of measurement the length of the connecting cable can influence the accuracy of the tem­perature indication. To compensate for the extra resistance of the cable up to 5can be calibrated. Connect the correct tempera­ture sensor to the EXA instrument and insert it in a stable temperature bath of a known value. Check the temperature indicated at this set­ting in °C or °F and adjust the value if necessary. Now the EXA transmitter has been calibra­ted to compensate for the cable resistance.
7-11. Signalling of fail condition
ACCESS-CODE : 09 (see §7-2) DISPLAY : *BURN
Adjustment : X.X
Explanation:
Besides an indication at the display in the field, sometimes an indication of errors in the control room is also necessary. This is possi­ble by sending a special signal over the 2­wire connection to the receiving instrument. A signal of 22 mA is used, because it is out­side the normal analogue range of 4 to 20 mA. If at the receiving end an alarm is set to the value represented by 22 mA, it is obvious that the proper action can be taken from the control room too. The signal uses the same convention as used in thermocouple indica­tions for detecting break of the sensor (burn­out).
Default: 0 = OFF
7-12. Temperature compensation
coefficient adjustment
ACCESS-CODE : 10 (see § 7-2) DISPLAY : *T.C.
Adjustment : Adjust the value of the
manually set compensa­tion factor
NOTE: Access to this routine is only possible when manually set temperature compensation factor (α) is selected in §4-4.
Explanation:
In addition to the procedure described in
§4-4 it is possible to adjust the compenstion
factor directly. If the compensation factor of the sample liquid is known from laboratory experiments or has been previously determi­ned, it can be introduced here. Adjust the value between -10.00 to -10.00 % per °C. In combination with the reference temperature setting at §7-4 a linear com­pensation function is obtained, suitable for all kind of chemical solutions.
Kt- K
ref
x 100
α =
X
T - T
ref
x K
ref
Default: skipped, compensation for NaCI is automatic.
Page 38
X 0 OFF
1 ON
34
7-13. Percent by weight indication on
second display line
ACCESS-CODE : 11 (see § 7-2) DISPLAY : *%
Adjustment:(X)
Select the possibility to display % by weight on the second display line. When % indication is activated (Select 1) the display range can be adjusted: *0%: Adjust low span display value *100% Adjust high span display value
Explanation:
In case a conductivity measurement is used for concentration monitoring it can be con­venient to link the measured conductivity value to a % by weight concentration value. A linear concentration indication in % units is programmed by entering two values.
- X in 3 digits corresponds to 0% of the output value (= 4 mA)
- Y in 3 digits corresponds to 100% of the output value (= 20 mA)
Example:
0% output is 93.0% by weight
100% output is 99.0% by weight
The instrument uses interpolation between the entered values. As the relation between percent by weight concentration and con­ductivity is not linear in most cases, the pos­sibility to linearize the output to concentra­tion units can be used. Refer to §7-5 and
§7-6. The instrument becomes a concentra­tion meter by output function and (second) display (line) based on a conductivity mea­surement.
Default: OFF
7-14. Polarisation check
ACCESS-CODE : 12 (see §7-2) DISPLAY : *POL.CK
Adjustment: (X)
Generation of the fault E1 can be switched off.
Explanation:
The EXA SC200 normally checks the signal from the cell to search for distortion typical of capacitive or polarisation errors. If there is a problem with the installation or the cell becomes fouled this will trigger the E1 fault signal. In some installations this error detecting can cause unwanted signals during operation. Then the possibility to disable this check will be used.
Note: When 4-electrode measurement is chosen this checking is not performed.
Default: OFF
X 0 OFF
1 ON
Page 39
35
7-15. Passcode protection by three digit
code
ACCESS-CODE : 33 (see § 7-2) DISPLAY : *PASS
Adjustment(X.X.X)
0.X.X Protection on Maintenance level inactive X.0.X. Protection on Commissioning level inactive X.X.0 Protection on Service level inactive
#.X.X Protection on Maintenance level activated X.#.X Protection on Commissioning level activated X.X.# Protection on Service level activated
Note: # can be a digit from 1 to 9, and it will give a protection according to the schema­tic below of the programmed level. 0 = No passcode 5 = Passcode is 123 1 = Passcode is 111 6 = Passcode is 957 2 = Passcode is 333 7 = Passcode is 331 3 = Passcode is 777 8 = Passcode is 546 4 = Passcode is 888 9 = Passcode is 847
Explanation:
In some cases a protection of operation level is wanted. In this way unauthorized access to any of the 3 levels can be blocked by a simple passcode. When a passcode is selected for an operation level, access to that level can only be obtained after ente­ring the passcode. The display will show a message *PASS* to indicate the entry of the passcode.
