Teledyne 7600 User Manual

OPERATING INSTRUCTIONS FOR
Model 7600
NDIR Infrared Gas Analyzer
P/N M7600
ECO:
DANGER
Toxic gases and or flammable liquids may be present in this monitoring system. Personal protective equipment may be required when servicing this instrument. Hazardous voltages exist on certain components internally which may persist
for a time even after the power is turned off and disconnected. Only authorized personnel should conduct maintenance and/or servicing.
Before conducting any maintenance or servicing, consult with authorized supervisor/manager.
Teledyne Analytical Instruments
Model 7600
Copyright © 2005 Teledyne Instruments/ Analytical Instruments
All Rights Reserved. No part of this manual may be reproduced, transmitted, transcribed, stored in a retrieval system, or translated into any other language or computer language in whole or in part, in any form or by any means, whether it be electronic, mechanical, magnetic, optical, manual, or otherwise, without the prior written consent of Teledyne Instruments/ Analytical Instruments, 16830 Chestnut Street, City of Industry, CA 91749-
1580.
Warranty
This equipment is sold subject to the mutual agreement that it is warranted by us free from defects of material and of construction, and that our liability shall be limited to replacing or repairing at our factory (without charge, except for transportation), or at customer plant at our option, any material or construction in which defects become apparent within one year from the date of shipment, except in cases where quotations or acknowledgements provide for a shorter period. Components manufactured by others bear the warranty of their manufacturer. This warranty does not cover defects caused by wear, accident, misuse, neglect or repairs other than those performed by TI/AI or an authorized service center. We assume no liability for direct or indirect damages of any kind and the purchaser by the acceptance of the equipment will assume all liability for any damage which may result from its use or misuse.
We reserve the right to employ any suitable material in the manufacture of our apparatus, and to make any alterations in the dimensions, shape or weight of any parts, in so far as such alterations do not adversely affect our warranty.
Important Notice
This instrument provides measurement readings to its user, and serves as a tool by which valuable data can be gathered. The information provided by the instrument may assist the user in eliminating potential hazards caused by his process; however, it is essential that all personnel involved in the use of the instrument or its interface, with the process being measured, be properly trained in the process itself, as well as all instrumentation related to it.
The safety of personnel is ultimately the responsibility of those who control process conditions. While this instrument may be able to provide early warning of imminent danger, it has no control over process conditions, and it can be misused. In particular, any alarm or control systems installed must be tested and understood, both as to how they operate and as to how they can be defeated. Any safeguards required such as locks, labels, or redundancy, must be provided by the user or specifically requested of TI/AI at the time the order is placed.
Therefore, the purchaser must be aware of the hazardous process conditions. The purchaser is responsible for the training of personnel, for providing hazard warning methods and instrumentation per the appropriate standards, and for ensuring that hazard warning devices and instrumentation are maintained and operated properly.
Teledyne Instruments/ Analytical Instruments, the manufacturer of this instrument, cannot accept responsibility for conditions beyond its knowledge and control. No statement expressed or implied by this document or any information disseminated by the manufacturer or its agents, is to be construed as a warranty of adequate safety control under the user’s process conditions.
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Infrared Gas Analyzer
Specific Model Information
Instrument Serial Number: _______________________
Instrument Range: _______________
Calibrated for: _______________
Background Gas: _______________
Zero Gas: _______________
Span Gas: _______________
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Model 7600
Safety Messages
Your safety and the safety of others is very important. We have provided many important safety messages in this manual. Please read these messages carefully.
A safety message alerts you to potential hazards that could hurt you or others. Each safety message is associated with a safety alert symbol. These symbols are found in the manual and inside the instrument. The definition of these symbols is described below:
GENERAL WARNING/CAUTION: Refer to the instructions
for details on the specific danger. These cautions warn of specific procedures which if not followed could cause bodily Injury and/or damage the instrument.
CAUTION: HOT SURFACE WARNING: This warning is
specific to heated components within the instrument. Failure to heed the warning could result in serious burns to skin and underlying tissue.
