Yokogawa SC72 User Manual

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User’s Manual
Model SC72 Personal Conductivity Meter
IM 12D03D02-01E
IM 12D03D02-01E
3rd Edition
Page 2

Preface

Before using the Model SC72 Personal Conductivity Meter, read this manual thoroughly.
For safe use of this meter, the meter and the instruction manual include the following symbol marks.
Preface
WARNING
CAUTION
: Indicates that serious injury may result, if users fail to follow
instruction manual procedures.
: Indicates that minor injury to personnel, or serious damage to
the product, may result if users fail to follow procedures in the instruction manual.
WARNING
Do NOT use this instrument where there is a possibility of electrical shock. Do NOT touch any part of the electrode immediately after measuring very hot liquids —
otherwise, you may get burnt.
CAUTION
If the meter will not be used for an extended period of time, be sure to remove the battery. Otherwise battery leakage may occur, and may cause damage to the meter or cause erroneous meter operation.
The contents of this manual are subject to change without prior notice. Yokogawa Electric Corporation assumes no liability for damage, defects, or loss of the
product caused by any of the following:
User error; Inappropriate or out-of-specifications use of the product; Use in an unsuitable environment; Repair or modification of this or related products by persons other than Yokogawa-
authorized engineers.
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Preface
Liquid crystal display (LCD) display characters
The numeric LCD display is used to mimic alphabetic characters, as shown below:
Alphabet
A
B
C
D
E
F
G
H
I
J
K
L
M
Display
Alphabet
N
O
P
Q
R
S
T
U
V
W
X
Y
Z
Display DisplayNumerals
0
1
2
3
4
5
6
7
8
9
All display elements shown ON
Note Regarding Panels Shown in this Manual:
Panels shown in this manual should be regarded as examples. Actual panel format may vary depending on parameter settings and on type of connected sensor.
Showing all display elements lit
Display (gray represents flashing state)
F00.EPS
Flashing state: Lit state:
2
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Warranty and Service
Yokogawa products and parts are guaranteed to be free from defects in workmanship and materials under normal use and service for a period of (typically) 12 months from the date of shipment from the manufacturer.
Individual sales units may offer different warranty periods, so the original purchase order should be consulted for the conditions of sale. Damage caused by normal wear and tear, inadequate maintenance, corrosion, or due to chemical processes, is excluded from this warranty coverage.
In the event of a warranty claim, any items that are considered to be defective should be sent (freight paid) for repair or replacement (at Yokogawa discretion) to the service department of the relevant sales unit. The following information must be included in a letter accompanying the returned items:
Model code and serial number Copy of original purchase order showing the date Length of time used, and the measuring environment Fault symptoms, and circumstances of failure Statement whether service under warranty or out-of-warranty service is requested Complete shipping and billing instructions for return of goods, plus the name and
phone number of a contact person who can be reached for further information
Goods that have been in contact with process fluids must be decontaminated / disinfected before shipment, and a statement to this effect should be included. Safety data sheets for all process components that the goods have exposed to should also be included.
Preface
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Contents
CONTENTS
Preface...................................................................................................................... 1-1
1. Outline ................................................................................................................. 1-1
1.1 Features ......................................................................................................................... 1-1
1.2 Personal Conductivity Meter Specifications .................................................................. 1-2
1.3 When You Receive This Conductivity Meter................................................................. 1-3
1.4 Contents of Model SC72 Personal Conductivity Meter Package ................................. 1-4
1.5 Component Names and Functions ................................................................................ 1-5
1.6 Sensor Part Names and Functions ............................................................................... 1-6
1.7 Options (Available Separately) ...................................................................................... 1-8
1.8 Spare Parts .................................................................................................................... 1-8
2. Preparation.......................................................................................................... 2-1
2.1 Installing the Batteries ................................................................................................... 2-1
2.2 Connecting Sensor Cable.............................................................................................. 2-2
2.3 Setting Date and Time................................................................................................... 2-3
2.4 Setting Temperature Unit .............................................................................................. 2-4
2.5 Setting Cell Constant ..................................................................................................... 2-4
2.6 Setting Temperature Compensation Coefficient ........................................................... 2-6
3. Measurement ...................................................................................................... 3-1
3.1 Precautions .................................................................................................................... 3-1
3.2 Measurement Procedures ............................................................................................. 3-2
3.3 Measurement Panel....................................................................................................... 3-3
3.4 Saving Measured Value ................................................................................................ 3-3
4. Keyswitch Functions.......................................................................................... 4-1
4.1 Names and Functions of Keys ...................................................................................... 4-2
4.2 Liquid Crystal Display and Display Items ...................................................................... 4-4
4.3 Function Modes ............................................................................................................. 4-5
5. Handling of the SC72 Personal Conductivity Meter ........................................ 5-1
5.1 Tips to Maintain Meter Performance ............................................................................. 5-1
5.2 Washing the Electrode .................................................................................................. 5-2
5.3 Cleaning and Drying Connector .................................................................................... 5-3
5.4 Calibration with Standard Solution ................................................................................ 5-4
5.5 Storage and Maintenance ............................................................................................. 5-7
6. Troubleshooting ................................................................................................. 6-1
6.1 Causes of Abnormal Conductivity Display .................................................................... 6-1
6.2 Error Messages and Corrective Action ......................................................................... 6-2
6.3 Causes of Abnormal Measured Value .......................................................................... 6-4
6.4 Other conditions............................................................................................................. 6-4
7. Measuring Principles of this Instrument .......................................................... 7-1
7.1 What Is Conductivity? .................................................................................................... 7-1
7.2 Principles of Operation .................................................................................................. 7-2
7.3 Temperature Compensation and Finding Temperature Compensation Coefficient ..... 7-3
7.4 Wetted Part Materials of Sensors ................................................................................. 7-4
Appendix ..................................................................................................................... 1
Revision Record .......................................................................................................... i
4
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1. Outline

The Model SC72 Personal Conductivity Meter is an accurate, portable, easy-to-use conductivity meter. It includes not only self-diagnostic functions, to help ensure validity of readings, but also data storage functions to allow users to check past data. The meter is of waterproof construction so that it can safely be used outdoors on a rainy day, and can also withstand being accidentally dropped into water.

1.1 Features

Water r esistant case
When this meter is used with its dedicated sensor, it meets the requirements of class IP67 “Degree of Protection to be Provided by Enclosures” in IEC 60529.
Wide measurement range, and convenient “Auto Range” function
Sensors are available to cover measurement ranges between 0 to 2.000 mS/cm and 0 to 2 S/cm. Auto-range functions automatically set the optimum measurement range, making measurement easy.
Automatic temperature compensation
Automatic temperature compensation functions are provided for liquid measurement. Conductivity referenced to 258C can be obtained in solutions with temperature coefficients between 0.00 and 9.99%/8C. The temperature coefficients for NaCl solutions are already stored in the meter.
Calendar and time functions
Internal time functions allow “one-touch checking” of measurement date and time.
Data storage function
Up to 300 conductivities and temperature measurements, and their measurement date and time, can be saved. This function allows you to check past measurement data.
Automatic power off function
The meter will power off automatically if not operated during a preset time interval. The time interval can be set in one-minute increments in the range 1 to 120 minutes to
meet your application requirements. This automatic power off function can also be disabled, but it is wise to leave it enabled to conserve the batteries.
Simple alarm clock function
The meter can issue an alarm signal at a specified time. Even when meter power is turned off, the internal clock can issue an alarm signal.
Internal self-diagnostic functions display messages when appropriate. Bright easy-to view large LCD
Displays liquid conductivity, liquid temperature, temperature coefficient, date and time.
1. Outline
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1. Outline

