Teledyne 8800T User Manual

instruction manual
Model 8800T
TRACE MOISTURE ANALYZER
Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies
i
8800T User’s Manual Table of Contents
1.0 Overview of the 8800T .................................................1
2.1 Precautions using the sensor .........................................3
2.2 Sensor Technical Specifications ...................................4
2.3 Sensor Installation & Sampling Techniques .................4
2.3.1 In-situ Installation ......................................................5
2.3.2 Extractive Installation ................................................7
2.4 Troubleshooting unexpected readings ..........................9
3.1 Precautions using the 8800T .......................................13
3.1.1 Electromagnetic Compatibility Considerations .......13
3.2 Instrument Technical Specifications ...........................14
3.3 Installation ..................................................................15
3.3.1 Mechanical Installation ............................................15
3.3.2 Electrical Installation ...............................................16
3.4 Operating the Instrument ............................................17
3.4.1 Starting up ................................................................17
3.4.2 Display Conventions ................................................17
3.4.3 Push Buttons ............................................................19
3.4.4 Operating State ........................................................19
3.4.4.1 Viewing Dewpoint Mode ......................................20
3.4.4.2 Viewing Temperature at the Sensor ......................20
3.4.4.3 Start Calibration (SpanCheck™) Mode ................21
3.4.4.4 Viewing Serial Number Mode ..............................24
3.4.5 SetUp State ..............................................................24
3.5 Troubleshooting the Instrument ..................................28
Appendix A: Operating State User Interface flowchart ....31
Appendix B: Set-Up State User Interface flowchart .........32
Appendix C: 8800T Mechanical Drawing ........................34
Appendix D: 8800T Electrical Connections .....................35
Appendix E: Sensor/SpanCheck™ Theory of Operation .36
Appendix F: Pressure Correction ......................................39
Appendix G: Current vs. Dewpoint ..................................40
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Appendix H: Uncertainty in LBS & ppmV calculations ..43
Appendix I: Sensor Response Time ..................................44
Appendix J: Return Authorization Request ......................45
iii
Section 1: Introduction
1.0 Overview of the 8800T
The 8800T is a microprocessor based 4-20mA loop powered (2 wire) hygrometer, for measuring moisture content in gases in the range from -100°C to +20°C. The measurement is displayed on the instrument’s custom LCD, and is trans­mitted by varying the current drawn (4-20mA) from the power supply. The current varies linearly proportional to the selected measurement units. An optional digital output is available which modulates/demodulates the 4-20mA loop line without interfering with its operation. With this option the 8800T is capable of communicating with properly equipped Personal Computers or other RS-232 capable con­trollers. Three front panel buttons provide the user with a wide variety of features. The 8800T’s advanced design allows it to be housed in a small stainless steel enclosure behind the sensor probe, thus the instrument and sensor are a single integrated unit. The 8800T uses the Teledyne HTF™ sensor which is encap­sulated in sintered stainless steel, thus it is capable of com­ing into contact with a wide variety of environments. However one should keep in mind that the sensor is a sensi­tive device and it should be handled accordingly.
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page 2
Section 2: Sensor and Sampling Techniques

2.1 Precautions using the sensor

The Teledyne HTF™ Al2O3 sensor is designed and field proven to be highly reliable, rugged and maintenance free.
However the user should consider the following precau­tions:
To avoid the need for prolonged dry-down (when expecting to measure dewpoints dryer than -65ºC), do not expose the sensor to room air longer than necessary (1 - 2 minutes). Thus, do not open the sensor container before you are ready to install the sensor.
The sensor container has desiccant to keep the sensor dry during shipping and to avoid damage due to conden­sation. Close the container immediately after removing the sensor to avoid degradation of the desiccant.
Do not throw away the sensor container, you may use it again to transport the sensor between locations, to store it between uses or to ship it back to the factory for certi­fication. The container can be attached to the loop cable, by trapping the cable with the lid strap.
Do not expose the sensor to corrosive gases such as gases containing chlorine, ammonia or HCl. (SO2 can be monitored when the moisture content is low).
Except for the XTR65W sensor:
1. Do not expose the sensor to liquid water, as it may get damaged.
2. Do not breathe directly onto the sensor, as condensa­tion may form which could damage the sensor element.
Do not install the sensor near heat sources such as radia­tors or air ducts.
Do not install the sensor in places subject to extreme mechanical vibration or shock. If this is not avoidable, use resilient mounting. If in doubt, call your representa-
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tive.
Do not disassemble the porous metal filter encapsula­tion, as this will damage the sensor and void your fac­tory warranty.
Prior to installation of the probe, ensure that no contam­inants are present in the system (e.g. oil, liquid water).

