Teledyne 6200A User Manual

MODEL 6200A

TRS ANALYZER

MANUAL ADDENDUM

TELEDYNE ANALYTICAL INSTRUMENTS

03655 Rev. A, August, 2000

TABLE OF CONTENTS

TABLE OF CONTENTS TABLE OF FIGURES

1.0 WARRANTY

1.1 Claims for damaged shipments

1.2 Claims for shipping discrepancies

2.0 INTRODUCTION

2.1 Specifications

2.1.1 Analyzer Specifications

2.1.2 TRS Converter Specifications

2.2 The Sulfides Analyzer

2.3 Configurations

2.4 The TRS – Total Reduced Sulfur Converter

2.5 Installation

2.6 Operation and Calibration

2.6.1 Calibration Theory

2.6.2 Zero and Span Calibration Procedure

2.7 M501TRS Temperature Controller

2.7.1 Changing the Temperature Set Point

2.7.2 Adjusting the P-I-D Parameters

3.0 TROUBLESHOOTNG

4.0 MAINTENANCE

4.1 SO2 Analyzer Maintenance

4.2 Changing the Quartz Tube

4.3 Checking the Converter Efficiency

4.4 Sample Diluter Maintenance

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I I 1

2 2

3 3 3 4 4 8 10 12 12 13 14 14 15

17 19

19 19 19 20

TAI - Thermal Converter Operator Manual - Page i

TABLE OF FIGURES

FIGURE 2.1 – STANDARD CONFIGURATION 5 FIGURE 2.2 – WITH IZS OPTION 6 FIGURE 2.3 – WITH M702 CALIBRATOR OPTION 7 FIGURE 2.4 – TRS CONVERTER LAYOUT 9 FIGURE 2.5 – PNEUMATIC CONNECTIONS 11 FIGURE 3.1 – TRS WIRING DIAGRAM 18 FIGURE 4.1 – DILUTER FLOW BLOCK ASSEMBLY 21

TAI - Thermal Converter Operator Manual - Page i

TABLE OF TABLES

TABLE 2.1 – TRS CONVERTER SPECIFICATIONS TABLE 2.2 – ZERO CALIBRATION PROCEDURE TABLE 2.3 – SPAN CALIBRATION PROCEDURE TABLE 2.4 – TEMPERATURE CONTROLLER - INITIAL SETTINGS TABLE 2.5 – TEMPERATURE CONTROLLER - SECONDARY MENU

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3 13 14 16 16

TAI - Thermal Converter Operator Manual - Page i

TAI - Thermal Converter Operator Manual - Page 1

1.0 WARRANTY

TELEDYNE ANALYTICAL INSTRUMENTS

Prior to shipment, TAI equipment is thoroughly inspected and tested. Should equipment failure occur, TAI assures its customers that prompt service and support will be available.

COVERAGE

After the warranty period and throughout the equipment lifetime, TAI stands ready to provide on-site or inplant service at reasonable rates similar to those of other manufacturers in the industry. All maintenance and the first level of field troubleshooting are to be performed by the customer.

GENERAL

TAI warrants each Product manufactured by TAI to be free from defects in material and workmanship under normal use and service for a period of one year from the date of delivery. All replacement parts and repairs are warranted for 90 days after the purchase.

If a Product fails to conform to its specifications within the warranty period, TAI shall correct such defect by, in TAI's discretion, repairing or replacing such defective Product or refunding the purchase price of such Product.

02024c

The warranties set forth in this section shall be of no force or effect with respect to any Product: (i) that has been altered or subjected to misuse, negligence or accident, or (ii) that has been used in any manner other than in accordance with the instruction provided by TAI or (iii) not properly maintained.