NOTE: For the Maintenance and Commissioning level the passcode entry is always requested when entering from the measure mode.
- For the Service level the passcode entry is requested after pushing the YES-key.
- When the Service level protection is activa­ted, the passcode cannot be changed by unauthorized persons.
Default: 0.0.0.
No Passcode protection.
7-16. Restore default setting
ACCESS-CODE : 55 (see §7-2) DISPLAY : ERASE
Adjustment: YES Erase all program-
med values and replace them by defaults.
NO Keep all program-
med values as befo­re.
Explanation:
This entry is provided to make it possible to start from the default values given by Yokogawa and thus erase all previously pro­grammed information.
WARNING: Do not use this code without proper authori­ty as all settings and programmed functions will be lost!!
WARNING
Do not enter service codes that are not mentioned in this booklet.
Page 40
11 12 14 13 17 15 16
G - +
36
8. CLASSIFICATION
1 conductivity sensor with integral SC41-SP34
temperature sensor such as (but SC49-FP08 not limited to) SC41-SP24
SC41-EP14 SC41-EP04
These are all passive sensor to be regarded as "simple apparatus" i.e. devices which coply with clause 1.3 of EN 50014.
SC 200 S Vout = 14.4 V max. Iout = 72.8 mA max. C ext = 1300 nF max L ext = 8.0 mH max.
BASEEFA Nr. Ex 89C2379
connecting cables such as (but not limited to): WU40-LH18 WU40-LH2 WU40-LH5
Certified Barrier with electronic current limitation and the fllowing characteristics: V max. out = 31.5 V, Imax. out = 35 mA, P max. out = 1.1 W type : Yokogawa Bard 400 (BASEEFA Cert. Ex 84B2257x)
Any shunt zenerdiode safety barrier certified by BASEEFA or any EEC approeved certification body to [EEx ia] II C or [EEx ib] ii C where the output current is limited by a resistor "R" directly in the output line such as that Imax.out = Vmax.out/R and not exceeding the following char­acteristics: Vmax.out = 28 V; Imax.out = 93.3 mA and Pmax.out = 8.66 W. such as (but not limited to): type: MTL 728
MTL 788 (BASEEFA Cert. Ex 832452) MTL 788 R Stahl 8981/31-280/085/00 (P.T.B. Cert. Ex-78/2007X)
any shunt zenerdiode safety barrier or supply unit or isolated repeater certified by BASEEFA or any EEC approevd certification body to [EEx ib] ii C or [EEx ib] ii C where the output current is limited in a different way and not exceeding the following characteristics: Vmax.out = 22 V and Imax.out = 85 mA such as (but noy limited to): type: Camille Bauer Sineax 84-2B1-511
Sineax 89-2B1-511
(P.T.B. Cert. Ex-81/2044X)
NON HAZARDOUS AREA
or
or
ZONE 1
or
ZONE 2
SYSTEM CERTIFICATE EXA200 INSTRUMENTS BASEEFA NO Ex 892380
8-1. Cenelec
Ex-classification: EEx ib [ia] IIC T4 Zone 0 or 1 Zone 1
Page 41
SC 200 S V
out
= 14.4 V max.
I
out
= 129 mA max.
C ext = 1 µF max L ext = 2.3 mH max.
31.5 Vmax 4-20 mA
+ –
11 12 14 13 17 15 16
37
8-2. FM
connecting cables such as (but not limited to): WU40-LH18 WU40-LH2 WU40-LH5 10 meter Maximum
HAZARDOUS LOCATION
FMRC-Approved Barrier
To be installed in accordance with ANSI/RP 12.6 and NEC requirements
Maximum safe area voltage should not exceed 250 V
RMS
NON HAZARDOUS LOCATION
Class I, Division I, Groups ABCD Vmax = 31.5 V Imax = 93.3 mA Ci = 5 nF Li = 16.5 uH
ControlDrawing for EXA 200 instruments
1 conductivity sensor with integral SC41-SP34
temperature sensor such as (but SC49-FP08 not limited to) SC41-SP24
SC41-EP14 SC41-EP04
These are all passive sensor to be regarded as "simple apparatus" i.e. devices which do neither store nor generate voltage over 1.2 V, currents over 0.1 A, power over 25 W or energy over 20 mJ
Page 42
38
The EXA SC200 can be used for both con­ductivity and resistivity measurement. As delivered the instrument is set for conducti­vity measurement.