2.2 Sensor Technical Specifications

Type: .................................Hyper Thin Film high capacitance Al2O3.
Dewpoint range:
XTR-100........................-148°F to +68°F (-100°C to +20°C)
XTR-65..........................-85°F to +68°F (-65°C to +20°C).
Capacitance:......................15nF to 200nF.
Accuracy:..........................±5.5°F (±3°C).
Repeatability:....................±0.9°F (±0.5°C).
Response time:..................see graph in Appendix I.
Temperature range:...........-10°C to +70°C.
Sample Flow range:
(linear velocity @ 1ATM):Static to 100m/s.
Storage temperature:. ........-40°F to+176°F (-40°C to +80°C).
Mechanical:.......................encapsulated in 100µ sintered stainless steel.
Calibration method: ..........SpanCheck™, sensor saturates at dewpoint above
+68°F (+20°C). NIST/NPL traceable multi-point factory calibration available optionally.

2.3 Sensor Installation & Sampling Techniques

Keep in mind that the moisture content at the sensor is not only due to the moisture of the gas being measured, but also due to desorption of water from tubing, trapped moisture (at the interconnection points, valves, filters and other hygro­scopic materials in the system), leaks in the system, and oth­ers. Thus the measurement may vary from the expectation, and therefore care should be taken in choosing the sampling technique utilized in the measurement. Factors such as gas pressure, flow rate, materials of construction, length and
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Section 2: Sensor and Sampling Techniques
diameter of tubing, number of interconnecting fittings, dead space in tubing and manifolds; will influence the measure­ment value and response time. The high capacitance HTF™ sensors can be installed either directly in the line to be sampled (in-situ), or in a slip stream of a sample system (extractive). To assure a long and accurate performance of the sensor, it should be protected from contaminants such as liquids (water, oil etc.), and particulates. The sintered stainless steel sensor encapsulation protects from particulates larger than 100 microns, finer particulates (e.g. from degraded desic­cant or rust) should be filtered with a particulate filter with suitable capability, do not use hygroscopic filter materials.

2.3.1 In-situ Installation

In-situ installation is recommended only for measurements where the gas pressure is expected to vary little, the gas is expected to be free of contaminants, the gas temperature is wit hin the oper a ting s pec if ic at ions of the se nsor , a nd th e re is no chance of liquids coalescing. Examples of applications suited for in-situ installations are: pure gases, output of des­iccant dryers (for instrument air), glove boxes, etc. For most other applications in-situ installation should be avoided for the following reasons:
Sample conditioning is almost always necessary to
avoid exposure of the sensor to liquid water and other contaminants, such as hydrocarbons, which may dam­age the sensor or affect accuracy over time.
Variations in line pressure affect the reading of the sen-
sor because dewpoint varies with pressure.
If the gas line is under pressure, it is more likely that
water condensation occurs which may damage the sen­sor.
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Under a pressurized system removal of the sensor with-
out the installation of isolation valves can be dangerous.
If in-situ installation is required, bypass mounting is prefer­able; make sure to install the sensor at the upper surface of the gas line to minimize its exposure to liquid water, should condensation occur, the XTR65W sensor is best suited for these applications. Also consider the need to isolate (depres­surize) before installing or removing the sensor.
4-20mA loop cable
Main
Gas Line
8800T
oint Transmitter
Think
Read
Safety
www.xentaur.com
Mo
In-Line Installation, Sensor
Se
Manual
Measuring at Line Pressure
Ma
NOT RECOMMENDED
4-20mA loop cable
8800T
oint Transmitter
Think
Read
Safety
www.xentaur.com
Mo Se
Bypass Installation, Sensor
Manual
Ma
Measuring at Line Pressure
Safety shut-off Valve
Safety shut-off Valve
Sample Cell
Bypass
Main
Gas Line
Control
Valve *
* maintain differential pressure to provide adequate flow through sample cell
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Section 2: Sensor and Sampling Techniques