THE WARRANTIES SET FORTH IN THIS SECTION AND THE REMEDIES THEREFORE ARE EXCLUSIVE AND IN LIEU OF ANY IMPLIED WARRANTIES OF MERCHANTABILITY, FITNESS FOR PARTICULAR PURPOSE OR OTHER WARRANTY OF QUALITY, WHETHER EXPRESSED OR IMPLIED. THE REMEDIES SET FORTH IN THIS SECTION ARE THE EXCLUSIVE REMEDIES FOR BREACH OF ANY WARRANTY CONTAINED HEREIN. TAI SHALL NOT BE LIABLE FOR ANY INCIDENTAL OR CONSEQUENTIAL DAMAGES ARISING OUT OF OR RELATED TO THIS AGREEMENT OF TAI'S PERFORMANCE HEREUNDER, WHETHER FOR BREACH OF WARRANTY OR OTHERWISE.

TERMS AND CONDITIONS

All units or components returned to TAI should be properly packed for handling and returned freight prepaid to the nearest designated Service Center. After the repair, the equipment will be returned, freight prepaid.

1.1 Claims for damaged shipments

All instruments should be thoroughly inspected immediately upon receipt. Material in the container should be checked against the enclosed packing list. If the contents are damaged and/or the instrument fails to operate properly, the carrier and TAI should be notified immediately.

The following documents are necessary to support claims:

Original freight bill and bill of lading

•

Original invoices or photocopy of original invoice

•

Copy of the packing list

•

Photographs of damaged equipment and container

•

1.2 Claims for shipping discrepancies

All containers should be checked against packing list immediately upon receipt. If a shortage occurs, notify the carrier and TAI immediately. TAI will not be responsible for shortages against the packing list unless they are reported immediately.

The following information is necessary to make a claim:

The instrument model number

•

Serial number

•

Sales order number or purchase order number

•

Upon receipt of a claim, TAI will advise disposition of the equipment for repair or replacement.

TAI - Thermal Converter Operator Manual - Page 2

2.0 INTRODUCTION

This manual addendum should be used in conjunction with the standard Model 6200A.

2.1 Specifications

2.1.1 Analyzer Specifications

The specifications for the SO2 analyzer are contained in the standard Model 6200A manual.

2.1.2 M501TRS Converter Specifications

TABLE 2.1 – M501TRS Converter Specifications

Specification Value Unit

Flow Rate 1000 Cc/min maximum TRS Concentration 20 ppm Converter Temperature 950 – 1050 Dilution Ratio 4.3:1 Number Conversion Eff. (H2S) >98 % Power 220 VAC, 50/60 Hz, 220 watts Weight 24 lbs

11 kg

Dimensions 7 x 17 x 22 inches

178 x 432 x 559 mm

TAI - Thermal Converter Operator Manual - Page 3

2.2 The 6200A Sulfides Analyzer

The TAI Model 6200A Sulfides Analyzer, is designed to measure mixed sulfur impurities, collectively referred to as TRS, in carbon dioxide (CO2) gas. Since there is no SO2 scrubber in the system, the instrument reading is the sum of the reduced sulfur compounds and SO2. The 6200A consists of a modified 6200A UV Fluorescence SO2 Analyzer and a M501TRS high temperature quartz converter.

The M501TRS converts sulfur compounds to SO2 at high temperature by flowing the gas through a hot quartz tube, the resultant reaction is as follows:

TRS + O2 --> SO

Since the gas being analyzed is CO2, which generally contains no oxygen, there is an assembly that injects a small amount of air into the sample stream resulting in about 4% oxygen in the sample. The added oxygen allows the sulfur compounds to be oxidized to SO2. Any SO2 present in the sample is unaffected by the converter. The sample gas then passes to a modified 6200A analyzer where the converted compounds are analyzed as SO2.

2.3 Configurations

There are three configurations available:

1. The standard unit consisting of: A modified 6200A Fluorescent SO2 Analyzer

•

A M501TRS High Temperature Converter

•

See Figure 2.1 for the pneumatic diagram

•

2. The standard unit described above plus: An Internal Zero/Span (IZS) Option with H2S permeation tube

•

The IZS option uses sample gas, passed through a charcoal scrubber to dilute H2S from

•

the perm tube plus a converter bypass valve to assure a high quality zero/span calibration. See Figure 2.2 for the pneumatic diagram

•

3. The standard unit described above plus: An external PRC-6000 calibrator for blending tanks of H2S or SO2 span gas with CO2.

