Hanna Instruments HI 38017 User Manual

Instruction Manual
HI 38017
Free & Total
Chlorine
Low and Medium
Range
SPECIFICATIONSSPECIFICATIONS
SPECIFICATIONS
SPECIFICATIONSSPECIFICATIONS
Range 0 to 0.7 mg/L (ppm) as Chlorine (LR)
0 to 3.5 mg/L (ppm) as Chlorine (MR)
Smallest Increment LR: 0.02 mg/L
MR: 0.1 mg/L Analysis Method Colorimetric Sample Size 10 mL (LR), 5 mL (MR) Number of Tests 200 Case Dimensions 235x175x115 mm (9.2x6.9x4.5") Shipping Weight 696 g (24.6 oz.)
INSTRUCTIONSINSTRUCTIONS
INSTRUCTIONS
INSTRUCTIONSINSTRUCTIONS
READ THE ENTIRE INSTRUCTIONS BEFORE USING THE KIT
• To measure chlorine in the 0-0.7 mg/L range, verify that the mirror, its holder and the disc are pre-installed in the checker disc. If not, install them as shown in the figure.
• Remove the cap and add the specific test reagent: Free Chlorine: 1 packet of Total Chlorine: 1 packet of DPD Free Chlorine reagent. DPD Total Chlorine reagent.
Test Kit with
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Dear Customer, Thank you for choosing a Hanna Product. Please read the instruction sheet carefully before using the
test kit. It will provide you with the necessary information for correct use of the kit. If you need additional information, do not hesitate to e-mail us at tech@hannainst.com.
Remove the chemical test kit from the packing material and examine it carefully to make sure that no damage has occurred during shipping. If there is any noticeable dam­age, notify your Dealer or the nearest Hanna office immediately.
Each kit is supplied with:
HI 93701-0 Free Chlorine reagent, packets (100 pcs);
• HI 93711-0 Total Chlorine reagent, packets (100 pcs);
• Demineralizer Bottle with filter cap for about 12 liters of deionized water (depending on the hardness level of water to be treated)
• 1 checker disc (containing a mirror, a mirror holder and the disc);
• 2 glass vials with caps
• 1 plastic pipette (3 mL).
Note: Any damaged or defective item must be returned in
its original packing materials.
;
;
SIGNIFICANCE AND USESIGNIFICANCE AND USE
SIGNIFICANCE AND USE
SIGNIFICANCE AND USESIGNIFICANCE AND USE
Chlorine is the most commonly used water disinfectant in applications that vary from treatment of drinking water and wastewater, pool and spa sanitization, to food pro­cessing and sterilization. Chlorine present in water binds with bacteria, leaving only a part of the original quantity (free chlorine) to continue its disinfecting action. If the free chlorine level is improper with respect to pH, water will have an unpleasant taste and odor and the disinfecting potential of the chlorine will be diminished.
Free chlorine reacts with ammonium ions and organic compounds to form chlorine compounds resulting in dimin­ished disinfecting capabilities compared with free chlorine. Chlorine compounds together with chloramines form com­bined chlorine. Combined chlorine and free chlorine together result in total chlorine.
While free chlorine has a much higher disinfectant poten­tial, combined chlorine has a much higher stability and has a lesser volatility.
Note: mg/L is equivalent to ppm (parts per million).
CHEMICAL REACTIONCHEMICAL REACTION
CHEMICAL REACTION
CHEMICAL REACTIONCHEMICAL REACTION
The reaction between chlorine and the DPD reagent causes a pink tint in the sample which is proportional to the chlorine concentration.
ISTR38017 02/00 PRINTED IN ITALY
• Use the pipette to fill each glass vial with 10 mL of sample (up to the mark).
• Insert one of the vials into the left hand opening of the checker disc. This is the blank.
Remove the cap and fill the Demineralizer Bottle with tap water.
• Replace the cap and shake gently for at least 2 minutes. The dem­ineralized water is now ready.
• Flip open the top of the Demineralizer Bottle cap. By gently squeezing the bottle, add demineralized water to the other vial up to the 20 mL mark. Replace the cap and shake to mix.
10 mL
• Replace the cap and mix.
• In the case of Total Chlo­rine determination, wait for 2 minutes to allow reaction to occur. This is the reacted sample.
• Remove the cap and insert the reacted sample into the right hand opening of the checker disc.
• Hold the checker disc so that a light source illumi­nates the samples from the top.
• Keep the checker disc at a distance of 30-40 cm (12­16") from the eyes to match the color. Rotate the disc while looking at the color test windows and stop when you find the color match. Read the value in the result window and divide it by 5 to obtain mg/L (or ppm) of Chlorine.
• To measure chlorine in the 0-3.5 mg/L range, remove the disc, mirror and its holder, if pre-installed. Then install just the disc as shown here.
• Use the pipette to fill each glass vial with 5 mL of sample (up to the mark) and insert one of them into the left hand opening of the checker disc. This is the blank.
• Add to the other vial demineralized water up to the 10 mL mark and shake to mix.
• Then add to the vial the specific test reagent:
Free Chlorine: 1 packet of Total Chlorine: 1 packet of DPD Free Chlorine reagent. DPD Total Chlorine reagent.
5 mL
you find the color match. Read the value in the result window directly in mg/L (or ppm) of Chlorine.
For best results: Perform the reading three times and take
the average value (divide by 3 the sum of the three numbers). Intensely colored samples will make the color matching difficult and they should be adequately treated before performing the test. Suspended matter in large amounts should be removed by prior filtration.
Caution: Ultraviolet radiation may cause fading of colors.
When not in use, keep the disc protected from light, in a cool and dry place.
Interferences: bromine, iodine, fluorine, ozone, oxidized
manganese and chromium.
REFERENCESREFERENCES
REFERENCES
REFERENCESREFERENCES
Adaptation of the EPA recommended DPD method 330.5.
HEALTH AND SAFETYHEALTH AND SAFETY
HEALTH AND SAFETY
HEALTH AND SAFETYHEALTH AND SAFETY
The chemicals contained in this kit may be hazardous if improperly handled. Read the relevant Health and Safety Data Sheet before performing this test.
• Replace the cap and mix. In the case of Total Chlorine determination, wait for 2 minutes to allow reaction to occur. This is the reacted sample.
• Remove the cap and insert the reacted sample into the right hand opening of the checker disc.
• Hold the checker disc so that a light source illuminates the samples from the back of the windows.
• Keep the checker disc at a distance of 30-40 cm (12­16") from the eyes to match the color. Rotate the disc while looking at the color test windows and stop when
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