WARNING: ELECTRICAL SHOCK HAZARD: Dangerous
voltages appear within this instrument. This warning is specific to an electrical hazard existing at or nearby the component or procedure under discussion. Failure to heed this warning could result in injury and/or death from electrocution.
Technician Symbol: All operations marked with this symbol
are to be performed by qualified maintenance personnel only.
No
Symbol
CAUTION: THE ANALYZER SHOULD ONLY BE USED FOR THE
NOTE: Additional information and comments regarding a
specific component or procedure are highlighted in the form of a note.
PURPOSE AND IN THE MANNER DESCRIBED IN THIS MANUAL.
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Infrared Gas Analyzer
IF YOU USE THE ANALYZER IN A MANNER OTHER THAN THAT FOR WHICH IT WAS INTENDED, UNPREDICTABLE BEHAVIOR COULD RESULT POSSIBLY ACCOMPANIED WITH HAZARDOUS CONSEQUENCES.
This manual provides information designed to guide you through the installation, calibration operation and maintenance of your new analyzer. Please read this manual and keep it available.
Occasionally, some instruments are customized for a particular application or features and/or options added per customer requests. Please check the front of this manual for any additional information in the form of an Addendum which discusses specific information, procedures, cautions and warnings that may be peculiar to your instrument.
Manuals do get lost. Additional manuals can be obtained from TI/AI at the address given in the Appendix. Some of our manuals are available in electronic form via the internet. Please visit our website at: www.teledyne-ai.com.
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Model 7600
Table of Contents
List of Figures ...............................................................................x
List of Tables...............................................................................xii
Introduction.................................................................................15
1.1 Overview 15
1.2 Main Features of the Analyzer 15
1.3 Options Available 17
1.4 Applications 17
1.5 Description of the Main Unit 18
Installation................................................................................... 21
2.1 Unpacking the Analyzer 21
2.2 Choosing a Location 22
2.3 Mounting the Analyzer 23
2.4 Mounting the Input/Output Terminal Module 23
2.5 Gas Connections 25
2.5.1 Internal Piping Diagram 25
2.5.2 External Piping Diagram 27
2.5.3 Gas Conditioning 28
2.5.4 Flowrate 29
2.5.5 Preparation of Calibration Gas 29
2.5.6 Purging the Analyzer 30
2.5.7 Sample Gas Pressure 30
2.5.8 Example configuration of gas sampling system 30
2.6 Electrical Connections 32
2.6.1 Power Inlet 32
2.6.2 Input/Output Terminal Module 33
2.7 Testing the System 34
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Infrared Gas Analyzer
Operation .....................................................................................35
3.1 General Information 35
3.2 Display and Available Menus 36
3.3 The Display Screen 38
3.3.1 Measurement Mode 38
3.3.2 Setting/Selection Screen 40
3.4 Basic Operation 41
3.5 Setting Up the Analyzer in the User Mode 42
3.5.1 Switch Ranges 42
3.5.1.1 Manual Range Switching 43
3.5.1.2 Range identification contact operation 44
3.5.1.3 Remote Range Selection 45
3.5.1.4 Autoranging 46
3.5.2 Calibration Parameters 46
3.5.2.1 Calibration Value 46
3.5.2.2 Setting of Manual Zero Calibration 48
3.5.2.3 Setting of calibration range 50
3.5.2.4 Setting of auto calibration component/range 51
3.5.3 Alarm Setting 53
3.5.3.1 Configuring the Alarms 55
3.5.3.2 Hysteresis Setting 56
3.5.4 Setting of Auto Calibration 58
3.5.4.1 Auto Calibration 58
3.5.4.2 Gas Flow Time Setting 59
3.5.4.3 Cycle Setting Range 60
3.5.4.4 Remote Start 62
3.5.4.5 Forced Run/Stop of Auto Calibration 62
3.5.5 Setting of Auto Zero Calibration 65
3.5.5.1 Auto Zero Calibration 65
3.5.5.2 Forced run/stop of auto zero calibration 68
3.5.6 Peak Alarm Setting 70
3.5.7 Parameter Setting 73
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Model 7600
3.5.7.1 Output Hold 75
3.5.7.2 Average Value Reset: 78
3.5.7.3 Response Time 79
3.5.7.4 Average Period 79
3.5.7.5 Backlight Timer 80
3.5.7.6 Maintenance mode 81
3.6 Maintenance Mode 82
3.6.1 Sensor Input Value 83
3.6.2 Error Log 84
3.6.3 Calibration Log 84
3.6.4 Optical Adjustment 85
3.6.5 Moisture Interference Adjustment 86
3.6.6 Output Adjustment Screen 86
3.6.7 Other Parameters 87
3.7 Calibration 90
3.7.1 Zero Calibration 90
3.7.2 Span Calibration 91
Maintenance ................................................................................93
4.1 Routine Maintenance 93
4.2 Daily Check and Maintenance Procedures 93
4.3 Analyzer Maintenance 94
4.3.1 Sample Cell Cleaning 94
4.3.2 Cleaning the Cell Block 97
4.4 Optical Zero Adjustment 99
4.5 Moisture Interference Compensation Adjustment 102
4.6 Error Messages 104