1.2 Personal Conductivity Meter Specifications

Applicable measurement range:
• Sensors for high purity water measurement (cell constant: 0.05 cm-1) Conductivity: 0 to 2mS/cm, 0 to 20mS/cm, 0 to 200mS/cm, 0 to 40MV•cm Temperature: 0 to 808C*
• For general-purpose sensors (cell constant: 5 cm-1) Conductivity: 0 to 20mS/cm, 0 to 200mS/cm, 0 to 2mS/cm, 0 to 20mS/cm,
0 to 200mS/cm,
Temperature: 0 to 808C*
• For chemical-corrosion-resistant sensors (cell constant: 5 cm-1) Conductivity: 0 to 20mS/cm, 0 to 200mS/cm, 0 to 2mS/cm, 0 to 20mS/cm,
0 to 200mS/cm
Temperature: 0 to 808C*
• Sensors for high-conductivity measurement (cell constant: 50 cm-1) Conductivity: 0 to 2mS/cm, 0 to 20mS/cm, 0 to 200mS/cm, 0 to 2S/cm Temperature: 0 to 808C*
Resolution: Conductivity: Least significant digit: 1 digit;
Temperature: 0.18C
Repeatability (Conductivity):
62% (65% for general-purpose sensor on 0 to 200mS/cm measurement range)
Accuracy (Temperature): 60.78C (in the range 0 to 708C)
618C (when exceeding 708C)
Temperature compensation range:
variable 0.00 to 9.99%/8C, also (preset) NaCl solution temperature coefficient Measurement converted to conductivity at standard temperature of 258C
Measured liquid temperature: 0 to 808C (0 to 508C when the sensor cable is immersed in
Ambient temperature:0 to 508C Construction: IEC 60529, IP67 class of protection from environment Power requirement: Two of size AA batteries (LR6) Automatic power off interval: May be set in range 1 to 120 minutes Battery life: About 200 hours of continuous use, for long-life alkaline battery (life
may vary depending on battery type and ambient conditions)
External dimensions: Approximately 150 (H) x 61 (W) x 42 (D) mm (not including
protruding portions)
Weight: Approximately 220 g (including batteries)
1
1
1
1
water)
1-2
*1: Display range is from -10 to 1208C.
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EMC Compliance: EMI (Emission): EN 61326-1 Class B
Test Item
Electromagnetic radiation disturbance
Frequency Range
30 to 1000 MHz
CISPR 16-1 and 16-2
EMS (Immunity): EN 61326-1 Table 2 (For industrial locations)
Test ItemNo.
Electrostatic
1
discharge
RF amplitude
2
modulated electromagnetic field
* A: Normal performance within the specification limits: ±20% of the measured value. B: Temporary degration or less of function or performance which is self-recoverable. ** Display value may be affected by strong electromagnetic field.
Test Specification Basic Standard
4 kV (contact) 8 kV (air)
80 to 1000 MHz, 10 V/m (unmodulated) 80% AM (1 kHz)
1.4 to 2.0 GHz, 10 V/m (unmodulated)
80% AM (1 kHz)
2.0 to 4.0 GHz,
3 V/m (unmodulated) 80% AM (1 kHz)
IEC 61000-4-2
IEC 61000-4-3

1.3 When You Receive This Conductivity Meter

Confirm that all SC72 meter package components (refer to Contents of Model SC72 Personal Conductivity Meter Package in Section 1.4 and sensor models described in Sec.
1.6, “Sensor Part Names and Functions.”) have been received. Carefully inspect the
meter and sensor, referring to Section 1.5, “Component Names and Functions” when assembling meter and sensor.
Particular attention should be taken:
* Not to twist or force the cable. * Not to hit or drop the meter. * Not to get the sensor connector dirty.
1. Outline
Basic Standard
T0101.EPS
Performance
Criteria*
A
B**
A
A
T0102.EPS
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1. Outline

1.4 Contents of Model SC72 Personal Conductivity Meter Package

Quick Manual
SC72 - - - AA
User's
Manual
1
3
2
4
Instrument Card
6
5
1-4
7
11 11 11 11
SC72 - 11 - - AA SC72 - 31 - - AA
*1 *1 *1 *1
Model Suffix code SC72
Sensors -00
-11
-21
-23
-31
-41
Label -J language - E
- -AA
*1 The meter model number and cell constants, as well as the sensor model no. (SC72SN-u-AA), are shown on the nameplate.
8
SC72 - 21 - - AA SC72 - 23 - - AA
Specification
Personal conductivity meter Meter only, without sensor With sensor for high purity water measurement (cable length: 0.75m) With general-purpose sensor (cable length: 0.75m) With general-purpose sensor (cable length: 3m) With chemical-resistant sensor (cable length: 0.75m) With sensor for high-conductiivity measurement (cable length: 0.75m) Japanese English Always -AA
9
SC72 - 41 - - AA
Name
No.
Personal conductivity meter
1
Two dry batteries
2
Two i nstruction manual
3
Non-slip pads (two)
4
Hand strap
5
Instrument card
6
Sensor for high purity water
7
measurement General-purpose sensor
8
Chemical-resistant sensor
9
Sensor for high-conductivity
10
measurement Sensor cleaner
11
(five cotton swabs)
10
F010401.EPS
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1.5 Component Names and Functions

1. Outline
O-ring
Sensor cable connector
Used to connect a dedicated conductivity sensor to the
personal conductivity meter.
Can attach hand strap here
Display
Displays conductivity,
temperature, and temperature coefficient simultaneously.
Key switches
PERSONAL SC METER
MODEL STYLE No.
E000001
2004.
Battery box cover fixing screw
SC72 S1.0
Instrument name plate
with model number and serial number
F010501.EPS
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1. Outline

1.6 Sensor Part Names and Functions

Four types of sensors are available for use with the Model SC72 Personal Conductivity Meter:
(1) sensor for high purity water measurement (cell constant 0.05 cm-1), (2) general-purpose sensor (cell constant 5 cm-1), (3) chemical-resistant sensor (cell constant 50 cm-1), and (4) sensor for high-conductivity measurement (cell constant 50 cm-1). Check the model
number and cell constant on the name plate to confirm which type of sensor you have.
Model number and cell constants display plate example
MODEL
SC72SN
SUFFIX NO.
SC72SN Conductivity sensors for personal conductivity meter
Specification
SC72SN
-11
-19
-21
-23
-29
-31
-39
-41
-49
-AA
1: Part number of SC82 (previous model).
* *2: Waterproofing is not guaranteed if you use SC82-type conductivity sensor in conjunction
with SC72 meter.
Conductivity sensor for personal conductivity meter For SC72; for high purity water measurement (cable length: 0.75m) For SC82; for high purity water measurement (cable length: 0.75m) For SC72; for general purpose type (cable length: 0.75m) For SC72; for general purpose type (cable length: 3m) For SC82; for general purpose type (cable length: 0.75m) For SC72; for chemical-resistant type (cable length:
0.75m) For SC82; for chemical-resistant type (cable length:
0.75m)
*
For SC72; for high conductivity measurement (cable length: 0.75m) For SC82; for high conductivity measurement (cable length: 0.75m) Always -AA
CELL CONST
Made in Japan
2
*
2
2
*
S1.0000001-11-AA STYLE
Cell constants
RemarksModel Suffix code
K9221XB
2
*
K9221XA
K9221XC
K9221XD
F010601.EPS
1
*
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Sensor for high purity water measurement
SC72 - 11 - - AA
Model number and
cell constants display plate
Watertight cover
Prevents moisture from entering
connector and causing leakage between pins.
Connector
Connects sensor cable to
conductivity meter
Outer electrode
connection
(SUS316
stainless seel)
Inner electrode
(SUS316
stainless seel)
(SC72SN-11-AA)
*1
Sensor body
Outer electrode (SUS316 stainless seel)
*1
Sensor
cable
Sensor grip
Plastic body can
withstand temperatures up to 808C.
General-purpose sensor
Model number and
cell constants display plate
SC72SN-23-AA)
Watertight
cover
Connector
*1(SC72SN-21-AA,
Sensor body
Cover (Plastic)
SC72 - 21 - - AA SC72 - 23 - - AA
Inner electrode (Titanium)
Edge electrode (Titanium)
1. Outline
*1
Sensor cable
Sensor grip
F010602.EPS
Chemical-resistant sensor
Model number and
cell constants display plate
Watertight
cover
*1(SC72SN-31-AA)
SC72 - 31 - - AA
*1
Sensor
cable
Sensor for high-conductivity measurement
SC72 - 41 - - AA
Model number and
cell constants display plate
Watertight
cover
Connector
*1(SC72SN-41-AA)
Connector
Air vent
Sensor body (glass)
Inner electrode (platinum black)
Sensor grip
Air vent
*1 SC72SN-u will be described on sensor's name plate for the model number.
*1
Sensor grip
Sensor body (glass)
Inner electrode (platinum black)
Sensor cable
F010603.EPS
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1. Outline

