Model ZR202S
Integrated type Explosion-proof
Zirconia Oxygen Analyzer
IM 11M13A01-04E
IM 11M13A01-04E
6th Edition
Introduction
Thank you for purchasing the ZR202S Integrated type Explosion-proof Zirconia Oxygen Analyzer.
Please read the following respective documents before installing and using the ZR202S Integrated
type Explosion-proof Zirconia Oxygen Analyzer.
The related documents are as follows.
General Specications
Model ZR22S and ZR202S
Explosion-proof Direct In Situ Zirconia Oxygen Analyzer
* the “E” in the document number is the language code.
User’s Manual
Model ZR202S
Integrated type Explosion-proof Zirconia Oxygen Analyzer
Model ZR22A, ZR202A
Heater Assembly
Model EXAxt ZR Series
HART Protocol
* the “E” or “EN” in the document number is the language code.
<Introduction>
ContentsDocument numberNote
GS 11M13A01-01E
ContentsDocument numberNote
IM 11M13A01-04E(This manual)
IM 11M12A01-21E
IM 11M12A01-51E
i
An exclusive User’s Manual might be attached to the products whose sufx codes or option codes
contain the code “Z” (made to customers' specications). Please read it along with this manual.
The EXAxt ZR Integrated type Explosion-proof Zirconia Oxygen Analyzer has been developed for
combustion control in various industrial processes. There are several version of this analyzer so you
can select one that matches your application.
Optional accessories are also available to improve measurement accuracy and automate calibration.
An optimal control system can be realized by adding appropriate options.
This instruction manual describes almost all of the equipment related to the EXAxt ZR.
You may skip any section(s) regarding equipment which is not included in your system.
Regarding the HART Communication Protocol, refer to IM 11M12A01-51E.
IM11M12A01-51E has been published as “Model EXAxt ZR series HART protocol”.
Regarding Separate type Explosion-proof Zirconia Oxygen Analyzer, refer to IM 11M13A01-02E.
< Before using the equipment, please read any descriptions in this manual related to the equipment
and system that you have, on appropriate use and operation of the EXAxt ZR. >
Models and descriptions in this manual are listed below.
Model
ZR202S Integrated type Explosion-proof
Zirconia Oxygen Analyzer
ZO21R-L Probe Protector
ZA8FFlow Setting Unit
(for manual calibration use)
— Automatic Calibration Unit
—Calibration Gas Unit Case (Part No.
E7044KF)
—Check Valve
(Part No. K9292DN, K9292DS)
ZO21SStandard Gas Unit
CMPL: Customer Maintenance Parts List
Product Name
Specication
Description in this manual
Installation
Operation
Maintenance
This manual consists of twelve chapters. Please refer to the reference chapters for installation,
operation and maintenance.
Table and Contents
Chapter
1. Overview Equipment models and system conguration examples
Outline
Installation Operation
Relates to
Maintenance
CMPL
2. Specications Standard specication, model code (or part number),
dimension drawing for each equipment
3. InstallationInstallation method for each equipment
4. PipingExamples of piping in two standard system
congurations
5. WiringWiring procedures such as “Power supply wiring”,
“Output signal wiring” or others
6. ComponentsMajor parts and functions are described
7. StartupBasic procedure to start operation of EXAxt ZR.
Chapter 7 enables you to operate the equipment
immediately.
8. Detailed Data
Setting
9. CalibrationDescribes the calibration procedure required in the
10. Other
Functions
11. Inspection and
Maintenance
12. Troubleshooting This chapter describes measures to be taken when an
CMPL (parts list)User replaceable parts list
: Read and completely understand before operating the equipment.
: Read before operating the equipment, and refer to it whenever necessary.
: Recommended to read at least once.
Details of key operations and displays
course of operation
Other functions described
How to conduct maintenance of EXAxt ZR and
procedures for replacement of deteriorated parts
abnormal condition occurs
IM 11M13A01-04E
ATEX Documentation
This is only applicable to the countries in the European Union.
<Introduction>
iii
GB
DK
E
NL
SK
CZ
I
LT
LV
EST
PL
SF
P
F
D
S
SLO
H
BG
RO
M
GR
IM 11M13A01-04E
iv
Precautions in Handling Explosion-proof Zirconia Oxygen Analyzer
The explosion-proof zirconia oxygen analyzer (Model ZR202S) are designed as explosion-proof
instruments.
When using either of these instruments in an explosion-susceptible hazardous area, note the
following and observe the given precautions:
Use only the supplied, the explosion-proof zirconia oxygen analyzer (Model ZR202S) and
accessories, or any explosion-proof certication may be invalidated.
For the details, refer to the system congurations in the manual.
<Introduction>
CAUTION
Only trained persons use this instrument in industrial locations.
Explosion-proof Approval followings:
ZR202S-A (ATEX); Ex db IIB+H2 T2 Gb, Ex tb IIIC T300°C Db
ZR202S-B (FM); Class I, Division 1, Groups B, C and D, Class II/III, Division 1,
Groups E, F and G, T2
ZR202S-C (CSA); Class I, Division 1, Groups B, C and D, Class II/III, Division 1,
Groups E, F and G, T2
ZR202S-D (IECEx); Ex db IIB+H
T2 Gb, Ex tb IIIC T300°C Db
2
For the safe use of this equipment
WARNING
EXAxt ZR is very heavy. Be sure not to accidentally drop it. Handle safely to avoid injury.
Connect the power supply cord only after conrming that the supply voltage matches the rating of this
equipment. In addition, conrm that the power is switched off when connecting power supply.
Some process gas is dangerous to people. When removing this equipment from the process line for
maintenance or other reasons, protect yourself from potential poisoning by using a protective mask or
ventilating the area well
CAUTION
Requirements for explosion-proof use:
The ambient temperature is in the range of -20 to +55ºC. The surface temperature of the ZR202S is
not over the temperature class T2 (300ºC)*
* The surface temperature of the amplier box does not exceed 70ºC.
Oxygen concentration of sample/reference /calibration gas shall not exceed that found in normal air,
typically 21 vol%.
IM 11M13A01-04E
<Introduction>
NOTE
The cell (sensor) at the tip of the probe is made of ceramic (zirconia element). Do not drop the
equipment or subject it to pressure stress.
• Do NOT allow the sensor (probe tip) to make contact with anything when installing the analyzer.
• Avoid any water dropping directly on the probe (sensor) of the analyzer when installing it.
• Check the calibration gas piping before introducing the calibration gas to ensure that there is no
leakage of the gas. If there is any leakage of the gas, the moisture drawn from the sample gas
may damage the sensor.
• The probe (especially at the tip) becomes very hot. Be sure to handle it with gloves.
(1) About This Manual
• This manual should be passed on to the end user.
• The contents of this manual are subject to change without prior notice.
v
• The contents of this manual shall not be reproduced or copied, in part or in whole, without
permission.
• This manual explains the functions contained in this product, but does not warrant that those will
suit the particular purpose of the user.
• Every effort has been made to ensure accuracy in the preparation of this manual. However,
should any errors or omissions come to the attention of the user, please contact the nearest
Yokogawa Electric representative or sales ofce.
• This manual does not cover the special specications. This manual may not be changed on any
change of specication, construction and parts when the change does not affect the functions or
performance of the product.
• If the product is used in a manner not specied in this manual, the safety of this product may be
impaired.
NOTE
This instrument is tested and certied as explosion-proof type. Please note that the construction of the
instrument, installation, external wiring, maintenance or repair is strictly restricted, and non-observation or negligence of this restriction would result in dangerous condition.
(2) Safety and Modication Precautions
•Follow the safety precautions in this manual when using the product to ensure protection and
safety of personnel, product and system containing the product.
IM 11M13A01-04E
vi
<Introduction>
(3) The following safety symbols are used on the product as well as in this manual.
WARNING
This symbol indicates that the operator must follow the instructions laid out in this manual in order to
avoid the risk of personnel injury electric shock, or fatalities. The manual describes what special care
the operator must exercise to avoid such risks.
CAUTION
This symbol indicates that the operator must refer to the instructions in this manual in order to prevent
the instrument (hardware) or software from being damaged, or a system failure from occurring.
NOTE
This symbol draws attention to information essential for understanding the operation and functions.
Protective Ground Terminal
Function Ground Terminal (Do not use this terminal as the protective
ground terminal.)
Alternating current
IM 11M13A01-04E
Special descriptions in this manual
This manual indicates operation keys, displays and drawings on the product as follows:
• Operation keys, displays on the panel
Enclosed in [ ]. (Ex. “MODE” key)
When the instrument arrives, unpack the package with care and check that the instrument has not
been damaged during transportation. In addition, please check that the specication matches the
order, and required accessories are not missing. Specications can be checked by the model codes
on the nameplate. Refer to Chapter 2 Specications for the list of model codes.
l Details on operation parameters
When the EXAxt ZR Integrated type Explosion-proof Zirconia Oxygen Analyzer arrives at the user
site, it will operate based on the operation parameters (initial data) set before shipping from the
factory.
Ensure that the initial data is suitable for the operation conditions before conducting analysis. Where
necessary, set the instrument parameters for appropriate operation.
For details of setting data, refer to chapters 7 to 10.
When user changes the operation parameter, it is recommended to note down the changed setting
data.
l Product Disposal:
The instrument should be disposed of in accordance with local and national legislation/regulations.
Trademark Acknowledgments
• All other company and product names mentioned in this user’s manual are trademarks or registered trademarks of their respective companies.
• We do not use TM or ® mark to indicate those trademarks or registered trademarks in this user’s
manual.
IM 11M13A01-04E
u CE marking products
Authorized Representative in EEA
The Authorized Representative for this product in EEA is Yokogawa Europe B.V. (Euroweg 2, 3825
HD Amersfoort, The Netherlands).
Identication Tag
This manual and the identication tag attached on packing box are essential parts of the product.
Keep them together in a safe place for future reference.
Users
This product is designed to be used by a person with specialized knowledge.
l How to dispose the batteries:
<Introduction>
ix
This is an explanation about the new EU Battery Directive (DIRECTIVE 2006/66/EC). This directive is
only valid in the EU.
Batteries are included in this product. Batteries incorporated into this product cannot be removed by
yourself. Dispose them together with this product.
When you dispose this product in the EU, contact your local Yokogawa Europe B.V.ofce. Do not
dispose them as domestic household waste.
Battery type: Manganese dioxide lithium battery
Notice:
The symbol (see above) means they shall be sorted out and collected as ordained in ANNEX II in
DIRECTIVE 2006/66/EC.
IM 11M13A01-04E
x
<Introduction>
u After-Sales Warranty
l Do not modify the product.
l Yokogawa warrants the product for the period stated in the pre-purchase quotation.
Yokogawa shall conduct dened warranty service based on its standard.
l During the warranty period, for repair under warranty carry or send the product to the
local sales representative or service ofce. Yokogawa will replace or repair any damaged
parts and return the product to you.
• Before returning a product for repair under warranty, provide us with the model name and serial
number and a description of the problem. Any diagrams or data explaining the problem would
also be appreciated.
• If we replace the product with a new one, we won’t provide you with a repair report.
l In the following cases, customer will be charged repair fee regardless of warranty period.
• Failure of components which are out of scope of warranty stated in instruction manual.
• Failure caused by usage of software, hardware or auxiliary equipment, which Yokogawa did not
supply.
• Failure due to improper or insufcient maintenance by user.
• Failure due to modication, misuse or outside-of-specications operation which Yokogawa
does not authorize.
• Failure due to power supply (voltage, frequency) being outside specications or abnormal.
• Failure caused by any usage out of scope of recommended usage.
• Any damage from re, earthquake, storms and oods, lightning, disturbances, riots, warfare,
radiation and other natural changes.
l Yokogawa does not warrant conformance with the specic application at the user site.
Yokogawa will not bear direct/indirect responsibility for damage due to a specic applica-
tion.
l Yokogawa will not bear responsibility when the user congures the product into systems
or resells the product.
l Maintenance service and supplying repair parts will be covered for ve years after the
production ends. For repair for this product, please contact the nearest sales ofce described in this instruction manual.
IM 11M13A01-04E
<Introduction>
xi
IM 11M13A01-04E
<CONTENTS>
Model ZR202S
Integrated type Explosion-proof Zirconia Oxygen Analyzer
12.2.2 Remedies When Alarms are Generated ..........................................12-5
12.3 Measures When Measured Value Shows an Error ...................................... 12-9
12.3.1 Measured Value Higher Than True Value ........................................12-9
12.3.2 Measured Value Lower Than True Value ......................................12-10
12.3.3 Measurements Sometimes Show Abnormal Values ..................... 12-10
Customer Maintenance Parts List ......................................CMPL 11M13A01-04E
Customer Maintenance Parts List ..........................................CMPL 11M3D1-01E
Revision Information ...............................................................................................i
IM 11M13A01-04E
Blank Page
<1.Overview>
ZR202S Integrated type Explosion-proof
Hazardous Area
unit case
1. Overview
The EXAxt ZR Integrated type Explosion-proof Zirconia Oxygen Analyzer is used to monitor and
control the oxygen concentration in combustion gases, in boilers and industrial furnaces, for wide
application in industries which consume considerable energy-such as steel, electric power, oil and
petrochemical, ceramics, pulp and paper, food, or textiles, as well as incinerators and medium/small
boilers. It can help conserve energy in these industries. The EXAxt ZR also contributes to preservation
of the earth’s environment in preventing global warming and air pollution by controlling complete
combustion to reduce CO2, SOx and NOx.
The EXAxt ZR Integrated type Explosion-proof Zirconia Oxygen Analyzer integrates both probe
and converter. The analyzers need not use a sampling device, and allow direct installation of the
probe in the wall of a flue or furnace to measure the concentration of oxygen in the stack gas of the
temperature up to 700°C.
The probe uses a high-reliability Zirconia sensor and a heater assembly that can be replaced on site.
The analyzer is equipped with three infrared switches, which enable the user to operate the equipment
without opening the cover on site. Analyzer calibration can also be fully automated and the automatic
calibration unit is provided. Choose the equipment which best suits your needs so that an optimal
combustion control system can be obtained.
1-1
Some examples of typical system conguration are illustrated below:
1.1 < EXAxt ZR > System Conguration
The system configuration should be determined by the conditions; e.g. whether the calibration is to
be automated, and whether flammable gas is present and requires safety precautions. The system
conguration can be classied into two basic patterns as follows:
1.1.1 System 1
This system is for monitoring and controlling oxygen concentration in the combustion gases of a
large-size boiler or heating furnace. Instrument air (clean and dry air of oxygen concentration 21%)
is used as the reference gas and the span gas for calibration. Zero gas is fed from a cylinder during
calibration. The gas ow is controlled by the ZA8F ow setting unit (for manual valve operation).
Zirconia Oxygen Analyzer
Stop valve
or
Check valve
Reference gas
Calibration gas
*1
Flowmeter
Needle
valve
Air Set
Instrument air
Span gas
Non-hazardous Area
100 to 240 V AC
~
Contact input
Analog output, contact output
Digital output (HART)
Figure 1.1 Example of System 1
Note:
The installation temperature limits range for integrated type analyzer is -20 to 55°C.
*1 Shield cable:
Use shielded signal cables, and connect the shields to the FG terminal of the analyzer.
*2 When a zirconia oxygen analyzer is used, 100%N
Use approx. 1 vol%O2 gas (N2-based).
ZA8F
Flow Setting Unit
gas cannot be used as the zero gas.
2
Pressure
reducing
valve
Calibration gas
*2
Zero gas
cylinder
F1-1E.ai
IM 11M13A01-04E
1-2
<1. Overview>
1.1.2 System 2
This example, System 2, represents typical applications in large boilers and heating furnaces, where
is a need to monitor and control oxygen concentration. Instrument air (clean, dry) is used as the
reference gas and span gas for calibration. Zero gas is supplied from a gas cylinder.
System 2 uses the automatic calibration unit, with auto-switching of the calibration gas. A “combustible
gas detected” contact input turns off power to the heater. There’s also contact output from the analyzer
that can be used to operate a purge gas valve to supply air to the sensor.
ZR202S Integrated type Explosion-proof
Zirconia Oxygen Analyzer
Automatic
Calibration Unit
Reference gas
Span gas
Calibration gas (Zero)
Hazardous Area
*1
Air Set
Instrument air
Pressure
reducing
valve
Calibration gas
unit case
*2
Zero gas cylinder
Non-hazardous Area
100 to 240 V AC
~
Contact input
Analog output, contact output
Digital output (HART)
Figure 1.2 Example of System 2
1.2 < EXAxt ZR > System Components
1.2.1 System Components
System Components
ZR202S Integrated type Zirconia Oxygen Analyzers
ZO21R Probe Protector for Zirconia Oxygen Analyzers
ZO21S Standard Gas Unit
Automatic Calibration Unit for integrated type Analyzer
L9852CB, G7016XH Stop Valve for Calibration gas line
K9292DN,K9292DS Check Valve for Calibration gas line
G7003XF/K9473XK, G7004XF/K9473XG Air Set
G7013XF, G7014XF Pressure Reducing Valve for Gas Cylinder
ZR202A Heater Assembly (Spare Parts for ZR202S)
: Items required for the above system example
: To be selected depending on each application. For details, refer to corresponding chapter.