4.6.1 Error Log File 106
4.6.2 Error Log Screen 106
4.6.3 Deleting Error Hstory 107
Appendix.................................................................................... 109
A.1 SPECIFICATIONS 109 A.2 Standard Functions 111
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Infrared Gas Analyzer
A.3 Optional Functions 115 A.4 Performance: 116 A.5 Standard Requirements for Sample Gas 117 A.6 Installation Requirements 118 A.7 EC Directive Compliance 118 A.8 Terminal Block Connections 119 A.9 Description on Terminal Block 120
Index...........................................................................................125
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Model 7600
List of Figures
Figure 1-1: Model 7600A Infrared Gas Analyzer...........................16
Figure 1-2: Model 7600 Description..............................................19
Figure 2-1: Slide Rail Mounting Dimensions .................................23
Figure 2-2: Input/Output Terminal Module.....................................24
Figure 2-3: Mounting the I/O Module............................................. 24
Figure 2-4: Internal Piping with Single or Dual Measuring Units ... 26
Figure 2-5: External Piping with Single Inlet and Outlet................27
Figure 2-6: External Piping with Two Pair of Inlet/Outlet (1).......... 28
Figure 2-7: External Piping with Two Pair of Inlet/Outlet (2).......... 28
Figure 2-8: Five Component Analysis System .............................. 31
Figure 2-9: Model 7600 Electrical Connections.............................32
Figure 2-10: Noise Suppression.................................................... 33
Figure 2-11: I/O Cable Connection................................................ 33
Figure 3-1: Front Panel of the Model 7600.................................... 35
Figure 3-2: Interface Keys on the Front Panel...............................35
Figure 3-3: Display Modes and Menu Hierarchy...........................37
Figure 3-4: Example Screen—5 Component Analysis 12
Channels................................................................................38
Figure 3-5: Setting/Selection Screen Areas .................................. 41
Figure 3-6: Hysteresis Example for a High Limit Alarm................. 57
Figure 3-7: Example Auto Calibration ........................................... 61
Figure 3-8: Example Auto Zero Calibration................................... 67
Figure 3-9: Peak Alarm Example ..................................................72
Figure 3-10: Output Hold for Manual Calibration........................... 75
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Infrared Gas Analyzer
Figure 3-11: Output Hold for Auto Calibration ...............................76
Figure 3-12: Output Hold for External Hold ...................................76
Figure 3-13: Average Value Reset................................................79
Figure 3-14: Example Average Period ..........................................80
Figure 4-1: Top Cover Removal....................................................95
Figure 4-2: Sample Cell Removal..................................................95
Figure 4-3: Sample Cell.................................................................96
Figure 4-4: IR Window Assembly..................................................97
Figure 4-5: Detector Secure Nut....................................................98
Figure 4-6: Cell Block Assembly....................................................99
Figure 4-7: Optical Adjustment Display for Dual Optical System
Option...................................................................................100
Figure 4-8: Optical Zero Adjustment............................................101
Figure 4-9: Beam Adjustment Plate.............................................102
Figure 4-10: Bubbler Apparatus ..................................................103
Figure 4-11: The Error Log Screen..............................................107
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Model 7600
List of Tables
Table 2-1: Correspondence of Measured Components and
Measuring Units..................................................................... 27
Table 2-2: Zero and Span Gas......................................................29
Table 4.1 Troubleshooting and Maintenance................................ 93
Table 4-2: Components of Optical Adjustment Screen ............... 100
Table 4-3: Error Messages .......................................................... 104
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Infrared Gas Analyzer
DANGER
COMBUSTIBLE GAS USAGE
This is a general purpose instrument designed for use in a non-hazardous area. It is the customer's responsibility to ensure safety especially when combustible gases are being analyzed since the potential of gas leaks always exist.