1.7 Options (Available Separately)

The following options are available for the Personal Conductivity Meter for your convenience. When ordering, specify part number shown below.
Standard solution
(Part no.: K9221ZA)
0.1mol/l NaCl solution for calibration (250ml)
This soft black carrying case holds conductivity meter and sensor.
Soft case
(Part no.: B9269KJ)
Approx. 280
Approx. 140
(Part no.: K9220XN)
Unit: mm
Approx. 30
This stand holds the sensor when the conductivity meter is used on a table. It is made of rustproof stailess steel.

1.8 Spare Parts

O-rings and gaskets are important parts to ensure that the SC72 meter is water resistant. Replace these parts as required. Refer to Section 5.5, “Storage and Maintenance” for replacement.
O-ring and gasket set
(Part no.: K9654AY)
Sensor stand
F010701.EPS
1-8
Two battery box gaskets Two sensor connection O-rings
F010801.EPS
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2. Preparation

2.1 Installing the Batteries

Install the batteries first.
CAUTION
Select a relatively moisture-free location when installing batteries in the meter. When installing batteries, observe correct polarity (battery orientation). Failure to do so
may damage to the meter. Remove batteries from the meter if it is to be stored for an extended period of time. Do not leave dead batteries in the meter. They may leak and cause meter failure or
erratic operation of the meter. When replacing batteries, replace both batteries at the same time. If only one battery is
replaced, the new battery may discharge into the old battery, which may leak chemicals and damage the meter.
If the battery box gasket is damaged or dirty then the unit may no longer be waterproof; replace the gasket in this case.
(1) Loosen the screw holding the battery
box cover using a coin or similar object.
(2) Remove the battery box cover, and
then install the batteries observing polarity diagram inside.
(3) Make sure the gasket on the inside
458 or more
Batteries
Gasket
Press with your fingers
rim of the battery box is free of foreign material.
(4) Put the cover back on. Insert the tabs
on the top of the cover into the slots at an angle of at least 458 and lower the cover into position.
(5) Press the both ends of the cover down
with your fingers and tighten the screw to fix the cover onto the unit using a coin or similar object.
Note: Do not attempt to tighten further
when you feel resistance before the cover is fastened in place. Loosen the screw once and retighten.
2. Preparation
F020101.eps
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2. Preparation

2.2 Connecting Sensor Cable

Connect the sensor cable as shown below.
CAUTION
Select a relatively moisture-free location when connecting the sensor cable. When connecting the sensor cable, tighten by turning only the silver locknut, do not turn
the cable or waterproof cover. Also take care not wet or contaminate the connector. Model SC82 sensors can be connected, but these are not guaranteed to be waterproof
when used with this meter.
(1) Pull the waterproof cover along the
sensor cable away from the connector to expose the locknut.
(2) Connect the connector to the meter
body*. Then tighten firmly by turning only the locknut.
* Align the slots of the sensor cable
connector with the posts of the connector on the meter.
(3) Move the waterproof cover toward
the connector until it contacts with the O-ring* on the meter body.
* Make sure that the O-ring is free of
foreign material.
(4) Push and rotate the waterproof cover
1/4 turn (90 degrees) clockwise to lock into place.
(2)
Waterproof cover
O-ring
(3)
Locknut (Silver)
(1)
(4)
F020201.eps
Caution: It is recommended that, as far as possible, you leave the sensor connected to the
meter to help ensure that the connector does not get dirty.
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2.3 Setting Date and Time

After installing the batteries, set the date and time. Note that if the power is turned off before setting “minutes,” start with the date setting when you turn on the power next time.
If you replace the batteries, the date is not affected, but the time is reset. Reenter the time.
Caution: If the sensor is not connected then an error will be displayed on the meter.
• Setting method
After installing batteries, press and hold the all display elements turn on and the date setting display automatically appears. Set year,
month, day, hours, and minutes as follows: Caution: If you stop part way through the date and time setting then the meter will beep
and the date and time will not be updated.
After
POWER
pressing
key for at least 1 sec.
POWER
key for at least one second. Then
2. Preparation
Year setting
After several seconds
F/ENT
F/ENT
to confirm
to confirm
to set
Day setting Hour setting (24-hour format)
to set
F/ENT F/ENT
to confirm
to set
After several seconds
Month setting
to set
F/ENT
to confirm
Minute setting
to set
to confirm
or
F020301.EPS
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2. Preparation

2.4 Setting Temperature Unit

Default temperature units are 8C. To change to 8F, refer to Sec. 4.3 (13) Set temperature units (tP.U) panel.

2.5 Setting Cell Constant

Even for sensors of the same type, each sensor has its own distinct cell constant. So, set the proper cell constant as indicated on the sensor cable.
Whenever sensors are replaced, be sure to change the cell constant setting in the meter accordingly. Cell constants once set are stored in non-volatile memory and are not lost even when the batteries are replaced.
• Setting cell constants
Press the
Refer to Sec. 4.3 (4).
F/ENT
key to switch to function mode. Then select the C.C display with the key and access the cell constant setting display with the key to set the cell constant, then press the
F/ENT
key to confirm it.
F/ENT
key. Use the
2-4
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F/ENT
for Function mode
select C.C
for C.C panel
F/ENT
to enter C.C
F/ENT
2. Preparation
MEAS
You can abort this procedure at any time by pressing mode.
IM 12D03D02-01E
F020501.EPS
MEAS
to revert to measurement
2-5
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2. Preparation

2.6 Setting Temperature Compensation Coefficient

As described in Section 7.3, liquid conductivity varies with liquid temperature. Therefore, if concentration is measured by conductivity, the conductivity must be converted to equivalent conductivity at a certain temperature. This instrument incorporates standard temperature conversion functions to convert liquid conductivity measurements to equivalent conductivity at 258C. To display equivalent liquid conductivity at 258C, set the temperature compensation coefficient as described in this section.
Temperature coefficient for NaCl solutions is stored in this instrument. If any other solution is used, set the temperature compensation coefficient manually.
Refer to Sec. 4.3 (2) Temperature compensation setting (t.Co) panel.
2-6
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• Set the temperature compensation coefficient
F/ENT
for Function mode
select t.Co
for t.Co panel
F/ENT
For NaCl solutions Manual setting
select NaCl or %/8C (%/8F)
2. Preparation
F/ENT
MEAS
IM 12D03D02-01E
F/ENT
Set the temperature compensation coefficient with the keys.
F/ENT
MEAS
The temperature coefficient you set is displayed here
F020601.EPS
2-7
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2. Preparation
2-8
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3. Measurement

3.1 Precautions

(1) Be sure to check that the cell constant and the temperature coefficient are set
correctly.
(2) Check that the plastic cover (for general-purpose sensor) and outer electrode (for
high purity water measurement) are secure.
(3) Do not use the SC72 meter to measure liquids with temperatures over 808C. (If the
sensor grip is immersed, liquid temperature shall be below 508C.) Do not use the meter to measure extremely corrosive liquids such as solutions of hydrofluoric acid.
(4) Remove dirt and stains from the meter with soft tissue. If necessary, wipe the
meter case with neutral detergent.
(5) If any problem with the meter arises during measurement, refer to the
Troubleshooting section later in this manual to determine the cause.
(6) After finishing measurement, flush stains on the sensor and measured solutions
with water, and store the meter (refer to Chapter 5, “Handling of the SC72 Personal Conductivity Meter”).
When the meter is used on a table:
The meter is designed as a portable instrument; however, to use it on a table, attach non­slip pads (supplied with the instrument) at top and bottom of the meter to stop it from moving when the sensor is moved.
3. Measurement
IM 12D03D02-01E
Non-slip pads
PERSONAL SC METER
MODEL
SC72
STYLE
S1.0
No.
E000001
2004.
F0301.EPS
Figure 3.1 Position of Non-slip Seats
3-1
Page 23
3. Measurement