•

See Figure 2.3 for the pneumatic diagram

•

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FIGURE 2.1 – BASIC CONFIGURATION

TAI - Thermal Converter Operator Manual - Page 5

FIGURE 2.2 – WITH IZS OPTION

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FIGURE 2.3 – WITH M702 CALIBRATOR OPTION

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2.4 The M501TRS – Total Reduced Sulfur Converter

The M501TRS oxidizes reduced sulfur compounds to SO2 in a high temperature quartz oven.

Power to the heater is controlled by a front panel mounted programmable temperature controller. Power to the heater is switched by a solid state switch. An over-temperature alarm contact closure is located on the rear panel. The alarm set point is adjustable in the temperature controller. The heater temperature is

WARNING !

INSURE PROPER LINE VOLTAGE IS SELECTED PRIOR

TO PLUGGING UNIT INTO POWER SOURCE.

WARNING !

THE QUARTZ TUBE AND HEATER ARE VERY HOT

DO NOT TOUCH

sensed by a Type K (chromel-alumel) thermocouple probe inserted in the bore alongside the quartz tube.

The quartz tube carrying the sample mixture runs through the core of the heater and is heated by radiation from electrical heating elements at the heater bore surface. See Figure 2.4 for a layout view of the converter.

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FIGURE 2.4 – TRS CONVERTER LAYOUT

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2.5 Installation

The 6200A comes in two chassis. There is a power cord for each that should be plugged into the correct voltage and frequency receptacle. See the tag on the rear panel of each chassis for the voltage and frequency settings. The power connection must be made by an approved three-wire-grounded power cord.

The pneumatic connections are shown in Figure 2.5.

Connection to the TRS analyzer must be made with Teflon or stainless steel tubing.

•

Connect the sample inlet to the labeled fitting.

•

The sample exhaust must be routed to a well ventilated area away from the air inlet for the zero

•

air scrubber on the rear panel.

CAUTION !

DO NOT BLOCK THE SIDE AND BACK

VENTILATION OF THE M501TRS

CONVERTER

The overall pneumatic diagrams of the Model 6200A are shown in Figures 2.1, 2.2, and 2.3.

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FIGURE 2.5 – PNEUMATIC CONNECTIONS

TAI - Thermal Converter Operator Manual - Page 11

2.6 Operation and Calibration

Refer to the 6200A manual for the overall operation of the SO2 analyzer. This unit has some unique operating characteristics and calibration procedures detailed below.

2.6.1 Calibration Theory

The basic purpose of this instrument is to analyze CO2 sample gas for sulfur containing impurities. Unlike similar analysis, there is not any zero air available. The following procedure will to allow the instrument to be zeroed and spanned using the CO2 sample gas that may contain impurities.

The CO2 gas used for zero air is routed from the sample inlet through a charcoal scrubber to remove any SO2 present.

This gas then passes through the converter and into the reaction cell for measurement. When the signal is stable, the value Z1 is stored.

Since there are numerous other sulfur containing gasses, it is not possible to determine how well the charcoal will scrub compounds other than SO2. A 3-way valve is used to bypass the M501TRS converter, so the sample gas now passes through a charcoal scrubber, then directly to the reaction cell.

The instrument is allowed to collect data with the converter bypassed and this reading is stored as Z2. This is the actual instrument zero reading.

Span calibration uses span gas generated by a H2S permeation tube, which has been diluted by scrubbed CO2 described above.

During this phase, the converter MUST be in the pneumatic pathway so the H2S can be oxidized to SO2 and thus measured. However, the converter will not only convert the H2S, but also any impurities that were not scrubbed by the charcoal, thus producing an anomalously high reading. (If there is no additional impurities in the CO2 gas, the correction factor will be zero.)