The customer should ensure that the principles of operating this equipment are well understood by the user. Misuse of this product in any manner, tampering with its components, or unauthorized substitution of any component may adversely affect the safety of this instrument.
WARNING
Since the use of this instrument is beyond the control of Teledyne Instruments/ Analytical Instruments, referred as TI/AI, no responsibility by TI/AI, its affiliates, and agents for damage or injury from misuse or neglect of this equipment is implied or assumed.
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Model 7600
Teledyne Analytical Instruments xiv
Infrared Gas Analyzer Introduction
Introduction
1.1 Overview
The Model 7600 Infrared Gas Analyzer is a microprocessor based infrared gas analyzer used to measure the concentration of NO, SO CO
, CO and CH4 contained in sample gas. It is based on the principle
2
that different molecular species have unique absorption spectrum in the infrared, and the intensity of absorption is determined by the Lambert­Beer law.
In addition to the infrared analyzer, the Model 7600 can also be equipped with a built-in compact paramagnetic O2 sensor or employ an external zirconia oxygen sensor to increase to 5 the number of simultaneous component species the unit can analyze.
,
2
Teledyne's Series 7600 Infrared (IR) Gas Analyzer is conveniently packaged in either a 19" rack mount or NEMA-4 wall mount enclosure. The NEMA-4 enclosure can be X or Z-purged to satisfy hazardous area installation requirements.
A high-sensitivity mass flow type twin detector is used for infrared measurements. By utilizing a single beam, double path design in conjunction with a serial dual-layer transmission detector, the Series 7600 delivers long term, drift-free performance.
The concentration of the desired gases is displayed on a large, easy­to-read back-lit LCD. Figure 1-1 shows the standard rack mountable Model 7600. The user interface is very intuitive and the menu / mode selection buttons, which are readily accessible, provide the operator with dynamic control and extensive diagnostic capabilities.
1.2 Main Features of the Analyzer
The Model 7600 Infrared Gas Analyzer is designed for accurate and reliable gas analysis and is easy to operate. The following features are standard on the 7600 instrument:
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Introduction Model 7600
Figure 1-1: Model 7600A Infrared Gas Analyzer
Simultaneous measurement of up to five components
Excellent long-term stability
Large, easy to read LCD display showing all simultaneous
measurements and computations
Slide-out, chassis design to facilitate any optical or
maintenance adjustments required to fine tune analyzer performance (7600A)
Multiple, in-depth on-screen analyzer functions easily
accessible using the front-panel user interface buttons
Follow & Hold output signal control (during calibration)
Remote range change control
Low / Hi limit alarms
Range ID signals
Auto-calibration with user adjustable frequency and gas flow
time setting programming capabilities
Remote auto-calibration initiation
Auto-calibration status contacts
Teledyne Analytical Instruments 16
Infrared Gas Analyzer Introduction
Instrument or calibration error contact outputs
Extra functions included such as average value computation,
O2 conversion
Pump ON/OFF contact
1.3 Options Available
Percent O
detector — Paramagnetic (built-in) or ZrO2
2
(externally installed), user preference
O
correction (the conversion of measured CO and SO2
2
readings into values at standard O2 concentration). Consult factory for more detail for this function.
