2.1 Information regarding operating instructions 8
2.2 Warranty and liability 8
3 Transport, storage, place of installation 9
3.1 Conditions of transport and storage 9
3.2 Place of installation 9
3.3 Unpacking 9
3.4 Delivery scope 9
4 Installations and starting up 10
4.1 Calorimeter C 200 10
4.2 Installation 10
4.3 Switchin on the system 12
4.4 Display and operating elements 12
4.5 Confi guring the system 13
4.6 System settings 14
4.7 Filling the calorimeter for the fi rst time 15
4.8 Switchin off the system 16
4.9 Coding decomposition vessel 16
4.10 Oxygen station C 248 16
5 Calorimetric measurements 17
5.1 Determining the calorifi c value 17
5.2 Corrections 17
5.3 Information about the sample 18
5.4 Calibration 19
6 Preparing and performing measurements 19
6.1 Decomposition vessel C 5010 19
6.2 Preparing the decomposition vessel 20
6.3 Preparing the measurement 21
6.4 Performing the measurement 22
6.5 Cleaning the decomposition vessel 23
6.6 Errors in the measuring procedure 24
3
7 Service menue 26
7.1 Operation 26
7.2 Description of service menue options 26
8 Cleaning and maintenance 27
8.1 Inner vessel fi lter 27
8.2 Filler 27
8.3 Micro fi lter 27
8.4 Maintaining the water circulation 28
8.5 Decomposition vessels 28
8.6 Cleaning informations 28
9 IKA® - Accessories and consumables 29
9.1 Accessories 29
9.2 Consumables 29
10 Technical data 30
4
CE-Declaration of conformity
CE – KONFORMITÄTSERKLÄRUNG DE
Wir erklären in alleiniger Verantwortung, dass dieses Produkt den Bestimmungen der Richtlinien 89/ 336 EG, 89/ 392
EG und 73/ 23 EG entspricht und mit folgenden Normen und normativen Dokumenten übereinstimmt: EN 61010,
EN 50082, EN 55014 und EN 60555.
CE – DECLARATION OF CONFIRMITY EN
We declare under our sole responsibility that this product corresponds to the regulations 89/ 336 EEC, 89/ 392 EEC
and 73/ 23 EEC and conforms with the standards or standardized documents: EN 61010, EN 50082, EN 55014 and
EN 60555.
DÉCLARATION DE CONFORMITÉ CE FR
Nous déclarons sous notre responsabilité que se prodiut est conforme aux réglementations 89/ 336 CEE, 89/ 392 CEE
et 73/ 23 CEE et en conformité avec les normes ou documents normalisés suivant: EN 61010, EN 50082, EN 55014 et
EN 60555.
DECLARACION DE CONFORMIDAD DE CE ES
Declaramos por nuestra responsabilidad propia que este producto corresponde a las directrices 89/ 336 CEE, 89/ 392
CEE y 73/ 23 CEE y que cumple las normas o documentos normativos siguientes: EN 61010, EN 50082, EN 55014 y
EN 60555.
CE – DICHIARAZIONE DI CONFORMITÀ IT
Dichiariamo, assumendone la piena responsabilità, che il prodotto è conforme alle seguenti direttive CCE 89/ 336, CCE
89/ 392 e CCE 73/ 23, in accordo ai seguenti regolamenti e documenti: EN 61010, EN 50082, EN 55014 e EN 60555.
5
1 Safety instructions
For your protection
• Read the operating instructions in full
before starting up and follow the safety
instructions.
• Keep the operating instructions in a place whe-
re they can be accessed by everyone.
• Ensure that only trained staff work with the ap-
pliance.
• Follow the safety instructions, guidelines,
occupational health and safety and acci-
dent prevention regulations.
• Wear your personal protective equipment
in accordance with the hazard category
of the medium to be processed.
• Calorimeter system C 200 may only be used to
determine the calorific value of solid and fluid
materials. Only the appropriate original IKA®
decomposition vessels may be used for this
purpose. For detailed information, please see
the operating instructions for the decomposition vessels.
• The maximum extra energy added to the de-
composition vessel must not exceed 40,000 J
(select the test mass accordingly). The permitted operating pressure of 230 bar must not be
exceeded. The maximum permitted operating
temperature must not exceed 50 °C.
•
Do not overfill the decomposition vessel with
sample. Only fill the decomposition vessel with
oxygen to a maximum pressure of 40 bar.