To correct for this error, the software computes a span correction by the following equation:

Z3 = Z1 - Z2

Where:

Z2 = Zero reading with the converter bypassed. Z1 = Zero reading with the converter in place Z3 = Zero gas impurity correction factor

TAI - Thermal Converter Operator Manual - Page 12

When the span gas reading stabilizes, Z3 is subtracted from the span reading, yielding the actual H2S span gas value as follows:

[H2S]

Actual

= [H2S]

Apparent

– Z3

Where:

Z3 = Zero gas impurity correction factor [H2S] [H2S]

The [H2S]

Actual

= Analyzer response to H2S perm tube + impurities in the zero air.

Apparent

= H2S span reading corrected for impurities in zero air.

Actual

is the reading used to compute the span concentration.

2.6.2 Zero and Span Calibration Procedure

The following is a concise summary of the steps required to zero and span calibrate the 6200A. Please refer to the standard 6200A manual for a more complete description of the calibration procedure.

Table 2.2 – Zero Calibration Procedure

Step

Number

Press CALZ With sample gas flowing into the sample inlet of the

Action Comment

instrument, press CALZ, which routes sample air into the charcoal scrubber.

2. Press ZERO ZERO starts Phase 1 of the zero calibration procedure, allowing zero to be measured with the converter in the pneumatic pathway. Allow 10 min for stable zero.

Press ENTR

After allowing the instrument to stabilize, press ENTR, to store the Z1 zero value with the converter in the pathway. The ZERO key now re-appears, which starts Phase 2

of the zero calibration. Allow 10 min for stable zero.

4. Press ENTR The converter is not in the pathway. Allow the instrument to stabilize on the new zero value, then press ENTR to store the Z2 zero value.

Press EXIT

Returns instrument to SAMPLE mode.

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Table 2.3 – Span Calibration Procedure

Step

Number

2. Press SPAN With the converter in the pathway, the instrument will

Press CALS With sample gas flowing into the sample inlet of the

Press ENTR

Press EXIT

Action Comment

instrument, press CALS, which routes sample air into the charcoal scrubber, then over the H2S permeation tube.

respond to H2S from the perm tube plus any impurities in the zero air.

After allowing the instrument to stabilize, press ENTR. The instrument will use the span reading, corrected for impurities, to compute the actual H2S span value.

Returns instrument to SAMPLE mode.

2.7 M501TRS Temperature Controller

The heater temperature is maintained by a front panel-mounted programmable controller. The “Fuji Electric PXZ Series Operation Manual” is included with the documentation for this instrument. The controller has been set up at the factory. Should further adjustments be necessary, a brief summary of the operation of the controller is included.

By pressing the PV/SV button in the lower left corner of the controller, you can see the Present Value “PV” (actual temperature) or the Set Value “SV” (Set point Value).

2.7.1 Changing the Temperature Set Point

The temperature can be adjusted to optimize conversion efficiency, follow these steps:

1. Select SV with the PV/SV button,

2. Select the Set-Point value at approximately 960oC by Press the "up-arrow" under the digit you want to change, (the digit will flash).

NOTE:

DO NOT SET THE TEMPERATURE HIGHER THAN 1050OC

TAI - Thermal Converter Operator Manual - Page 14

3. Press the "up-arrow" under the digit or the "down-arrow" at the left to scroll the digit to the desired value.

4. Repeat for the other two digits,

5. Press the ENTER button.

6. Select PV with the PV/SV button to observe the actual temperature. Allow temperature to equilibrate for a minimum of 30 to 45 minutes.

NOTE:

It is normal for the ceramic heating element to emit a red glow

at the operating temperature.

2.7.2 Adjusting the P-I-D Parameters

In the event that the control parameters must be changed or in the event that a new controller is installed, it must be reprogrammed to suit the thermal characteristics of the instrument. It is recommended that the Auto Tune function be used to set the control functions if reprogramming is necessary.

The following table is a guide to the approximate values for setting the parameters that will produce the initial settings for the autotune function. Below is a summary of the autotune procedure, refer to the Fuji Manual for more detailed information.

To perform Auto Tune function, set the parameter A7 to 1, then press ENTER.