This chapter describes the specications for the following:
ZR202S Integrated type Explosion-proof Zirconia Oxygen Analyzer (See Subsection 2.1.2)
ZO21R-L Probe Protector (See Subsection 2.1.3)
ZA8F Flow Setting Unit (See Subsection 2.2.1)
Automatic Calibration Unit (See Subsection 2.2.2)
ZO21S Standard Gas Unit (See Section 2.3)
Other equipments (See Section 2.4)
CAUTION
Requirements for explosion-proof use:
The ambient temperature is in the range of -20 to +55°C. The surface temperature of the ZR202S is
not over the temperature class T2 (300°C)(*)
(*) The surface temperature of the amplier box does not exceed 70°C.
2-1
Oxygen concentration of sample/reference/calibration gas shall not exceed that found in normal air,
typically 21 vol%.
2.1 General Specications
2.1.1 Standard Specications
Measured Object: Oxygen concentration in combustion exhaust gas and mixed gas (excluding
inammable gases. May not be applicable corrosive gas such as ammonia
and chlorine is present - Contact with YOKOGAWA and its agency.
Measurement System: Zirconia system
Measurement Range: 0.01 to 100 vol%O
Output Signal: 4 to 20 mA DC (maximum load resistance 550 Ω)
Setting Range: Any setting in the range of 0 to 5 through 0 to 100 vol%O
or partial range
Digital Communication (HART): 250 to 550 Ω, depending on number of eld devices connected
to the loop (multi-drop mode).
Note: HART is a registered trademark of the HART Communication Foundation.
Display Range: 0 to 100 vol%O
2
2
(in 1 vol%O2),
2
Warm-up Time: Approx. 20 min.
Explosion-proof Approval:
ATEX Flameproof: ZR202S-A;
Applicable Standard: EN 60079-0: 2012+A11: 2013, EN 60079-1: 2014,
EN 60079-31: 2014
Certicate Number: KEMA 04ATEX2156 X
Type of protection: Ex db IIB+H
T2 Gb, Ex tb IIIC T300°C Db
2
IM 11M13A01-04E
2-2
<2. Specications>
Eqipment Group: II
Category: 2GD
Temperature class for Ex “db”: T2
The maximum surface temperature for Ex “tb”: T300°C
Degree of protection of enclosure: IP66
NAME PLATE
MODEL : Specified model code
SUFFIX : Specified suffix code
STYLE : Style code
AMB. TEMP : Ambient temperature
NO. : Serial No. and year of production*
1
Yokogawa Electric Corporation : The manufacturer name
Tokyo 180-8750 JAPAN : The manufacturer address*
2
No. KEMA 04ATEX2156 X
Ex db IIB+H2 T2 Gb,
Ex tb IIIC T300°C Db
FM Explosion-proof: ZR202S-B
Applicable Standard: FM3600 1998, FM3615 1989, FM3810 2005, ANSI/NEMA 250 1991
Type of protection: Explosion-proof for Class I, Division 1, Groups B, C and D
Dust-ignitionproof for Class II/III, Division 1, Groups E, F and G
Enclosure Rating: NEMA 4X
Temperature Class: T2
Type of protection: Explosion-proof for Class I, Division 1, Groups B, C and D
Dust-ignitionproof for Class II/III, Division 1, Groups E, F and G
Enclosure: Type 4X
Temperature Class: T2
The country of origin
*1: The third to seventh gure from the last shows the year of production.
e.g. 27D327560 2005.02
The year of production
*2: “180-8750” is a zip code which represents the following address.
Type of protection: Ex db IIB+H
Temperature class for Ex “db”: T2
The maximum surface temperature for Ex “tb”: T300°C
Degree of protection of enclosure: IP66
T2 Gb, Ex tb IIIC T300°C Db
2
<2.Specications>
NAME PLATE
MODEL : Specified model code
SUFFIX : Specified suffix code
STYLE : Style code
AMB. TEMP : Ambient temperature
NO. : Serial No. and year of production*
Yokogawa Electric Corporation : The manufacturer name
Tokyo 180-8750 JAPAN : The manufacturer address*
2-3
1
2
No. IECEx KEM 06.0006X
Ex db IIB+H2 T2 Gb,
Ex tb IIIC T300°C Db
*1: The third to seventh gure from the last shows the year of production.
*2: “180-8750” is a zip code which represents the following address.
The country of origin
e.g. 27D327560 2005.02
The year of production
2-9-32 Nakacho, Musashino-shi, Tokyo Japan
Safety, EMC, and RoHS conformity standards
Installation altitude based on IEC 61010: 2000 m or less
Category based on IEC 61010: II (Note)
Pollution degree based on IEC 61010: 2 (Note)
Note: Installation category, called over-voltage category, species impulse withstand voltage.
Category II is for electrical equipment.Pollution degree indicates the degree of existence of solid,
liquid, gas or other inclusions which may reduce dielectric strength. Degree 2 is the normal indoor
environment.
Safety: Conforms to EN 61010-1, EN 61010-2-030, CAN/CSA-C22.2 No. 61010.1 certied,
UL Std. No. 61010-1 certied
EMC: Conforms to EN 61326-1*, Class A, Table 2,
EN 61326-2-3, EN 61000-3-2
*: Inuence of immunity environment (Criteria A ): ±20% of F. S.
EMC Regulatory Arrangement in Australia and New Zealand (RCM) EN61326-1 Class A
Korea Electromagnetic Conformity Standard
RoHS: EN 50581
CAUTION
This instrument is a Class A product, and it is designed for use in the industrial environment.
Please use this instrument in the industrial environment only.
Repeatability: ± 0.5% Maximum value of set range; Range from 0 to 5 vol%O
less than 0 to 25 vol%O2 range
± 1 % Maximum value of set range; Range from 0 to 25 vol%O2 or more and
up to 0 to 100 vol%O
.
2
or more and
2
IM 11M13A01-04E
2-4
<2. Specications>
Linearity: (Excluding standard gas tolerance)
(Use oxygen of known concentration (with in the measuring range) as the
zero and span calibration gases.)
± 1% Maximum value of set range; Range from 0 to 5 vol%O2 to 0 to 25
vol%O2. (Sample gas pressure: within ± 4.9 kPa)
± 3% Maximum value of set range; Range from 0 to 25 vol%O2 or more and
less than 0 to 50 vol%O2. (Sample gas pressure: within ± 0.49 kPa)
± 5% Maximum value of set range; Range from 0 to 50 vol%O2 to 0 to 100
vol%O2. (Sample gas pressure: within ± 0.49 kPa)
Drift: (Excluding the rst two weeks in use)
Both zero and span ± 2% Maximum value of range set/month
Response Time: Response of 90% within 5 seconds. (Measured after gas is introduced from
calibration gas inlet and analog output starts changing.)
2.1.2 ZR202S Integrated type Explosion-proof Zirconia Oxygen Analyzer
Can be operated in the eld without opening the cover using optical switches.
Display: 6-digit LCD
Switch: Three optical switches
Output Signal: 4 to 20 mA DC, one point (maximum load resistance 550 Ω)
Digital Communication (HART): 250 to 550 Ω, depending on quantity of eld devices connected to
the loop (multi-drop mode).
Note: HART is a registered trademark of the HART Communication Foundation.
Contact Output Signal: Two points (one is fail-safe, normally open)
Contact Input Signal: Two points
Sample Gas Temperature: 0 to 700°C
It is necessary to mount the cell using Inconel cell-bolts when the temperature
measures more than 600°C.
High-temperature service ― greater than 700°C ― is not available.
A ame arrestor may corrode if sample gas contains the following corrosive gases
under 380°C or over.
Greater than 5000 ppm SO
2
Greater than 1000 ppm NO
Greater than 50 ppm HCl
Sample Gas Pressure: -5 to +5 kPa
No pressure uctuation in the furnace should be allowed.
Oxygen concentration of sample gas:
For explosion-proof use, not more than that found in normal air, typically 21 vol%
Probe Length: 0.4, 0.7, 1.0, 1.5, 2.0 m
Probe Material: 316 SS (JIS)
Ambient Temperature: -20 to +55°C (- 5 to +70°C on the case surface)
Storage Temperature: -30 to +70°C
Ambient Humidity: 0 to 95%RH (non-condensing)
Power Supply Voltage: Ratings; 100 to 240 V AC, Acceptable range; 85 to 264 V AC
Power Supply Frequency:
Power Consumption: Max. 300 W, approx. 100 W for ordinary use.
Reference Gas System: Instrument Air
IM 11M13A01-04E
Ratings; 50/60 Hz, Acceptable range; 45 to 66 Hz
<2.Specications>
Instrument Air System:
Pressure; 50 kPa + the pressure inside the furnace
150 kPa + the pressure inside the furnace with automatic calibration unit or
check valve. (It is recommended to use air which has been dehumidied by
cooling to dew point -20°C or less, and dust or oil mist are removed.)
Consumption; Approx. 1.5 Nl/min
Oxygen concentration of calibration gas:
For explosion-proof use, not more than that found in normal air, typically 21 vol%
Wetted Material: 316 SS (JIS), Zirconia, 304 SS (JIS) (ange),
Hastelloy B, (Inconel 600, 601)
Construction: Heater and thermocouple replaceable construction. Equivalent to NEMA 4X/IP66
(Achieved when pipes are installed at calibration gas and reference gas inlets and
exhaust pipe is installed so that reference gas can be exhausted to clean
atmosphere. Excluding probe top.)
(Achieved when the cable entry is completely sealed with a cable gland.)
Gas Connection: Rc 1/4 or 1/4 NPT(F)
Wiring Connection: ATEX: M20 by 1.5 mm, 1/2 NPT select one type (4 pieces)
FM: 1/2 NPT (4 pieces)
CSA: 1/2 NPT (4 pieces)
IECEx: M20 by 1.5 mm, 1/2 NPT select one type (4 pieces)
2-5
Installation: Flange mounting
Probe Mounting Angle: Horizontal to vertically downward.
Case: Aluminum alloy
Finish: Polyurethane corrosion-resistance coating
Weight: Insertion length of 0.4m: approx. 15 kg (ANSI 150 4)
Functions:
Display Function: Displays values of the measured oxygen concentration, etc.
Alarm, Error Display: Displays alarms such as “AL-06” or errors such as “Err-01” when any such
Calibration Functions:
Insertion length of 1.0m: approx. 17 kg (ANSI 150 4)
Insertion length of 1.5m: approx. 19 kg (ANSI 150 4)
Insertion length of 2.0m: approx. 21 kg (ANSI 150 4)
status occurs.
Automatic Calibration; Requires the Automatic Calibration Unit. It calibrates
automatically at specied intervals.
Semi-automatic Calibration; Requires the Automatic Calibration Unit. Input
calibration start signal by optical switch or contact, then it calibrates
automatically afterwards.
Manual Calibration; Calibration with opening/closing the valve of calibration
gas in operation interactively with the optical switch.
Maintenance Functions: Can operate updated data settings in daily operation and checking.
Display data settings, calibration data settings, test settings (current output
loop check, contact input/output check).
Setup Functions: Initial settings suit for the plant conditions when installing the analyzer.
Current output data settings, alarm data settings, contact data settings, other
settings.
IM 11M13A01-04E
2-6
<2. Specications>
Display and setting content:
Display Related Items: Oxygen concentration (vol%O2), current output value (mA), air ratio,
moisture quantify (in hot gases) (vol%H2O), cell temperature (°C ), thermocouple
reference junction temperature (°C ), maximum/minimum/average oxygen
concentration (vol%O2), cell e.m.f. (mV), cell internal resistance (Ω), cell condition (in
four grades), heater on-time rate (%), calibration record (ten times), time (year/month/
day/hour/minute)
Calibration Setting Items: Span gas concentration (vol%O
), zero gas concentration (vol%O2),
2
calibration mode (automatic, semi-automatic, manual), calibration type and method
(zero-span calibration, zero calibration only, span calibration only), stabilization time
(min.sec), calibration time (min.sec), calibration period (day/hour), starting time (year/
month/day/hour/minute)
Output Related Items: Analog output/output mode selection, output conditions when warming-up/
maintenance/calibrating/abnormal, 4 mA/20 mA point oxygen concentration (vol%
), time constant.
O
2
Alarm Related Items: Oxygen concentration high alarm/high-high alarm limit values (vol%O
Contact Related Items: Selection of contact input 1 and 2, selection of contact output 1 and 2
(abnormal, high-high alarm, high alarm, low alarm, low-low alarm, maintenance,
calibrating, range switching, warming-up, calibration gas pressure decrease,
ameout gas detection (answer-back of contact input)
Converter Output: One mA analog output (4 to 20 mA DC (maximum load resistance of
550 Ω)) with mA digital output (HART) (minimum load resistance of
250 Ω).
Range; Any setting between 0 to 5 through 0 to 100 vol%O
in 1 vol%O2, or partial
2
range is available (Maximum range value/minimum range value 1.3 or more)
For the log output, the minimum range value is xed at 0.1 vol%O2.
4 to 20 mA DC linear or log can be selected. Input/output isolation.
Output damping: 0 to 255 seconds. Hold/non-hold selection, preset value setting possible with hold.
Contact Output: Two points, contact capacity 30 V DC 3 A, 250 V AC 3 A (resistive load)
Contact Input: Two points, voltage-free contacts
Self-diagnosis: Abnormal cell, abnormal cell temperature (low/high), abnormal calibration, A/D
IM 11M13A01-04E
One of the output points can be selected to either normally energized or normally
de-energized status.
Delayed functions (0 to 255 seconds) and hysteresis function (0 to 9.9 vol%O
) can
2
be added to high/low alarms.
The following functions are programmable for contact outputs.
(1) Abnormal, (2) High-high alarm, (3) High alarm, (4) Low-low alarm, (5) Low alarm,
(6) Maintenance, (7) Calibration, (8) Range switching answer-back, (9) Warm-up,
(10) Calibration gas pressure decrease (answer-back of contact input), (11) Flameout
gas detection (answer-back of contact input).
Contact output 2 is set to normally operated, xed error status.
The following functions are programmable for contact inputs.
(1) Calibration gas pressure decrease alarm, (2) Range switching (switched range is
xed), (3) External calibration start, (4) Process alarm (if this signal is received, the
heater power turns off)
converter abnormal, digital circuit abnormal
<2.Specications>
Calibration: Method; zero/span calibration
Calibration mode; Automatic, semi-automatic and manual (All are operated using optical
switches).
Either zero or span can be skipped.
Zero calibration gas concentration setting range;
0.3 to 100 vol%O2 (in 0.01 vol%O2).
Span calibration gas concentration setting range;
4.5 to 100 vol%O2 (in 0.01 vol%O2).
Use nitrogen-balanced mixed gas containing 0 to 10 vol%O2 scale of oxygen for standard
zero gas and 80 to 100 vol%O2 scale of oxygen for standard span gas.
Calibration period; Date/time setting: maximum 255 days/23 hours
*1 The thickness of the ange depends on its dimensions.
*2 Inconel probe bolts and U shape pipe are used. Use this option for high temperature use (ranging from 600 to700°C).
*3 Specify either /CV or /SV option code.
*4 Specify either /SCT or /PT option code.
*5 No need to specify the option codes, /CV and /SV, since the check valves are provided with the Automatic Calibration Unit.
*6 Sun shield hood is still effective even if scratched. Hood is necessary for outdoor installation out of sun shield roof.
*7 Recommended if sample gas contains corrosive gas like chlorine.
*8 Piping for reference gas must be installed to supply reference gas constantly at a specied ow rate.
*9 When selecting code -B (FM certied explosion-proof) or -C (CSA certied explosion-proof), select code -T(1/2 NPT).
*10 Conrm inside diameter of pipe attached to customer’s ange in case that -A or -E is selected.
*11 The cable entry devices (cable glands etc.) and blind plugs shall be in type of protection Ex “db” or Ex “tb”, suitable for the
*12 Output signal limits: 3.8 to 20.5 mA. Specify either /C2 or /C3 option code.
*13 When using ZR202S as CE marking compliance product, select -A (ATEX certied ameproof).
*14 "-Q" is the explosion-proof type of EAC with Pattern Approval for Russia. "-R" is the explosion-proof type of EAC for
-A
-B
-C
-D
-Q
-R
-070
-100
-150
-200
-C
-A
-B
-C
-E
-F
-G
-K
-L
-M
-P
-R
-S
-W
-A
-B
NAMUR NE43 compliant
-T
-T
Valves
Tag plates
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
- - - - - - - - - -
/C Inconel bolt (*2)
/CV
/SV
/HHood (*6)
/SCT
/PT
/C2
/C3
ATEX certied ameproof (*11)
FM certied explosion-proof
CSA certied explosion-proof
IECEx certied ameproof (*11)
EAC with PA certied explosion-proof (*14)
EAC certied explosion-proof (*14)
0.4 m
0.7 m
1.0 m
1.5 m
2.0 m
SUS316
Stainless steel with Inconel calibration gas tube (*7)
ANSI Class 150 2 RF SUS304 (JIS) (*10)
ANSI Class 150 3 RF SUS304 (JIS)
ANSI Class 150 4 RF SUS304 (JIS)
DIN PN10 DN50 A SUS304 (JIS) (*10)
DIN PN10 DN80 A SUS304 (JIS)
DIN PN10 DN100 A SUS304 (JIS)
JIS 5K 65 FF SUS304 (JIS)
JIS 10K 65 FF SUS304 (JIS)
JIS 10K 80 FF SUS304 (JIS)
JIS 10K 100 FF SUS304 (JIS)
JPI Class 150 4 RF SUS304 (JIS)
JPI Class 150 3 RF SUS304 (JIS)
Westinghouse
Not required
Horizontal mounting (*5)
Vertical mounting (*5)
Rc 1/4
1/4 NPT (Female)
M20x1.5 mm
1/2NPT (*9)
Check valve (*3)
Stop valve (*3)
Stainless steel tag plate (*4)
Printed tag plate (*4)
Failure alarm down-scale:
Output status at CPU failure and hardware error is 3.6 mA or less
(*12)
Failure alarm up-scale:
Output status at CPU failure and hardware error is 21.0 mA or
more (*12)
conditions of use and correctly installed. They shall provide a degree of ingress protection of at least IP66.