Check the set pressure on the pressure reducer.
Perform a leakage test before each combustion
process (follow operating instructions for decomposition vessel!).
• Some materials tend to explode when combus-
ted (e.g. due to formation of peroxide), which
could cause the decomposition vessel to crack.
• Standard decomposition vessels may not
be used for testing explosive samples.
• If the burning behaviour of a material is unk-
nown, it must be tested before combustion in
the decomposition vessel (risk of explosion). If
you are burning unknown samples, leave the
room or keep your distance from the calorimeter.
• Benzoic acid may only be combusted in its
pressed form! Flammable dust and powder
must be first pressed. Oven-dry dust and pow
der such as splints, hay, straw etc. explode
when combusted! Always wet these materials first! Highly flammable liquids with a low
vapour pressure (e.g. tetramethyl dihydrogen
disiloxane) must not directly touch the cotton
thread!
• Furthermore, toxic combustion residue in the
form of gases, ashes or condensation, for example, is possible in the inner wall of the decomposition vessel.
• When handling combustion samples, com-
bustion residue and auxiliary materials, please
observe the relevant safety regulations. The
following materials, for example, could pose a
handling oxygen.
Warning: oxygen as a compressed gas is
oxidising; intensively aids combustion; can
react violently with flammable materials.
Do not use oil or grease!
• Caution - magnetism! Effects of the mag-
netic field have to be taken into account (e.g.
data storage media, cardiac pacemakers ...).
• When using stainless steel crucibles tho-
roughly check their condition after each expe-
riment. If the material gets thinner, the crucible
may catch fire and damage the decomposition
vessel. Crucibles must not be used for more
than 25 combustions for safety reasons.
• The decomposition vessel is manufactured in
accordance with the directive for pressure
equipment 97/23/EC.
This is indicated by the CE symbol with the ID
number of the notified body. The decompositi-
on vessel is a category III pressure device. The
decomposition vessel has undergone an EC
prototype test. The CE declaration of confor-
mity confirms that this decomposition vessel
corresponds to the pressure device described in
the EC prototype test certificate. The decompo-
sition vessel has undergone a pressure test
6
with test pressure of 330 bar and a leaka-
ge test with oxygen at 30 bar.
• Decomposition vessels are experiment autocla-
ves and must be tested by a technical expert
after each use.
Individual use is understood here to include a
series of experiments performed under roughly
the same conditions in terms of pressure and
temperature. Experiment autoclaves must be
operated in special chambers (C 2000, C 5000,
C 7000, C 200).
• The decomposition vessels must undergo re-
peated tests (internal tests and pressure tests)
performed by the technical expert. The frequency of these tests is to be determined by
the operator on the basis of experience, type
of operation and the material used in the decomposition vessel.
• The declaration of conformity becomes
invalid if mechanical modifications are
carried out to the experiment autoclaves
or if tightness can no longer be guaran-
teed as a result of major corrosion (e.g.
pitting by halogens).
• The threads on the body of the decomposition
vessel and the union nut are subject to considerable stress in particular and must therefore be
checked regularly for wear.
• The condition and function of the seals must
be checked and ensured by way of a leakage
test (see operating instructions for decompo-
sition vessel!).
• Only technical experts may perform pressure
tests and service work on the decomposition
vessel.
• We recommend that you send the decomposition vessel to our factory for inspec-
tion, and if necessary, repair after 1000
tests or after one year or sooner depen-
ding on use.
• For the purposes of these operating instructions
a technical expert is someone
1.
who guarantees to conduct the tests properly
on the basis of his training, knowledge and experience gained through practical work,
2. who is sufficiently reliable,
3. who is not subject to any instructions in terms
of the test activity,
4. who has suitable test equipment if necessary,
5. who can provide appropriate proof of the requirements listed in 1.
• National directives and laws must be observed
for operating pressure vessels!
•
Anyone operating a pressure vessel must keep it
in a proper condition, operate it properly, supervise it, carry out the necessary maintenance and
repair work immediately and implement the
safety measures required in the circumstances.
• Pressure vessels must not be used if they have
defects which could pose a risk to staff or third
parties. The pressure equipment directive can
be obtained from Carl Heymanns or Beuth publishers.
•
The C 248 oxygen station must be set up at least
1.5 m far away from the calorimeter.
For protection of the equipment
• The voltage stated on the type plate must cor-
respond to the mains voltage.