The controller will begin the autotune process, which takes several minutes. The decimal point at the lower right of the display will blink, indicating the controller is autotuning. During the process, the temperature may oscillate ±100oC or more. When the process is completed, the decimal point will stop blinking.

TAI - Thermal Converter Operator Manual - Page 15

Table 2.4 – Temperature Controller - Initial Settings

PRESS DISPLAY INITIAL VALUE

SEL SEL SEL SEL

SEL

SEL SEL SEL SEL

Table 2.4 shows a Secondary Menu of parameters that set more basic parameters of the controller, these include the thermocouple type, the temperature units etc.

P PROP BAND i INTEGRAL d DERIVATIVE TIME AL LOW ALARM

SETPOINT AH HIHG ALARM

SETPOINT

7C CYCLE TIME HYS HYSTERESIS A7 AUTOTUNE LOC LOCK

Table 2.5 – Temperature Controller - Secondary Menu

UP/DOWN SET TO “11” SET TO “10” SET TO “7.7” SET TO “50” (C BELOW FINAL SETPOINT)

SET TO “50” (C ABOVE FINAL SETPOINT)

SET TO “2” SET TO “3” SET TO “0” (OFF) “0” (OPEN) “1” (LOCKED) “2” (SV ONLY OPEN)

PRESS DISPLAY PARAMETER VALUE

SEL HOLD TILL p-n1 SEL p-n2 SEL SEL SEL SEL SEL SEL SEL SEL SEL SEL SEL

p-dF DIGITAL FILTER P-SL LOWER LIMIT P-SU UPPER LIMIT P-AL ALARM TYPE2 P-AH ALARM TYPE 1 P-An HYTERESIS

P-dP DECIMAL LOCATION PVOF PROCESS OFFSET

SVOF SET POINT OFFSET P-F FUZZY FUZZY LOGIC

SET TO “0” SET TO “3” (TYPE K THERMOCOUPLE) SET TO “5” SET TO “32” (32C) SET TO “1050” (1050C) SET TO “900” SET TO “1050” SET TO “3” SET TO “0” LEAVE AT “0” LEAVE AT “0” SET TO “ºC” (CENTIGRADE) SET TO “ON”

TAI - Thermal Converter Operator Manual - Page 16

3.0 TROUBLESHOOTNG

NO POWER: Plugged in?

Switched on? Circuit breaker Tripped?

NOT HEATING: PV/SV switch to PV. Is it heating?

PV/SV switch to SV. Set point correct? Socket in place on back of controller? Check M501TRS wiring diagram Figure 3.1

TRS ANALYZER UNSTABLE: Leak-check.

(Pressurize and see if pressure falls. Use soap bubble to find leak.)

EFFICIENCY <90%: Leaking? Leak-check.

Plugged? Compare flow through and bypassing converter. Flow too high? Set-point temperature optimized? Span gas correct? Contaminated? Check inside of Teflon tubing.

CONVERTER TEMP UNSTABLE: Perform autotune procedure in Section 2.7.2.

TAI - Thermal Converter Operator Manual - Page 17

FIGURE 3.1 – TRS WIRING DIAGRAM

TAI - Thermal Converter Operator Manual - Page 18

4.0 MAINTENANCE

4.1 SO2 Analyzer Maintenance

Maintenance of the SO2 analyzer is covered in Section 8 of the 6200A manual.

4.2 Changing the Quartz Tube

1. Turn off M501TRS and allow it to cool to room temperature.

2. See Figure 2.4. – M501TRS Layout

3. Remove the screws from the top inside of the front panel and fold panel downward.

4. Loosen front and rear fittings at each end of the tube.

5. Carefully slide tube out of heater – the ceramic bushings at each end of the heater are very fragile.

6. Slide in new tube and re-connect fittings.

7. Leak check the unit.

8. Check the converter efficiency. See Section 4.3

4.3 Checking the Converter Efficiency

After maintenance it is good practice to check the converter efficiency. To check the converter efficiency, perform the following procedure:

1. Obtain a gas blender that will create H2S span gas (either permeation tube or tank) with CO2 gas as the diluent. Remember that rotameters and mass flow controllers are calibrated with air or nitrogen. Using them with CO2 will produce large calibration errors. Since CO2 gas has considerably different characteristics, use flowmeters such as soap bubble, or BIOS – DryCal flowmeters that measure volume flow.