ZR202S Integrated type Explosion-proof Zirconia Oxygen Analyzers
±2
t
±3
50.8
Ø
±3
52
Ø
tolerance (mm)L (m)
0.4
0.7
1.0
1.5
2.0
±5
±7
±8
±10
±12
256.5
FLANGE
Rc1/4 or 1/4 NPT (F)
Reference Gas Inlet
±3
156
±3
49
±3
87
Ø
49
ر3123
±2
±2
48.5
2-9
Unit : mm
±3
170
±3
122
Flange
ANSI Class 150 2 RF 304 SS (JIS)
ANSI Class 150 3 RF304 SS (JIS)
ANSI Class 150 4 RF 304 SS (JIS)
DIN PN10 DN50 304 SS (JIS)
DIN PN10 DN80 304 SS (JIS)
DIN PN10 DN100 304 SS (JIS)
JIS 5K 65 FF 304 SS (JIS)
JIS 10K 65 FF 304 SS (JIS)
JIS 10K 80 FF 304 SS (JIS)
JIS 10K 100 FF 304 SS (JIS)
JPI Class 150 4 RF 304 SS (JIS)
JPI Class 150 3 RF 304 SS (JIS)
Westinghouse
With sun shield hood (option code /H)
±2
Rc1/4 or 1/4 NPT (F)
Calibration Gas Inlet
Rc1/4 or 1/4 NPT (F)
Reference Gas Outlet
ABC
152.4
120.6
190.5
152.4
228.6
190.5
165
125
200
160
220
180
155
130
175
140
185
150
210
175
229
190.5
190
152.4
155
± 4± 3
274
25
4 - Ø19
Ø
19
4 -
Ø
19
8 -
Ø
18
4 -
Ø
18
8 -
Ø
18
8 -
Ø
15
4 -
Ø
19
4 8 -
Ø
19
Ø
19
8 8 -
Ø
19
Ø
19
4 -
Ø
t
19
24
24
18
20
20
14
18
18
18
24
24
±3
125
4-M20 ×1.5 or 4-1/2 NPT
Cable Connection Port (Female)
n-Ø C
FLANGE
150
Ø
Ø
F2-1E.ai
B
A
± 3
150
F2-2E.ai
Material of hood : Aluminum
IM 11M13A01-04E
2-10
<2. Specications>
• External Dimensions
With Automatic Calibration Unit (Horizontal Mount)
156 ±3
348 ±3
AUTOMATIC CALIBRATION UNIT
DisplayTerminal box
244
Unit : mm
258
MAX44214
Span gas inlet
Rc1/4 or 1/4NPT(Female)
HORIZONTAL INSTALL
With Automatic Calibration Unit (Vertical Mount)
AUTOMATIC CALIBRATION UNIT
160
45
●●
166.5
166.5
40
66.540
Zero gas inlet
Rc1/4 or 1/4NPT(Female)
Reference gas inlet
Rc1/4 or 1/4NPT(Female)
Reference gas inlet
Rc1/4 or 1/4NPT(Female)
60
180
• Standard Accessories
FuseA1113EF13.15 A
Allen wrenchL9827AB1For lock screw
IM 11M13A01-04E
40
66.540
MAX44
Span gas inlet
Rc1/4 or 1/4NPT(Female)
●●
VERTICAL INSTALL
ItemParts. No.Q'tyDescription
Zero gas inlet
Rc1/4 or 1/4NPT(Female)
F2-3E.ai
<2.Specications>
2.1.3 ZO21R Probe Protector
Used when sample gas ow velocity is approx. 10 m/sec or more and dust particles wears the
detector in cases such as pulverized coal boiler of uidized bed furnace (or burner) to protect the
detector from wearing by dust particles.
Insertion Length: 1.05, 1.55, 2.05 m.
Flange: JIS 5K 65A FF equivalent. ANSI Class 150 4 FF (without serration) equivalent .
However, ange thickness is different.
Material: 316 SS (JIS), 304 SS (JIS) (Flange)
Weight: 1.05 m; Approx. 6/10 kg (JIS/ANSI),
1.55 m; Approx. 9/13 kg (JIS/ANSI),
2.05 m; Approx. 12/16 kg (JIS/ANSI)
Installation: Bolts, nuts, and washers are provided for detector, probe protector and process-side
Air pressure ;
without check valve ; sample gas pressure + approx.50 kPaG
with check valve ; sample gas pressure + approx.150 kPaG
Instrument air
Approx. 1.5 L/min.
F2-5E.ai
IM 11M13A01-04E
2-14
<2. Specications>
2.3 ZO21S Standard Gas Unit
CAUTION
Standard Gas Unit (Model ZO21S) must not be located in hazardous area.
This is a handy unit to supply zero gas and span gas to the detector as calibration gas. It is used in
combination with the detector only during calibration.
The ZO21S does not conform to CE marking.
Standard Specications
Function:
Sealed Zero Gas Cylinders (6 provided): E7050BA
Capacity: 1 l
Filled pressure: Approx. 686 kPaG (at 35°C)
Composition: 0.95 to 1.0 vol%O
Power Supply: 100, 110, 115, 200, 220, 240 V AC ±10%, 50/60 Hz
Power Consumption: Max. 5 VA
Case material: SPCC (cold rolled steel sheet)
Paint Color: Mainframe; Munsell 2.0 GY3.1/0.5 equivalent
Piping: Ø6 х Ø4 mm exible tube connection
Weight: Approx. 3 kg
Model and Codes
ModelSufx codeOption codeDescription
ZO21S - - - - - - - - - - - - - - - - - - - - - - - - Standard gas unit
Portable unit for calibration gas supply consisting of span gas (air) pump, zero
gas cylinder with sealed inlet, ow rate checker and ow rate needle valve.
2 + N2 balance
Cover; Munsell 2.8 GY6.4/0.9 equivalent
-2
-3
-4
-5
-7
-8
-J
-E
- - - - - - - - - - - - -
- - - - - - - - - - - - -
- - - - - - - - - - - - -
- - - - - - - - - - - - -
- - - - - - - - - - - - -
- - - - - - - - - - - - -
- - - - - - - - - - - - -
- - - - - - - - - - - - -
200 V AC 50/60 Hz
220 V AC 50/60 Hz
240 V AC 50/60 Hz
100 V AC 50/60 Hz
110 V AC 50/60 Hz
115 V AC 50/60 Hz
Japanese version
English version
External Dimensions
Zero gas cylinder (6 cylinder): E7050BA
IM 11M13A01-04E
1600
354
228
92
253
Unit: mm
Flow checker
Span gas valve
Zero gas valve
Gas outlet
F2-6E.ai
<2.Specications>
2.4 Other Equipment
2.4.1 Stop Valve (L9852CB, G7016XH)
This valve mounted on the calibration gas line in the system using ZA8F ow setting unit for manual
calibration.
Standard Specications
Material: 316 SS (JIS)
Connection: Rc 1/4 or 1/4 FNPT
Weight: Approx. 200 g
Part No.Description
L9852CBJoint: Rc 1/4, Material: 316 SS (JIS)
G7016XHJoint: 1/4 FNPT, Material: 316 SS (JIS)
Unit : mm
2-15
Analyzer
Approx. 100
Nipple
G7209XA 2-Rc1/4
K9470ZN 2-1/4NPT
Ø48
40
2.4.2 Check Valve (K9292DN, K9292DS)
This valve is mounted on the calibration gas line (directly connected to the detector).
This valve prevents the sample gas from entering the calibration gas line. Although it functions as
a stop valve, operation is easier than a stop valve as it does not require opening/closing at each
calibration.
Screw a check valve, instead of a stop valve into the calibration gas inlet of the detector.
Standard Specications
Material: 304 SS (JIS)
58
(Full open length)
L9852CB 2-Rc1/4
G7016XH 2-1/4NPT
F2-7.1E.ai
Connection: Rc1/4 or 1/4 FNPT
Pressure: 150 kPaG or more and 350 kPaG or less
Weight: Approx. 90 g
Part No.Description
K9292DNJoint: Rc 1/4, Material: 304 SS (JIS)
K9292DSJoint: 1/4 FNPT, Material: 304 SS (JIS)
*1 Sufx code of length should be selected as same as ZR202S installed.
(Note) The heater is made of ceramic, do not drop or subject it to pressure stress.
-070
-100
-150
-200
-N
- - - - - - - - - - -
- - - - - - - - - - -
- - - - - - - - - - -
- - - - - - - - - - -
- - - - - - - - - - -
- - - - - - - - - - -
- - - - - - - - - - -
* Outlet
Primary safety valve
Part No.
G7013XF
G7014XF
0.4 m
0.7 m
1 m
1.5 m
2 m
with Jig
None
Stop valve
Approx. 174
* Outlet
Rc1/4
1/4 NPT female with adapter
W22 (Right hand screw)
Secondary
safety valve
Approx. 82
F2-10E.ai
Inlet
IM 11M13A01-04E
2-18
<2. Specications>
External Dimensions
Ø 45
Jig for change
(K9470BX)
Model & Codes
ZR202A-040
ZR202A-070
ZR202A-100
ZR202A-150
ZR202A-200
Ø21.7
552
852
1152
1652
2152
L
K9470BX
30
Weight (kg)
Approx. 0.8
Approx. 1.2
Approx. 1.6
Approx. 2.2
Approx. 2.8
Unit : mm
L±12
F2-11E.ai
IM 11M13A01-04E
<3. Installation>
3. Installation
This chapter describes installation of the following equipment:
3.1 Model ZR202S Integrated type Explosion-proof Zirconia Oxygen Analyzer
3.2 Model ZA8F Flow Setting Unit
3.3 Case Assembly (E7044KF) for Calibration gas Cylinder
3.1 Installation of ZR202S Zirconia Oxygen Analyzer
3.1.1 Installation Location
The following should be taken into consideration when installing the analyzer:
(1) Easy and safe access to the analyzer for checking and maintenance work.
(2) Ambient temperature of not more than 55°C, and the terminal box should not be affected by
radiant heat.
(3) A clean environment without any corrosive gases.
3-1
(4) No vibration.
(5) The sample gas satises the specications described in Chapter 2.
(6) No sample gas pressure uctuations.
CAUTION
• The ambient temperature of the ZR202S Integrated type Explosion-proof Zirconia Oxygen
Analyzer should be between - 20°C and 55°C.
IM 11M13A01-04E
3-2
<3. Installation>
3.1.2 ATEX Flameproof Type
ZR202S–A Analyzer for use in hazardous area:
Note 1: Applicable Standard: EN 60079-0: 2012+A11: 2013, EN 60079-1: 2014,
Certicate Number: KEMA 04ATEX2156 X
The symbol “X” placed after certicate number indicates that the equipment is subjected to
Type of protection: Ex db IIB+H2 T2 Gb, Ex tb IIIC T300°C Db
Equipmant Group: II
Category: 2GD
Temperature class for Ex “db”: T2
The maximum surface temperature for Ex “tb”: T300°C
Degree of protection of enclosure: IP66
Note 2: Wiring
• All wiring shall comply with local installation requirement.
Note 3: Operation
EN 60079-31: 2014
special conditions for safe use. Refer to Note 6.
• Keep to “WARNING” on the Analyzer.
WARNING: DO NOT OPEN WHEN AN EXPLOSIVE GAS ATMOSPHERE IS PRESENT
POTENTIAL ELECTROSTATIC CHARGING HAZARD-READ USER’S
MANUAL (IM11M13A01-04)
FOR INSTALLATION AND SAFE USE, READ IM11M13A01-04
USE AT LEAST 80°C HEAT RESISTANT CABLES & CABLE GLANDS
• Take care not to generate mechanical sparking when accessing to the analyzer and peripheral
devices in hazardous area.
Note 4: Maintenance and Repair
• The analyzer modication or parts replacement by other than authorized representative of
Yokogawa Electric Corporation is prohibited and will void the certication.
Note 5: Cable Entry
• The threaded type of cable entry is marked beside the cable entry according to the following
markings.
Threaded type : Marking
M20x1.5 : M
1/2 NPT : N
• The cable entry devices (cable glands etc.) and blind plugs shall be in type of protection Ex “db” or
Ex “tb”, suitable for the conditions of use and correctly installed. They shall provide a degree of
ingress protection of at least IP66.
Note 6: Special conditions for safe use
IM 11M13A01-04E
Electrostatic charge may cause an explosion hazard. Avoid any actions that cause the generation of
electrostatic charge, such as rubbing with a dry cloth.
If it is mounted in the area where the use of Ex “tb” apparatus is required, it shall be installed in such
a way that the risk from electrostatic discharges and propagating brush discharges caused by rapid
ow of dust is avoided.
<3. Installation>
Note 7: Special fastener
Hexagon socket head cap screws below are special fastener according to EN60079-0: 2012+A11:
2013 (see the gure below). Material property classes of them are A2-50 or better.
The symbol “X” placed after certicate number indicates that the equipment is subjected to
special conditions for safe use. Refer to Note 6.
Type of protection: Ex db IIB + H2 Gb,
Ex tb IIIC T300ºC Db
Temperature class for Ex “db”: T2
The maximum surface temperature for Ex “tb”: T300ºC
Degree of protection of enclosure: IP66
Note 2: Wiring
• All wiring shall comply with local installation requirement.
Note 3: Operation
• Keep to “WARNING” on the Analyzer.
WARNING: DO NOT OPEN WHEN AN EXPLOSIVE GAS ATMOSPHERE IS PRESENT
POTENTIAL ELECTROSTATIC CHARGING HAZARD-READ USER’S
MANUAL (IM11M13A01-04)
FOR INSTALLATION AND SAFE USE, READ IM11M13A01-04
USE AT LEAST 80ºC HEAT RESISTANT CABLES & CABLE GLANDS
• Take care not to generate mechanical sparking when accessing to the analyzer and peripheral
devices in hazardous area.
Note 4: Maintenance and Repair
• The analyzer modication or parts replacement by other than authorized representative of
Yokogawa Electric Corporation is prohibited and will void the certication.
IM 11M13A01-04E
3-6
<3. Installation>
Note 5: Cable Entry
• The threaded type of cable entry is marked beside the cable entry according to the following
markings.
Threaded type : Marking
M20x1.5 : M
1/2 NPT : N
• In case of ANSI 1/2 NPT plug, ANSI hexagonal wrench should be applied to screw in.
• The cable entry devices (cable glands etc.) and blind plugs shall be in type of protection Ex “db” or
Ex “tb”, suitable for the conditions of use and correctly installed. They shall provide a degree of
ingress protection of at least IP66.
Note 6: Special conditions for safe use
Electrostatic charge may cause an explosion hazard. Avoid any actions that cause the generation of
electrostatic charge, such as rubbing with a dry cloth.
If it is mounted in the area where the use of Ex “tb” apparatus is required, it shall be installed in such
a way that the risk from electrostatic discharges and propagating brush discharges caused by rapid
ow of dust is avoided.
Note 7: Special fastener
Hexagon socket head cap screws below are special fastener according to IEC 60079-0: 2011 (see
the gure below). Material property classes of them are A2-50 or better.
Special fastener
Figure 3.4 Special fastener
IM 11M13A01-04E
<3. Installation>
3.1.6 Probe (Detector) Insertion Hole
CAUTION
• The outside dimension of the probe may vary depending on its options. Use a pipe that is large
enough for the probe. Refer to Subsection 2.1.2 for the dimensions.
• If the probe is mounted horizontally, the calibration gas inlet and reference gas inlet should face
downwards.
• The sensor (zirconia cell) at the probe tip may deteriorate due to thermal shock if water drops are
allowed to fall on it, as it is always at high temperature.
(1) Do not mount the probe with the tip higher than the probe base.
(2) The probe should be mounted at right angles to the sample gas ow or the probe tip should point
downstream.
3-7
(vertical)
100 mm
Bounds of the probe
insertion hole area
Flange matches
the detector size
(horizontal)
*1
100 mm
Figure 3.5 Example of forming probe insertion hole
3.1.7 Installation of the Probe (Detector)
CAUTION
*1
Type Outside diameter of probe
Standard 52 mm in diameter
With probe protector 60.5 mm in diameter
Four-hole flange Eight-hole flange
F3-3E.ai
• The cell (sensor) at the tip of the probe is made of ceramic (zirconia). Do not drop the probe, as
impact will damage it.
• A gasket should be used between the anges to prevent gas leakage. The gasket material
should be heatproof and corrosion-proof, suited to the characteristics of the sample gas.
The following should be taken into consideration when mounting the probe:
(1) Make sure that the cell mounting screws (four bolts) at the probe tip are not loose.
