Manual VersionSoftware Version Version dateChanges
1.0n/aJuly 2004First edition
2.0n/aApril 2007New template
LanguageOrder Number
English03077063001
e
For more information, see:
Software on page G-5
Service Manual on page G-6
91xx pH/Electrolyte Analyzers
Service Manual
This Service Manual is for the maintenance and repair of 91xx pH/Electrolyte
Analyzers (9110 pH Analyzers and 9120, 9130, 9140, 9180 and 9181 Electrolyte
Analyzers).
91xx pH/Electrolyte AnalyzersEvery effort has been made to ensure that all the information contained in this
manual is correct at the time of printing. However, Roche Diagnostics GmbH reserves
the right to make any changes necessary without notice as part of ongoing product
development.
Any customer modification to the instrument will render the warranty or service
agreement null and void.
Software updates are done by Roche Service representatives.
9180 Electrolyte Analyzers SN > 12001 are IVD compliant.
Intended use
This manual contains all of the information required for maintenance and repair of
91xx pH/Electrolyte Analyzers (9110 pH Analyzers and 9120, 9130, 9140, 9180 and
9181 Electrolyte Analyzers).
The user must be familiar with the function and operation of the instrument to fully
understand the processes described here.
e
For more information about 91xx pH/Electrolyte Analyzers, refer to corresponding
Instructions for Use.
Observe the service and repair procedures described in this manual and use only
genuine Roche replacement parts and Roche-approved materials to guarantee the full
functionality of the 91xx pH/Electrolyte Analyzers.
e
For the order numbers of replacement parts, refer to:
91xx pH/Electrolyte Analyzers Spare Part List
Roche DiagnosticsApril 2007
Service Manual · Version 2.03
Page 4
Copyrights
Trademarks
91xx pH/Electrolyte Analyzers
e
For an overview of possible revisions and available software versions, see:
The contents of this document may not be reproduced in any form or communicated
to any third party without the prior written consent of Roche Diagnostics. Every
effort is made to ensure its correctness. Subject to change without notice.
COBAS, LIFE NEEDS ANSWERS, ROCHE MICROSAMPLER, SNAPPAK, ISETROL
are trademarks of Roche.
Contact addresses
Manufacturer
All other trademarks are the property of their respective owners.
Roche Diagnostics GmbH
D-68298 Mannheim / Germany
www.roche.com
Roche DiagnosticsApril 2007
4Service Manual · Version 2.0
Page 5
91xx pH/Electrolyte Analyzers
Contents
Ver s io n Hi s to r y 3
Edition notice 3
Intended use 3
Copyrights 4
Trademarks 4
Contact addresses 4
Contents 5
Preface 9
How to use this manual 9
Where to Find Information 9
Conventions used in this manual 10
System DescriptionPart A
1 Safety information
Important information A-5
Operating safety information A-6
Important notes and warnings A-6
Disinfectants A-7
Deproteinizer A-7
Other disinfectants A-7
ESD protection measures A-8
Explanation of the phenomenon A-8
Influence of electrostatic charges on components A-8
Why is ESD protection so important today? A-9
How can ESD protection be guaranteed? A-9
Conclusion A-9
Roche DiagnosticsApril 2007
Service manual · Version 2.05
Print functions menu B-9
QC sample menu B-10
Daily maintenance menu B-11
Operator functions menu B-12
Program instrument menu B-13
Page 6
91xx pH/Electrolyte Analyzers
Service functions menu B-14
Calibration sequence B-15
7 Software operation 9120, 9130, 9140
Software operation 9120, 9130, 9140 B-19
Overview B-19
Overall program operating flow B-20
Main menu B-21
Measurement sequence B-22
Print functions menu B-23
QC/standard/urine sample menu B-24
Daily maintenance menu B-25
Operator functions menu B-26
Program instrument menu B-27
Service functions menu B-28
Calibration sequence B-29
8 Software operation 9180
Software operation 9180 B-33
Overview B-33
Overall program operation flow B-34
Main menu B-35
Measurement sequence B-36
Print functions menu B-37
QC/standard/dialysate/urine sample menu B-38
Daily maintenance menu B-39
Operator functions menu B-40
Program instrument menu B-41
Service functions menu B-42
Calibration sequence (1) (Example Na/K/Li
calibration) B-43
Calibration sequence (2) (Example Na/K/Li
calibration) B-44
Power-up B-45
9 Software operation 9181
Software operation 9181 B-49
Overview B-49
Overall program operting flow B-50
Main menu B-51
Manual measurement sequence B-52
Automated measurement sequence B-53
Print functions menu B-54
QC/std/dialysate/urine sample menu B-55
Daily maintenance menu B-56
Operator functions menu B-57
Program instrument menu B-58
Service functions menu B-59
Calibration sequence (1) (example Na/K/Li
calibration) B-60
Calibration sequence (2) (example Na/K/Li
calibration) B-61
Power-up sequence B-62
10 Service functions
Service functions B-65
TEST ELECTRODES B-65
TEST SAMPLE SENSOR B-65
TEST SnapPak SENSOR (9180 and 9181 only) B-65
TEST LANGUAGE SWITCH (9180 and 9181 only)
B-65
TEST SAMPLE DOOR (except 9181) B-66
TEST PROBE (9181 only) B-66
TEST AUTOSAMPLER (9181 only) B-66
TEST PUMP B-66
TEST PINCH VALVES B-67
TEST INTERFACE B-67
TEST AMPLIFIER B-67
ENTER SERVICE CODE B-67
Miscellaneous functions B-69
Error messages and troubleshooting D-5
Status-LEDs D-5
STATUS: NOT CALIBRATED D-5
STANDARD A NOT DETECTED D-5
STANDARD B NOT DETECTED, STANDARD C
NOT DETECTED (9180/9181 only) D-6
CHECK SAMPLE CONTACTS(9110), CHECK
SAMPLE SENSOR (9120/30/40/80/81) D-6
CHECK REFERENCE HOUSING D-7
PLEASE CLOSE SAMPLE DOOR (except 9181) D-7
NO SAMPLE D-8
CLEANING FLUID NOT DETECTED D-8
CONDITIONING FLUID NOT DETECTED (except
9110) D-8
INTERFACE ERROR D-9
Roche DiagnosticsApril 2007
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91xx pH/Electrolyte Analyzers
PAPER JAM OR PRINTER DEFECT D-9
CHECK ELECTRODES D-9
## NOT CAL’D D-9
CLOG IN SAMPLE PATH (9110 only), CLOG
CHECK FLUID PATH (except 9110) D-11
↑↑↑↑ ↓↓↓↓ (Out of range) D-11
↑ ↓ (Temparature out of range) D-11
Software G-5
Service Manual G-6
Version 1.0 G-6
Version 2.0 G-6
Roche DiagnosticsApril 2007
Service manual · Version 2.07
Page 8
91xx pH/Electrolyte Analyzers
Roche DiagnosticsApril 2007
8Service manual · Version 2.0
Page 9
91xx pH/Electrolyte Analyzers
Preface
This manual contains all of the information required for the maintenance and repair
of the 91xx pH/Electrolyte Analyzers.