Communication functions:
RS-232C (9 pins D-Sub connector)
Half-duplex bit serial
Modbus protocol
1.4 Applications
The Model 7600 Infrared Gas Analyzer is a versatile analytical instrument tool and is ideally suited for multi-parameter gas analysis requirements for applications such as:
Combustion control within the power, pulp and paper, steel,
and cement industries
Heat treating / Inert gas blanketing atmosphere control
Bulk-gas impurity analysis within the air separation industry
Anaerobic digester / Bio-gas / Land-fill gas analysis
Vent gas analysis of oxyhydrochlorination reactors (EDC)
Off-gas analysis on PTA and Maleic Anhydride reactors
Fluid Catalytic Cracker (FCC) regeneration gas analysis
Ammonia / Fertilizer process gas stream analysis
Continuous Emissions Monitoring Systems (CEMS)
Teledyne Analytical Instruments 17
Introduction Model 7600
Biochemistry and fermentation,
Automotive emission analysis
Explosive and toxic gas analysis
Chemical analysis
Refinery operation
Research applications
1.5 Description of the Main Unit
Teledyne's Series 7600 Infrared Gas Analyzer measures the concentration of NO, SO2, CO2, CO, and CH4 in a gas mixture on a continuous basis. The Series 7600 can also be supplied with an oxygen sensor, which allows the simultaneous measurement of oxygen concentration as well. The NEMA-4 enclosure can be X or Z-purged to satisfy hazardous area installation requirements.
The system uses a high-sensitivity mass flow type twin detector for infrared measurements. A single beam, double path optical bench is installed in conjunction with a serial dual-layer transmission detector.
The concentration of the desired gases is displayed on a large, easy­to-read backlit LCD. The user interface is very intuitive and the menu / mode selection buttons, which are readily accessible, provide the operator with dynamic control and extensive diagnostic capabilities. See Figure 1-2.
The front panel mounted power switch turns the instrument on and off while the display switch controls power to the display.
Front panel mounted handles make sliding the instrument out of the panel rack or enclosure a simple task for easy maintenance.
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Infrared Gas Analyzer Introduction
Figure 1-2: Model 7600 Description
Gas connections for the 7600 instrument are made on the rear panel of the instrument using the ¼” NPT fittings installed. The standard instrument has two measuring units and a pair of inlet/outlet gas
connections exist for each unit. See Section 2.5 Gas Connections.
A power receptacle on the rear panel accepts the three-prong power cable supplied with the instrument. The Model 7600 operates on 100­240 VAC 50/60 Hz power. The power inlet conforms to EN60320 Protection Class 1 specifications.
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Introduction Model 7600
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Infrared Gas Analyzer Installation
Installation
Installation of the analyzer includes:
1. Unpacking the system.
2. Choosing a suitable location
3. Mounting the analyzer
4. Mounting the terminal module
5. Installing gas connections
6. Making electrical connections
7. Testing the installation.
CAUTION: READ THIS CHAPTER IN ITS ENTIRETY BEFORE
INSTALLING THE SYSTEM.
FOR INDOOR USE ONLY.
2.1 Unpacking the Analyzer
The Model 7600 Infrared Gas Analyzer is shipped with the following components:
7600 Analyzer
Input/Output terminal module set
Connection cable
Power cable
Fuse (2)
Cell window mounting tool
Slide rail (2)*
Relay board for auto calibration*
Relay board connection cable*
Instruction manual
Teledyne Analytical Instruments 21
Installation Model 7600
* These optional items are included if specified at the time of purchase
As soon as you receive the instrument, carefully unpack and inspect the analyzer and components for damage. Immediately report any damage to the shipping agent. The analyzer is shipped with all the materials you need to install and prepare the system for operation.
2.2 Choosing a Location
CAUTION: THIS UNIT IS NOT EXPLOSION-PROOF. DO NOT
INSTALL IT IN A LOCATION WHERE EXPLOSIVE OR FLAMMABLE GASES ARE PRESENT.
Select an installation location that meets the following criteria:
This instrument should be rack mounted, or mounted in a
steel enclosure.
Indoor location.
Vibration-free.
Not exposed to direct sunlight.
Clean and non-cluttered space.
Depending on the options selected at the time of purchase,
the model 7600 requires an AC power source of 100V to 240V AC.
Operating voltage: 85V to 264V AC
Rated frequency: 50/60 Hz
Power consumption: 250 VA max.