3.2 Measurement Procedures

Dipping sensor into liquid
To help avoid errors due to air bubbles around the sensor element (inner electrode), immerse the sensor into the liquid to be measured so that its air vent is below liquid level. To dislodge any air bubbles from the inner electrode, dip the sensor into the liquid and move it up and down two or three times.
Air vent
Measuring liquid level
Cover
Electrode element
Figure 3.2 Dipping Sensor in Liquid (for general-purpose sensors)
If air bubbles are on this section, measurement error may occur.
F0302.EPS
3-2
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3.3 Measurement Panel

Immerse the sensor into the liquid to be measured to display the liquid conductivity on the LCD display.
There are three measurement panel display types: the standard display, calendar, and clock display.
MEAS
Use the
key to toggle the display type.
Standard display Calendar display Clock display
conductivity
MEAS MEAS
3. Measurement
temperature
T emperature
compensation coefficient
This display appears when NaCl
solution is specified at temperature compensation coefficient setting.
day month yearMeasuring liquid
MEAS

3.4 Saving Measured Value

The meter offers two ways of storing measured values: HOLD for temporary storage and non-volatile data storage that retains data even if batteries are removed.
(1) HOLD
If the held (display no longer changes).
Press the
key is pressed during measurement, the measured values are temporarily
HOLD
MEAS
HOLD
key or
key to return to the measurement mode.
HOLD
HOLD
MEAS
or
F030401.EPS
hour : minute
F030301.EPS
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3. Measurement
(2) Data storage
DATA
If the
F/ENT
key is pressed during measurement, mark starts flashing. Press the
key, then currently measured data can be stored in nonvolatile memory. Data
stored are measured conductivity, measured temperature, date and time. Up to 300 data including individually deleted data can be stored. If you attempt to store more data,
is displayed.
If is displayed even though the number of data stored is less than 300, perform “defrag” [refer to Section 4.3 (15), “Defragment storaged data (DFLG) panel”]. By doing
so, you can increase the number of data to be stored. To check stored past data, refer to 4.3 (1) dAt (display stored measurement value) later
in this manual.
While is flashing, press the mode without storing data.
While is flashing, press or keys to abort data storage.
MEAS
Execute data storage.
Press key to store data while is flashing.
F/ENT
MEAS
key or
DATA
DATA
Abort data storage.
key to return to measurement
DATA
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4. Keyswitch Functions

There are seven membrane keys on the keyboard of the Personal Conductivity meter. The following key functions are provided.
* Display the conductivity, measured temperature and temperature coefficient. * Display the conductivity, date and time. * Hold conductivity and temperature measurements. * Store conductivity and temperature measured data. * Other functions such as parameter setting.
When meter is OFF, press for at least 1 sec. to turn on power. When meter is ON, press for about 2 sec. to turn off the power. Automatic Power OFF function default: 20 min. inactivity.
If you press this key during measurement, mark is displayed, and present measured values are held. To cancel, press
HOLD
or keys.
MEAS
If pressed during measurement, mark flashes.
F/ENT
Press key to store measured values in memory. To abort data storage and return to
MEAS
MEAS mode, press or key
DATA
again while mark is flashing.
Auto Power Off
POWER
MEAS
HOLD
F/ENT
DATA
4. Keyswitch Functions
Press to start measurement mode. If already in MEAS mode, it switches the display panel.
If pressed while in
MEAS mode, switches
to function mode. Also
used to enter set
value.
Change set value.
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4. Keyswitch Functions

4.1 Names and Functions of Keys

POWER
: Power ON/OFF key
If nothing is displayed on the LCD, hold down this key for about one second or more to turn the power on.
If something is displayed on the LCD, pressing and holding this key for about two seconds turns power off. If no keys are pressed during a certain time interval, power turns off automatically (refer to “A.oFF,” Set Auto Power Off Interval of Section 4.3 (10)).
Press the
: HOLD key
key to hold the currently-displayed conductivity and temperature
HOLD
HOLD
measurement values ( mark turns on). Press the
HOLD
key or
MEAS
key again to return to measurement mode
and turn mark off.
DATA
: Data key
When the meter is in measurement mode, pressing this key causes the mark to flash and the currently-displayed conductivity and temperature measurement values to be temporarily stored. Pressing the
key while the mark is flashing stores
F/ENT
the data and returns to measurement mode. To abort data storage, press the
DATA
key or
MEAS
key again; the mark
turns off and the meter returns to measurement mode.
MEAS
: Measurement key
In measurement mode, pressing this key toggles between different LCD display types (refer to Section 3.2, “Measurement Procedures”).
If this key is pressed while in any mode other than measurement mode, the instrument returns to measurement mode. If you want to cancel any operation, pressing this key returns you to measurement mode.
: Setting change key
Used to change settings.
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4. Keyswitch Functions
F/ENT
: Entry key
In measurement mode, pressing this key switches the meter to function mode (see Section 4.3, “Function Modes”). This key is also used to confirm set values.
Buzzer (Beep) sound
When a key is pressed, the buzzer beeps. Where the buzzer beeps once, or when it beeps three times continuously, the meaning is as follows:
(1) When the buzzer beeps once:
This means that key operation was accepted.
(2) When the buzzer beeps three times continuously:
This means that the key operation was not accepted.
To disable the above key entry beep, refer to Sec. 4.3 (11) Set buzzer ON/OFF (bZ.o) panel.
Note: the sound volume level of the beep cannot be adjusted by the user.
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4. Keyswitch Functions

4.2 Liquid Crystal Display and Display Items

Displays and their explanations are shown below.
Remaining battery life display
Temp. compensation setting mode
Manual range setting mode Data save mode
HOLD mode
Calibration with std. solution Cell constant set mode
(1) Remaining battery life display
Remaining battery life is always displayed stepwise. When display is , battery is normal. When a flashing is displayed, battery power is low. Replace the
batteries immediately if the above flashing battery symbol appears. Press confirm that display turns off, then refer to Sec. 2.1 for battery replacement procedure.
(2) T emperatur e compensation setting mode
This mark appears when temperature compensation is being set (refer to Temperature compensation setting (t.Co) panel in Section 4.3 (2))
(3) Manual range setting mode
Normally autoranging is used, and optimum range is selected automatically, but if fixed (manual) range setting is used then this mark appears (refer to Range selection (rnG) panel in Section 4.3 (3)).
(4) Data save mode
This mark appears when measured data are stored or when already-stored data are accessed (see Operation of DATA key in Section 4.1, or Display stored measurement value in Section 4.3 (1)).
(5) HOLD mode
This mark appears while measured data are being temporarily held (refer to Operation of
key in Section 4.1).
HOLD
POWER
F040201.EPS
and
(6) Calibration with standard solution
This mode display appears when the calibration with standard solution is conducted (refer to Calibration with standard solution (CAL) panel in Section 4.3 (5)).
(7) Cell constant set mode
This mode display appears when the sensor cell constants are manually set (refer to Cell constant setting (C.C) panel in Section 4.3 (4)).
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4.3 Function Modes