The user must be familiar with the function and operation of the instrument to fully
understand the processes described here.
e
For more information about instructions, refer to:
9180 Electrolyte Analyzers Instructions for Use
Observe the service and repair procedures described in this manual and use only
genuine Roche replacement parts and Roche-approved materials to guarantee the full
functionality of the 91xx pH/Electrolyte Analyzers.
e
For the order numbers of replacement parts, refer to:
91xx pH/Electrolyte Analyzers Spare Part List
e
For an overview of possible revisions and available software versions, see:
Software on page G-5
Service Manual on page G-6
How to use this manual
o
Keep this Service manual in a safe place to ensure that it is not damaged and remains available
for use.
o
This Service manual should be easily accessible at all times.
To help finding information quickly, there is a table of contents at the beginning of
the book and each chapter. In addition, a complete index can be found at the end.
Where to Find Information
In addition to the Service manual, the following documents are also provided to assist
in finding desired information quickly:
o91xx pH/Electrolyte Analyzers Instructions for Use
o9180 Electrolyte Analyzer Short Instruction
o91xx pH/Electrolyte Analyzers Service manual (PDF or iSDoc version in
GRIPS)
o91xx pH/Electrolyte Analyzers Spare Part List (PDF or iSDoc version in
GRIPS)
Roche DiagnosticsApril 2007
Service manual · Version 2.09
Page 10
Conventions used in this manual
Visual cues are used to help locate and interpret information in this manual quickly.
This section explains formatting conventions used in this manual.
SymbolsThe following symbols are used:
SymbolUsed for
aStart of procedure
oList item
e
hCall-up (software reference)
Cross-reference
Note
All sections or text locations marked with "NOTE" describe safe
procedures that are intended to provide the user with additional help.
Caution
All sections or text passages that are marked with this symbol describe
procedures or indicate conditions or dangers that could damage or
lead to malfunctions in the instrument, and which therefore should
never be attempted.
Warning
Sections marked with this symbol contain information that must be
observed for the prevention of personal injury (to patients, users or
third parties).
Risk of infection!
(according to the standard DIN EN 61010-2-101:2002) (Instrument)
91xx pH/Electrolyte Analyzers
Risk of infection!
(according to the standard DIN ISO 15223-1:2005) (Consumables)
High Voltage
Passages that are marked with this symbol warn of an immediate
danger in connection with electrical wiring or components.
ESD protection measures
All sections or passages that are marked with this symbol warn of
specific dangers in connection with static discharge. Packages that are
marked with this symbol must only be opened by trained technical
staff.
For more information about ESD protection measures, see ESD protection measures
on page A-8.
Roche DiagnosticsApril 2007
10Service manual · Version 2.0
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91xx pH/Electrolyte Analyzers
IVD symbolsInstruments: applicable for 9180 Electrolyte Analyzers SN > 12001.
The IVD symbols are used in accordance with DIN EN 980:2003, ISO 15223:2000 (as
per the In Vitro Diagnostics Directive 98/79/EC), and DIN EN ISO 780:1997.
SymbolDescription
This product complies with the requirements in the directive
98/79/EC on in vitro diagnostic medical devices.
Lot designation
Consumables: use by... (expiry date)
The consumables must be completely consumed by the indicated
date.
If a day is not indicated, apply the last day of the respective month.
Store at ...
The conditions necessary to preserve the product's shelf life before
opening.
For in vitro diagnostic use
"Grüner Punkt" (in Germany)
Manufacturer — according to directive 98/79/EC on in vitro
diagnostic medical devices
Store upright
Risk of infection!
(according to the standard DIN ISO 15223-1:2005) (Consumables)
Catalogue number
Caution (refer to accompanying documents). Please refer to safetyrelated notes in the manual, accompanying this instrument.
Please consult instructions for use
Serial number (model plate)
Roche DiagnosticsApril 2007
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91xx pH/Electrolyte Analyzers
Other symbolsThe following symbols are listed as additional information:
SymbolDescription
Electrodes:
This date indicates the limit of the maximum storage time of an
electrode. The electrode must be installed in the instrument no later
than the imprinted date.
If the installation takes place on the imprinted date, it still falls within
the specifications. The calculation of the “Install before” date is based
on the production date of the elctrode.
Danger symbol: T: Toxic (on the packaging of the reference electrode)
Rating: Inhalation, swallowing or skin contact with even small
quantities can lead to serious health risks, including fatal risks.
T: R23/33/50-53
N: S45/60/61/7
Characteristics of this type of item are severe, possible irreversible
damage to health through repeated or prolonged contact, particular
with carcinogenic, genetic or reproductive (danger to reproductive
capabilities) effects.
Caution: Avoid any contact with the human body. If you feel unwell,
contact a doctor immediately. Any substances with carcinogenic,
genetic or reproductive dangers are indicated appropriately. Always
observe the regulations when handling such substances.
Danger symbol: N: Dangerous to the environment (on the packaging
of the reference electrode)
Rating: If released into aquatic and non aquatic environments, can
cause immediate or delayed damage to ecosystems through a change
in environmental conditions.
These substances or their by-products can cause simultaneous
damage to sensitive environmental areas.
Caution: Depending on the potential for damage, do not allow the
substance to enter sewers, soils or the environment. Observe the
specific disposal regulations.
