Teledyne 8800P User Manual

instruction manual
Model 8800P
TRACE MOISTURE ANALYZER
Teledyne Analytical Instruments A Business Unit of Teledyne Electronic Technologies
8800P Series Trace Moisture Analyzer Instruction Manual
Sensor Serial No.: _______________ Instrument Serial No.: _______________
Your Representative is:
Except as may be provided by contract, this document and all specifica­tions and drawings contained are the property of Teledyne Analytical Instruments, are issued in strict confidence, and shall not be reproduced or copied or transmitted, in any form or by any means, or used as the basis for the manufacture or sale of apparatus, programs, or services without permission.
Copyright © 2000 by Teledyne Analytical Instruments
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1. Introduction
The 8800P is a portable, hand-held, microprocessor controlled, battery operated dew­point meter with built in dry-storage for the sensor. The instrument is ideally suited for all applications, where quick and precise measurements are required.
Standard Equipment:
1.8800P Portable Instrument with sensor, desiccant cartridge and lithium battery.
2. 2 VCO to Swagelok fittings and 2 Swagelok to barbed hose fittings.
3. Calibration bulb.
4. Shoulder strap.
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Optional Equipment:
5. VCO to VCO Fittings.
6. Pig tail.
7. Flexible stainless steel hose.
8. Pressure regulator, all stainless steel, (preset at 1.5 atm) with mounting bracket.
9. Coalescing filter, all stainless steel with mounting bracket.(not shown)
10.Wall transformer (with factory installed I/O option).
11.Replacement desiccant cartridge.
12.Padded transport case.
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2. Precautions
Warranty limitation: The 8800P’s sample cell/piston assembly should not be disas­sembled except by factory trained personnel. The warranty is voided, if the sample cell piston assembly is disassembled by the customer.
Avoid contaminated sample streams: The 8800P has been designed to allow for fast and precise measurements of dewpoints as low as -100 °C. Therefore, all surfaces in contact with the sample stream are made from electropolished stainless steel. This minimizes the time for the instrument to reach equilibrium with the sample stream, thus speeding up the measurement. The introduction of corrosive gases or gases contaminated with oils, solvents etc. may damage or coat the electropolished sur­faces and slow down the measurement. Surfaces contaminated with oils etc. can be cleaned by factory trained personnel (please contact your sales representative). Sur­faces damaged by corrosive gases are damaged permanently, causing longer response times. Gases containing chlorine, ammonia, HCl or SO2 may also cause
damage to the sensor. SO2 can be monitored when the moisture content is low.
Avoid liquid water: Avoid the introduction of liquid water into the sample cell, as this may damage the sensor. Do not breathe directly into the instruments sample ports, as condensation may form which could damage the sensor element. If liquid water can not be av oided, or der the XTR-65W senso r which is w ater proof , b ut has a limit ed range, and a slower dry down response.
Avoid high pressure: The 8800P has been designed for operation at pressures slightly above atmospher i c, however each sample cell/sensor piston/dry-storage assembly has been tes ted for pressures up to 120 PSI. Do not introduce sample streams, whi ch could cau se pressure rises ab ov e 100 PSI. Mak e your m easurements at atmospheric pressures, and use the pressure calculation feature to calculate dew­points at higher pressures. Ask your representative for a regulator installation kit.
Exercise Caution with Hazardous Gases: Please use appropriate precautions if the sample you are about to measure is hazardous. Place the unit in a safe area, if it is to be used with hazardous gases. Please be aware that the possibility of a small leak always exists. Such a leak will not influence the accuracy of the measurement, but may represent a risk if the sample gas is of hazardous nature.
Avoid Extreme temperatures: Do not install the unit near heat sources such as radia­tors or air ducts. The instruments’ operating temperature range is -10°C to 50°C.
Avoid Mechanical Vibration: Do not install the unit in places subject to extreme mechanical vibration or shock. Use resilient mounting, if shock and vibration are not avoidable. Call your representative if in doubt.
Avoid long exposures of sensor element to room air: For reasons explained later in this manual (section 7), do not expose the sensor to room ai r for longer then neces­sary (1 - 2 Minutes). The sensor is exposed to room air, when the sensor actuator is in the out position and no sample line is connected, or the sample gas is shut off. It is best to push the sensor bac k into d ry-storage , after a measu rement is co mplete d and whenever the instrument is not in use.
Do not force the Actuator: Remove any port obstructions (such as shipping caps) before operating the Actuator.
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3. Principle of Operation
Dewpoint sensors, like all hygroscopic materials, adsorb much faster than they desorb. Therefore, an accurate measurement will be obtained much faster, if at the beginning of the measurement, the sensor is at a dewpoint drier than the gas to be measured. The 8800P design allows the sensor to be moved directly between dry-storage and the sample cell, without any exposure to ambient air.