Outline
4. Keyswitch Functions
A variety of functions are supported by function mode. Press the
F/ENT
key to switch
from measurement mode to function mode. This mode supports the functions listed in the table below.
Note: The last selected and executed item is displayed when you switch to function
mode. Pressing the keys displays the items listed in Table 4.1 in turn.
Methods of setting items
Use the keys to move to the desired item. While the desired item is flashing, press the
To return from the function mode to the measurement mode, press the
Item*
dAt t.Co
rnG C.C CAL
dEL.A dAtE
tIME ALM A.oFF bZ.o SC.U tP.U VEr dFLG
F/ENT
key to set each item in detail.
Table 4.1 Items Set in Function Mode
1
Description
Display stored measurement value Temperature compensation setting Range selection
Cell constant setting Calibration with standard solution
Delete all stored measuring data Date setting
Time setting Alarm time setting
Set Auto Power Off interval Set buzzer ON/OFF Set measurement unit Set temperature unit
Version number display Defragment storaged data
*1: Numeric display used to simulate alphabetic character display. *2: 2: This data is not user-settable *3: The standard cell constant for the connected sensor is displayed.
Default*
no dAtA
0.00 %/ 8C Auto Standard cell constant*
2
2
2004, January, 1 0 hour 0 minute oFF 20 min on S/cm
8C
2
2
2
3
MEAS
For details, refer to:
Item (1) Item (2) Item (3) Item (4) Item (5) Item (6) Item (7) Item (8) Item (9) Item (10) Item (11) Item (12) Item (13) Item (14) Item (15)
key.
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4. Keyswitch Functions
Details about how to set each item are provided below.
(1) Display stored measurement value (dAt) panel
Used to display stored measurement values. mark appears in the top left corner of the display. The last-stored conductivity and temperature values are displayed first.
The stored data item number flashes in the lower left corner. Pressing the displays the date and time of this stored data, and pressing this key again allows
individual data to be deleted (refer to the figure next page). Pressing keys allows you to scroll through all past data. If no data are stored,
“no dAtA” is displayed at the bottom of the display.
• Individual deletion of stored data items
After displaying date and time of this stored data, pressing the panel with dEL. Pressing the
F/ENT
key on this panel switches to the Data Delete
panel. First is flashing, so use keys to switch to flashing , then press the
F/ENT
key to delete the stored measurement data that is currently displayed.
• Stored data item numbers after deletions
When you display the dEL panel, the number displayed at the bottom left indicates the stored data number relative to the beginning of the data store. This does not necessarily represent the number of stored data. If you delete a data item, item numbers of data that follow it will be decreased by one (see explanation below).
• Data display after deletion
If a data item is deleted, the data item after it is displayed. If there is no data after it (i.e. it was the last stored data item, the data item before it (if any) is displayed.
When data item 012 (lastest data) is deleted:
DATA
key
DATA
key displays a
4-6
Item 012 is deleted, so item 011 becomes the latest
When data item 011 is deleted
Item 011 is deleted, so item numbers of following items (only item 012 in this case) are decremented by 1.
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4. Keyswitch Functions
Stored measurement data
Latest data
F/ENT
When no stored data.
F/ENT
DATA
F/ENT
to display other data
DATA DATA
"Delete stored data" panel
DATA
Delete stored data
F/ENT
Year that data was storedDsy, month data was stored
DATA
Time stored
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4. Keyswitch Functions
(2) Temperature compensation setting (t.Co) panel
This panel is used to change the temperature compensation type and temperature coefficient setting. The TEMP mark appears on the panel.
• Automatic temperature compensation for NaCl solution
Press the keys to select NaCl . Then press the
• Manual temperature compensation coefficient setting
Press the keys to select %/8C (or %/8F). Then press the
F/ENT
key.
F/ENT
key. Use the
keys to set the temperature coefficient. Then press the
F/ENT
Use keys to select
F/ENT
For manual setting: When %/8C (or %/8F) is displayed, set the temperature coefficient with
keys. Press key to complete the temperature coefficient setting.
F/ENT
For NaCl: When NaCl is displayed, press key to confirm.
F/ENT
F/ENT
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key.
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4. Keyswitch Functions
(3) Range selection (rnG) panel
Change the current measuring range. Use the keys to change between autoranging and fixed range. For fixed range, mark appears.
Relationships between automatic and fixed ranges for different sensors
For general-purpose sensor
(SC72-21, -23)
*1 *1
Autorange
For chemical-resistant sensor
(SC72-31)
Autorange
(Example) For general-purpose sensor (SC72-21, -23) used with 0-200.0mS/cm
*1
Fixed range 5 (0-20.00mS/cm)
Fixed range 4 (0-200.0mS/cm)
Fixed range 3 (0-2.000mS/cm)
Fixed range 2 (0-20.00mS/cm)
Fixed range 1 (0-200.0mS/cm)
With sensor for high-conductivity
measurement (SC72-41)
Autorange
Fixed range 4
(0-2.000mS/cm)
Fixed range 3 (0-20.00mS/cm)
Fixed range 2 (0-200.0mS/cm)
Fixed range 1 (0-2.000S/cm)
With sensor for high-purity water
*1
measurement (SC72-11)
Fixed range 5 (0-20.00mS/cm)
Fixed range 4 (0-200.0mS/cm)
Fixed range 3 (0-2.000mS/cm)
Fixed range 2 (0-20.00mS/cm)
Fixed range 1 (0-200.0mS/cm)
Autorange
Fixed range 4
(0-40.0MVcm)
Fixed range 3 (0-2.000mS/cm)
Fixed range 2 (0-20.00mS/cm)
Fixed range 1 (0-200.0mS/cm)
F/ENT
Autorange
Press key
or key
*1
five times
Fixed range 1
F/ENT
Set range 1 fixed.
*1: Model no. of sensor alone is SC72SN-u. (refer to Sec. 1.6)
Refer to Relationships between automatic and fixed ranges... (above left)
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4. Keyswitch Functions
(4) Cell constant setting (C.C) panel
This panel with the mark is used to set the cell constant manually.
Use the keys to set the cell constant. Then press the
F/ENT
key.
Typical cell constants are as follows: For pure water sensor (SC72-11): 0.05 cm For general-purpose (SC72-21, -23) and chemical-resistant sensors (SC72-31): 5 cm Sensors for high-conductivity measurement: 50 cm
-1
-1
-1
When setting the cell constant, you should check the nameplate (attached to sensor cable) for the model number and cell constant.
The cell constant can be set in the range 6 20% of standard cell constant. For example, for general-purpose sensors with standard cell constant of 5 cm-1, a cell constant ranging from 4.00 to 6.00 can be set.
Once the cell constant is set, it remains stored in memory even when batteries are removed.
The general-purpose cell has the same cell constant whether used with SC72-21 or SC72­23 type.
Refer to Sec. 2.4 for cell constant setting procedure.
Use key to set the cell constant. Then press
F/ENT
the key to complete setting.
F/ENT
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4. Keyswitch Functions
(5) Calibration with standard solution (CAL) panel
This panel is used for calibration with standard solution. Refer to Sec. 5.4 for a description of the calibration procedure. In CAL mode, the mark appears at the top of the panel and all digits of the present measurement value flash.
After the measurement stabilizes, press the
F/ENT
key to display the measured value at
that time. Only the least significant digit flashes. Use the keys to set the desired calibration value, then press the
F/ENT
key to complete the calibration.
The meter internal cell constant is changed after completing calibration with standard solution. Referring to (4) cell constant setting (C.C) panel, confirm the updated cell constant value and rewrite the cell constant (refer to the value on the plate attached to the sensor cable. Rewritten cell constants remain even if batteries are removed.
To abort calibration using standard solution, press the
MEAS
key to return to
measurement mode.
All digits of measurement value are flashing
Least significant digit is flashing
F/ENTF/ENT
Press the key to complete calibration.
F/ENT
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4. Keyswitch Functions
(6) Delete all stored measuring data (dEL.A) panel
This panel is used for deleting all stored data. When you switch to this panel, is flashing. Use the keys to select .
Press the
F/ENT
key to delete all the data completely.
F/ENT
to set
F/ENT
to execute delete all
F/ENT
to abort
(7) Date setting (dAtE) panel
Set the date for the meter; year (four digits), month, day in order.
Use the keys to set year, month, and day. Then press the setting.
Year setting Month setting
F/ENT
F/ENT
F040306.EPS
F/ENT
key to complete
The calendar functions will be correct through to the year 2090.
4-12
Day setting
F/ENT
F/ENT
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(8) Time setting (tIME) panel
For the converter, set the time (24-hour display), minutes in order.
4. Keyswitch Functions
Use the keys to set hours and minutes. Then press the setting.
Hour setting (24-hr clock) Minute setting
F/ENT F/ENT
F/ENT
F/ENT
key to complete
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4. Keyswitch Functions
(9) Alarm time setting (ALM) panel
Alarm Enable (ON) / Disable (OFF) and alarm occurrence time (hours and minutes) can be set. Use the keys to set alarm time.
Alarm time setting methods are the same as for (8) Time setting (tIME). Alarms sounds for about 15 seconds continuously. Acknowledge alarm by pressing any
key to stop alarm sound. If no key is pressed to acknowledge the alarm occurrence, alarms sound for 15 seconds again three and six minutes after the preset alarm time.
Note: The day of the week is not displayed
F/ENT
alarm sounds at preset time every day
alarm sounds at preset time
from Monday to Friday
F/ENT
Hour setting (24-hr clock)
F/ENT
Minute setting
4-14
alarm sonds once at preset time
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4. Keyswitch Functions
(10) Set Auto Power Off interval (A.oFF) panel
Set the time interval for the power to turn off automatically if no key is pressed during a preset time interval. The Interval can be set to between 1 and 120 minutes. If “0 minutes” is set, automatic power OFF functions are disabled, so — without some care — batteries won’t last very long.
Use key to set
F/ENT
F/ENT
to confirm
F040310.EPS
(11) Set buzzer ON/OFF (bZ.o) panel
This panel is used to enable or disable the beep (“buzzer”) that sounds when keys are pressed.
Use the keys to enable / disable. Then press the
F/ENT
key to complete setting.
Note this function does not disable the Time Alarm sound in (9) above.
F/ENT
F/ENT
to turn ON (enable).
F/ENT
to turn OFF (disable).
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4. Keyswitch Functions
(12) Set measurement unit (SC.U) panel
Toggle the measurement value units between [S/cm] and [S/m].
Use the keys to toggle the measurement value units. Then press the to complete setting.
F/ENT
F/ENT
to set
to toggle
(13) Set temperature unit (tP.U) panel
Toggle the temperature units between [8C] and [8F].
Use the keys to toggle the temperature units. Then press the complete setting.
F/ENT
to toggle
F/ENT
F/ENT
key to
key
F040312.EPS
4-16
F/ENT
to set
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(14) Version number dispaly (VEr) panel
Displays program firmware version number. Can’t be set by the user.
F/ENT
4. Keyswitch Functions
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4. Keyswitch Functions
(15) Defragment storaged data (dFLG) panel
Up to 300 data can be stored. Unnecessary data can be individually deleted as in (1) Stored measurement data panel (dAt). At the same time, individual deletion does not free
up memory occupied by deleted data, so may be displayed even though less than 300 data are stored. In such a case, use defrag functions to compact storage and free
up the space occupied by deleted data, thereby allowing up to 300 data to be stored. While data defrag is in progress, do NOT turn off the power. In addition, before starting
data defrag, check that the battery power is normal to avoid battery voltage dropout during defrag.
• Performing data defrag
F/ENT
If the
key is pressed from the display shown below, flashes.
Use the keys to select , then press the
F/ENT
key. While defrag is in
progress, [WAIt] flashes (Note: if only a few data are deleted, you may not even see it). When defrag is complete, [End] is displayed.
F/ENT
to confirm
(if only a few data are deleted, you may not see this)
After a few seconds
F/ENT
F/ENT
to execute
to toggle
to abort
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5. Handling of the SC72 Personal Conductivity Meter