Danger symbol: Xi: Irritant
Rating: Although not corrosive, momentary, longer-lasting, or
repeated contact with skin or mucous membrane may result in
inflammation. Danger of sensitization during contact with skin
XI: R36/37/38, S 26-37
(when classified with R 43).
Caution: Avoid contact with eyes and skin, do not inhale vapors.
Do not use content if the packaging is damaged
Protective gloves, protective goggles and suitable protective clothing
must be worn
Roche DiagnosticsApril 2007
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91xx pH/Electrolyte Analyzers
AbbreviationsThe following abbreviations are used:
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1 Safety information91xx pH/Electrolyte Analyzers
Tab l e o f c onte nt s
Roche DiagnosticsApril 2007
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91xx pH/Electrolyte Analyzers1 Safety information
Important information
Important information
This Service Manual contains vital warning and safety information.
This instruments are intended to be used only for the specialized purpose described
in the instructions. The most important prerequisites for use, operation, and safety
are explained to ensure smooth operation. No warranty or liability claims will be
covered if the instrument is used in ways other than those described or if the
necessary prerequisites and safety measures are not observed.
The instrument may be operated only by persons whose qualifications enable them to
comply with the safety measures that are necessary during operation of the
instrument.
Suitable protective equipment, like laboratory clothing, protective gloves, protective
goggles and if necessary mouth protectors, must be worn to prevent direct contact
with biological working materials. In addition, a face mask is required if there is a
risk.
Adjustments and maintenance performed with removed covers and connected power
may be attempted only by a qualified technician who is aware of the associated
dangers.
Instrument repairs are to be performed only by the manufacturer or qualified service
personnel.
Only accessories and supplies either delivered by or approved by Roche are to be used
with the instrument. These items are manufactured especially for use with this
instrument and meet the highest quality requirements.
Operation of the instrument with solutions whose composition is not consistent with
that of the original solutions can negatively affect, above all, the long term
measurement accuracy. Deviations in the composition of the solutions can also
decrease the service life of the electrodes.
The quality control requirements must be completed at least once daily for safety
reasons. Because accurate measurement results depend not only on the proper
functioning of the instrument, but also on a number of other factors (such as
preanalytics), the results produced by the instrument should be examined by a
trained expert before subsequent decisions are reached that are based on the
measurement values.
Explanation:
"Caution, refer to accompanying documents“
Roche DiagnosticsApril 2007
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1 Safety information91xx pH/Electrolyte Analyzers
Operating safety information
Operating safety information
The instrument has been constructed and tested according to the following European
Standards:
oIEC/EN 61010-1:2001
oIEC/EN 61010-2-101:2002 (valid for 9180 Electrolyte Analyzers SN > 12001 only)
oIEC/EN 61010-2-081:2002 + A1:2003
It was delivered from the factory in flawless condition with regards to safety features.
In order to preserve this condition and ensure safe operation, the user must respect
the notices and warnings that are contained in this Service Manual
oThis instrument is classified under the protection class I according to
IEC/EN 61010-1.
oThe instrument meets the conditions for overvoltage category II.
oThe instrument meets the conditions for contamination level 2.
oDo not operate the instrument in an explosive environment or in the vicinity of
explosive anesthetic mixtures containing oxygen or nitrous oxide.
oIf an object or liquid enters the internal areas of the instrument, remove the
instrument from its power supply and allow an expert to check it thoroughly
before using it again.
oThe instrument is suitable for long-term operation indoors.
o
The power cord may be plugged into a grounded socket only. When using an extension cord,
make sure it is properly grounded.
o
Any rupture of the ground lead inside or outside the instrument or a loose ground connection
may result in hazardous operating conditions. Intentional disconnection of the grounding is not
permitted.
o
The instrument is not suitable for operation with a direct current power supply. Use only the
original mains plug delivered with the instrument.
Important notes and warnings
o
Never operate the analyzer in the vicinity of volatile or explosive gases
(e.g. anesthetic gases, etc.)!
o
The instrument must be connected to a 2-pin, grounded socket.
o
The power cable and the plug must be undamaged. Damaged power cables and plugs must be
replaced immediately.
o
Before opening the back panel switch off the instrument and disconnect the power cable.
o
Replace damaged fuses with the specified type of fuse.
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91xx pH/Electrolyte Analyzers1 Safety information
Disinfectants
o
Service and repair work must be done only as specified in this manual. Unqualified service or
repair work may result in warranty claims not being granted.
o
Use only suitable tools and test instruments for service and repair work.
o
Do not allow fluids to enter the interior of the instrument, because this may damage the
electronics.
o
Use only slightly moistened cloths or cotton sticks to clean the instrument.
Disinfectants
Use only liquid disinfectant such as protein remover (Roche deproteinizer) or an alcohol-based
(about 70%) surface disinfectant.
Do not spray disinfectant directly onto the instrument because this could cause malfunctions in the
electronics.
Do not use any type of bleaching agent. Exception: Roche Deproteinizer.
Deproteinizer
CompositionAqueous NaOCl solution with active chlorine (≤ 2%)
Hazards identificationDue to the basic and oxidizing character of the reagent ("Deproteinizer") local
First aid measures
Other disinfectants
Do not attempt to clean/decontaminate any part of the instrument before shutting it down and
unplugging it from the power source.
Before plugging in the instrument again and switching it on always wait for 15 minutes to allow the
disinfectant to evaporate.
irritations after contact with eyes, skin or mucous membranes cannot be excluded.
After inhalation:
After skin contact:
After eye contact:
After drinking:
breath fresh air, drink large amounts of water
wash with generous amounts of water, remove contaminated clothing
rinse eyes with generous amounts of water, contact an eye specialist
drink large amounts of water, avoid vomiting, contact a doctor
Use standard alcohol-based (70%) disinfectants to clean the surface of the
instrument. Read the product information first.
Never use standard disinfectant to clean the tubes and tubing paths under any circumstances!
Do not use any type of bleaching agent. Exception: Roche Deproteinizer.
Roche DiagnosticsApril 2007
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1 Safety information91xx pH/Electrolyte Analyzers
ESD protection measures
ESD protection measures
ESD = Electrostatic Sensitive Device
Explanation of the phenomenon
The most frequent cause of electrostatic discharge is friction of various materials such
as plastic, synthetic fiber, hard rubber or paper.
It can also be caused by bending or applying pressure to a material.