Plug: Comformity to EN60320 class I type 3-pin inlet
Operation conditions:
Ambient temperature: -5° to 45°C
Ambient humidity: 90 % RH or less, no condensation
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Infrared Gas Analyzer Installation
2.3 Mounting the Analyzer
The 19” rack mountable 7600 analyzer is designed for either a guide rail or slide rail mounting within a rack or cabinet. The guide rail method supports the weight of the instrument from the bottom and can be used when there is adequate space for removing the top cover for maintenance. The slide rail mount supports the instrument from sliders mounted on the side of the instrument as shown in Figure 2-1. The instrument is then able to slide out of the rack or enclosure for required access during maintenance.
Figure 2-1: Slide Rail Mounting Dimensions
2.4 Mounting the Input/Output Terminal Module
The input/output module is the electronic interface that handles the various signals to and from the analyzer. It consists of up to five terminal blocks, a communications connector, a cable connector, and a solenoid drive output connector mounted together on a single mounting plate. See Figure 2-2.
Mount the input/output terminal module to the rack or cabinet panel using the six M4 screws supplied. For grounding, see Figure 2-3.
Note: To avoid noise generated from external units, mount the
I/O terminal module mounting plate to the panel making sure there is adequate metal contact for continuity at the
Teledyne Analytical Instruments 23
Installation Model 7600
mounting surface. Connect the panel to the same ground as the analyzer main unit.
Figure 2-2: Input/Output Terminal Module
Figure 2-3: Mounting the I/O Module
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Infrared Gas Analyzer Installation
2.5 Gas Connections
Gas connections are made on the rear panel of the analyzer. Adhere to the following guidelines when making gas connections:
Use a corrosion resistant tube such as Teflon, stainless or
polyethylene to connect the instrument to a sampling system. Even if there is a danger of corrosion, refrain from using rubber or soft vinyl tubing. This would result in instrument inaccuracies due to gas absorption by the piping materials.
Pipe connection port is Rc1/4 female thread (or NPT1/4).
Piping should be cut as short as possible for quicker response. About 4 mm inner diameter is recommended.
Keep out dust and debris from the tubing and connections .
Always use clean tubing and fittings.
Connect the gas tube as follows:
Sample gas inlet: Attach the sample gas tube to the inlet
fitting. The sample gas should be filtered and dehumidified before passing into the analyzer. This port is also used to connect the zero and span calibration gases.
The gas flow should be constant within the range of 0.5
L/min ±0.2 L/min.
Sample gas outlet: Sample gas exits the analyzer through
the gas out port at atmospheric pressure. Exhaust gases must be vented safely.
Purge gas inlet: This connection is used for purging the
inside of the analyzer. Purging is not always required. See
Section 2.5.6 Purging the Analyzer. When required, use dry
N
or instrumentation air for the purge gas. Use a flow rate of
2
1L/min or greater).
2.5.1 Internal Piping Diagram
Note: When the purge gas inlet is provided, an internal
connection to measuring unit 2 is installed.
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Installation Model 7600
An internal piping diagram for an instrument with one or two measuring units is shown in Figure 2-4. When there are two measuring units, if a built-in oxygen sensor is used, it must be installed in measuring unit 2. The diagram shows the combination of two cells used in measuring unit #2. This is possible by combining ranges. When a single measuring unit is used, there is only a single inlet and outlet gas connection.
Figure 2-4: Internal Piping with Single or Dual Measuring Units
Depending on the options chosen, the analyzer can be configured in several ways. Table 2-1 lists the possible configurations for single and dual measuring units with 1 to 4 component meters.