9-1. How to change from conductivity to
resistivity measurement
- Remove the cover after loosening the 4 screws. Now you have access to the Dis­play Board.
- Loosen the 4 screws that hold this board in place and remove it from the enclosure.
- On the upper back side of the Display Board are 5 blue jumpers. Change the spring jumper as shown in the figure. Make sure that center contact spring is securely hold to have good contact.
Within 15 seconds after the jumper change, the EXA SC200 will automatically load de­fault data for resistivity measurement.
The SC200 transmitter can be reassembled now, following the opposite sequence as described above.
9-2.Resistivity measurement
As a resistivity measuring transmitter the EXA SC200 has the same function as described earlier in this manual.
The units mS/cm and µS/cm are replaced by k.cm and M.cm for resistivity meas­urement. If no unit is shown the unit is .cm and can be changed in k.cm by the key
if the “.” is flashing. See range adjustment in
section 4-2.
9. CHANGE FROM CONDUCTIVITY TO
RESISTIVITY MEASUREMENT
from
position for conductivity measurement
to
position for resistivity measurement
9-3.Maintenance of the transmitter
Calibration of the resistivity transmitter is done in the same way as described in sec­tion 5-1. The calibration values can be calculated as follows: k.cm = 1000 µS/cm .cm = 1000 mS/cm
Example:
The 0.001 % NaCI-solution has a conducti­vity value of 21.4 µS/cm. In resistivity mode the value is 1000/21.4 = 46.7 k.cm.
Page 43
39
10. SOFTWARE VERSION 3.0 COM­PARED TO VERSIONS 1* AND 2*.
In 1994 the software of EXA SC200 has un­dergone a major update as result of user feedback. New features are made accessi­ble by additional Service Codes to avoid programming conflicts with users of pre­vious versions.
10-2.Matrix compensation
ACCESS CODE : 13 Display : *MATR
Adjustment: 0 Only linear compensation (see access
code 10) 1 HCI pure water (0 - 100 °C)/CATION 2 Ammonia 3 Morpholine in pure water 4 Hydrochloric Acid (1-5%) 5 Nitric Acid (1-5%) 9
User adjustable matrix (see access code 15
NOTE: Access to this routine is only possible when manually set temperature compensation factor (α) is selected in §4-4.
Explanation:
The SC200 is equiped with a matrix type algorithm for accurate temperature compen­sation in various applications. Select the range as close as possible to the actual temperature/concentration range. The SC200 will compensate by interpolation and extrapolation. Consequently, there is no need for a 100 % coverage. If 9 is selected the temperature compensa­tion range for the user adjustable matrix can be set in access code 15. In access codes 16 and 19 the specific conductivity values at 5 different temperatures is entered.
The new features are:
10-1. Cell constant
ACCESS-CODE : 05 DISPLAY : 1.00xC Adjustments:
1. Select multiplying factor
2. Adjust the required cell constant
1. Select multiplying factor with keys YES and NO.
2. With keys > and ^ any cell con­stant between 0.01 and 50.0 cm
-1
can be selected.
Explanation:
1. Multiplying factor
- The multiplying factor is confirmed after
pressing the YES key.
- Change multiplying factor to 1.0-10­10-0.01-0.1-1.0 by pressing NO key and confirm selection with YES key.
2. The value of the cell constant is indicated
in the specifications of the cell and/or on its identification plate.
Adjust the required value of the cell after pressing the YES key to confirm the multi­plying factor. Select the digit to adjust with key > (digit flashes). With ^ key the value of the selected digit can be changed.
Example: Cell constant = 0.00985
a. Select multiplying factor 0.01 b. Adjust the value to .985
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40
10-3. Matrix temperature compensation
range
ACCESS CODE : 14 Display : *T1 °C
Adjustment: : After selecting 9 in Ac-
cess Code 13 the begin­and endscale value of temperature compensa­tion range of the users matrix can be adjusted using the keys . and ^.