5. Handling of the SC72 Personal Conductivity Meter

5.1 Tips to Maintain Meter Performance

The SC72 meter appears to be very simple, but is a precision instrument. To ensure that measurement accuracy is maintained, observe the following precautions regarding preliminary setting, measurement, maintenance and storage.
Preliminary setting, measurement, maintenance and storage:
Measurement
Preliminary
setting
Storage
Table 5.1 Observe the following precautions
Setting cell constant
Set specific electrode cell constant.
Preliminary setting
Measurement
Maintenenace
Storage
Setting temperature coefficient
Set liquid temperature coefficient when the standard temperature conversion is required (see Section 2.5) If standard temperature conversion is not requiresd, set 0.00.
• Select one of the three conductivity measurement ranges (0 to 200mS/cm, 0 to 200mS/cm, or 0 to 2S/cm) corresponding to the type of electrode used. Temperature measuring range is 0 to 808C.
When measurement is completed, thoughly wash electrode to remove the measured liquid.
• If the electrode gets stained or deformed, its cell constant may change. In this case, calibrate the meter with standard solution (see Section 5.4).
• Avoid high-temperature, high-humidity storage locations.
Maintenance
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5. Handling of the SC72 Personal Conductivity Meter

5.2 Washing the Electrode

Dirt or stains on the electrode may have an adverse effect on the cell constant, thereby making accurate conductivity measurement impossible. Therefore, after measurement, rinse the electrode in clean water (for example, tap water) to remove stains. Even if staining is not apparent, the sensor performance may have changed. If so, wash the electrode by moving the sensor up and down in hydrochloric acid (about 0.1 mol/l) or water with a little neutral detergent dissolved in it. [For general-purpose and pure-water sensors: if the electrodes are difficult to clean, wipe them gently from top to bottom with a cotton wool swab.] After cleaning the electrode, rinse it in water.
• General-purpose sensor
(The figure below shows the general-purpose sensor with the cover removed). Remove the cover, and wipe stains off the electrodes (inner electrode and tip element)
with a cotton swab. Rinse in a cleaning solution consisting of water containing a little neutral detergent, to remove stains from the electrode. After cleaning, wipe the electrode element (inner and edge electrodes) with tissue paper or cotton wool.
Inner electrode (titanium) Edge electrode (titanium)
F050201.EPS
• Sensor for high-purity water measurement
Remove the reference electrode part, and wipe the electrode elements (the shaded parts in the figure) with tissue paper or cotton wool.
Cotton wool swab
Reference electrode contact
Internal electrode
Reference electrode
F050202.EPS
* Corrosion-resistant sensors and sensors for high-conductivity measurements Use a beaker or the like containing water, dilute hydrochloric acid, or weak neutral
detergent; move the sensor up and down so it is immersed up to the air vent, and wash in tap water to clean out the air vent.
5-2
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5. Handling of the SC72 Personal Conductivity Meter

5.3 Cleaning and Drying Connector

If there is an electrical path between the connector pins, solution conductivity cannot be measured correctly. Clean the connector (shown in the figure) with a dry cloth, or a cloth moistened with pure undiluted alcohol, to remove moisture and/or stains. If necessary, use a hair dryer to dry any section that is likely to be difficult to wipe.
O-ring
Wipe off stains and/or moisture on meter connector with a dry cloth.
Check that there are no stains on the O-ring.
Hot air
Use a hair drier if necessary to remove moisture from connector of sensor cable.
F050301.eps
CAUTION
For free from moisture, use pure undiluted alcohol to clean the connectors. Dry connectors completely.
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5. Handling of the SC72 Personal Conductivity Meter