Discharges that are dangerous to components occur when "charged" bodies or
components do not have a discharge connection (ground) to discharge the
electrostatic charge.
The discharges normally do not have a high capacity, but there are often voltage
differences in the range of several thousand volts. The discharges are perceived as
small shocks or visible sparks.
Examples:oShoes with rubber soles:
Friction is caused by walking. A person develops an electrical charge different
from the ground. A discharge occurs when an object (e.g. door handle) is
contacted.
oSynthetic fiber clothing:
Discharge is audible and is visible in darkness.
The dryer the air the greater the risk of electrical discharge caused by friction.
Eectrostatic charges are less likely to build up in humid air, particularly when saturated with water
vapor.
The probability of ESD phenomena is therefore particularly great in a northern hemisphere winter
in centrally heated rooms where the humidity is low.
Influence of electrostatic charges on components
If a person with an electrostatic charge touches a component, a discharge over a
connection of an IC or semiconductor element may occur. The resulting voltages may
damage the component.
Critical situations can occur while repairing or testing components if they are lying
on a more or less conductive surface (e.g. table top) and a person with an electrostatic
charge touches them. A discharge through a critical component connection can also
occur in this case.
Roche DiagnosticsApril 2007
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91xx pH/Electrolyte Analyzers1 Safety information
ESD protection measures
Why is ESD protection so important today?
Formerly, current controlling semiconductors were mostly used (TTL, normal
transistors, etc.).
Today the principle of current logic is virtually the only technology in use in MOS
and CMOS components.
Currents generated by an electrostatic discharge (as much as several kV!) destroy the
sensitive component inputs or cause hidden damage. This damage is generally not
immediately detectable.
Another effect is that the clearances inside the ICs continuously become smaller. The
internal wires become thinner and thinner, the allowable maximum input voltages
become smaller and the effects of any discharges become more and more critical.
How can ESD protection be guaranteed?
A continuous discharge is required when working on an electronic assembly. Do this
as follows:
oUse ESD wrist bands (special wrist bands connected to a protective ground).
oRepairs and tests on assemblies must only be conducted on tables with ESD mats
connected to grounds or ESD wrist bands.
oAlways pick up components at the edge (e.g. like a photo).
oComponents must always be transported in ESD packages or appropriate storage
or shipping containers (use original packaging!).
oShoes with rubber soles or clothing of synthetic fibers must not be worn in
workshops where electronic components are repaired.
oUse a humidifier if necessary to maintain optimum humidity in the work area.
oDo not touch assemblies or components with the hand after testing.
oAlways transport and ship assemblies or components for repair in ESD protective
packaging only. This will prevent further damage that may result in
misinterpretation of the original cause of the fault.
The ESD mat consists of materials that have a very low, defined conductivity (1012 ohms).
The following materials prevent charges caused by friction from building up and protect the
component from damage.
o
ESD mats
o
ESD packages
o
Shipping containers
Conclusion
Of course, not all circuit boards and electronic assemblies require such careful
handling. An electrical board that only carries simple plug connectors does not
require ESD packaging.
In cases of doubt always use ESD packaging.
Roche DiagnosticsApril 2007
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1 Safety information91xx pH/Electrolyte Analyzers
ESD protection measures
Roche DiagnosticsApril 2007
A-10Service manual · Version 2.0
The 9110, 9120, 9130, 9140, 9180 and 9181 analyzers are equipped with a standard
serial interface output. This interface output is intended to be used with standard
commercially available computer systems.
The data transmitted through the serial interface port employs the ASCII code.
The serial interface is terminated on the rear cover with a 9-pin male DB-9 connector.
The signal levels are as follows:
oBinary 1 = -12 V to -3 V
oBinary 0 = +3 V to +12 V
Two stop bits follow the eight data bits to complete the 10 bit word.
A higher discharge current can be expected when using the serial interface. This must be checked by
suitably qualified personnel, depending on the local regulations.
The patient sample data is sent at the end of each measurement, the calibration report
is sent at the end of each calibration.
The interface is always on, independent of the printer settings; the data is always sent.
Note
The arrow up (e.g. out of normal range) is sent as HEX 18 (↑), the arrow down as HEX19 (↓) and
the ° (degree) is sent as HEX1A (→).
Roche DiagnosticsApril 2007
Service manual · Version 2.0A-19
The data link with the COMPACT 2/3 blood gas analyzer allows to combine ISE
results with pH/blood gas results on one printout. If Ca
9181, a pH-corrected Ca
sample report.
For connection of the 9180/9181 analyzer to the COMPACT 2/3 analyzer, the optional
Interface Kit is required. To install the kit, first turn both instruments off. Connect the
interface filter provided in the kit to the RS232 port on the 9180/9181. Then connect
one end of the cable to the interface filter, the other end to the COM 2 port on the
COMPACT 2/3. On the COMPACT 2/3, select 9180 under the COM 2 interface
options.
e
See COMPACT 2/3 Operator's Manual for details.
2+
2+
value will be calculated and printed on the combined
is activated on the 9180/
Roche DiagnosticsApril 2007
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91xx pH/Electrolyte Analyzers4 Description of modules
Tab l e o f c onte nt s
Description of modules
Insert introducing text here.
In this chapter
Description of modules ............................................................................................ A-23
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4 Description of modules91xx pH/Electrolyte Analyzers
Tab l e o f c onte nt s
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91xx pH/Electrolyte Analyzers4 Description of modules
Description of modules
Description of modules
After changing any part of the analyzer always perform a calibration of the analyzer as well as a full
QC measurement. QC measurements must be performed in their entirety (i.e., all three QC levels
must be measured). Omitting QC measurements or ignoring QC measurement results may lead to
incorrect patient measurements, which may result in incorrect clinical decisions, possibly
endangering the patient's health.
Mechanical assemblies
Front door assembly
For the 9110, 20, 30, 40 and 80 analyzers, the front door can be removed by moving
the analyzer to the edge of a work surface so the analyzer door, when opened, will
extend past the edge of the work surface. With one hand, hold the analyzer door near
the right side hinge pin and, with the other hand, gently apply pressure to the middle
rear area of the door. This will allow the right hinge pin to clear the retaining hole in
the main chassis. The door can then be removed from the analyzer.