(2) Where the probe is mounted horizontally, the calibration gas inlet and the reference gas inlet
should face downward.
IM 11M13A01-04E
3-8
<3. Installation>
3.1.8 Installation of the Probe Protector (ZO21R)
<Analyzer with a probe protector (Model ZO21R-L-- *B for dust wear protect>
The probe of the analyzer is used with a probe protector to prevent the sensor from being worn by
dust particles when there is a high concentration of dust and gas ow exceeds 10 m/s (ne-carbon
boiler or uid bed furnace).
(1) Put the gasket that is provided by user between the anges, and mount the probe protector in
the probe insertion hole. The probe protector should be installed so that the notch comes to the
downstream of the sample gas ow.
(2) Make sure that the sensor assembly mounting screws (four bolts) at the probe tip are not loose.
(3) When the probe is mounted horizontally, the calibration gas and reference gas inlet should face
downward.
1050, 1550, 2050
Direction of the sample gas flow
Probe top
Mount the protector so that the notch
is on the downstream side of gas flow.
Gasket (t1.5)
Figure 3.6 Mounting of probe with a probe protector (Dust wear protect)
3.2 Installation of ZA8F Flow Setting Unit
3.2.1 Installation Location
The following should be taken into consideration:
(1) Easy access to the unit for checking and maintenance work.
(2) Near to the analyzer
(3) No corrosive gas.
Unit: mm
Calibration gas inlet
Reference gas inlet
F3-4E.ai
IM 11M13A01-04E
(4) An ambient temperature of not more than 55°C and little changes of temperature.
(5) No vibration.
(6) Little exposure to rays of the sun or rain.
<3. Installation>
3.2.2 Mounting of ZA8F Flow Setting Unit
The ow setting unit can be mounted either on a pipe (nominal JIS 50A) or on a wall. It should be
positioned vertically so that the owmeter works correctly.
<Pipe Mounting>
(1) Prepare a vertical pipe of sufcient strength (nominal JIS 50A: O.D. 60.5 mm) for mounting the
ow setting unit. (The unit weighs approximately 2 to 3.5 kg.)
(2) Mount the ow setting unit on the pipe by tightening the nuts with the U-bolt so that the metal
tting is rmly attached to the pipe.
3-9
F3.5E.ai
Figure 3.7 Pipe Mounting
<Wall Mounting>
(1) Make a hole in the wall as illustrated in Figure 3.8.
Unit: mm
223
140
4 - Ø6 hole, or M5 screw
F3-6E.ai
Figure 3.8 Mounting holes
(2) Mount the ow setting unit. Remove the pipe mounting parts from the mount ttings of the ow
setting unit and attach the unit securely on the wall with four screws.
Figure 3.9 Wall mounting
F3-7E.ai
IM 11M13A01-04E
3-10
<3. Installation>
3.3 Insulation Resistance Test
Even if the testing voltage is not so great that it causes dielectric breakdown, testing may cause
deterioration in insulation and a possible safety hazard. Therefore, conduct this test only when it is
necessary.
The applied voltage for this test shall be 500 V DC or less. The voltage shall be applied for as short a
time as practicable to conrm that insulation resistance is 20 MΩ or more.
Remove wiring from the analyzer.
1. Remove the jumper plate located between terminal G and the protective grounding terminal.
2. Connect crossover wiring between L and N.
3. Connect an insulation resistance tester (with its power OFF). Connect (+) terminal to the
crossover wiring, and (-) terminal to ground.
4. Turn the insulation resistance tester ON and measure the insulation resistance.
5. After testing, remove the tester and connect a 100 kΩ resistance between the crossover wiring
and ground, to discharge.
6. Testing between the heater terminal and ground, contact output terminal and ground, analog
output/input terminal and the ground can be conducted in the same manner.
7. Although contact input terminals are isolated, insulation resistance test cannot be conducted
because the breakdown voltage of the surge-preventing arrestor between the terminal and
ground is low.
8. After conducting all the tests, replace the jumper plate as it was.
Contact input 1
Insulation
resistance
tester
+-
1
DI-1
8
FG
Contact input 2
2
DI-2
9
AO
(+)
Crossover wiring
3
DI-C4DO-15DO-16DO-27DO-2
10
AO
(-)
11
L
Crossover wiring
12
N
13
G
Remove
jumper
plate
14
FG
Figure 3.10 Insulation Resistance Test
IM 11M13A01-04E
Insulation
resistance
tester
Insulation
+-
resistance
tester
+-
F3-8E.ai
<4. Piping>
CAUTION
4. Piping
This chapter describes piping procedures in the two typical system congurations for EXAxt ZR
Integrated type Explosion-proof Zirconia Oxygen Analyzer.
• Ensure that each check valve, stop valve and joints used for piping are not leaking.
Especially, if there is any leakage at piping and joints for the calibration gas, it may cause
clogging of the piping or incorrect calibration.
• Be sure to conduct leakage test after setting the piping.
• Basically, apply instrument air (dehumidied by cooling to the dew point -20°C or lower, and
removing any dust, oil mist and the like) for the reference gas.
Do not loosen or remove any Flame Arrestor of gas inlet/outlet during piping.
The detector modication or parts replacement by other than authorized representative of Yokogawa
Electric Corporation is prohibited and will void ATEX Certication, FM Approval, CSA Certication and
IECEx Certication.
4-1
Flame Arrestor
F4-0E.ai
IM 11M13A01-04E3rd Edition : Dec.15,2014-00
4-2
<4. Piping>
4.1 Piping for System 1
The piping in System 1 is illustrated in Figure 4.1
ZR202S Integrated type Explosion-proof
Zirconia Oxygen Analyzer
Stop valve
or
Check valve
Reference gas
Calibration gas
ZA8F
Needle
valve
Flowmeter
Flow Setting Unit
Hazardous Area
Air Set
Instrument air
Span gas
Pressure
reducing
valve
Calibration gas
unit case
Zero gas
cylinder
Non-hazardous Area
~
Figure 4.1 Piping for System 1
Piping in System 1 is as follows:
• Mount the check valve or the stop valve through a nipple to the calibration gas inlet of the
equipment.
100 to 240 V AC
Contact input
Analog output, contact output
Digital output (HART)
F4-1E.ai
4.1.1 Piping Parts for System 1
Referring to Table 4.1, check that the parts required for your system are ready.
Table 4.1 Piping Parts
Equipment Piping location Parts NameDescription
Integrated type
Explosion-proof
Zirconia
Oxygen Analyzer
Note: Parts with marking * are used when required. General parts can be found on the local market.
Calibration gas inlet Stop valve or check valve Stop valve (L9852CB or G7016XH)
recommended by YOKOGAWA
Check valve (K9292DN or K9292DS)
provided by YOKOGAWA
Nipple * R1/4 or 1/4 NPTGeneral parts
Zero gas cylinderUser’s scope
Pressure reducing valve(G7013XF or G7014XF) recommended by
YOKOGAWA
Joint for tube connection * R1/4 or 1/4 NPTGeneral parts
Reference gas inlet Air set(G7003XF/ K9473XK or G7004XF/ K9473XG)
recommended by YOKOGAWA
Joint for tube connection * R1/4 or 1/4 NPTGeneral parts
IM 11M13A01-04E3rd Edition : Dec.15,2014-00
<4. Piping>
4.1.2 Piping for the Calibration Gas Inlet
This piping is to be installed between the zero gas cylinder and the ZA8F ow setting unit, and
between the ZA8F ow setting unit and the ZR202S analyzer.
The cylinder should be placed in a calibration gas unit case or the like to avoid any direct sunlight or
radiant heat so that the gas cylinder temperature may not exceed 40°C. Mount the pressure reducing
valve (recommended by YOKOGAWA) on the cylinder.
Mount the stop valve or the check valve (recommended by YOKOGAWA) through the nipple (found
on the local market) at the calibration gas inlet of the equipment as illustrated in Figure 4.2. (The stop
valve or the check valve may have been mounted on the equipment when shipped.)
Connect the ZA8F ow setting unit and the ZR202S analyzer to a 6 mm (O.D.) x 4 mm (I.D.) (or
nominal size 1/4 inches) or larger stainless steel pipe.
Piping for the reference gas outlet
6mm (O.D.) by 4mm (I.D.)
Piping for the reference gas inlet
6mm (O.D.) by 4mm (I.D.)
Stainless steel pipe
Piping for the calibration gas inlet
6mm (O.D.) by 4mm (I.D.)
Stainless steel pipe
Stop valve or check valve
Stainless steel pipe
4-3
Figure 4.2 Piping for the Calibration Gas Inlet
4.1.3 Piping for the Reference Gas Inlet
Reference gas piping is required between the air source (instrument air) and the ZA8F ow setting
unit, and between the ow setting unit and the ZR202S analyzer.
Insert the air set next to the ow setting unit in the piping between the air source and the ow setting
unit.
Use a 6 mm (O.D.) x 4 mm (I.D.) (or nominal size 1/4 inch) stainless steel pipe between the ow
setting unit and the analyzer.
4.1.4 Piping for the Reference Gas Outlet
If the ZR202S is exposed to rain or water splash, connect the pipe outlet on downward.
F4-2E.ai
IM 11M13A01-04E3rd Edition : Dec.15,2014-00
4-4
<4. Piping>
4.2 Piping for System 2
Piping in System 2 is illustrated in Figure 4.3. In System 2, calibration is automated; however, the
piping is basically the same as that of System 1. Refer to Section 4.1.
Adjust secondary pressure of both the air set and the zero gas pressure reducing valve so that these
two pressures are approximately the same. The ow rate of zero and span gases (normally instrument
air) are set by a individual needle valve. After installation and wiring, check the calibration contact
output (see Sec. 7.9.2), and adjust zero gas pressure reducing valve and calibration gas needle valve
so that zero gas ow is within the permitted range. Next check span gas calibration contact output and
adjust air set so that span gas ow is within the permitted range.
ZR202S Integrated type Explosion-proof
Hazardous Area
Zirconia Oxygen Analyzer
Automatic
Calibration Unit
Reference gas
Span gas
Calibration gas (Zero)
Note:
The installation temperature limits range for integrated type analyzer is -20 to 55 °C.
*1
Air Set
Pressure
reducing
valve
Calibration gas
unit case
Figure 4.3 Piping for System 2
Instrument air
*2
Zero gas cylinder
Non-hazardous Area
100 to 240 V AC
~
Contact input
Analog output, contact output
Digital output (HART)
F4-3E.ai
IM 11M13A01-04E3rd Edition : Dec.15,2014-00
<4. Piping>
Automatic Calibration Unit
• Installation of Automatic Calibration Unit
Horizontal mounting on the ZR202S (-A)
AUTOMATIC CALIBRATION UNIT
Display
Terminal box
244
Unit: mm
258
4-5
214
Span gas inlet
Rc1/4 or 1/4NPT(Female)
MAX44
HORIZONTAL INSTALL
Vertical mounting on the ZR202S (-B)
AUTOMATIC CALIBRATION UNIT
180MAX44
40
● ●
166.5
166.5
160
45
406066.540
●●
Span gas inlet
Rc1/4 or 1/4NPT(Female)
Zero gas inlet
66.540
Rc1/4 or 1/4NPT(Female)
Reference gas inlet
Rc1/4 or 1/4NPT(Female)
Reference gas inlet
Rc1/4 or 1/4NPT(Female)
Zero gas inlet
Rc1/4 or 1/4NPT(Female)
F4-4E.ai
Piping Diagram
Calibration gas
Reference gas
Check
valve
ZR202S body
Span gas
solenoid valve
Zero gas solenoid valve
Span gas flowmeter
Reference gas flowmeter
Needle valve
Zero gas flowmeter
SPAN IN
To Air set
REF. IN
To Zero gas cylinder
ZERO IN
F4-5E.ai
IM 11M13A01-04E3rd Edition : Dec.15,2014-00
<5. Wiring>
5. Wiring
This chapter describes wiring procedures necessary for the EXAxt ZR Integrated type Explosion-proof
Zirconia Oxygen Analyzer.
5.1 General
CAUTION
Be sure to read Subsections 3.1.2 to 3.1.5 where the important information on wiring is provided.
CAUTION
• Never supply current to the equipment or any other device constituting a power circuit in
combination with the equipment, until all wiring is completed.
• This product complies with CE marking.
Where a performance suit for CE marking is necessary, the following wiring procedure is necessary.
5-1
1. Install an external switch or circuit breaker to the power supply of the equipment.
2. Use an external switch or circuit breaker rated 5 A and conforms to IEC 947-1 or IEC 947-3.
3. It is recommended that the external switch or circuit breaker be mounted in the same room as
the equipment.
4. The external switch or circuit breaker should be installed within the reach of the operator, and
marked as the power supply switch of this equipment.
Wiring procedure
Wiring should be made according to the following procedure:
1. Be sure to connect the shield of the shielded line to FG terminal of the analyzer.
2. The most outer sheath of the signal line and the power cable should be stripped off to the
minimum necessary length.
3. Signal will be affected by noise emission when the signal lines, power cable and heater cable
are located in the same conduit. When using a conduit, signal lines should be installed in the
separate conduit from power and heater cables. Be sure to ground the metal conduit.
4. Mount the attached two blind plugs to unused cable connection gland(s) of the equipment.
5. The cables indicated in Table 5.1 are used for wiring.
After completing the wiring, screw the cover in the terminal box body and secure it with a lock screw.
6.
Table 5.1 Cable Specications
Terminal name of analyzer Name Need for shields Number of wires
L, N,
AO+, AO-Analog outputΟ2
DO-1, DO-2Contact output2 to 8
DI-1, DI-2, DI-CContact input3
Note *: When the case is used for protective grounding, use a 2-wire cable.
Power supply2 or 3 *
IM 11M13A01-04E
5-2
WARNING
<5. Wiring>
Cables that withstand temperatures at least 80°C should be used for wiring.
NOTE
• Select an appropriate cable O.D. for the cable gland size.
• Protective grounding should have the grounding resistance of 100 Ω or less.
5.1.1 Terminals for the External Wiring
Remove the terminal cover on the opposite side of the display to gain access to the external wiring
terminals.
DI
2CDO-2 DO-11
AO
-
+
F FG
L NFG
F5-1E.ai
Figure 5.1 Terminals for External Wiring
IM 11M13A01-04E
<5. Wiring>
5.1.2 Wiring
Make the following wiring for the equipment. It requires a maximum of four wiring connections as
shown below.
(1) Analog output signal
(2) Power and ground
(3) Contact output
(4) Contact input
5-3
Contact input 1
Contact input 2
1
DI-12DI-23DI-C4DO-15DO-16DO-27DO-2
8
FG
The protective grounding for the analyzer shall be connected either the protective ground terminal in the equipment
or the ground terminal on the case. Standard regarding grounding: Ground to earth, ground resistance: 100 Ω or less.
9
AO
(+)
Analog output
4-20 mA DC
Digital output
10
AO
Contact output 1
11
L
(-)
100 to 240 V AC,
50 or 60 Hz
Figure 5.2 Wiring Connection
5.1.3 Mounting of Cable Gland
For each wiring inlet connection of the equipment, mount the conduit appropriate for the screw size or
a cable gland.
12
N
Contact output 2
13
G
14
FG
F5-2E.ai
Rc1/4 or 1/4NPT
(Reference gas inlet)
25
Rc1/4 or 1/4NPT
(Calibration gas inlet)
Figure 5.3 Cable Gland Mounting
M20 x1.5, 1/2 NPT or the like
(Wiring connection)
Unit: mm
Cable gland
F5-3E.ai
IM 11M13A01-04E
5-4
<5. Wiring>
5.2 Wiring for Analog Output
This wiring is for transmitting 4 to 20 mA DC output signals to a device, e.g. recorder. Maintain the load
resistance including the wiring resistance of 550 Ω or less.
Analyzer
AO(+)
-)
AO(
Shielded cables
FG
Figure 5.4 Wiring for Analog Output
5.2.1 Cable Specications
Use a 2-core shielded cable for wiring.
5.2.2 Wiring Procedure
(1) M4 screws are used for the terminals. Use crimp-on terminals appropriate for M4 terminal
screws for cable connections. Ensure that the cable shield is connected to the FG terminal of the
equipment.
(2) Be sure to connect (+) and (-) polarities correctly.
Receiver
+
-
F5-4E.ai
CAUTION
• Before opening the cover, loosen the lock screw. If the screw is not loosened rst, the cover
will be improperly engaged to the body, and the terminal box will require replacement. When
opening and closing the cover, remove any sand particles or dust to avoid gouging the thread.
• After screwing the cover on the equipment body, secure it with the lock screw.
IM 11M13A01-04E
<5. Wiring>
5.3 Wiring Power and Ground Terminals
Wiring for supplying power to the analyzer and grounding the equipment.
Ground
5-5
Grounding to the earth terminal
on the equipment case
Equipment case
Crimp on terminal of
the ground wire
Grounding
terminal
Lock washer
Figure 5.5 Power and Grounding Wiring
5.3.1 Wiring for Power Line
Connect the power wiring to the L and N terminals of the equipment. For a three-core cable, ground
one core appropriately. Proceed as follows:
(1) Use a two-core or a three-core cable.
(2) M4 screws are used for the terminals. Use crimp-on terminals appropriate for M4 terminal
screws for cable connections.