2.3.2 Extractive Installation

For extractive installations we recommend our sample sys­tem ESS, which may be equipped with a variety of features, such as: isolation valve, coalescing or particulate filter, pressure regulator , calibration sample injection or ext raction port, pressure gauge, flow meter, weatherproof enclosure. Refer to the ESS literature for more information. If the resources to make your own sample system are avail­able, the following two diagrams may be used as a guideline to configure a simple system.
4-20mA loop cable
Safety shut-off Valve
oint Transmitter
Think Safety
8800T
Read
Manual
www.xentaur.com
Exhaust
Mo Se
Ma
Regulator or
Needle Valv e
Main
Gas Line
4-20mA loop cable
Regulator or
Needle Valv e
Main
Gas Line
Sample Cell
Extractive Installation, Sensor
Measuring at Line Pressure
8800T
oint Transmitter
Mo Se
Think
Read
Manual
Safety
Ma
www.xentaur.com
Exhaust
Sample Cell
Extractive Installation, Sensor
Measuring at Ambient Pressure
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8800T User’s Manual
It is generally recommended to measure at ambient pressure for the following reasons:
The readings will not be affected by variations in line
pressure.
The risk of exposing the sensor to liquid water is signif-
icantly reduced.
ppm readings are computed for a pressure of one atmo-
sphere (1 bar); and have to be corrected using software in the instrument, or a pressure nomograph, or calcula-
tor if the sensor is measuring at different pressures. If readings at line pressure are necessary, it is recommended to measure at ambient pressure and to use the instrument’s pressure compensation feature to calculate the dewpoint at line pressure. See appendix F. Please make sure that:
The sample is taken from the upper surface of the main
gas line. This avoids problems with contamination. The
sample should be taken away from pipe line walls where
flow rates may be low, and dewpoint changes may lag.
For dewpoints dryer than -40°F, use stainless steel tub-
ing only. Copper tubing is acceptable for dewpoints wet-
ter than -40°F. Do not use plastic, rubber or tygon tubing
under any circumstances, as measurements would be
incorrect and/or response time slow due to water reten-
tion inside these materials.
Try to run pipes to the sensor upwards, so that contami-
nants tend to fall back into the main line.
Keep the length of the sample line to the sensor as short
as possible.
Use small diameter pipes (1/4” or 1/8” OD).
Use sufficient flow rates (e.g. 1 l/min with 6 feet of 1/8”
piping is adequate). The flow rate will influence the sys-
tems’ response time.
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Section 2: Sensor and Sampling Techniques
Do not install any devices upstream of the sensor, such
as other measuring systems, flow meters etc., which are
not absolutely necessary as these are potential leak
sources.
Installation of a coalescing and / or particulate filter
ahead of the sensor is desirable to prevent any liquid or
particulate contamination of the sensor.
If filters are used upstream of the sensor, make sure
these contain non-hygroscopic filter materials only.
If pressure regulators, shut off valves etc. are used
upstream of the sensor, make sure these do not contain
rubber or other hygroscopic materials.

2.4 Troubleshooting unexpected readings

If erroneous readings are suspected on a newly acquired instrument, compare the serial number engraved on the sen­sor sintered filter, to the one stored in the instrument mem­ory. The two should be the same; if they are not, the instrument may not be calibrated with the installed sensor. To troubleshoot other problems, identify the unexpected reading category in the following table, and consider the possible causes and appropriate diagnostic action and rem­edy.
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Troubleshooting unexpected readings (table spans 2 pages)
Symptom Possible Cause
Reading is not
changing
Slow Response
Dry Reading SpanCheck™ wrongly set, or faulty sensor.
We t Read ing
Display Shows
Condensation in sample system.
1. Water vapor in the system.
2. Flow rate too low.
3. Sample pipe too large and/or too long.
4. Unsuitable sample pipe material.
5. Leaks
6. Hygroscopic materials in sample system
Leak in system or use of unsuitable pipe.
Comparison of readings with manual cooled­mirror instrument.
Prolonged exposure to wet gas.
6$7
Display Shows
1. In st ru men t F a i lu re
6+5
2.Short circuited sensor.
Display Shows
231
1. In st ru men t fai lu re.
2. Open circuit on sensor.
For non-sensor related problems (e.g. no reading on instru­ment) refer to section 3.5
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Section 2: Sensor and Sampling Techniques
Troubleshooting unexpected readings (continued from previous page)
Symptom Diagnostic/Remedy
Reading is not
changing
Slow Response
Dry Reading Veri fy SpanCheck™, or return sensor for full calibration to your representative.
We t Read ing
Display Shows
6$7
Display Shows
6+5
Display Shows
Condensation will occur if the temperature of the sample system, at any point is below (colder) the dewpoint temperature of the sample gas. Once having formed, the sample reaching the sensor will have a dewpoint equal to the temperature of the condensation, regardless of the dewpoint of the sample at the sample point.
It is usually more satisfactory to bleed a sample gas at atmospheric pressure through the sensor sampling chamber, and to use 1/8” (3mm) o.d. sample pipe.
See below re: sample pipe material, also see section 2.3
Cure the leak, or replace unsuitable pipe with copper or stainless steel. Flexible con­nections should be made with PTFE pipe. NEVER use rubber or plastic pipe.
This type of indicator reads about 10°C dry at about -50°C dewpoint due to tempera­ture gradi ent s wit hin the de vi ce. Th e error in cr ease s at drier levels.
Dry the sensor, install sensor in either a known dry gas stream i.e. instrument quality air or dry nitroge n, or place sensor in a dry can or bottle of desiccan t an d seal the con­tainer from outside air (the shipping container is designed for this purpose)
Remove (unscrew) sensor, if the instrument still reads instrum ent. Howeve r , if the instrument rea ds
Remove (unscrew) sensor and note that the meter reading returns to sensor, or apply approximately 20V DC, between the center pin & the filter body of the sensor, MOMEN T AR ILY with the s ensor in a known dry condition. Pola rit y is not important, but the contact MUST be very brief or the sensor may be damaged.
Remove (unscrew) the sensor. Short the center contact of the 8800T sensor connection to the case, if the ins trumen t read s
the instrument for service.
231
the problem is in the sensor, otherwise return
6+5
the problem is with the
6+5
then check possible cause #2
. Use a new
231
231
Check sensor connection or replace sensor.
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