2. Produce a calibration gas of 400 ppb H2S at a flow greater than the demand of the instrument, vent the excess gas out of the room.

3. Allow the 6200A to stabilize at span.

4. Adjust the converter efficiency by:

Lower the set-point temperature of the Converter in 5oC increments allowing 10

•

minutes minimum between increments until a drop of approximately 1% Full Scale is observed. Note the Thermal Converter temperature. Increase the set-point temperature in 5C increments allowing 10 minutes minimum

•

between increments until a drop of approximately 1% Full Scale is observed. Note the Thermal Converter temperature. Set the set-point value to fall midway between the low and high temperatures.

•

TAI - Thermal Converter Operator Manual - Page 19

If no drop off occurs when the temperature is raised to 1050C, select the set-point

•

temperature that maximizes analyzer reading.

4.4 Sample Diluter Maintenance

The sample diluter is used to inject a small amount of ambient air into the sample stream to provide oxygen for the converter. The diluter is located on the inside rear panel of the SO2 analyzer. It consists of a stainless steel block and 2 orifices to control the amount of sample and air that is blended.

There should be no periodic maintenance required on this assembly, but a diagram is included in case rebuilding of this assembly is required. The assembly is shown in Figure 4.1.

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FIGURE 4.1 – DILUTER FLOW BLOCK ASSEMBLY

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INSTRUCTION MANUAL

MODEL 6200A

SULFUR DIOXIDE ANALYZER

SERIAL NO. _______________

TELEDYNE ANALYTICAL INSTRUMENTS

16830 CHESTNUT STREET

CITY OF INDUSTRY, CA 91749-1020

TOLL-FREE: 888.789.8168

FAX: 626.961.2538

TEL: 626.934.1500

E-MAIL: tetci_customerservice@teledyne.com

WEB SITE: www.teledyne-ai.com

02164

REV. G

12/12/98

TAI Model 6200A SO2 Analyzer Operator Manual, 02164, Rev. G

Table of Contents

1 HOW TO USE THIS MANUAL..................................................................1-1

AFETY MESSAGES

1.1 S

2 GETTING STARTED.................................................................................2-1

NSTALLATION

2.1 I

LECTRICAL AND PNEUMATIC CONNECTIONS

2.2 E

NITIAL OPERATION

2.3 I

3 SPECIFICATIONS, AGENCY APPROVALS, WARRANTY .....................3-1

PECIFICATIONS

3.1 S

3.2 EPA E

3.3 W

QUIVALENCY DESIGNATION

ARRANTY

................................................................................................................ 3-3

4 THE 6200A SO2 ANALYZER .................................................................... 4-1

RINCIPLE OF OPERATION

4.1 P

NSTRUMENT DESCRIPTION

4.2 I

4.2.1 Sensor Module, Reaction Cell, Detector............................................................4-4

4.2.2 Pneumatic Sensor Board...................................................................................4-4

4.2.3 Computer Hardware and Software .................................................................... 4-4

4.2.4 V/F Board ..........................................................................................................4-5

4.2.5 Front Panel ........................................................................................................ 4-5

4.2.6 Power Supply Module........................................................................................4-8

4.2.7 Pneumatic System............................................................................................. 4-8

.................................................................................................... 1-2

............................................................................................................ 2-1

................................................................ 2-1

..................................................................................................... 2-6

........................................................................................................ 3-1

............................................................................... 3-2

.......................................................................................... 4-1

......................................................................................... 4-4

5 SOFTWARE FEATURES..........................................................................5-1

NDEX TO FRONT PANEL MENUS

5.1 I

5.1.1 Sample Menu .................................................................................................... 5-3