1 2 C DODODI12
~
100~240 V AC
50/60 Hz
+AO
-
FGL N GFG
Jumper plate
F5-5E.ai
5.3.2 Wiring for Ground Terminals
The ground wiring of the analyzer should be connected to either the ground terminal of the equipment
case (M5) or the terminal inside of the equipment (M4). Proceed as follows:
(1) Keep the ground resistance of 100 Ω or less (JIS D style (Class 3) grounding).
(2) When connecting the ground wiring to the ground terminal of the equipment case, be sure that
the lock washer is in contact with the case surface (see Figure 5.5.).
(3) Ensure that the jumper plate is connected between the G terminal and the FG terminal of the
equipment.
(4) The size of external ground screw thread is M5.
Each cable should be terminated corresponding crimp-on terminals.
(5) No intermediate parts are used for the ground terminal inside of the equipment. Use crimping
terminal for connection to the ground terminal inside of the equipment in order to avoid corrosion
by high contact potentials.
(6) In order to prevent the earthing conductor from loosening, the conductor must be secured to the
terminal, tightening the screw with torque of approx. 1.2 N•m (for M4) or 2.0 N•m (for M5).
(7) Care must be taken not to twist the conductor.
IM 11M13A01-04E
5-6
<5. Wiring>
5.4 Wiring for Contact Output
The equipment can output a maximum of two contact signals. These contact outputs can be used for
different applications such as a low alarm or high alarm.
Do the contact output wiring according to the following requirements.
Hazardous Area
Analyzer
DO-1
DO-1
DO-2
DO-2
Figure 5.6 Contact Output Wiring
5.4.1 Cable Specications
The number of cores varies depending on the number of contacts used.
5.4.2 Wiring Procedure
(1) M4 screws are used for the terminals. Use crimp-on terminals appropriate for M4 terminal
screws for cable connections.
(2) The contact output relays are rated 30 V DC 3A, 250 V AC 3A. Connect a load (e.g. pilot lamp
and annunciator) within these limits.
Non-hazardous Area
Terminal Box
Annunciator or the like
#1 Output
#2 Output
F5-6E.ai
5.5 Wiring for Contact Input
The analyzer can execute specied function when receiving contact signals.
To use these contact signals, proceed wiring as follows:
Hazardous Area
AnalyzerTerminal box
DI-1
DI-2
DI-C
Figure 5.7 Contact Input Wiring
5.5.1 Cable Specications
Use a 2-core or a 3-core cable for this wiring. Depending on the number of input(s), determine which
cable to use.
Non-hazardous Area
Contact input 1
Contact input 2
F5-7E.ai
IM 11M13A01-04E
<5. Wiring>
5.5.2 Wiring Procedure
(1) M4 screws are used for the terminal of the analyzer. Each cable should be equipped with the
corresponding crimp contact.
(2) The ON/OFF level of this contact input is identied by the resistance. Connect a contact input
that satises the descriptions in Table 5.2.
Table 5.2 Identication of Contact Input ON/OFF
Closed Open
Resistance 200 Ω or less 100 kΩ or more
5-7
IM 11M13A01-04E
Blank Page
<6. Components>
Terminal box,
Flame arrestor assembly mounting screw
Flame arrestor assembly
6. Components
This chapter describes the names and functions of components for the major equipment of the
EXAxt ZR Integrated type Explosion-proof Zirconia Oxygen Analyzer.
6.1 ZR202S Zirconia Oxygen Analyzer
Integrated type Explosion-proof Zirconia Oxygen Analyzer
Explosion-proof
Flame arrestor assembly
6-1
Flange
used to mount the detector.
Selectable from JIS, ANSI or DIN
standard models.
Screw
Bolt
Pipe support
Probe
This part is inserted in the furnace.
Selectable of length from 0.4, 0.7,
1.0, 1.5, 2.0 m.
U-shaped pipe
Washer
Calibration gas
pipe opening
Contact
Metal O-ring
Sensor (cell)
Filter
Figure 6.1 Integrated type Explosion-proof Zirconia Oxygen Analyzer
Probe
F6-1E.ai
IM 11M13A01-04E
6-2
F6-3E.ai
Flowmeter for
Span gas
Horizontal
Vertical
<6. Components>
6.2 ZA8F Flow Setting Unit, Automatic Calibration Unit
Reference gas
flow setting valve
Span gas
flow setting valve
Zero gas
flow setting valve
Flowmeter for
reference gas
Flowmeter for
calibration gas
Figure 6.2 ZA8F Flow Setting Unit
mounting
Flowmeter for
Reference gas
Flowmeter for
Zero gas
Span gas
ZERO INREF INSPAN INZERO INREF INSPAN IN
flow setting
valve
Flowmeter for
Span gas
Span gas
flow setting
valve
mounting
Flowmeter for
Reference gas
F6-2E.ai
Flowmeter for
Zero gas
Zero gas
flow setting valve
Figure 6.3 Automatic Calibration Unit
IM 11M13A01-04E
Span gas
flow setting valve
Reference gas
flow setting valve
Reference gas
flow setting valve
<7. Startup>
7. Startup
The following describes the minimum operating requirements — from supplying power to the analyzer
to analog output conrmation to manual calibration.
7-1
Check piping and
wiring connections
Set up valves
Supply power
Confirm equipment
type setting
Select gas to be measured
Set output ranges
Check current loop
Check contact action
Calibrate analyzer
Set detailed data
Place in normal operation
F7-1E.ai
Figure 7.1 Startup Procedure
For system tuning by HART communication, refer to the IM 11M12A01-51E ''HART Communication
Protocol''.
IM 11M13A01-04E
7-2
<7. Startup>
7.1 Checking Piping and Wiring Connections
Refer to Chapters 4 and 5, earlier in this manual, for piping and wiring conrmations.
7.2 Valve Setup
Set up valves and associated components used in the analyzer system in the following procedures:
(1) If a stop valve is used in the calibration gas inlet, fully close this valve.
(2) If instrument air is used as the reference gas, adjust the Air set secondary pressure so that
the air pressure of sample gas pressure plus approx. 50 kPa (plus approx. 150 kPa for with
check valve) (300 kPa maximum) is obtained. Turn the reference gas ow setting valve in
the ZA8F ow setting unit to obtain the ow of 800 to 1000 mL/min. (Turning the valve shaft
counterclockwise increases the rate of ow. When turning the valve shaft, if the valve has a lock
nut, rst loosen the lock nut.) After completing the valve setup, be sure to tighten the lock nut.
NOTE
The calibration gas ow setting will be described later. Fully close the needle valve in the ow setting
unit.
7.3 Supplying Power to Analyzer
CAUTION
To avoid temperature changes around the sensor, it is recommended that the power be continuously
supplied to the Oxygen Analyzer if it is used in an application where its operations and suspensions
are periodically repeated.
It is also recommended to ow a span gas (instrument air) beforehand.
Supply power to the analyzer. A display as in Figure 7.2, which indicates the detector’s sensor
temperature, then appears. As the heat in the sensor increases, the temperature gradually rises
to 750°C. This takes about 20 minutes after the power is turned on, depending somewhat on the
ambient temperature and the sample gas temperature. After the sensor temperature has stabilized
at 750°C, the analyzer is in the measurement mode. The display panel then displays the oxygen
concentration as in Figure 7.3. This is called the basic panel display.
F7-2E.ai
Figure 7.2 Display of Sensor Temperature Figure 7.3 Measurement Mode Display
While Warming Up
%
F7-3E.ai
IM 11M13A01-04E
<7. Startup>
7.4 Operation of Infrared Switch
7.4.1 Display and Switches
This equipment uses an infrared switch that enables operation with the cover closed. Figure 7.4
shows the infrared switch and the display. Table 7.1 shows the three switch (keys) and functions.
4: Decimal point
7-3
1: Data display area
2: Infrared switch
F7-4E.ai
3: Engineering-unit
display area
µMmNkgalbbl %
scftm3 /d /s /h /m
>
>
ENT
Figure 7.4 Infrared switch and the display
1. Data display area: Displays the oxygen concentration, set values, alarm numbers, and error
numbers.
2. Infrared switch: Three switches perform data setting operations.
3. Engineering-unit display area: The percent sign appears when the oxygen concentration is
displayed.
4. Decimal point: A decimal point is displayed.
Table 7.1 Switch and Function
Switch Function
>
^
ENT1. Used to change the basic panel display to the parameter selection display.
1. Moves the position of the digit to the right. If you continuously touch the key, the position
of the digit will move continuously to the right, nally returning to the leftmost position
after reaching the rightmost position of the digit.
2. Selects Yes or No.
3. When you touch this key together with the [ENT] key, the previous display then appears,
or the operation will be cancelled.
Used to change values. If you continuously touch this key, the value of the digit will increase
continuously, e.g., from 1 to 2 to 3 (for numeric data), or from A to B to C (for alphabetic
characters), and nally return to its original value.
2. Used to enter data.
3. Advances the operation.
The three infrared switches are activated by completely touching the glass surface of the switch. To
touch any of the keys continuously, rst touch the surface and then completely remove your nger
from the surface. Then touch it again.
Infrared switches consist of two elements: an infrared emitting element and an infrared acceptance
element. Infrared light-waves from the element bounces on the operator’s nger and are reected
back to the acceptance element, thereby causing the infrared switch to turn on and off, depending
on the strength of the reected light-waves. From this operating principles, carefully observe the
following:
IM 11M13A01-04E
7-4
<7. Startup>
CAUTION
1. Be sure to put the equipment case cover back on. If this is not done, the infrared switch will not
reect the infrared light-waves, and a “dSPErr” error will be issued.
2. Before placing the equipment in operation, be sure to wipe off any moisture or dust on the glass
surface if it is wet or dirty. Also make sure your ngers are clean and dry before touching the
glass surface of the switch.
3. If the infrared switches are exposed to direct sunlight, they may not operate correctly. In such a
case, change position of the display or install a sun cover.
7.4.2 Display Conguration
The parameter codes provided for the equipment are used to control the equipment display panels
(see below). By selecting appropriate parameter codes, you can conduct calibration and set operation
parameters. Figure 7.5 shows the conguration of display items. The parameter codes are listed in
groups of seven; which are briey described in Table 7.2.
To enter parameters, you rst need to enter the password, refer to Subsection 7.4.3.
Touch the [ >] key and [ ENT] key at same time to revert to the main screen.
Basic panel display
%
Password entry display
Group A setup display
Group B setup display
Group C setup display
Group D setup display
Parameter code
selection display
Figure 7.5 Display Conguration
IM 11M13A01-04E
Group E setup display
Group F setup display
Group G setup display
F7-5E.ai
<7. Startup>
Table 7.2 Display Functions
Display Function and item to be set
Basic panel Displays the oxygen concentration in normal operation, or displays the detector
heater temperature while warming up. If an error or alarm arises, the corresponding
error or alarm number appears.
Password entry Enters the password for the parameter code selection display.
Group A setup Displays detailed data, such as the cell voltage or temperature.
Group B setup Sets and performs calibration.
Group C setup Sets analog output.
Group D setup Sets an alarm.
Group E setup Sets the contact inputs and contact outputs.
Group F setup Selects the type of equipment and sets the parameters for computation.
Group G setup Performs the current-loop or contact checks.
7.4.3 Entering Parameter Code Selection Display
This subsection briey describes the password entry procedure for entering the parameter code
selection display. The password is 1102 - it cannot be changed to a different password.
Table7.3 Parameter Code Selection
Switch operationDisplayDescription
>∧
ENT
21.0%
Warm-up is complete, and the basic panel is now displayed.
7-5
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
PASSno
0000
1000
1000
1100
1100
1102
1102
A01
Continuously touch the [ENT] key for at least three seconds
to display “PASSno”.
Touch the [ENT] key again. This allows you to change the leftmost
digit that is ashing.
Set the password 1102. If you touch the [∧] key, the digit that is ashing will
be 1.
Touch the [>] key to move the position of the digit that is ashing to the
right one digit.
Touch the [∧] key to change the numeric value to 1.
Touch the [>] key again to move the position of the digit that is ashing to
the right one more digit. Continuously touch the [>] key, and the position of
the digit that is ashing will move continuously to the right.
Touch the [∧] key to change the numeric value to 2. Continuously touch [∧]
key, and the numeric value increases continuously.
If you touch the [ENT] key, all the digits ash.
Touch the [ENT] key again to display A01 on the parameter code selection
display.
The symbol [ ] indicates that the key is being touched. Light characters indicate that the digits are ashing.
IM 11M13A01-04E
7-6
<7. Startup>
CAUTION
• If no key is touched for at least 20 seconds during password entry, the current display will
automatically switch to the basic panel display.
• If no key is touched for at least 10 minutes during parameter code selection, the current display
will automatically switch to the basic panel display.
7.4.4 Selecting Parameter Codes
Table7.4 Parameter Code
Switch operationDisplayDescription
>∧
ENT
A01
Password has been entered and the parameter code selection display has
appeared. Character A is ashing, indicating that character A can be changed.
>∧
>∧
>∧
>∧
>∧
>∧
>∧
The symbol [ ] indicates that the key is being touched. Light characters indicates that the digits are ashing.
ENT
ENT
ENT
ENT
ENT
ENT
ENTSet
A01
A01
A01
b01
C01
d01
Value
If you touch the [>] key once, the position of the digit that is ashing will move to
the right. This allows you to change 0.
Touch the [>] key again to move the position of the digit that is ashing to the right
one more digit. This enables you to change numeric value to 1.
Touch the [>] key again to return the position of the digit that is ashing to A.
Continuously touch the [>] key, and the position of the digit that is ashing will
move continuously to the right.
If you touch the [∧] key once, character A will change to b.
Touch the [∧] key once to change to C.
Continuously touch the [∧] key, and the value of the digit that is ashing will
increase continuously, from d to E to F to G to A. Numeric values will change from
0 to 1 to 2 to 3 … to 8 to 9 and back to 0. However, numbers that are not present
in the parameter codes will be skipped. Each digit is changed independently. Even
though a low-order digit changes from 9 to 0, a high-order digit will not be carried.
After you select the desired character, touch the [ENT] key. The set data will be
displayed.
IM 11M13A01-04E
<7. Startup>
7.4.5 Changing Set Values
(1) Selecting numeric values from among preset values
Switch operationDisplayDescription
>∧
>∧
ENT
ENT
The set value is displayed after the parameter code selection. An example of how
0
to select either 0, 1, or 2 as the set value is given below.
(The currently set value is 0.)
Touch the [∧] key once to change the current value from 0 to 1.
1
7-7
>∧
>∧
>∧
(2) Entering numeric values such as oxygen concentration values and factors
Switch operationDisplayDescription
>∧
>∧
>∧
>∧
>∧
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
C01
00.0
00.0
09.0
09.0
09.8
Touch the [∧] key again to change to the numeric value to 2.
2
If you touch the [∧] key again, the numeric value will return to 0.
0
Continuously touch the [∧] key, and the numeric values will change continuously.
Display the desired numeric value and touch the [ENT] key.
The display will then return to the parameter code selection
The set value is displayed after the parameter code selection.
An example of entering “9.8” is given below. (The currently set value is 0.0)
Touch the [>] key to move the position of the digit that is ashing to the digit to
be changed. Continuously touch the [>] key, and the position of the digit that is
ashing will move continuously to the right.
Touch the [∧] key to set the numeric value to 9.
Continuously touch the [∧] key, and the numeric value will change in sequence
from 0 to 1 to 2 to 3 … to 8 to 9 and back to 0.
Touch the [>] key to move the position of the digit that is ashing to the right.
Touch the [∧] key to set the numeric value to 8.
>∧
>∧
>∧
(3) If invalid numeric values are entered.
Switch operationDisplayDescription
>∧
>∧
>∧
ENT
ENT
ENT
ENT
ENT
ENT
09.8
09.8
C11
98.0
Err
00.0
Where the correct numeric value is displayed, touch the [ENT] key.
If you touch the [ENT] key again, the ashing stops and the current set value will
be in effect.
Touch the [ENT] key once again to return to the parameter code selection display.
If an invalid numeric value (beyond the input range specied) is entered,
“Err” will appear for two seconds after touching the [ENT] key.
“Err” appears for two seconds, and the display returns to the rst set value.
Re-enter the numeric value.
IM 11M13A01-04E
7-8
<7. Startup>
7.5 Conrmation of Equipment Type Setting
This equipment can be used for both the Oxygen Analyzer and the Humidity Analyzer. If you choose
optional specication /HS at the time of purchase, the equipment is set for the Humidity Analyzer.
Before setting the operating data, be sure to check that the desired model has been set.
Note that if the equipment type setting is changed after operating data are set, the operating data
that have been set are then initialized and the default settings remain. Set the equipment type with
parameter code [F01]. See Table 10.7, later in this manual.
CAUTION
Note that if the equipment type is changed, operation data that have already been set are initialized
(reverting to the default setting).
Table 7.5 Equipment Type Setting Procedure
Switch operationDisplayDescription
>∧
ENT
A01
Display after the password has been entered.
>∧
>∧
>∧
>∧
>∧
>∧
>∧
The symbol [ ] indicates that the key is being touched. Light characters indicates that the digits are ashing.
ENT
ENT
ENT
ENT
ENT
ENT
ENTBasic
F01
F01
panel
display
Touch the [∧] key to switch to Group F. If an unwanted alphabetic character after F
has been entered, continuously touch the [∧] key to return to the original.