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Infrared Gas Analyzer Installation
/
/
Table 2-1: Correspondence of Measured Components and Measuring Units
Measuring components Measuring unit 1 Measuring unit 2
1-component meter for NO, SO
, CO2, CO and CH4
2
2-component meter for NO/SO
and CO
2
2
CO
2-component meter for
Each component None
2
CO
2
None
NO/SO CO
NO CO
NO/CO 3-component meter for
NO/SO
/CO
2
4-component meter for NO/SO
/CO2/CO
2
NO/SO
NO/SO
CO
2
CO2/CO
2
2.5.2 External Piping Diagram
There are several ways to bring sample gas to the analyzer depending on the number of inlet/outlet gas connections on your instrument Recommended piping diagrams are shown in Figures 2-5, 2­6 and 2-7. Figure 2-5 is a schematic for an instrument with a single pair of inlet/outlet gas connections. Figures 2-6 and 2-7 are used when there are two pair of inlet/outlet connections. Note that a NO2/NO converter is used when NO measurement is used for NOx analysis.
Figure 2-5: External Piping with Single Inlet and Outlet
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Installation Model 7600
Figure 2-6: External Piping with Two Pair of Inlet/Outlet (1)
Figure 2-7: External Piping with Two Pair of Inlet/Outlet (2)
2.5.3 Gas Conditioning
For optimum performance, the sample gas should be treated as
follows:
A filter should be installed to remove any dust or particles in
the sample gas. For a final stage filter, use a filter that can remove dust particles of 0.3 μm.
Teledyne Analytical Instruments 28
Infrared Gas Analyzer Installation
The dew point of the sample gas must be lower than the
ambient temperature to avoid condensation in the analyzer. If vapor is contained in the sampling gas, the dew point should be lowered to 0°C by using a dehumidifier.
If SO
mist is contained in the sample gas, use a mist filter or
2
cooler to remove the SO2 mist. Other mists should be removed by using an appropriate mist filter or cooler.
Corrosive gases such as Cl
, F2 and HCl, if contained in the
2
sample gas in considerable amounts, will shorten the life of the instrument.
Sample gas temperature should be within 0 to 50°C. Hot gas
should not be fed directly into the instrument.
2.5.4 Flowrate
Use a flowrate of 0.5L/min ±0.2L/min. The sample system should be designed to avoid any flow fluctuation during measurement.
Use a flowmeter to observe the flow reading as shown in the external piping diagrams of Figures 2.5, 2.6 and 2.7.
2.5.5 Preparation of Calibration Gas
Routine calibration using calibration gases is required for optimizing the performance of this instrument. Once a week is a suggested calibration frequency. Table 2-2 indicates the zero and span gas required for calibration.
Table 2-2: Zero and Span Gas
Zero gas
Span gas other than for O
2
Span gas for
analysis
O
2
Teledyne Analytical Instruments 29
Analyzer without
O
2
N
gas N2 gas Dry air
2
Gas concentration of 90% or more of full scale
NA
Analyzer with built-in
O2
Gas concentration of 90% or more of full scale
Gas concentration of 90% or more of full scale
Gas concentration of 90% or more of full scale
1 to 2% O
Analyzer with external
zirconia O2 sensor
2
Installation Model 7600
2.5.6 Purging the Analyzer
In general, purging the analyzer is not required unless one of the
following cases apply:
A combustible gas component is contained in sample gas.
Corrosive gas is contained in the atmospheric air at the
installation site.
The same gas as the sample gas component is contained in
the atmospheric air at the installation site.
In the above situations, the inside of analyzer should be purged
with instrument air or N2. Use a purge flow rate of about 1 L/min.
Use a filter to remove dust or mist from the purge gas.
2.5.7 Sample Gas Pressure
The sample gas pressure at the outlet should be atmospheric
pressure.
2.5.8 Example configuration of gas sampling system
A typical system configuration with five component gas analysis for monitoring combustion exhaust gas from boiler, refuse incinerator, etc. is shown in Figure 2-8. Contact Teledyne for specific application system configuration or further information.
The system shown is comprised of:
Model 7600—with dual measuring unit option and external
zirconia oxygen sensor.
Gas Extractor—with stainless steel filter of standard mesh 40
μm equipped with integral heater.
Mist Filter—to remove condensate, mist and dust from the
sample before it enters the analyzer.
Safety Drain Trap—with two compartments for positive and
negative pressure. It monitors and adjusts the sample gas pressure.
Gas Aspirator—to aspirate the sample gas.
Electronic Gas Cooler—used to dry the sample gas to a dew
point of approximately 2°C (35.6°F).
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