Needle unit assembly
The 9181 front panel can be removed by tilting it slightly away from the analyzer and
lifting it straight up. The plastic window can also be replaced in the field by gently
pressing from the rear of the window and snapping the plastic window out toward the
front of the analyzer door. The door magnets cannot be replaced in the field as they
are glued in place with conductive adhesive.
Due to the update of the 9180 Electrolyte Analyzer according to IVDD compliance a new shielded
front door "FRONT DOOR 9180" is available and compatible with any 9180 Electrolyte Analyzer
(old type SN < 11999 and new type SN > 12001) and with 9120, 30, 40 Electrolyte Analyzers.
Further information: see the 91xx Spare Parts List.
e
See the 91xx Spare Parts List for a detailed reference of the parts of this assembly.
To remove the 9110 fill port for replacement or cleaning, grasp the white tab on the
fill port and rotate the bayonet-style connector counter-clockwise. Gently pull the fill
port forward to remove. Replacement can be accomplished in the reverse order.
During removal, be careful not to bend the needle.
The 9110 fill port assembly is desinged for easy removal without the use of tools, for
cleaning, changing tubing or replacement. First, disconnect the sample intake tube on
the left side of the fill port assembly from the sample preheater. Grasp the fill port
assembly and pull it forward carefully. Disconnect the wire from the needle arm. To
reassemble, reconnect the wire, press the fill port assembly into place and reconnect
the tubing.
The 9110 wash port located on the underside of the flap can be removed by appying
pressure to one side to overcome the snap fit. To reinsert, align wash port and apply
pressure to snap into place.
The 9120, 30, 40, 80 and 81 sample needle and fill port are both designed for easy
replacement by the user. To remove the fill port assembly for replacement, pull the fill
Roche DiagnosticsApril 2007
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4 Description of modules91xx pH/Electrolyte Analyzers
Description of modules
port holder towards the front for easy access. Then, press the two plastic tabs on the
fill port to allow removal of the fill port from the fill port holder. The sample needle
can also be removed and is supplied as a one-piece assembly including the intake
tubing.
To remove the 9120, 30, 40, 80 and 81 sample needle, grasp the needle near the white
holder block and pull up to unsnap the sample needle from its position. To replace
the assembly, align a replacement sample needle and press the replacement assembly
into place.
Two (9110) or three screws (9120, 30, 40, 80, 81) located on the left side of the
assembly hold the needle unit assembly in place. To access the two rear screws, turn
power off and remove the rear panel. The rear panel can be moved away from the unit
for easier access by unplugging the wire harness from the power supply. The SBC
board can now be removed by removing the screws which secure the SBC board and
disconnecting the cables on the SBC board.
Disconnect the connector to the lamp board which supplies the Door Open signal.
The two rear screws which secure the needle unit can now be removed using a Philips
screwdriver (9110) or an Allen wrench (9120, 30, 40, 80, 81). Then, remove the front
securing screw (n./a. on the 9110), the sample intake tubing and the reagent supply
tubing (red tag) from the fill port. The needle unit can now be removed from the
front of the analyzer for replacement.
Electrode holder assembly
Peristaltic pump assembly
e
See the 91xx Spare Parts List for a detailed reference of the parts of the needle unit.
To remove the electrode holder assembly from the analyzer, first unplug the sample
intake tubing on the right side of the module, then the preheater cable (9110 only) or
the sample sensor cable (9120, 30, 40, 80 and 81), then remove the reference solution
tubing connector and last, take out the waste tube (green tag) at the left side of the
electrode holder. The electrode holder can now be removed by pressing the two
plastic tabs (right and left side of the module) and sliding the module forward. Press
the plastic tabs again to release the second detent and completely remove the module
from the analyzer. The sample preheater or the sample sensor and/or the left side
electrode holder can be removed and replaced by removing the screws on the under
side of this module.
e
See the 91xx Spare Parts List for a detailed reference of the parts of this assembly.
Replacement of the roller assembly of the peristaltic pump can be accomplished by
removing the pump tubing and firmly pulling the roller assembly toward the front. To
replace the roller assembly, align the roller and the flat on the motor shaft and press
the replacement roller into position.
To remove the motor, first remove the rear panel assembly and SBC Board.
e
For details, see Rear panel assembly on page A-25, SBC board on page A-26.
Now, the electrical connector on the lamp board can be accessed to unplug the motor
connector. The motor can now be removed by removing four screws located on the
front of the housing near the peristaltic pump.
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Description of modules
Solenoid assembly
Removal of each solenoid is identical. Each solenoid valve has a removable pressure
piece which is held in place by a solenoid cap. To remove the pressure piece, locate the
arrow on the solenoid cap and remove the solenoid cap by sliding it off the solenoid
shaft in the direction of the arrow. This exposes the pressure piece which can now be
removed from the solenoid shaft. To replace pressure piece and cap, energize the
solenoid as described in TEST PINCH VALVES on page B-67. This extends the
solenoid shaft to the outermost position for ease in replacing pressure piece and cap.
Removal of the pressure piece and cap is required prior to removing the solenoid and
allows for easier replacement of the tubing under each solenoid.
To remove the solenoid assembly, the rear panel and the SBC Board (described in
Rear panel assembly on page A-25 and SBC board on page A-26) must be removed
first.
e
For details, see Rear panel assembly on page A-25, SBC board on page A-26.
Each solenoid has an electrical connection to the lamp board which must be
unplugged prior to removal of the solenoid. At this point, remove the two screws on
the front panel to remove the solenoid assembly.
Printer assembly
Note
The 9110 R-solenoid incorporates two heat sinks and is not interchangeable with the other
solenoids.
The printer assembly is designed to allow for easy removal by the user which can be
accomplished without removal of the electrical power to the analyzer. Slide the paper
tray forward to allow access to the printer, tear the paper roll and completely remove
it together with the paper tray. Slide fingers under the printer assembly and pull the
printer forward. This will disengage the printer from the interconnector and enable
removal of the assembly from the front of the analyzer. Removal of the printer should
be performed for replacement and for removal of a paper jam.
To replace the printer, locate the printer slide and insert the printer assembly. Press
firmly into place to ensure electrical connection of the printer.
Note
Never attempt to dislodge paper from the printer with a paper clip or similar object to avoid
damage to the print head or printer platen.