5.4 Calibration with Standard Solution

Note: Calibration with standard solution means to measure a standard solution of
accurately-known conductivity and to adjust SC72 meter so that the displayed measured value is the same as the known conductivity value of the standard solution.
If the sensor has been used for a long time, and does not look clean despite washing, recalibrate the SC72 meter with standard solution to check if cell constant is normal.
If “ ” occurs during calibration with standard solution, replace the sensor. Note that if calibration with the standard solution shows that the cell constant has
changed, update the cell constant value on the sensor cable with the new data.
Notes for calibration with standard solution:
Types of standard solution
Use NaCl (sodium chloride) or KCl (potassium chloride) solutions.
(1) NaCl (sodium chloride) solution
When NaCl solution is used, the temperature coefficient of NaCl is built into the temperature compensation functions of the meter so conductivity converted to 25 8C can be readily obtained regardless of liquid temperature. Standard NaCl solution of 0.1 mol/l (normal unit expressing concentration of solution) is available as an option from Yokogawa. For more details, see Section 1.7.
When the sensor for high purity water measurement is used, dilute the standard solution with pure water to obtain 0.001 ml/l solution of conductivity 1 mS/cm. Conductivity is as follows:
0.1 mol - NaCl solution: conductivity 10.67 mS/cm at 258C
0.001 mol/l - NaCl: conductivity 123.9 mS/cm at 258C
(2) KCl solution
Table 5.2 describes how to make KCl solution of different concentrations, and lists their conductivities.
5-4
Table 5.2 How to make KCl solutions, and their conductivities
(based on JIS K 0102)
KCl
solution
A
B
C
D
How to make
Dissolve 74.2460g of KCl in water to get 1l at 20618C.
Dissolve 7.4365g of KCl in water to get 1l at 20618C. Dissolve 0.7440g of KCl in water to get 1l at 20618C.
Dissolve 100ml of standard solution C avobe in water to get 1l at 20618C.
KCl standard solution, mS/cm
08C
65176
7138
773.8
188C 97838
11167
1220.5
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258C 111342
12856
1408.8
146.93
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5. Handling of the SC72 Personal Conductivity Meter
* Before calibrating the meter with standard solution, check that the electrode is clean. If stains are found, clean the electrode first. Also check that the cover (of general-purpose sensor) and outer electrode (of sensor for high purity water measurement) are secure. Cell constant is affected by stains or loose cover.
When calibrating, ensure that measuring range is set so that you can enter conductivity to as many digits as possible. For example, in the table above, the conductivity of standard solution C at 258C is 1408.8. If the meter is set to autorange, or to a manual range of 0 to 2.000 mS/cm, you could set this as 1.409 (four digits). However if the range were set to 0 to 200.0 mS/cm, you could only enter conductivity value as 1.4 (only two digits accuracy, which is inadequate for calibration with standard solution.
Before calibrating the meter with standard solution
Check and set the following items before calibrating the meter with standard solution.
(1) Check sensor for stains
Check that there are no stains on the sensor. Also check that the meter cover (for general-purpose sensor) or outer electrode (for sensor for high purity water sensor) are not loose.
(2) Setting temperature coefficients
When the meter is calibrated with a NaCl solution, set a temperature coefficient (indicated by “NaCl”) for NaCl solution. When it is calibrated with a KCl standard solution, set a temperature coefficient of 0.00 (%/8C).
(3) Standard solution temperature
For a NaCl standard solution, check that the standard solution temperature is in the range 258C 6 108C.
For a KCl standard solution, stabilize its temperature at 258C 6 18C or 188C 6 18C. If it is difficult to maintain the above temperatures, set the temperature coefficient of KCl
standard solution in the meter. To find the temperature coefficient, refer to table 5.2 above and to Section 7.3, “Temperature Compensation and Finding Temperature Compensation Coefficient.”
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5. Handling of the SC72 Personal Conductivity Meter
Procedures for calibration with standard solution
POWER
Water
Std. sol.
Wash sensor with water completely.
Whole measurement value is flashing
Wait until the measured value is stable.
Thoroughly wipe off the washing water from the
electrodes before immersing the sensor in standard solution.
F/ENT
F/ENT
Set the conductivity of the standard solution.
F/ENT
Select CAL mode
Least significant figit of the measuremet value is flashing
Complete the calibration
F/ENT
Refer to Section 4.3, “Function Modes,” for temperature coefficient and cell constant settings.
5-6
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5. Handling of the SC72 Personal Conductivity Meter

5.5 Storage and Maintenance

• Method of storage
Care is required when storing the SC72 meter. To maintain the SC72 meter in good condition, observe the following:
(1) After measurement, thoroughly wash the sensor in water. (2) Leave the sensor connected to the meter body, to protect the connector from
staining. Connector contamination could affect connector leakage resistance and thus conductivity reading accuracy, or affect the waterproofing afforded by the O­ring.
(3) Do not place any object on top of the sensor or on the top of SC72 meter.
• Storage location
When the SC72 meter is not being used, store it in a safe place. If it is to be stored for a long time, store it:
* In a dry place (low humidity) at normal temperatures. * Out of direct sunshine. * Do not store it in a corrosive gas atmosphere. * In a location free from water condensation.
• Replacing O-rings or gaskets
Gaskets for the battery box and O-rings for sensor connections can be replaced. If they are very dirty or damaged, replace them with new ones.
CAUTION
When installing O-rings and gaskets, clean them and their mounting surface with a cloth moistened with alcohol so that they are free from dirt. Otherwise, water resistance may not be assured.
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5. Handling of the SC72 Personal Conductivity Meter
(1) Replacing O-rings
Install the O-ring on the cylindrical flat part as shown in the figure.
O-ring
(2) Replacing gaskets
Install the gasket with its raised part facing downwards on the groove of th meter case. Gaskets are symmetrical (on the right and left, and on the front and rear).
F050501.EPS
Gasket
SC72 meter top
Raised part
5-8
F050502.EPS
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6. Troubleshooting

6.1 Causes of Abnormal Conductivity Display

The measured temperature is stable, but the conductivity reading is unstable, or an unrealistic value is displayed, check the following:
(1) Is maintenance required, and has handling of the meter been adequate? (2) Does the battery need replacement? (3) Is SC72 meter unserviceable?
If any problem is evident, follow the procedure shown in Section 6.2 to determine the cause and fix the problem. If you cannot fix it, contact your nearest Yokogawa sales office.
d Displayed value unstable
Abnormal
d Displayed value unrealistic d Error message displayed
Components need replacement
d Battery
Needs maintenance
d Needs recalibration with standard solution d Electrode stained d Electrical leakage in connector
6. Tr oubleshooting
IM 12D03D02-01E
SC meter failure
d Contact Yokogawa.
F0601.EPS
Figure 6.1 Causes of abnormality
6-1
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6. Tr oubleshooting

6.2 Error Messages and Corrective Action

Table 6.1 Error Message
Error message
Err1 Err2 Err3 Err6
or
*1 Alphabet values simulated on a numeric display
*1
Name
Temperature compensation computation value out of range Out of temperature measurement range Calibration error Meter electronics failure Out of measuring range
(1) Err1 Temperature compensation computation value out of range
Cause:
When the standard temperature conversion is made to conductivity at 258C, this instrument performs temperature compensation computation based on the preset temperature coefficient.
Err1 is displayed in cases where temperature compensation computation is impossible because the preset temperature coefficient is improper or a solution with a large temperature coefficient is measured at temperatures lower or higher than 258C.
Corrective action:
* Reset the temperature coefficient to the correct value. * Measure solution at about 258C.
(2) Err2 Out of temperature measurement range
Cause:
This error occurs if the measurement liquid temperature is outside the range -10 to 1208C, or if sensor cables are disconnected.
Note: The liquid temperature should never be outside the range 0 to 808C.
Corrective action:
* Set the liquid temperature to 0 to 808C. * Replace the sensor. (Refer to Sec. 1.6)
T0601.EPS
6-2
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6. Tr oubleshooting
(3) Err3 Calibration error
Cause:
When the calibration with standard solution is made, each time cell constants are changed. Err3 occurs if the conductivity of the standard solution is wrong, or changed cell constants are beyond 6 20% of the standard cell constant, due to a damaged sensor.
Corrective action:
* Use correct standard solution conductivity. (Refer to Sec. 5.4) * Replace the sensor. (Refer to Sec. 1.6)
(4) Err6 Meter electronics failure
Cause:
Err6 occurs if the meter electronics fails.
Corrective action:
* Contact your nearest Yokogawa sales office.
(5) or Out of measurement range
Cause:
Conductivity is over the maximum value on the range.
Corrective action:
For manual ranging, select an appropriate range. If value exceeds maximum of highest range (or when on autorange), use a more appropriate sensor (see Sec. 4.3 (3)).
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6. Tr oubleshooting

6.3 Causes of Abnormal Measured Value

If error messages do not occur, but measured values seem incorrect, check the following:
* Are cell constants and temperature coefficients correctly set? * Is the sensor properly connected to the meter? * Are bubbles attached to the electrode portion? * Is the sensor damaged or dirty?