• Removable parts must be refitted to the appli-
ance to prevent the infiltration of foreign objects, liquids etc.
• Protect the appliance and accessories from
bumps and impacts.
7
2 User information
2.1 Information regarding operating instructions
General hazard
This symbol indicates information which is essential for the safety of your health. Failure to observe this information can cause damage to
health and injuries.
This symbol indicates information which is important for ensuring that the appliance functions without any technical problems. Failure to
observe this information could damage the calorimeter system.
This symbol indicates information which is important for ensuring that calorimetric measurements are performed effi ciently and for using the calorimeter
system. Failure to observe this information can result in inaccurate measurements.
TIP
2.2 Warranty and liability
You have purchased an original IKA
manufactured to the latest, highest quality standards. According to IKA®'s conditions of warranty, this product is guaranteed for 12 months.
To ensure the long-term precision and function
of the calorimeter system, we recommend that
you conclude a maintenance agreement (annual
maintenance) with IKA® or an authorised IKA®
workshop. If the fi rst maintenance is carried out
within 12 months of purchase, the warranty will
be extended to 24 months.
In the case of a warranty claim, please contact
the responsible representative or the supplier.
You can also return the appliance directly to
IKA®- WERKE.
Please enclose the sales invoice and the reason
for the claim and state the name of the contact
person at your company. Freight charges are to
be paid by the sender.
This symbol indicates references to the optimization of operatinal sequences
are characterized.
Attention - Risk of damage due to magnetism.
Numbers , , etc. indicate guidelines in the following sections which
must always be carried out in order.
®
product,
Please read these operating instructions carefully.
IKA®- WERKE only consider themselves to be
responsible for the safety, reliability and performance of the appliance when
• the appliance has been operated in accordance
with the operating instructions,
• only persons authorised by the manufacturer
interfere with the appliance,
•
only original parts and original accessories are
used for repairs.
IKA®- WERKE do not accept liability for damage
or costs resulting from accidents, misuse of the
appliance or unauthorised changes, repairs or
upgrades.
8
3 Transport, storage, place of installation
3.1 Conditions of transport and storage
• The system must be protected against mecha-
nical impact, vibrations, dust deposits and corrosive ambient air during transportation and
storage.
• It is also important to ensure that the relative
humidity does not exceed 80%.
3.2 Place of installation
Please observe the respective country-specifi c regulations for operating pressure equipment when
installing the appliance. A constant ambient temperature is an important requirement for ensuring
the high measuring accuracy of the system. The
following conditions must therefore be fulfi lled at
the place of installation:
• No direct solar radiation
• No draughts (e.g. beside windows, doors, air
conditioning)
• Sufficient distance to radiators and other heat
sources
3.3 Unpacking
• Only the original packing may be used for trans-
portation.
• The appliance must be completely emptied be-
fore storing and transportation.
• The (constant) room temperature should be
around 20 °C ... 25 °C
• The system must be installed on a level surface.
• An adequate power supply corresponding to
the nameplates on the system components.
• Oxygen supply (99.95 % pure oxygen, quality
3.5; pressure 30 bar) with pressure display and
shut-off device (C 29 reducing valve, acces-
sories)
Please unpack the system components carefully
and check for any damage. When you unpack
the equipment, check for any damages which
may have occurred during transportation.
3.4 Delivery scope
1 x Basic device C 200
1 x Decomposition vessel C 5010
1 x Ignition adaptor
1 x Attachment set
1 x Table power supply
Make a note of any damage and report it immediately (post, railway, shipping company).
1 x Power cable
1 x Operating instructions
1 x Water emptying hose (length: 1 m)
1 x Oxygen station C 248
1 x Measuring cup (2 l)
9
4 Installation and starting up
4.1 Calorimeter C 200
Measuring cell cover
Tank fillers
Display
Keyboard
Fill level display
4.2 Installation
All the connections for draining as well as the peripherals are on the back of the appliance.
Connecting the table power supply
Connect the calorimeter to the table power supply (4-pin plug ). Check that the voltage information on the rating plate of the power supply
unit matches your mains supply. Connect the power line of the plug to the voltage source.
PC connector
Printer connector
ON/OFF switch
Table power supply connector
Table power supply
Connecting peripherals
When connecting peripherals make sure that
both they and the calorimeter are switched off at
ON/OFF switch .
10
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