Due to the update of the 9180 Electrolyte Analyzer according to IVDD compliance a new printer
assembly "PRINTER MODULE, ISE" is available and compatible with 9110 pH Analyzers and
with any 9120, 30, 40, 80 and 81 Electrolyte Analyzer.
e
Further information: see the 91xx Spare Parts List.
Rear panel assembly
To remove the rear panel assembly, ensure that the power cord has been disconnected
from the analyzer. Remove the four corner screws to expose the rear panel. The power
supply module located on the rear panel assembly can now be removed by removing
the three screws securing the circuit board and by disconnecting the wiring
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4 Description of modules91xx pH/Electrolyte Analyzers
Description of modules
interconnections. The main power receptacle can also be replaced by removing the
two screws holding this assembly.
Due to the update of the 9180 Electrolyte Analyzer according to IVDD compliance a new power
supply module "POWER SUPPLY 9180 >SN 12001" is available and compatible with 9180
Electrolyte Analyzers serial number > 12001 only.
The former power supply "MODULE POWER SUPPLY, ISE" is still available and has to be used
for 9180 Electrolyte Analyzers SN < 11999, for 9110 pH Analyzers and for 9120, 30, 40 and 81
Electrolyte Analyzers.
e
Further information: see the 91xx Spare Parts List.
After changing the main board or the power supply always perform a measurement of protective
ground resistance to ensure a safe connection of the system ground. Always measure with the power
cord attached to the analyzer. The resistance measurement has to be done between the ground pin
of the power plug and several ground connectors placed on each of the analyzer's electronic
components such as power supply or main board and shielding. The total resistance should not
exceed 0.5 ohms. Be sure to consider the resistance of the ohmmeter's connecting cables.
SBC board
After the rear panel has been removed, the SBC Board is accessible for removal. This
circuit board can be removed by removing the seven screws securing the board to the
housing and by disconnecting electrical connectors from the power supply module,
display board and lamp board.
e
For details, see Rear panel assembly on page A-25.
The electrode push pins can now be replaced by simply pulling the connecting pin
from its socket. When installing the board, make sure to place the plastic washers
under the screw heads.
Due to the update of the 9180 Electrolyte Analyzer according to IVDD compliance a new SBC
board "MAINBOARD 9180 >SN 12001" is available and compatible with 9180 Electrolyte
Analyzers serial number > 12001 only. The former SBC board "MAINBOARD 9180 <SN 11999"
is still available and has to be used for 9180 Electrolyte Analyzers SN < 11999.
Further information: see the 91xx Spare Parts List.
After changing the main board or the power supply always perform a measurement of protective
ground resistance to ensure a safe connection of the system ground. Always measure with the power
cord attached to the analyzer. The resistance measurement has to be done between the ground pin
of the power plug and several ground connectors placed on each of the analyzer's electronic
components such as power supply or main board and shielding. The total resistance should not
exceed 0.5 ohms. Be sure to consider the resistance of the ohmmeter's connecting cables.
Note
Due to the update of the 9180 Electrolyte Analyzer according to IVDD compliance the printouts,
display messages and data links sequences of the 9180 Electrolyte Analyzers serial number > 12001
will show "Roche" instead of "AVL". This also applies to 9180 Electrolyte Analyzers serial number
< 11999 in case of replacing the main board "MAINBOARD 9180 >SN 12001" or the program set
"PROGRAM SET 9180".
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Description of modules
Lamp board
The rear panel and SBC board must be removed to gain access to the lamp board.
Remove one screw and washer which hold the board in place and remove the
electrical connectors to remove this board.
Display board
The rear panel and SBC board must be removed to gain access to the display board.
Remove three screws and 50 degree spacers and unplug the preheater or sample
sensor cable from the front and the ribbon cable to the SBC board to remove the
display board.
Fluidic Module
Standard A
Standard A is drawn to the electrode module by vacuum provided by the peristaltic
pump.
9110 pH Analyzers:When Standard A is to be aspirated into the electrode module, solenoid valve A and R
9120, 30, 40, 80, 81 Electrolyte
Analyzers:
Standard B
are opened. Standard A is then drawn from the ISE SnapPak
TM
until Sample Contact
1 detects Standard A bridging the T-piece and Sample Contact 1. At this point,
solenoid valve V is opened and solenoid valve A is closed. The standard is pumped up
the tubing, through the wash portand into the sample needle until Sample Contact 2
detects the standard. The peristaltic pump slows down and the standard moves into
the electrode module until detected by Sample Contact 3 (bridge between sample
preheater tube and reference electrode). Then, the pump stops.
When Standard A is to be aspirated into the electrode module, solenoid valve A is
opened and solenoid valves B, V and R are closed. Standard A is then drawn from the
ISE SnapPak
TM
, to the fill port, through the sample needle and is sensed by the
sample sensor. At this point, solenoid valve V is opened and solenoid valve A is closed
as the peristaltic pump continues to pump Standard A into the electrode module. As
the trailing edge of the Standard A sample is sensed by the sample sensor, the
peristaltic pump stops.
During the time Standard A is aspirated into the electrode module, the reference
housing is pressurized due to the peristaltic pump providing pressure to the reference
solution line and solenoid valve R being closed. An amount of reference solution is
forced out through the reference junction to provide contact to the sample.
The process for Standard B is identical to that of Standard A with the exception of the
operation of solenoid valve B. This solenoid valve is operated in reverse order of
Standard A aspiration.
Standard C (not on 9110)
The process for Standard C is identical to that of Standard A with the exception of the
operation of solenoid valve C. This solenoid valve is operated in reverse order of
Standard A aspiration.
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4 Description of modules91xx pH/Electrolyte Analyzers
Description of modules
Cleaning solution (9110 only)
The cleaning routine within the 9110 pH Analyzer is automatic with cleaning solution
being aspirated through the system every 40th sample or every 24 hours. Automatic
operator-initiated cleaning can also be performed, by selecting ELECTRODE CLEANING from the main menu. The cleaning routine is very similar to the
aspiration of Standard A or B with solenoid valve C being opened to allow cleaning
solution to be aspirated through the fluidic path. The timing of the cleaning solution
routine allows for a larger volume of cleaning solution to be aspirated than the
Standard A or B cycles to ensure that cleaning solution covers the electrodes, wash
port, fill port, sample needle and preheater during the cleaning cycle.