Sensor in Sensor In
dry-storage position measuring position
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1. Sample Ga s In 7. Sensor Actuator
2. Sample Gas Out 8. Desiccant Chamber
3. Piston 9. Filter Mesh
4. Sample Cell 10.Electronic Board
5. Sensor 11.Instrument Case
6. Spring loaded PTFE seals
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The drawing on the left shows the 8800P with the sensor in dry-storage position. The sen­sor is enclosed in a gas-tight container and surrounded by desiccant. The sample gas passes through the sample chamber and prepares the environment for measurement. Blocking of the outlet port will pressurize the sample ch amber and move the piston into the position sho wn on the right. The sensor is no w exposed to the sampl e gas without ev er having b een exposed to am bient air . Af ter t he measurement is taken, pushing in the sen­sor actuator will return the sensor into dry-storage, where it will dry down and ready itself for another fast measurement.
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A note about dry-storage The dry-storage consist of a stainless steel container filled with desiccant. The elec­tropolished st ainless steel sensor guard slides between the dry-storage and the sample cell through a spring energized PTFE seal, assuring maximum possible gas tightness and minimum gas transport between the two chambers when the sensor is moved. When in dry-storage, the sen sor guar d is separ ated from the de siccant b y a stai nless stee l wire mesh with a thic kness of 127µ (0. 005”) and a me sh size of 100µ . This k eeps the distance between the sensor and the desiccant to a minimum, which is critical for fast and low dry­downs, while protectin g the sensor from contaminatio n with desiccant par ticles. The factory supplied desiccant provides dry-storage dewpoints as low as -80°C when fresh. When the sensor is pushed into dry-storage it will take some time to dry down completely and reach equilibrium with the dewpoint in the dry-storage. The dry-down time to equilibrium depends on how wet the sensor was before it was returned to dry­storage, and in case that it was completely wet, how long it had remained in wet condi­tion. To take full advantage of the dry-storage, make sure, that the dry-storage dewpoint is below the expected dewpoint of the sample gas by periodically checking the indicated dewpoint afte r the senso r has remain ed in dry-storag e f or an e x tended period of time , f or example o ver night. Replace the d esiccant cartridge, if th e dry-storag e de w point is m uch higher than -80°C and above your expected sample dewpoints.
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4. Operating the 8800P
4.1. Sample Hook-up
4.1.1. Fittings
The 8800P can be hooked up to the sample gas using a variety of fittings, depending on the application. The instruments’ sample ports are 1/4” VCO female, to assure proper seals for even the lowest dewpoint measurements. Depending on the application and needs, we recommend the use of on e of the following methods of attachment:
•VCO stainless steel hoses, available optionally.
•VCO nections are acceptable.
•VCO above -65°C and should in all cases be used only with PTFE tubing.
4.1.2 Recommended Pipes
Stainless steel pipes should be used exclusively, for dewpoints below -65°C. Your repre­sentative ha s a fle xible s tainless steel ho se av ailab le. The length of the sam ple line to the instrument should be kept as short as possible, to assure fast equilibrium. We recommend the attachment of at lea st 12" long stainless stee l pipe at the outlet port to avoid bac k flow of ambient air when sampling at low flow rates, ask your representative for the optional pigtail. PTFE tubes are perfectly acceptable, and offer advantages due to their flexibility, for dew­points above -65°C. However, PTFE tubes should be kept as short as possible. Under no circumstance s use rubber or plastic tu bes, which are bo th, hygr oscopic and per­meable. No valid measurements can be expected when such materials are used.
VCO: This method is ideal for all applications, including the use of flexible
Swagelok: This method is suitable for all applications where rigid pipe con-
Swagelok ➜ Barbed Hose Fitting: This method is acceptable for dewpoints
4.1.3. Sample conditioning
Pre-filters: Do not use any pre-filters for oil, particles or liquid water when measuring dewpoints below -65°C. Pre-filters store and release water vapor, and slow down and distort the measurement at low dewpoints.
Pressur e re gulators: Do not use a pressure regulator containing any materials other than stainless steel, for dewpoints below -65°C. To ensure the use of the right prod­uct, use regulators provided by your sales representative.
4.2. Measuring
Turn the unit on by pushing the Power button.
Select the desired engineering units, using the up or down buttons.
Take note of the indicated dewpoint while the sensor is still in dry-storage.
Introduce the sample gas into the unit while the output port is unobstructed. Wait one minute, for ev ery 10°C below 0°C of expected dewpoint, to allow the sample chamber to adapt to the sample dewpoint.
Block the outlet po rt. The small pressure build-up in the sample chamber should be sufficient to push out the piston and move the sensor into the sample chamber. If not sufficient, assist by gently pulling on the sensor actuator located on the front of the
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