Touch the [ENT] key for conrmation. If 0 (zero) is entered, the oxygen analyzer is
0
already set. If 1 (one) is entered, the humidity analyzer has been set.
Change the setting following the steps below.
Continuously touch the [∧] key, and the position of the digit will change from 1 to 0
0
to 1 to 0. Release the [ENT] key when 0 is displayed.
Touch the [ENT] key. The numeric value will ash.
0
Touch the [ENT] key again to stop the numeric value from ashing.
0
Touch the [ENT] key once again, and the display will change to the parameter
code.
Touch the [>] key together with the [ENT] key to return to the basic panel display.
(This is not required if you proceed to make another setting.) (The displayed
numeric values indicate the measurement gas concentration.)
IM 11M13A01-04E
<7. Startup>
7.6 Selection of Measurement Gas
Combustion gases contain moisture created by burning hydrogen in the fuel. If this moisture is
removed, the oxygen concentration might be higher than before. You can select whether the oxygen
concentration in a wet gas is to be measured directly, or compensated for its dry-gas value before use.
Use the parameter code [F02] to set the measurement gas. For details on the parameter code, see
Table 10.7, later in this manual.
Table 7.6 Setting Measurement Gas
Switch operationDisplayDescription
>∧
ENT
A01
Display after the password has been entered.
7-9
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENTBasic
F01
F01
F02
0
1
1
1
F03
panel
display
Touch the [∧] key to switch to Group F. If an unwanted alphabetic character after F
has been entered, continuously touch the [∧] key to return to the original.
Touch the [>] key to move the position of the digit that is ashing to the right.
Touch the [∧] key to change the numeric value to 2. If an unwanted numeric value
has been entered, continuously touch the [∧] key to return to the original.
Touch the [ENT] key for conrmation. If 0 (zero) is entered, the oxygen
concentration in a wet gas is already set. If the oxygen concentration in a dry gas is
to be entered, follow the steps below to set 1 (one).
Continuously touch the [∧] key, and the position of the digit will change from 1 to 0
to 1 to 0. Release the [ENT] key when 1 (one) is displayed.
Touch the [ENT] key. The numeric value will ash.
Touch the [ENT] key again to stop the value from ashing.
Touch the [ENT] key once again, and the display will change to the parameter
code selection panel.
Touch the [>] key together with the [ENT] key to return to the basic panel display.
(This is not required if you proceed to make another setting.) (The displayed
numeric values indicate the measurement gas concentration.)
The symbol [ ] indicates that the key is being touched. Light characters indicates that the digits are ashing.
7.7 Output Range Setting
This section sets forth analog output range settings. For details, consult Section 8.2,“Current Output
Setting”, later in this manual.
Minimum Current (4 mA) and Maximum Current (20 mA) Settings
Use the parameter codes [C11] to set the oxygen concentration at 4 mA and [C12] to set the oxygen
concentration at 20 mA. The following shows where 10%O2 is set at 4 mA and 20%O2 at 20 mA.
IM 11M13A01-04E
7-10
<7. Startup>
Table 7.7 Minimum and Maximum Current Setting Procedure
Switch operationDisplayDescription
>∧
ENT
A01
Display after the password has been entered.
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
C01
C01
C11
000
000
010
010
010
C11
Set the oxygen concentration at 4 mA. Change the parameter code to C11.
Touch the [∧] key to switch to Group C.
Touch the [>] key to move the position of the digit that is ashing to the right.
Touch the [∧] key to enter the numeric value to 1.
Touch the [ENT] key to display the current set value (0% O2 has been set).
Touch the [>] key to move the position of the digit that is ashing to the right.
Touch the [∧] key to change the numeric value to 1.
If you touch the [ENT] key, all the digits ash.
Touch the [ENT] key again to stop the ashing.
Touch the [ENT] key once again, and the display will switch to the parameter code
selection display.
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENTBasic
C11
C12
025
025
020
020
020
C12
panel
display
Set the oxygen concentration at 20 mA. Touch the [>] key to move the position of
the digit that is ashing to the right.
Touch the [∧] key to enter the numeric value to 2.
Touch the [ENT] key to display the current set value.
Touch the [>] key to move the position of the digit that is ashing to the right.
Touch the [∧] key to change the numeric value to 0. The numeric value will change
from 5 to 6 ... to 9 and back to 0.
If you touch the [ENT] key, all the digits ash.
Touch the [ENT] key again to stop the ashing.
Touch the [ENT] key once again to switch to the parameter code selection display.
Touch the [>] key together with the [ENT] key to return to the basic panel display.
(This is not required if you proceed to make another setting.)(The displayed
numeric values indicate the measurement gas concentration.)
The symbol [ ] indicates that the key is being touched. Light characters indicates that the digits are ashing.
IM 11M13A01-04E
<7. Startup>
7.8 Checking Current Loop
The set current can be output as an analog output. This enables the checking of wiring between the
analyzer and the receiving instrument. Current loop checking is performed using parameter code
[G01].
Table 7.8 Checking Current Loop
Switch operationDisplayDescription
>∧
ENT
A01
Display after the password has been entered.
7-11
>∧
>∧
>∧
>∧
>∧
>∧
>∧
The symbol [ ] indicates that the key is being touched. Light characters indicates that the digits are ashing.
ENT
ENT
ENT
ENT
ENT
ENT
ENTBasic
G01
00.0
10.0
10.0
10.0
G01
panel
display
Touch the [∧] key to switch to Group G.
Touch the [ENT] key. The current output remains preset with the output-hold
feature (Section 2.3).
Touch the [∧] key to set the numeric value to 1 (to set a 10-mA output).
Touch the [ENT] key to have all the digits ash.
Touch the [ENT] key again to stop the ashing.
A 10-mA output is then issued.
Touch the [ENT] key once again to switch to the parameter code selection display.
At that point, the current output returns to the normal value.
Touch the [>] key together with the [ENT] key to return to the basic panel display.
7.9 Checking Contact I/O
Conduct a contact input and output check as well as an operation check of the solenoid valves for the
optional automatic calibration unit.
Table 7.9 Parameter Codes for Checking Contact I/O
Check item Parameter code Set value and contact
Contact output 1G110Open
Contact output 2G120Open
Automatic calibration solenoid valve
(zero gas)
Automatic calibration solenoid valve
(span gas)
Contact input 1G210Open
Contact input 2G220Open
G150Off
G160Off
action
1Closed
1Closed
1On
1On
1Closed
1Closed
IM 11M13A01-04E
7-12
<7. Startup>
7.9.1 Checking Contact Output
Follow Table 7.10 to check the contact output. The table uses an example with contact output 1.
Table 7.10 Checking Contact Output
Switch operationDisplayDescription
>∧
ENT
A01
Display after the password has been entered.
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENTBasic
G01
G01
G11
0
1
1
1
G11
panel
display
Touch the [∧] key to switch to Group G.
Touch the [>] key to move the position of the digit that is ashing to the right one
digit.
Touch the [∧] key to enter 1.
Touch the [ENT] key to have 0 (zero) ash. The contact output is then open.
Touch the [∧] key to set 1 (one).
Touch the [ENT] key. The ashing continues.
Touch the [ENT] key again to stop the ashing, and the contact output will be
closed.
Touch the [ENT] key once again to switch to the parameter code selection display.
The contact output then returns to the original state.
Touch the [>] key together with the [ENT] key to return to the basic panel display.
(This is not required if you proceed to make another setting.)
(The displayed numeric values indicate the measurement gas concentration.)
The symbol [ ] indicates that the key is being touched. Light characters indicates that the digits are ashing.
CAUTION
• If you conduct an open-close check for the contact output 2, Err-01 (cell voltage failure) or Err02 (heater temperature abnormal) will occur. This is because the built-in heater power of the
detector, which is connected to contact output 2, is turned off during the above check. So, if the
above error occurs, reset the equipment or turn the power off and then back on to restart (refer to
Section 10.4, “Reset”, later in this manual).
IM 11M13A01-04E
<7. Startup>
7.9.2 Checking Calibration Contact Output
The calibration contacts are used for the solenoid valve drive signals for the Automatic Calibration
Unit. This output signal enables you to check the equipment operation. Check the owmeter gas ow
for that operation.
Follow the steps in Table 7.11. The table uses an example with a zero gas solenoid valve.
Table 7.11 Checking Calibration Contact Output
Switch operationDisplayDescription
>∧
ENT
A01
Display after the password has been entered.
7-13
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
G01
G01
G11
G11
G15
0
1
1
1
Touch the [∧] key to switch to Group G.
Touch the [>] key to move the position of the digit that is ashing to the right one
digit.
Touch the [∧] key to enter 1.
Touch the [>] key to move the position of the digit that is ashing to the right one
digit.
Touch the [∧] key to enter 5.
Touch the [ENT] key to have 0 ash.
The solenoid valve remains closed.
Touch the [∧] key to enter 1.
Touch the [ENT] key. The ashing continues.
Touch the [ENT] key again to stop the ashing, and the solenoid valve will be open
to let the calibration gas ow.
>∧
>∧
The symbol [ ] indicates that the key is being touched. Light characters indicates that the digits are ashing.
ENT
ENTBasic
G15
panel
display
Touch the [ENT] key once again to switch to the parameter code selection display.
The solenoid valve will then be closed.
Touch the [>] key together with the [ENT] key to return to the basic panel display.
(This is not required if you proceed to make another setting.)
(The displayed numeric values indicate the measurement gas concentration.)
IM 11M13A01-04E
7-14
<7. Startup>
7.9.3 Checking Contact Input
Follow Table 7.12 to check the contact input. The table uses an example with contact input 1.
Table 7.12 Checking Contact Input
Switch operationDisplayDescription
>∧
ENT
A01
Display after the password has been entered.
>∧
>∧
>∧
>∧
>∧
>∧
The symbol [ ] indicates that the key is being touched. Light characters indicates that the digits are ashing.
ENT
ENT
ENT
ENT
ENT
ENTBasic
G01
G01
G21
G21
panel
display
Touch the [∧] key to switch to Group G.
Touch the [>] key to move the position of the digit that is ashing to the right one
digit.
Touch the [∧] key to enter 2.
Touch the [ENT] key. 0 is displayed with the contact input open. If the contact input
0
is closed, the display will be 1 (one).
This enables you to check whether or not the wiring connections have been
properly made or not.
Touch the [ENT] key once again to switch the parameter code selection display.
Touch the [>] key together with the [ENT] key to return to the basic panel display.
IM 11M13A01-04E
<7. Startup>
7.10 Calibration
The analyzer is calibrated in such a way that the actual zero and span gases are measured and those
measured values are used to agree with the oxygen concentrations in the respective gases.
There are three types of calibration procedures available:
(1) Manual calibration conducting zero and span calibrations, or either of these calibrations in turn.
(2) Semi-automatic calibration which uses the infrared switches or a contact input signal and
conducts calibration operations based on a preset calibration time and stable time.
(3) Automatic calibration conducted at preset intervals.
Manual calibration needs the ZA8F Flow Setting Unit to allow manual supply of the calibration gases.
Semi-automatic and automatic calibrations need Automatic Calibration Unit to allow automatic supply
of the calibration gases. The following sections set forth the manual calibration procedures. For details
on semi-automatic and automatic calibrations, consult Chapter 9, “Calibration” later in this manual.
7.10.1 Calibration Setup
Set the following three items before carrying out a calibration. Parameter codes for these set items are
listed in Table 7.13.
(1) Mode setting
There are three calibration modes: manual, semi-automatic, and automatic.
Select the desired mode. This section uses manual mode for calibration.
7-15
(2) Oxygen concentration in zero gas
Enter the zero gas oxygen concentration for calibration.
(3) Oxygen concentration in span gas
Enter the span gas oxygen concentration for calibration. If instrument air is used, enter 21 vol%
. When using the ZO21S Standard Gas Unit (for use of the atmospheric air as a span gas),
O
2
use a hand-held oxygen analyzer to measure the actual oxygen concentration, and then enter it.
CAUTION
If instrument air is used for the span gas, dehumidify the air to a dew point of -20°C and remove any
oil mist or dust.
Incomplete dehumidifying or unclean air will have an adverse effect on the measurement accuracy.
Table 7.13 Calibration Parameter Codes
Set item Parameter code Set value
Calibration modeB030 Manual calibration
1 Semi-automatic, Manual calibration
2 Automatic, Semi-automatic, Manual calibration
Zero gas oxygen concentrationB01Enter oxygen concentration.
Span gas oxygen concentrationB02Enter oxygen concentration.
IM 11M13A01-04E
7-16
<7. Startup>
Table 7.14 Calibration Setup Procedure
Switch operationDisplayDescription
>∧
ENT
A01
Display after the password has been entered.
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
b01
001.00
001.00
000.00
000.00
000.90
000.90
000.98
000.98
Set the zero gas concentration. Switch the parameter code to B01.
Here, set 0.98%.
Touch the [ENT] key to display the currently set value.
%
Touch the [>] key to move the position of the digit that is ashing to 1.
%
Touch the [∧] key to change to 0.
%
Touch the [>] key to move the position of the digit that is ashing to the
%
right one digit.
Touch the [∧] key to change the numeric value to 9.
%
Touch the [>] key to move the position of the digit that is ashing to the
%
right one digit.
Touch the [∧] key to change the numeric value to 8.
%
Touch the [ENT] key to have all the digits ash.
%
>∧
>∧
Set the span gas concentration by above procedure, set 21%.
>∧
>∧
>∧
>∧
>∧
>∧
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENTBasic panel
000.98
b01
b03
0
0
0
b03
display
Touch the [ENT] key again to stop the ashing.
%
Touch the [ENT] key once again to switch to the parameter code selection
display.
Next, set the calibration mode. Switch the parameter code to B03.
Touch the [ENT] key to display the currently set value.
If it is 0 (manual calibration), you can leave it as is. If it is other than 0,
change it to 0 (zero).
Touch the [ENT] key. The numeric value will ash.
Touch the [ENT] key again to stop the ashing.
Touch the [ENT] key once again to switch to the parameter code selection
display.
Touch the [>] key together with the [ENT] key to return to the basic panel
display. (This is not required if you proceed to make another setting.)
(The displayed numeric values indicate the measurement gas
concentration.)
The symbol [ ] indicates that the key is being touched. Light characters indicates that the digits are ashing.
IM 11M13A01-04E
<7. Startup>
7.10.2 Manual Calibration
The following describes how to conduct a calibration.
Preliminary
Before conducting a manual calibration, be sure that the ZA8F Flow Setting Unit zero gas ow valve
is fully closed. Open the zero gas cylinder pressure reducing value so that the secondary pressure will
be a sample gas plus approx. 50 kPa (or sample gas pressure plus approx. 150 kPa when a check
valve is used, maximum pressure rating is 300 kPa).
Calibration Implementation
This manual assumes that the instrument air is the same as the reference gas used for the span gas.
Follow the steps below to conduct manual calibration. When using the ZO21S Standard Gas Unit (for
use of the atmospheric air as a span gas), use a hand-held oxygen analyzer to measure the actual
oxygen concentration, and then enter it.
Table 7.15 Conducting Calibration
Switch operationDisplayDescription
>∧
ENT
A01
Display after the password has been entered.
7-17
>∧
>∧
>∧
>∧
>∧
>∧
>∧
ENT
ENT
ENT
ENT
ENT
ENT
ENT
b10
CAL
CAL
SPAn Y
21.00
%
OPEn
/20.84
20.84
%
Switch the parameter code to B10.
(The key operations for this procedure are omitted.)
Touch the [ENT] key, and “CAL” will be displayed.
To cancel the above, touch the [>] key and [ENT] key together to return to
the B10 display.
If you touch the [ENT] key again, “CAL” then ashes.
To cancel the above, touch the [>] key and [ENT] key together, the display
will return to the B10 display.
If you touch the [ENT] key again, “SPAn Y” appears (Y is ashing).
If you omit the span calibration, touch the [>] key, and change “Y” to “N”.
If you touch the [ENT] key, the display then jumps to “ZEro Y”.
Touch the [ENT] key to display the calibration gas value, in other words, the
span gas concentration set in Subsection 7.10.1, “Calibration Setup”.
To cancel the above, touch the [>] key and [ENT] key together, then the
display returns to “SPAn Y”.
If you touch the [ENT] key, “OPEn” and the currently measured value are
displayed alternately. Open the Flow Setting Unit span gas ow valve and
adjust the span gas ow to 600 ± 60 ml/min. To do this, loosen the valve lock
nut and gently turn the valve control (shaft) counterclockwise.
Check the calibration gas owmeter for conrmation.
If the automatic calibration unit is connected, open the span gas solenoid
valve, and the measured value changes to the span gas value.
When the display becomes stable, proceed to the next step.
To cancel the above, touch the [>] key and [ENT] key together, then the
display returns to “SPAn Y”.
If you touch the [ENT] key, all the digits ash. At that point, no calibration is
conducted yet.
Continue to the next page
IM 11M13A01-04E
7-18
<7. Startup>
Switch operationDisplayDescription
>∧
>∧
>∧
>∧
ENT
ENT
ENT
ENT
ZEro Y
0.98
OPEn
/0.89
0.89
If you touch the [ENT] key again, the ashing stops and “ZEro Y” appears.
Close the span gas ow valve. Secure the span gas lock nut for leakage.
If the automatic calibration unit is connected, close the span gas solenoid
valve.