5.1.2 Set-Up Menu ..................................................................................................... 5-4

AMPLE MODE

5.2 S

........................................................................................................... 5-7

5.2.1 Test Functions ................................................................................................... 5-7

5.2.2 CAL, CALS, CALZ, Calibration Functions........................................................ 5-10

SET-UP MODE

5.3

......................................................................................................... 5-12

5.3.1 Configuration Information (CFG) ..................................................................... 5-12

5.3.2 Automatic Calibration (AutoCal)....................................................................... 5-12

5.3.3 Data Acquisition System (DAS) ....................................................................... 5-12

5.3.4 Range Menu .................................................................................................... 5-13

5.3.5 Password Enable............................................................................................. 5-17

5.3.6 Time of Day Clock ...........................................................................................5-17

5.3.7 Diagnostic Mode.............................................................................................. 5-17

5.3.8 Communications Menu .................................................................................... 5-17

5.3.9 Variables Menu (VARS)................................................................................... 5-18

................................................................................. 5-1

TAI Model 6200A SO2 Analyzer Operator Manual, 02164, Rev. G

6 OPTIONAL HARDWARE AND SOFTWARE............................................ 6-1

ACK MOUNT OPTIONS

6.1 R

ERO/SPAN VALVES

6.2 Z

NTERNAL ZERO/SPAN

6.3 I

UTOCAL

6.4 A

ERMEATION TUBE (USED WITH

6.5 P

6.6 4-20

6.7 S

TATUS OUTPUT

6.8 RS-232 I

ETUP OF

- S

URRENT LOOP OUTPUT

A, C

........................................................................................................ 6-9

NTERFACE

6.8.1 Setting Up the RS-232 Interface...................................................................... 6-10

6.8.2 Command Summary........................................................................................ 6-13

6.8.3 TEST Commands and Messages.................................................................... 6-17

6.8.4 WARNING Commands And Messages ...........................................................6-18

6.8.5 CALIBRATION Commands and Messages ..................................................... 6-19

6.8.6 DIAGNOSTIC Commands and Messages....................................................... 6-20

6.8.7 DAS Commands and Reports ......................................................................... 6-21

6.8.8 VARIABLES Commands and Messages ......................................................... 6-24

.............................................................................................. 6-1

................................................................................................... 6-1

(IZS) .......................................................................................6-3

AND ZERO/SPAN VALVES

IZS

OPTION

) ...............................................................6-6

..................................................... 6-3

............................................................................. 6-9

................................................................................................. 6-10

7 CALIBRATION AND ZERO/SPAN CHECKS ........................................... 7-1

7.1 M

7.2 M

7.3 M

7.4 A

7.5 A

7.6 C

7.7 U

7.8 EPA P

7.9 S

7.10 C

7.11 R

ANUAL ZERO/SPAN CHECK OR CALIBRATION THROUGH THE SAMPLE PORT ANUAL ZERO/SPAN CHECK OR CALIBRATION WITH ZERO/SPAN VALVES OPTION

ANUAL ZERO/SPAN CHECK WITH UTOMATIC ZERO/SPAN CHECK UTOMATIC ZERO/SPAN CALIBRATION ALIBRATE ON SE OF

OR ZERO/SPAN VALVES WITH REMOTE CONTACT CLOSURE

IZS

ROTOCOL CALIBRATION

PERMEATION TUBE

IZS O

.................................................................................. 7-7

.................................................................................... 7-9

PTION

............................................................ 7-7

......................................................................... 7-7

....................................................................... 7-8

.................. 7-4

........... 7-6

........................ 7-8

7.8.1 Calibration of Equipment ...................................................................................7-9

7.8.2 Calibration Gas Sources.................................................................................. 7-10

7.8.3 Data Recording Device.................................................................................... 7-12

7.8.4 Dynamic Multipoint Span Calibration ............................................................... 7-12

7.8.5 SO

Calibration Procedure............................................................................... 7-13