Explanation:
In service codes 14 to 18 the SC200 trans­mitter can be fingerprinted to one particular application. In access code 13 you have the possibility to adjust the compensation range. After having access to this routine adjust the beginscale value of the compensation range. After entering the beginscale value the display indicates T5 °C and the endscale value can be adjusted. The temperatures T2, T3 and T4 are found proportionally. Notes:
1. In defining the temperature compensation range, it is important to select T1 and T5 in such a way that the 5 reference temperatu­res are user friendly. Example: T1 = 0 and T5 = 80 °C gives ref-
erence temperatures of 0, 20, 40, 60 and 80 °C.
2. The minimum span for the range is 50 °C(Error code 17 indicates a temperature range of less than 50 °C).
10-4. Matrix data
ACCESS CODE : 15,16,17,18,19 Display : *L1*T1
Adjustment : After adjusting the range
in access code 14 it is necessary to fill the ma­trix.
Explanation:
In these access codes the specific conducti­vity values can be entered for 5 different concentrations of the process liquid; each one in one specific access code (15 to 19). Adjust the conductivity value of the first solu­tion at temperature T1 using keys > and ^. Confirm the adjustment by pressing the ENT key. The display indication changes to “L1 xT2”. Now the conductivity value at tempe­rature T2 can be adjusted. Continue this process until “SERV” is displayed and adjustment is finished. Repeat the procedures for solutions 2 to 4 in access codes 16 to 19.
NOTES:
1. Use the table on page 42 to record your pro-grammed values. It will make pro­gramming easy for duplicate systems or in case of data loss.
2. Each matrix column has to increase in con­ductivity value: L1 .Tx<L2.Tx<L3.Tx<L4.Tx<L5.Tx
3. Error code E4 occurs when two standard solutions have identical conductivity values at the same temperature within the temperature range.
Page 45
41
10-5. Selection between ”soft” or ”hard”
FAIL Situations
ACCESS CODE : 20 Display : *ERR.01
Adjustment: NO Error 01 is skipped; next error is
shown
YES 0 = Soft alarm
1 = Hard alarm Pressing ENTER confirms the selec­tion
Explanation:
As described in chapter 6, the error codes marked with an asterisk(*) normally will trig­ger a number of actions. If soft alarm action is selected, the FAIL message flag is flashing. The output func­tions will not go into BURN OUT position and the contact outputs continue to opera­te. If hard alarm function is selected, the output goes into BURN OUT signal if programmed that way in Access Code 09: and the FAIL flag is shown in the display.
10-6. Selection between yes or no E6
Fail-message.
Page 46
42
Matrix example actual example actual example actual example actual example action
CODE 14 TEMPERATURE T1 ... T5 O 25 50 75 100
CODE 15 SOLUTION 1 L1 31 53 76 98 119
CODE 16 SOLUTION 2 L2 86 145 207 264 318
CODE 17 SOLUTION 3 L3 146 256 368 473 575
CODE 18 SOLUTION 4 L4 195 359 528 692 847
CODE 19 SOLUTION 5 L5 215 412 647 897 1134
Temp. 0 ppb 4 ppb 10 ppb 20 ppb 100 ppb
Cation 1 0 0,00975 0,152 0,31 0,62 1,23 Conductivity 25 0,0559 0,25 0,50 1 2 µS/cm 50 0,1752 0,385 0,70 1,35 2,70
75 0,4092 0,62 0,96 1,7 3,3 100 0,7681 0,98 1,3 2,1 3,9
Ammonia 2 0 0,00975 0,122 0,23 0,43 0,82 Conductivity 25 0,0559 0,25 0,50 1,0 2,0 µS/cm 50 0,1752 0,41 0,80 1,62 3,35
75 0,4092 0,65 1,13 2,3 4,8 100 0,7681 1 1,52 2,9 5,9
Morpholine 3 0 0,00975 0,149 0,30 0,59 1,15 Conductivity 25 0,0559 0,25 0,50 1 2 µS/cm 50 0,1752 0,375 0,70 1,38 2,8
75 0,4092 0,60 0,97 1,8 3,55 100 0,7681 0,98 1,38 2,35 4,5
1% 2% 3% 4% 5%
Hydrochloric 4 0 65 125 179 229 273 Acid 15 91 173 248 317 379 mS/cm 30 114 217 313 401 477 1-5% 45 135 260 370 474 565
60 159 301 430 549 666
Nitric Acid 5 0 39,5 76,1 113,4 147,2 179,5 mS/cm 20 57,4 108,5 161,4 210 258 1-5% 40 81,4 148,1 215 275 330
60 99,9 180,8 260 331 397 80 127,8 217 299 374 448
10-7 Matrix examples
Page 47
Page 48
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