If zero gas calibration is omitted, touch the [>] key to change “Y” to “N”.
Next, if you touch the [ENT] key, the display jumps to “CALEnd”.
Touch the [ENT] key to display the calibration gas value.
%
This value must be the zero gas concentration set in Subsection 7.10.1,
“Calibration Setup,” earlier in this manual.
To cancel the above, touch the [>] key and [ENT] key together, then the
display returns to “ZEro Y”.
If you touch the [ENT] key, “OPEn” and the currently measured value are
displayed alternately. Open the Flow Setting Unit zero gas ow valve and
adjust the zero gas ow to 600 ± 60 ml/min. To do this, loosen the valve
lock nut and gently turn the valve control (shaft) counterclockwise.
Check the calibration gas owmeter for conrmation.
If the automatic calibration unit is connected, open the zero gas solenoid
valve, and then the measured value changes to the zero gas value.
When the display becomes stable, proceed to the next step.
To cancel the above, touch the [>] key and [ENT] key together, then the
display returns to “ZEro Y”.
If you touch the [ENT] key, all the digits ash. At that point, no calibration is
%
conducted yet.
>∧
>∧
>∧
The above “display” is a result of switch operations.
The symbol [
“/” indicates that the characters are displayed alternately.
[Cancel] indicates the procedure to stop the key operations.
ENT
ENT
ENTBasic
] indicates the keys are being touched, and the light characters indicate “ashing.”
CALEnd
b10
panel
display
Touch the [ENT] key again to get the measured value to agree with the zero
gas concentration. Close the zero gas ow valve.
Secure the valve lock nut for leakage during measurement.
If the automatic calibration unit is connected, close the zero gas solenoid
valve. “CALEnd” ashes during the output hold time. If “output hold” is
specied in the “Output Hold Setting,” it remains as an analog output (see
Section 8.3).
When the preset output hold time is up, the calibration is complete.
The output hold time is set to 10 minutes at the factory.
If you touch both the [>] key and [ENT] key at the same time during the
preset Output Hold Time, the calibration is aborted and the parameter code
selection display appears.
If you touch the [>] key and [ENT] key together, then the basic panel display
appears.
IM 11M13A01-04E
<8. Detailed Data Setting>
8. Detailed Data Setting
8.1 Setting Display Item
Display items are dened as items displayed on the basic panel display.
Parameter code [A00] or [F08] is used to set the display items as shown in Table 8.1. The oxygen
concentration is set at the factory before shipment. In addition, if the data initialization is performed,
the oxygen concentration will be set.
Table 8.1 Display Item
Values set with A00 or F08Items displayed on the basic panel display
0Indicates the oxygen concentration.
1 or 2 For humidity analyzers only. (if 1 or 2 is set for the oxygen analyzer,
“0.0” is only displayed on the basic panel display.)
3Displays an item for the current output.
If the output damping has been set for the current output, values
involving the output damping are displayed.
8-1
CAUTION
If you set “3” in the parameter code [A00] or [F08], be sure to select “Oxygen Concentration” in the
following mA output setting (see Section 8.2, “Current Output Setting”).
8.2 Current Output Setting
This section describes setting of the analog output range. Table 8.2 shows parameter codes for the
set items.
Table 8.2 Current Output Parameter Codes
Set item Parameter code Set value
Analog output C01 0Oxygen concentration
14 mA (xed *1)
24 mA (xed *1)
Output mode C03 0Linear
1Logarithm
Min. oxygen concentration C11 Oxygen concentration at 4 mA
Max. oxygen concentration C12 Oxygen concentration at 20 mA
Output damping constant C30 0 to 255 seconds
*1: For the oxygen analyzer, set 0 (zero) only for parameter code C01.
When it is set, the current output is 4-mA xed regardless of the oxygen concentration.
IM 11M13A01-04E
8-2
<8. Detailed Data Setting>
8.2.1 Setting Minimum Oxygen Concentration ( at 4 mA) and Maximum Oxygen
Concentration ( at 20 mA)
Set the oxygen concentration values at 4 mA and 20 mA.
The minimum concentration of oxygen for the minimum current (4 mA) is 0%O
or 6% to 76%O2.
2
The maximum concentration of oxygen for the maximum current (20 mA) ranges from 5% to 100%
O2, and must be greater than 1.3 times the concentration of oxygen set for the minimum. If it does not
fall within this input range setting, the setting will be invalid, and the previous set values will remain.
Setting example 1
If the setting (for a 4 mA current) is 10%O
, you must set the oxygen concentration for the maximum
2
(20 mA) point at 13%O2.
Setting example 2
If the setting (for a 4 mA current) is 75%O
, you must set the oxygen concentration for the maximum
2
(20 mA) point at 98%O2 (75 × 1.3).
(Numbers after the decimal point are rounded up.)
CAUTION
• When you select logarithmic mode, the minimum output remains constant at 0.1%O2, and the
parameter [C11] display remains unchanged.
8.2.2 Entering Output Damping Constants
If a measured value adversely affected by a rapid change in the sample gas oxygen concentration is
used for the control means, frequent on-off actions of the output will result. To avoid this, the analyzer
allows the setting of output damping constants ranging from 0 to 255 seconds.
8.2.3 Selection of Output Mode
You can select a linear or logarithmic output mode. The former provides linear characteristics between
the analog output signal and oxygen concentration.
8.2.4 Default Values
When the analyzer is delivered or data are initialized, the current output settings are by default as
shown in Table 8.3.
Table 8.3 Current Output Default Values
Item Default setting
Min. oxygen concentration
Max. oxygen concentration
Output damping constant 0 (seconds)
Output mode Linear
0%
25%
O
2
O
2
CAUTION
IM 11M13A01-04E
• When you select logarithmic mode, the minimum output remains constant at 0.1%O2, and the
parameter [C11] display remains unchanged.
<8. Detailed Data Setting>
8.3 Output Hold Setting
The “output hold” functions retain an analog output signal at a preset value during the equipment’s
warm-up time or calibration or if an error arises.
Table 8.4 shows the analog outputs that can be retained and the individual states.
Table 8.4 Analog Output Hold Setting
Equipment
status
Output hold
values available
4 mA O
20 mA O
Without hold featureOOO
Retains output from just
before occurrence
Preset value
(2.4 to 21.6 mA)
O: The output hold functions are available.
*1: The output hold functions on error occurrence are unavailable when option code “/C2” or “/C3” (NAMER NE 43 compliant) is
specied.
During warm-up
OOO
During maintenance
OOO
During calibration During error
8-3
occurrence (*1)
O
8.3.1 Denition of Equipment Status
(1) During warm-up
“During warm-up” is the time required after applying power until the sensor temperature
stabilizes at 750°C, and the equipment is in the measurement mode. This status is that the
sensor temperature is displayed on the basic panel.
(2) During maintenance
“During maintenance” is the time from when a valid password is entered in the basic panel
display to enable the parameter code selection display until the display goes back to the basic
panel display
(3) During calibration (see Chapter 9, Calibration)
In the manual calibration, proceed with the calibration operation with the parameter code
[B10] to display the span gas conrmation display for the rst span calibration, thus starting the
calibration time when the [ENT] key is touched. After a series of calibrations is complete and the
preset output stabilization time has elapsed, the calibration time will be up. Figure 8.1 shows the
denition of “during calibration” in the manual calibration.
IM 11M13A01-04E
8-4
<8. Detailed Data Setting>
Switch operationDisplay
>∧
ENT
b10
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
CAL
CAL
SPAn Y
21.00
%
OPEn/20.84
20.84
%
ZEro Y
0.98
%
OPEn/0.89
Output hold time
during calibration
>∧
>∧
>∧
>∧
Figure 8.1 Denition of During Calibration
In a semi-automatic calibration, “during calibration” is the time, starting when a calibration instruction
is executed with an infrared switch or a contact input, to make a series of calibrations, until the preset
output stabilization time elapses.
In an automatic calibration, “during calibration” is the time, starting when automatic calibration is
carried out at the calibration start time, until the preset output stabilization time elapses.
(4) “Error” appears when Err-01 to Err-04 are being issued
ENT
ENT
ENT
ENT
0.89
CALEnd
b10
Basic panel
display
%
IM 11M13A01-04E
<8. Detailed Data Setting>
8.3.2 Preference Order of Output Hold Value
The output hold value takes the following preference order:
During error occurrence
During calibration
Preference order (high)
During maintenance
During warm-up
8.3.2E.siki
For example, if the current output is set to “4 mA” during maintenance, and “without hold” output
during calibration is preset, the output is held at 4 mA in the maintenance display. However, the output
hold is released at the time of starting the calibration, and the output will be held again at 4 mA after
completing the calibration and when the output stabilization time elapses.
8.3.3 Output Hold Setting
Table 8.5 lists parameter codes with set values for individual set items.
Table 8.5 Parameter Codes for Output Holding
Set items Parameter code Set value
During warm-up C04 04 mA
120 mA
2Holds Set value
During maintenance C05 0Without hold feature
1Last measured value
2Holds set values
During calibration C06 0Without hold feature
1Last measured value
2Holds set values
During error occurrence C07 0Without hold feature
1Last measured value
2Holds set values
Note: “C07” is not displayed when option code “/C2” or “/C3” (NAMUR NE 43 compliant) is specied.
8-5
8.3.4 Default Values
When the analyzer is delivered, or if data are initialized, output holding is by default as shown in
Table 8.6.
Table 8.6 Output Hold Default Values
Status Output hold (min. and max. values)Preset value
During warm-up 4 mA4 mA
During maintenance Holds output at value just before maintenance started4 mA
During calibrationHolds output at value just before starting calibration4 mA
During error occurrence Holds output at a preset value3.4 mA
IM 11M13A01-04E
8-6
<8. Detailed Data Setting>
8.4 Oxygen Concentration Alarms Setting
The analyzer enables the setting of four alarms ― high-high, high, low, and low-low alarms ―
depending upon the oxygen concentration. The following section sets forth the alarm operations and
setting procedures.
8.4.1 Setting the Alarm Values
(1) High-high and high alarm values
High-high alarms and high alarms are issued when they are set to be detected with parameter
codes [D41] and [D42], and if the measured values exceed the preset oxygen concentration
values specied with [D01] and [D02].
The oxygen alarm set values can range from 0 to 100%O2.
(2) Low and low-low alarm values
Low alarms and low-low alarms are issued when they are set to be detected with parameter
codes [D43] and [D44], and if the measured values are lower than the preset oxygen
concentration values specied with [D03] and [D04].
The oxygen alarm set values can be set in the range of 0 to 100%O
8.4.2 Alarm Output Actions
If the measured values of the oxygen concentration uctuate between normal (steady-state) values
and alarm setting, there may be a lot of alarm-output issuing and canceling. To avoid this, set the
delay time and allow for hysteresis for alarm canceling under the alarm output conditions, as Figure
8.2 shows.
.
2
When the delay time is set, an alarm will not be issued so quickly even if the measured value differs
from the steady-state and enters the alarm setpoint range.
If the measured value remains within the alarm setpoint range for a certain period of time (for the
preset delay time), an alarm will result.
On the other hand, there will be a similar delay each time the measured value returns to the steady
state from the alarm setpoint range (canceling the alarm status).
If hysteresis is set, alarms will be canceled when the measured value is less than or more than the
preset hysteresis values.
If both the delay time and hysteresis are set, an alarm will be issued if the measured value is in the
alarm setpoint range and the delay time has elapsed.
When the alarm is reset (canceled), it is required that the measured value be beyond the preset
hysteresis value and that the preset delay time.
Refer to Figure 8.2 for any further alarm output actions. The delay time and hysteresis settings are
common to all alarm points.
Alarm range
C
D
Hysteresis
2.0%
7.5%
High limit alarm setpoint
5.5%
A
B
Alarm output
Figure 8.2 Alarm Output Action
IM 11M13A01-04E
Oxygen concentration
ON
OFF
Delayed time:
5 seconds
Delayed time:
5 seconds
Delayed time:
5 seconds
F8-2E.ai
<8. Detailed Data Setting>
In the example in Figure 8.2, the high alarm point is set to 7.5vol%O2, the delayed time is set to ve
seconds, and hysteresis is set to 2vol%O2.
Alarm output actions in this gure are expressed as follows:
A. Although the oxygen concentration value exceeds the high limit alarm setpoint, it falls below the
high limit alarm setpoint before the preset delay time of ve seconds elapses. So, no alarm is
issued.
B. The oxygen concentration value exceeds the high limit alarm setpoint and the delay time elapses
during that measurement. So, an alarm is issued.
C. Although the oxygen concentration value falls below the hysteresis set value, the value rises
again and exceeds the hysteresis set value before the preset delay time elapses. So, the alarm
is not canceled.
D. The oxygen concentration value falls below the hysteresis set value and the preset delay time
elapses, so the alarm is canceled.
8.4.3 Alarm Setting
Set the alarm setpoints following Table 8.7 listing parameter codes.
Table 8.7 Parameter Codes for Oxygen Concentration Alarms
Even with alarms set, if “Not detected” has been set in the above alarm detection, no alarm is issued.
Be sure to set “Detected” in the above alarm detection if you use alarm features.
IM 11M13A01-04E
8-8
<8. Detailed Data Setting>
8.4.4 Default Values
When the analyzer is delivered, or if data are initialized, the default alarm set values are as shown in
Table 8.8.
Table 8.8 Alarm Setting Default Values
Set item Set value
High-high alarm setpoint 100%O
High alarm setpoint 100%O
Low alarm setpoint 0%O
Low-low alarm setpoint 0%O
Alarm hysteresis 0.1%O
Delayed alarm action 3 seconds
High-high alarm detection Not detected
High alarm detection Not detected
Low alarm detection Not detected
Low-low alarm detection Not detected
2
2
2
2
2
8.5 Contact Output Setting
8.5.1 Contact Output
Mechanical relays provide contact outputs. Be sure to observe relay contact ratings. (For details, see
Section 2.1, “General Specications”.) The following sets forth the operation mode of each contact
output. Contact output 1 you can select open or closed contact when the contact is “operated”.
For contact output 2, contact is closed. The relay for contact output 1 is energized when its contacts
are closed and vice versa. Accordingly, when no power is supplied to the equipment, those contacts
remain open. In addition, the relay for contact output 2 is energized when the corresponding contact is
open and de-energized when that contact is closed.
Table 8.9 Setting Contact Outputs
Operating state When no power is applied to this equipment
Table 8.10 Parameter Codes for Contact Output Setting
Set item Parameter code Set value
Contact output 1
Operation E10 0Operated in closed status.
Error E20 0Not operated if an error occurs.
High-high alarm E21 0Not operated if a high-high alarm
High alarm E22 0Not operated if a high alarm
Low alarm E23 0Not operated if a low alarm
Low-low alarm E24 0Not operated if a low-low alarm
During maintenance E25 0Not operated during
During calibration E26 0Not operated during calibration.
Output range change E27 0Not operated when changing
During warm-up E28 0Not operated during warming up.
Calibration gas
pressure
decrease
Unburnt gas
E29 0Not operated while a calibration
E32 0Not operated while an unburnt
detection
Note 1: Contact output 2 remains closed.
Note 2: The oxygen concentration alarm must be preset (see Section 8.4).
Note 3: Range change answer-back signal. For this action, the range change must be preset during the setting of contact inputs
Note 4: Calibration gas pressure decrease answer-back signal. Calibration gas pressure decrease must be selected beforehand
Note 5: Non-combusted gas detection answer-back signals. “Non-combusted gas” detection must be selected during the setting of
(see Section 8.5).
during the setting of contact inputs.
contact inputs.
(Normally de-energized)
1Operated when open. (Normally
energized)
(Note 1)
1Operated if an error occurs.
occurs.
1Operated if a high-high alarm
occurs.
(Note 2)
occurs.
1Operated if a high alarm occurs.
(Note 2)
occurs.
1Operated if a low alarm occurs.
(Note 2)
occurs.
1Operated if a low-low alarm
occurs.
(Note 2)
maintenance.
1Operated during maintenance
(see Subsection 8.3.1).
1Operated during calibration (see
Subsection 8.3.1).
ranges.
1Operated when changing
ranges.
(Note 3)
1Operated during warming up.
gas pressure decrease, contact
is being closed.
1Operated while a calibration gas
pressure decrease, contact is
being closed.
(Note 4)
gas detection, contact is being
closed.
1Operated while an unburnt
gas detection, contact is being
closed.
(Note 5)
8-9
IM 11M13A01-04E
8-10
<8. Detailed Data Setting>
WARNING
• Contact output 2 is linked to the detector’s heater power safety switch. As such, if contact
output 2 is on, the heater power stops and an Err-01 (cell voltage abnormal) or Err-02 (heater
temperature abnormal) occurs.
8.5.3 Default Values
When the analyzer is delivered, or if data are initialized, contact outputs are by default as shown in
Table 8.11.
Table 8.11 Contact Output Default Settings
Item Contact output 1 Contact output 2
High-high alarm
High alarm
Low alarm
Low-low alarm
ErrorO
During warm-upO
Output range change
During calibration
During maintenanceO
Calibration gas pressure
Unburnt gas detection
Operating contact status Open Closed (xed)
O: Present
decrease
NOTE
The above blank boxes indicate the items have been set off.