6.4 Other conditions

• An alarm sounds
The alarm clock is set (see Sec. 4.3 (9) and change setting as required).
• T o Enable / Disable Key-Pr ess Audible Feedback (buzzer)
Refer to Sec. 4.3 (11) to change setting as required.
6-4
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7. Measuring Principles of this Instrument

7. Measuring Principles of this Instrument

7.1 What Is Conductivity?

Conductivity of a solution is defined as the ability of the solution to conduct electric current. It is the reciprocal of the resistance between two sensors (both of areas 1 m2) at a distance of 1 m apart in the solution.
1 S/cm = 100 S/m Figure 7.1 shows the conductivities of typical solutions.
0.01 0.1110100 [mS/m]
0.1110100 1000 [mS/cm]
110100 1000 [mS/cm]
0.1110100 [S/m]
Pure water
Deionized
water
Distilled
water
Figure 7.1 Conductivity of Typical Solutions
Organic
acid
Reservoir
water
Sea
water
Salt water (1 to 27%)
Strong acid and
alkali solutions
F0701.EPS
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7. Measuring Principles of this Instrument

7.2 Principles of Operation

AC power supply Ammeter
F0702.EPS
Figure 7.2 Operational Schematic
Dip two metallic plates (used as sensor electrodes) in a solution and apply a certain voltage to flow current (I):
E
I = (1)
Rc
where Rc = solution resistance between two sensors The relationship between Rc and conductivity K is expressed by:
Rc = J • (2)
where J = constant (also called cell constant) — determined by sensor and distance between two sensors From equations (1) and (2) above, we obtain:
K = I (3)
E and J are constant, so the conductivity (K) can be obtained by measuring the current (I).
1
K
J
E
7-2
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7. Measuring Principles of this Instrument
7.3 Temperature Compensation and Finding Temperature
Compensation Coefficient
• Temperatur e Compensation
Table 7.1 shows the conductivity ratio at each liquid temperature when the conductivity of a NaCl solution at 258C is 1.
Table 7.1 Conductivity Ratios at Different Temperatures in
NaCl solutions
08C258C
0.542 11.531
508C
758C
2.103
1008C
2.677
T0701.EPS
As shown in the above table, liquid conductivity changes with liquid temperature. So, in order to compare conductivities, conductivity values at a fixed liquid temperature are needed. This SC72 meter includes standard temperature conversion functions, to display a liquid conductivity value converted to 258C, so this meter can be used for such conductivity measurement comparisons. Temperature compensation coefficients of an NaCl solution are stored in the SC72 meter. No other temperature coefficient setting is required (for NaCl solutions).
Table 7.2 shows temperature coefficients of various electrolytic solutions.
Table 7.2 Temperature Coefficients of Electrolytic Solutions
Solutions
Lithium benzoate solution
Sodium acetate solution Potassium chloride solution Sodium hydroxide solution Sulfuric acid
• Finding Temperature Coefficient
If temperature coefficient tables containing the liquid to be measured can not be found, measure conductivity twice at two liquid temperatures between 10 and 308C with temperature coefficient set to 0.00 and use the equation shown below to find approximate temperature coefficient (a).
Temperature coefficient (%/8C)
1mol/l 1/10mol/l
---
2.20
1.74
1.74
1.07
2.28
2.20
---
---
---
1/1000mol/l
2.28
2.20
1.98
1.87
1.38
T0702.EPS
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7. Measuring Principles of this Instrument
a = Temp. coef. 3 100 (%/8C)
K 2 K
2
1
K ( t 2 25 ) 2 K ( t 2 25 )
1
221
where t , t : liquid temperature (8C)
12
K : conductivity at t
11
K : conductivity at t
22
(Calculation example)
To find the temperature coefficient of liquid with conductivity - 124.5 (S/cm at liquid temperature 18.08C and 147.6 (S/cm at liquid temperature 31.08C, substitute t1 = 18.0, t2 = 31.0, K1 = 124.5, K2 = 147.6 in the equation above, thus we can obtain:
a = 3 100
= 3 100
147.6 2 124.5
124.53(31.0225)2147.6 3(18.0225)
23.1
747.02(21033.2)
= 1.298
Set the temperature coefficient 1.30 in the SC72 meter (as meter allows three digits to be entered).
• Checking if meter is working correctly
When the temperature coefficient already set is accurate, the conductivity displayed should be constant regardless of liquid temperature (within permitted temperature range). Check that the temperature coefficient already set is accurate. When the liquid temperature is lowered, if a larger conductivity is indicated, the temperature coefficient already set is too small; whereas, if a smaller conductivity is indicated, the temperature coefficient already set is too large. In such a case, change the temperature coefficient such that the measured conductivity does not change with temperature.

7.4 Wetted Part Materials of Sensors

• For general-purpose sensor
Titanium (sensor) Polyphenylene sulfite resin, Polypropylene resin (insulated area and cover) Fluoro rubber (O-ring)
• Sensor for high purity water measurement
SUS 316 stainless steel (electrode element) Polypropylene resin (insulated area) Fluoro rubber (O-ring)
• Chemical-resistant sensor
Glass, platinum black (electrode element)
Sensor for high-conductivity measurement
Glass, platinum black (electrode element)
7-4
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Appendix

Key-Operation Flow Chart (for reference)
Typical screens are shown. Refer to the corresponding section in the body of the manual for details.
Appendix
d When turn on power
POWER
First time used, or after replace batteries
F/ENT
F/ENT
F/ENT
F/ENT
Toggle display type
MEAS
MEAS
MEAS
or
d Temporary hold
HOLD
HOLD
MEAS
IM 12D03D02-01E
F/ENT
d Storing data
DATA
DATA
MEAS
F/ENT
T01.EPS
1
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Appendix
d Function Mode
Display stored measurement value
Temperature compensation
setting
Range selection
F/ENT
F/ENT
or
DATA
DATA
DATA
DATA
F/ENT
F/ENTF/ENT
F/ENT
F/ENT
F/ENT
F/ENT
F/ENT
T02.EPS
2
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d Function Mode
Cell constant setting
Calibration with
standard solution
Delete all stored
measurement data
Date setting
Appendix
Time setting
F/ENT
F/ENT
F/ENT
F/ENT
F/ENT
F/ENT
F/ENT
F/ENT
F/ENT
F/ENT
F/ENT
F/ENT
F/ENT
F/ENT
d Switching to Function Mode d Reverting to Measurement Mode
Measurement status
F/ENT
Measurement status
MEAS
T03.EPS
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3
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Appendix
d Function Mode
Alarm time setting
Set Auto Power OFF
interval
Set buzzer ON/OFF
Set measurement unit
Set temperature unit
F/ENT
F/ENT
F/ENT
F/ENT
F/ENT
F/ENT
F/ENT
d Function Mode
F/ENT
F/ENT
Version number
display
F/ENT
F/ENT
F/ENT
Deflagment
storaged data
F/ENT
F/ENT
T04.EPS
4
IM 12D03D02-01E
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Revision Record

Manual Title : Model SC72 Personal Conductivity Meter Manual Number : IM 12D03D02-01E
Edition Date Remark (s)
1st Aug. 2004 Newly published 2nd Apr. 2008 Addition of information on EMC compliance: P.1-3
Addition of CAUTION: P2-2 Correction: P.1, 1-2, 1-6, 2-1, 2-3, 3-1, 3-3, 4-1. 4-5,
App-1, App-4
3rd Aug. 2009 Change of information on EMC compliance: P.1-3
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