Reference solution
The reference housing is filled automatically using the second winding of the
peristaltic pump and solenoid valve R. The reference solution connector allows for
the reference housing tubing to be plugged into the reference solution circuit. As the
peristaltic pump aspirates reference solution, solenoid valve R is opened to allow
excess solution to be pumped into the reference return line of the ISE SnapPak
TM
.
A check valve is placed in the return line to ensure that the KCl output is constant
(9110 only).
Waste liquids
Calibration standard and sample waste are pumped out of the left side of the
electrode module (green-banded tubing) through the peristaltic pump to the waste
line of the ISE SnapPak
line of each ISE SnapPak
SnapPak
TM
.
TM
. An internal one-way valve is incorporated into the waste
TM
Main tube set (all models)/ Intake tube set (9110 only)
The main tube set is supplied as a pre-cut tubing harness with the fluidic
interconnections preassembled. Replacement of the tube set should be performed
annually. For removal of the tubing, first remove the ISE SnapPak
compartment. This will allow access for removal of the white TPR block which is the
main interconnection between the ISE SnapPak
removed by grasping the front surface and pulling forward. Next, remove tubing from
each solenoid valve. Follow the procedure outlined in Section 4.1.5 for disassembly of
the solenoid valves to enable fluidic tubing to be easily removed at each solenoid.
e
For details, see Rear panel assembly on page A-25, SBC board on page A-26.
Pull the two pump windings at the peristaltic pump tube set off the pump roller and
remove the white reference solution tube connector. Remove the white TPR reference
solution block by grasping the front of the block and pulling forward. The three tube
connections are labeled with green, blue and red tags. All remaining tubes can now be
removed and the entire tubing harness can be discarded.
to prevent any waste products from leaking out of the ISE
TM
from the reagent
TM
and the tubing. This block can be
Fit the replacement tubing harness and assemble in reverse order as disassembly.
Reference the Tube Diagram on the next page for correct tube locations.
Intake Tube Set (9110 only)The intake tube set comprises three pieces of tubing. A short piece (red tag) fits
between the white T-piece and the standard contact. The long piece can be positioned
between the standard contact and the wash port. The remaining tube can be fitted
between the sample needle and the preheater tube.
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91xx pH/Electrolyte Analyzers4 Description of modules
Description of modules
Sample Contacts (9110 only)
The 9110 fluid detection is based on the principle of measuring the impedance in a
sample contact path. There are three sample contacts in the 9110 pH Analyzer.
Sample Contact 1 senses standard solution draws.
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4 Description of modules91xx pH/Electrolyte Analyzers
Description of modules
SAMPLE
SAMPLE PROBE
ASSEMBLY
PROBE
FILLPORT
RED
BLUE
LENOID V
SO
AIR VENT
R
PRE
HEATE
YELLOW DOT
pH
REF
GREEN
ELECTRODE ASSY
PERI PUMP
SOLENOID C
OID B
SOLEN
SOLENOID A
FLUID
CONNECTOR
9110 FLUIDIC DIAGRAM
OID R
YELLOW DOT
REFERENCE
CONNECTOR
Figure A-19110 fluidic diagram
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A-30Service manual · Version 2.0
SOLEN
LVE
REF
WASTE
CHECK VA
CLEANING
REF. RETURN
A
B
FLUID PACK
Page 45
91xx pH/Electrolyte Analyzers4 Description of modules
Description of modules
SAMPLE
SAMPLE PROBE
ASSEMBLY
PROBE
FILLPORT
RED
BLUE
LENOID V
SO
AIR VENT
Cl
Ca
K
YELLOW DOT
Na
REF
GREEN
ELECTRODE ASSY
PERI PUMP
LENOID B
SO
LENOID A
SO
FLUID
CONNECTOR
9120, 9130, 9140 FLUIDIC DIAGRAM
A
OID R
YELLOW DOT
REFERENCE
CONNECTOR
Figure A-29120, 9130, 9140 fluidic diagram
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SOLEN
REF
WASTE
REF. RETURN
B
NOT USED C
FLUID PACK
Page 46
4 Description of modules91xx pH/Electrolyte Analyzers
Description of modules
SAMPLE
SAMPLE PROBE
ASSEMBLY
PROBE
FILLPORT
RED
9180/9181 FLUIDIC DIAGRAM
BLUE
SOLENOID V
AIR VENT
LiClCa
K
YELLOW DOT
Na
REF
GREEN
ELECTRODE ASSY
PERI PUMP
LENOID B
SO
ID A
SOLENO
SOLENOID C
FLUID
CONNECTOR
A
B
OID R
YELLOW DOT
REFERENCE
CONNECTOR
SOLEN
REF
WAS TE
REF. RETURN
C
FLUID PACK
Figure A-39180, 9181 fluidic diagram
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91xx pH/Electrolyte Analyzers4 Description of modules
Description of modules
Electronics
ISE SBC card
Power circuitsPower is supplied to this circuit board through connector JP3 from the power supply
assembly. Test points are provided to measure supply voltages, and light emitting
diodes D1 through D5 are turned on to indicate each supply voltage present on the
card. Since each LED is connected in series after the fuse, a blown fuse results in the
respective LED turned off.
Four additional voltage regulator circuits are mounted on the ISE SBC II Card.
IC U2 and IC U3 provide -8 VDC and +8 VDC (9180/9181: -5 VDC and
+5 VDC) and are used to provide the supply voltages for the analog circuitry. IC U1
develops the supply voltage used to operate the peristaltic pump and provide either
+10 VDC or +22 VDC. The +22 VDC is supplied only for the FAST speed and
+10 VDC is used for all other pump speeds. Signal FAST/SLOW determines which
supply voltage is selected.
U5 switches the voltage between 22 VDC and 12.5 VDC (16 VDC on the 9110) which
supplies the solenoids. When a solenoid is turned on, the voltage switches to 22 VDC
for 0.5 sec, then it returns to 12.5 VDC (16 VDC on the 9110).
The circuit which includes Q7 and R5 provides necessary switching for the measuring
chamber illuminator LEDs.