IM 11M13A01-04E
<8. Detailed Data Setting>
8.6 Contact Input Setting
The analyzer contact inputs execute set functions by accepting a remote (contact) signal. Table 8.12
shows the functions executed by a remote contact signal.
Table 8.12 Contact Input Functions
Set item Function
Calibration gas pressure
decrease
Measuring range change While contact input is on, the analog output range is switched to 0-25%O
Calibration start If a contact signal is applied, semi-automatic calibration starts (only if the semi-
Unburnt gas detection If a contact signal is on, the heater power will be switched off. (An one-to
While a contact signal is on, neither semi-automatic nor automatic calibrations
can be made.
automatic or automatic mode has been setup). Contact signal must be applied
for at least one second. Even though a continuous contact signal is applied, a
second calibration cannot be made. If you want to make a second calibration,
turn the contact signal off and then back on.
11-second time interval single-output signal is available as a contact signal.)
If this operation starts, the sensor temperature decreases and an error occurs.
To restore it to normal, turn the power off and then back on, or reset the analyzer.
.
2
8-11
CAUTION
• To conduct a semi-automatic calibration, be sure to set the Calibration setup mode to
“Semi-automatic” or “Automatic”.
8.6.1 Setting Contact Input
To set the contact inputs, follow the parameter codes given in Table 8.13.
Table 8.13 Parameter Codes for Contact Input Settings
Set item Parameter code Set value
Contact input 1 (function) E01 0Invalid
Contact input 2 (function) E02 0Invalid
Contact input 1 (action) E03 0Operated when closed
Contact input 2 (action) E04 0Operated when closed
1Calibration gas pressure
decrease
2Measuring range change
3Calibration
4Unburnt gas detection
1Calibration gas pressure
decrease
2Measuring range change
3Calibration
4Unburnt gas detection
1Operated when open
1Operated when open
8.6.2 Default Values
When the analyzer is delivered, or if data are initialized, the contact inputs are all open.
IM 11M13A01-04E
8-12
<8. Detailed Data Setting>
8.7 Other Settings
8.7.1 Setting the Date-and-Time
The following describe how to set the date-and-time. Automatic calibration works following this setting.
Use parameter code [F10] to set the date-and-time.
Table 8.14 Data-and-time Settings
Switch operationDisplayDescription
>∧
ENT
F10
Select the parameter code F10.
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
>∧
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
ENT
00.01.01
00.01.01
00.06.01
00.06.01
00.06.21
00.06.21
07.18
14.30
14.30
If you touch the [ENT] key, the current date will be displayed. The display
on the left indicates the date - January 1, 2000. To set June 21, 2000,
follow the steps below:
Touch the [>] key to move the position of the digit that is ashing to the
right.
Touch the [∧] key to change to 6.
Touch the [>] key to move the position of the digit that is ashing to the
right one digit.
Touch the [∧] key to change to 2.
Touch the [>] key to move the position of the digit that is ashing to the
right one digit.
Let the rightmost character ash, and touch the [>] key to display the time.
Continuously touch the [>] key, then the date and time are alternately
displayed. Displayed on the left is 7:18 a.m.
Omitted here.
Touch the [∧] key and enter the current time in same way as the date has
been entered, on a 24-hour basis. 2:30 p.m.
Displayed on the left means 2:40 p.m.
If you touch the [ENT] key, all the digits ash.
IM 11M13A01-04E
>∧
>∧
The symbol ( ) indicates that the corresponding keys are being touched, and the light characters indicate ashing.
ENT
ENT
14.30
F10
Touch the [ENT] key again to set the time.
If you touch the [>] and [ENT] keys together, the parameter code selection
display appears.
<8. Detailed Data Setting>
8-13
8.7.2 Setting Periods over which Average Values are Calculated and Periods over
which Maximum and Minimum Values Are Monitored
The equipment enables the display of oxygen concentration average values and maximum and
minimum values under measurement (see Subsection 10.1.1, later in this manual). The following
section describes how to set the periods over which oxygen concentration average values are
calculated and maximum and minimum values are monitored.
Procedure
Use the parameter-code table below to set the average, maximum and minimum oxygen
concentration values. Periods over which average is calculated and periods over which maximum and
minimum values are monitored can be set, ranging from 1 to 255 hours. If the set ranges are beyond
the limits specied, an “Err” will be displayed.
Table 8.15 Parameter Codes for Average, Maximum and Minimum Values
Set item Parameter code Set range Units
Periods over which average values
are calculated
Periods over which maximum
and minimum values are monitored
F11 1 to 255 Hours
F12 1 to 255 Hours
Default Value
When the analyzer is delivered, or if data are initialized, periods over which average values are
calculated are set to one hour, and periods over which maximum and minimum values are monitored
are set to 24 hours.
IM 11M13A01-04E
8-14
<8. Detailed Data Setting>
8.7.3 Setting Fuels
Input Parameters
The analyzer calculates the moisture content contained in exhaust gases.
The following sets forth the fuel parameters necessary for calculation and their entries.
The moisture quantity may be mathematically expressed by:
(water vapor caused by combustion and water vapor contained in the exhaust gas)
Moisture quantity =
=
Gw + Gw1
+ (water vapor contained in air for combustion)
actual exhaust gas(including water vapor) per fuel
G
x 100
x 100
=
=
where,
Ao : Theoretical amount of air per unit quantity of fuel, m
G: Actual amount of exhaust gas (including water vapor) per unit quantity of fuel,
m
Gw : Water vapor contained in exhaust gas per unit quantity of fuel (by hydrogen
and moisture content in fuel), m
Gw1: Water vapor contained in exhaust gas per unit quantity of fuel (moisture content
in air), m
Go: Theoretical amount of dry exhaust gas per unit quantity of fuel, m
m: Air ratio
X : Fuel coefficient determined depending on low calorific power of fuel, m
Z : Absolute humidity of the atmosphere, kg/kg ....... Figure 8.17
Gw + (1.61 x Z x m x Ao )
.
.
3
/kg (or m3 /m3)
3
/kg (or m3 /m3 )
Gw + (1.61 x Z x m x Ao)
Go + Gw + (m - 1) Ao + (1.61 x Z x m x Ao)
X + Ao x m
3
/kg (or m3 /m3 ) ............ 1 in Table 8.8
x 100
x 100
3
/kg (or m3 /m3 ) ............ 2 in Table 8.8
............ Equation 1
............ Equation 2
3
/kg (or m3 /m3 )
3
/kg (or m3 /m3 ) ... 3 in Table 8.8
8.7.3E.siki
Fill in the boxes with fuel parameters in Equation 2 above to calculate the moisture content. Use Ao,
Gw and X shown in Table 8.16. If there are no appropriate fuel data in Table 8.16, use the following
equations for calculation.
Find the value of “Z” in Equations 1 and 2 using Japanese Industrial Standards JIS B 8222. If a
precise measurement is not required, obtain the value of “Z” using a graph for the absolute humidity
indicated by a dry and wet bulb hygrometer.
IM 11M13A01-04E
<8. Detailed Data Setting>
8-15
For liquid fuel
Amount of water vapor in exhaust gas (Gw) = (1/100) {1.24 (9h + w)} [m /kg]
Theoretical amount of air (Ao) = {(12.38 / 10000) x H1} – 1.36 [m /kg]
3
3
Low calorific power = H1
X value = {(3.37 / 10000) x Hx} – 2.55 [m /kg]
3
where, H1: low calorific power of fuel
h: Hydrogen in fuel (weight %)
w: Moisture content in fuel (weight %)
Hx: Same as numeric value of H1
For gaseous fuel
Amount of water vapor in exhaust gas = (1/100) {(h2) + 1/2 ∑y (Cy hy) + w} [m /m ]
3
Theoretical amount of air = 11.2 x (H1/10000) [m /m ]
3
3
3
Low calorific power = H1
3
X value = (1.05 / 10000) x Hx [m /m ]
3
where, H1: low calorific power of fuel
h: Hydrogen in fuel (weight %)
w: Moisture content in fuel (weight %)
Hx: Same as numeric value of H1
For solid fuel
Amount of water vapor in exhaust gas (Gw) = (1/100) {1.24 (9h + w)} [m /kg]
Theoretical amount of air = {(1.01 x (H1 / 1000)} + 0.56 [m /kg]
where, w: Total moisture content in use (weight %)
h: Hydrogen content (weight %)
The average hydrogen content of coal mined in Japan, which is a dry ash-free type, is
5.7 %. Accordingly, “h” may be expressed mathematically by:
h = 5.7 [{100 – (w + a)} / 100] x (100 – w) / (100 – w1)
where, a: Ash content [%]
w1: Moisture content [%], analyzed on a constant humidity basis
Hh: Higher calorific power of fuel [kJ/kg]
H1: Low calorific power of fuel [kJ/kg]
Hx: Same numeric value of H1
F8-3E.ai
Figure 8.3 Fuel Calculation Formula
IM 11M13A01-04E
8-16
<8. Detailed Data Setting>
40
39
0.046
38
37
36
35
34
33
32
31
30
Wet-bulb
temperature, °C
25
24
22
20
18
16
14
12
10
8
6
4
2
0
-2
29
28
27
26
0.044
0.042
0.040
0.038
0.036
0.034
0.032
0.030
0.028
0.026
0.024
0.022
0.020
0.018
0.016
0.014
0.012
0.010
0.008
0.006
0.004
0.002
Absolute
humidity, kg/kg
Figure 8.4 Absolute Humidity of Air
IM 11M13A01-04E
0
2468
10 12 14 16 18 20 22 24 26 28 30 32 34 36
Dry-bulb temperature, °C
38
40
0.000
F8-4E.ai
<8. Detailed Data Setting>
Table 8.16 Fuel Data
For liquid fuel
•
properties
Type
Kerosene
Light oil
Heavy
oil
A
class
1
Heavy oil
B
class 2
Heavy
oil
C
class
3
Fuel
No.1
No.2
No.1
No.2
No.3
No.4
Specific
weight
kg/l
0.78~
0.83
0.81~
0.84
0.85~
0.88
0.83~
0.89
0.90~
0.93
0.93~
0.95
0.94~
0.96
0.92~
1.00
0.94~
0.97
Chemical component
(weight percentage)
CHO
14.0
85.7
85.6
13.2
12.0
11.8
11.3
10.9
10.7
10.9
10.5
0.7
0.7
0.4
0.5
0.5
0.5
0.5
85.9
84.6
84.5
86.1
84.4
86.1
83.0
N
0.5
0.5
0.4
0.4
0.4
0.4
0.4
0.5
1.2
0.5
2.0
3.0
1.5
3.5
1.5
3.5
S
Ash
w
content
0.0 0.0
0.0 0.0
0.3
0.05
0.4
0.05
0.5
0.05
0.5
0.1
0.5
0.1
0.6
0.1
2.0
0.1
Calorific power
kJ/kg
Higher
order
46465
45879
45544
45125
43827
43952
43116
43660
43032
Lower
order
43535
43032
42739
42320
41274
41441
40646
41190
40604
Theoretical
amount of
air for
combustion
Nm3/kg
11.4
11.2
10.9
10.8
10.7
10.7
10.5
10.7
10.3
Amount of combustion
gas Nm3/kg
CO
2 H
O
2
1.59
1.56
1.59
1.47
1.60
1.34
1.58
1.32
1.27
1.58
1.61
1.22
1.58
1.20
1.61
1.22
1.55
1.18
SO
0.00
0.00
0.00
0.01
0.02
0.01
0.02
0.01
0.02
2N2
9.02
8.87
8.61
8.53
8.44
8.43
8.32
8.43
8.18
Total
12.17
11.93
11.55
11.44
11.31
11.27
11.12
11.27
10.93
8-17
X
value
0.96
0.91
0.89
0.86
0.77
0.79
0.72
0.77
0.72
For gas fuel
•
Fuel
properties
Type
Coke oven
gas
Blast furnace
gas
Natural gas
Propane
Butane
(Gases)
Oxygen
Nitrogen
Hydrogen
Carbon
monoxide
Carbon dioxide
Methane
Ethane
Ethylene
Propane
Butane
Specific
weight
kg/Nm
0.544
1.369
0.796
2.030
2.530
1.43
1.25
0.09
1.25
1.96
0.72
1.34
1.25
1.97
2.59
Chemical component
(weight percentage)
3
COTotalH
9.0
CO2CH
2
4
50.525.92.63.9 0.1 8.0 20428 18209
CmH
O2N
n
25.0 2.0 20.053.0
2.0 88.4 3.2 1.64.2
C
3H8
C
3H8
90%, C4H
10%, C4H
10%
10
90%
10
(Molecular Formula)
O
2
N
2
H
2
CO
CO
2
CH
4
C2H
6
C2H
4
C3H
8
C4H
10
2
Calorific power
kJ/Nm
Higher
2CO
order
3391 3349
37883 34074
102055 93976
125496 115868
12767
12642
39750
69638
62991
99070
118623
128452
3
Lower
order
10758
12642
35820
63744
59060
91255
Theoretical
amount of
air for
combustion
3/m3
Nm
4.455
0.603
9.015
24.63
30.37
2.390
2.390
9.570
16.74
14.35
23.91
31.09
0.45
0.45
0.98
3.10
3.90
1.0
1.0
2.0
2.0
3.0
4.0
1
Combustion
product,
3
Nm
/ m
H2O
1.10
0.02
1.88
4.10
4.90
1.0
N
3.60
1.01
7.17
19.5
24.0
1.89
2
1.89
7.57
2.0
13.2
3.0
11.4
2.0
18.9
4.0
24.6
5.0
3
2
5.15
1.48
10.03
26.7
32.8
2.89
2.89
10.6
18.2
15.4
25.9
33.6
3
X
value
0.46
0.08
0.86
2.36
2.91
0.27
0.32
0.90
1.60
1.48
2.29
2.98
2
1
3
T8-16E.ai
IM 11M13A01-04E
8-18
Procedure
Use the parameter code table below to set fuel values.
Table 8.17 Setting Fuel Values
Amount of water vapor in
exhaust gas
Theoretical amount of airF21 1 to 20 m
X value F22 0 to 19.99
Absolute humidity of the
atmosphere
Default Values
When the analyzer is delivered, or if data are initialized, parameter settings are by default, as shown in
Table 8.18.
Table 8.18 Default Settings of Fuel Values
Amount of water vapor in exhaust gas 1.00 m
Theoretical amount of air 1.00 m
X value 1.00
Absolute humidity of the atmosphere 0.1000 kg/kg
<8. Detailed Data Setting>
Set item Parameter code Set value Engineering units
3
F20 0 to 5 m
F23 O to 1 kg/kg
Item Default setting
3
/kg (m3)
3
/kg (m3)
/kg (m3)
3
/kg (m3)
8.7.4 Setting Purging
Purging is to remove condensed water in the calibration gas pipe by supplying a span calibration
gas for a given length of time before warm-up of the detector. This prevents cell breakage during
calibration due to condensed water in the pipe.
Open the solenoid valve for the automatic calibration span gas during purging and after the purge time
has elapsed, close the valve to start warm-up.
Purging is enabled when the cell temperature is 100°C or below upon power up and the purge time is
set in the range of 1 to 60 minutes.
Displayed alternately
Figure 8.5 Display during Purging
Procedure
Use the parameter-code table below to set the purging time.
The allowable input ranges from 0 to 60 minutes.
Table 8.19 Purging Time
F8-5E.ai
Purging time F150 to 60 minutes
Default Value
When the analyzer is delivered, or if data are initialized, purging time is set to 0 minutes.
IM 11M13A01-04E
Set item Parameter code Set range Units
<9. Calibration>
9. Calibration
9.1 Calibration Briefs
9.1.1 Principle of Measurement
This subsection sets forth the principles of measurement with a zirconia oxygen analyzer before
detailing calibration.
A solid electrolyte such as zirconia allows the conductivity of oxygen ions at high temperatures.
Therefore, when a zirconia-plated element with platinum electrodes on both sides is heated up in
contact with gases having different oxygen partial pressures on each side, the element shows the
action of the concentration cell. In other words, the electrode in contact with a gas with a higher
oxygen partial pressure acts as a negative electrode. As the gas comes in contact with the zirconia
element in this negative electrode, oxygen molecules in the gas acquire electrons and become ions.
Moving in the zirconia element, they eventually arrive at the positive electrode on the opposite side.
There, the electrons are released and the ions return to the oxygen molecules. This reaction is
indicated as follows:
Negative electrode: O
Positive electrode: 2 O 2- O2 + 4 e
+ 4e 2 O
2
2-
9-1
The electromotive force E (mV) between the two electrodes, generated by the reaction, is governed
by Nernst’s equation as follows:
E = -RT/nF ln Px/Pa......................................................Equation (1)
where, R: Gas constant
T: Absolute temperature
n: 4
F: Faraday’s constant
Px: Oxygen concentration in a gas in contact with the negative zirconia electrode (%)
Pa: Oxygen concentration in a gas in contact with the positive zirconia electrode (%)
Assuming the zirconia element is heated up to 750°C, then we obtain equation (2) below:
E = -50.74 log Px/Pa......................................................Equation (2)
With this analyzer, the sensor (zirconia element) is heated up to 750°C, so Equation (2) is valid.
At that point, the relationship as in Figure 9.1 is effected between the oxygen concentration of the
measurement gas in contact with the positive electrode and the electromotive force of the sensor
(cell), where a comparison gas of air is used on the negative electrode side.
IM 11M13A01-04E
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