7.8.6 Calibration Frequency...................................................................................... 7-19

7.8.7 Other Quality Assurance Procedures ..............................................................7-19

7.8.8 Summary of Quality Assurance Checks ..........................................................7-21

7.8.9 ZERO and SPAN Checks ................................................................................ 7-22

7.8.10 Recommended Standards for Establishing Traceability ................................7-23

PECIAL CALIBRATION REQUIREMENTS FOR DUAL RANGE OR AUTO RANGE

ALIBRATION QUALITY EFERENCES

......................................................................................................... 7-26

............................................................................................ 7-25

.................. 7-24

TAI Model 6200A SO2 Analyzer Operator Manual, 02164, Rev. G

8 MAINTENANCE ........................................................................................8-1

8.1 M

8.2 R

8.3 R

8.4 R

8.5 C

8.6 C

8.7 P

8.8 L

8.9 L

8.10 EPROM R

AINTENANCE SCHEDULE EPLACING THE SAMPLE PARTICULATE FILTER EPLACING THE PERMEATION TUBE (OPTION EPLACING THE LEANING ORIFICE AND ORIFICE FILTER LEANING THE REACTION CELL NEUMATIC LINE INSPECTION

EAK CHECK PROCEDURE IGHT LEAK CHECK PROCEDURE

IZS Z

EPLACEMENT PROCEDURE

........................................................................................... 8-1

ERO AIR SCRUBBER (OPTION

...................................................................... 8-5

................................................................................... 8-6

...................................................................................... 8-6

.......................................................................................... 8-9

............................................................................... 8-10

..................................................................... 8-10

............................................................. 8-2

)............................................................... 8-4

)..................................................... 8-4

9 DIAGNOSTIC, TROUBLESHOOTING......................................................9-1

9.1 O

PERATION VERIFICATION

- 6200A D

9.1.1 Fault Diagnosis with TEST Variables................................................................. 9-3

9.1.2 Fault Diagnosis with WARNING Messages ....................................................... 9-9

9.1.3 Fault Diagnosis using DIAGNOSTIC Mode ..................................................... 9-11

9.1.4 6200A Internal Variables .................................................................................9-18

9.1.5 Test Channel Analog Output ........................................................................... 9-20

9.1.6 Factory Calibration Procedure (Quick Cal) ...................................................... 9-21

9.2 P

ERFORMANCE PROBLEMS

....................................................................................... 9-23

9.2.1 AC Power Check ............................................................................................. 9-23

9.2.2 Flow Check...................................................................................................... 9-24

9.2.3 No Response to Sample Gas .......................................................................... 9-24

9.2.4 Negative Concentration Display....................................................................... 9-25

9.2.5 Excessive Noise ..............................................................................................9-25

9.2.6 Unstable Span ................................................................................................. 9-26

9.2.7 Unstable Zero .................................................................................................. 9-27

9.2.8 Inability to Span ............................................................................................... 9-27

9.2.9 Inability to Zero ................................................................................................ 9-28

9.2.10 Non-Linear Response.................................................................................... 9-28

9.2.11 Slow Response.............................................................................................. 9-29

9.2.12 Analog Output Doesn't Agree With Display Concentration ............................ 9-29

9.3 E

LECTRONIC SUBSYSTEM TROUBLESHOOTING AND ADJUSTMENTS

9.3.1 Computer, Display, Keyboard.......................................................................... 9-30

9.3.2 RS-232 Communications................................................................................. 9-33

9.3.3 Voltage/Frequency (V/F) Board ....................................................................... 9-36

9.3.4 Status/Temp Board.......................................................................................... 9-42

9.3.5 Power Supply Module...................................................................................... 9-45

9.3.6 Flow/Pressure Sensor .....................................................................................9-49

9.3.7 Reaction Cell Temp .........................................................................................9-53

9.3.8 Preamp Board ................................................................................................. 9-53

9.3.9 PMT Cooler ..................................................................................................... 9-53

9.3.10 HVPS (High Voltage Power Supply) .............................................................. 9-56

IAGNOSTIC TECHNIQUES

...................................... 9-3

............................... 9-30

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