The following list identifies the test points, fuses and LEDs for each respective DC
supply voltage:
Test pointVoltageFuseRatingLED
TP1+24 VDCF31.25 ATD3
TP2+5 VDCF1/F22.0 AT/1.6 ATD1/D2
TP3-12 VDCF40.3 ATD4
TP4+12 VDCF50.3 ATD5
TP5Ground
Ta b le A -5Voltage test points, LEDs
Test pointVoltage
TP6-8 VDC (9180/9181: -5 VDC)
TP7+22/12 VDC
TP8+8 VDC (9180/9181: +5 VDC)
+
TP9Na
TP10K
TP11Ca
TP12Temperature
TP13+10.000 V ref. voltage
TP14-2.500 V ref.voltage (-2.500 V on the 9110)
TP15Sample sensor (sample contact voltage on the 9110)
TP16+22/12.5 VDC (+22/+16 VDC on the 9110)
Ta b le A -6Voltage test points
channel (pH channel on the 9110)
+
channel (not used on the 9110)
2+
/Cl– channel (Li+ 9180/9181 only; not used on the 9110)
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4 Description of modules91xx pH/Electrolyte Analyzers
Description of modules
Valve d r iv e rsThe solenoids are activated by transistors Q9 - Q13. To open the solenoid, a 0.5-
second pulse of 22 V is applied, then the voltage drops down to 12.5 V (16 V on the
9110) to hold the solenoid open.
Pump motor driver/cover sensorThe pump driver circuit IC U9 and IC U10 provide the drive and control for the
peristaltic pump. Signals PUMPEN, Pump Enable and PUMPSTEP, Pump Step Pulses
enable IC U10 to provide the necessary control to driver IC U9 which supplies pump
drive signals PHASE A through PHASE D to control peristaltic pump operation.
IC U11 operates with signal DCLOSED from the sample door light gate to provide
signal DOOR which detects the status of the sample door (open or closed).
Input amplifiersIC U13, U14 and U15 (9110/9180/9181: U13 only) provide high to low input
impedance matching for each Electrode input. Offset generator IC U12D and
amplifiers IC U12A, U12B and U12C provide the necessary gain and offset for each
electrode channel. TP9, TP10 and TP11 provide test points for the Na
the 9110), K
+
and Cl–/Ca2+/Li+ channels respectively.
+
(TP9: pH on
9110 only: IC U300 is used as the input amplifier for the reference electrode, IC U12A
is used for the subtraction of the reference electrode signal from the pH electrode
signal. For sample detection, the reference electrode is switched to ground (relay
K300) during aspiration.
Temperature sensorThis circuit is used in the 9110 pH Analyzer to amplify the signal of the temperature
Analog channel selector and A/D
converter
MicroprocessorMicroprocessor IC U31, EPROM IC U25 (9180/9181: U40) and MOSTEK Real Time
SnapPak Sensor (9180/9181
only)
sensor in the preheater. This is an optional circuit which is used in the 9140, 9180 and
9181.
The circuit creates a temperature-dependent voltage which is converted by software to
degrees Celsius. R54 can be adjusted for correct temperature display.
Analog inputs from the input amplifiers are selected via signals ADSEL0 through
ADSEL2 and are multiplexed by IC U19. This multiplexed signal is then fed to the A/
D Converter IC U20. IC U21 supplies the necessary reference voltage (2500mV) for
the A/D Converter and can be measured at TP14.
Clock/RAM IC U22 form the components of the central processing system. IC U23
Address Demultiplexer, IC U24 Programmable Array Logic (PAL) and IC U28
provide serial data buses (9180/9181: U23, U24 and U28 not present). IC U34
through IC U38 convert serial data to parallel data and provide printer data, display
data, solenoid valve control and peristaltic pump control (9110: U34 not present).
This fashion of serial to parallel data conversion is used to prevent analyzer lock-up by
peripheral devices. The RS232 serial interface is a direct input/output from the
microprocessor utilizing interface driver and receiver U29 and U30.
Optical detector ISO1 provides a signal indicating if the ISE SnapPak™ is in place.
This signal is fed to U41 which converts the light gate input to a digital logic output
indicating SnapPak position (IN or OUT).
Lamp board
The lamp board contains the LED array used to illuminate the measuring chamber
and the interconnectors used for all solenoids, the peristaltic pump, door sensor and
sample turntable (9181 only). A ribbon cable from the SBC Board supplies the
electrical connection for each signal through connector JP6.
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Description of modules
Display board
The display board contains the LCD display, sample contact circuit (9110 only) or
sample sensor connector, the preheater (9110 only) and the YES and NO switches
used for operation of the analyzer. Power and signal interconnection is accomplished
via a ribbon cable from the SBC board through JP2 on the display board.
9110 onlyThe sample contact circuit consists of a square wave generator U1B which generates a
500 Hz signal. U1A amplifies the signal, D2 and C3 rectify the square wave. The gain
can be adjusted with R10. The sample contact output provides a DC voltage, which is
proportional to the square wave amplitude. During sample aspiration, the preheater
tube and the sample contact 1 tube are connected to the square wave via relay K1.
The heater control circuit controls two transistors which are placed in the preheater
block. A thermistor provides temperature feedback to the setting of potentiometer
R20. The signal difference drives the base of the heating transistors via buffer U2C.
U2D shuts the system off in case the thermistor opens. U2B limits the maximum
heating current during warm-up. U1C and attached circuit is used as an AC/DC
converter to create negative voltage -V
9181 onlyDisplay boards utilized in the 9181 analyzer also contain circuitry for both the needle
mechanism motor control and position sensor. The autosampler "Table Present"
signal is also buffered through U1 on this board.
, using square wave generator U1B.
SS
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4 Description of modules91xx pH/Electrolyte Analyzers
Description of modules
Roche DiagnosticsApril 2007
A-36Service manual · Version 2.0
Software operation of the 9110 pH Analyzers can be accessed by YES/NO selection on
the analyzer front panel. The following flow chart diagrams are provided to identify
operating sequences of the 9110 pH Analyzers:
1
Overall Program Operation Flow
2
Main Menu
3
Measurement Sequence
4
Print Functions Menu
5
QC/Standard/Urine Sample Menu
6
Electrode Cleaning Menu
7
Operator Functions Menu
8
Program Instrument Menu
9
Service Functions Menu
10
Calibration Sequence
Roche DiagnosticsApril 2007
Service manual · Version 2.0B-5