Teledyne 4700 Pocket Manual

4700 Refrigerated
Sampler
This pocket guide is not intended to replace the instruction manual. Read the instruction manual thoroughly before operating the sampler.
COPYRIGHT © 2003 by Teledyne Isco, Inc., 4700 Superior St., Lincoln, Nebraska, U.S.A. 68504
Phone: (402) 464-0231 Toll Free: (800) 228-4373 FAX: (402) 465-3022
Part #69-4703-085 Released: January 10, 2007
4700 Refrigerated
Sampler

Table of Contents

1. Introduction
1.1 Features . . . . . . . . . . . . . . . . . . . . . . . 1-1
1.2 Specifications . . . . . . . . . . . . . . . . . . . 1-6
2. Installation
2.1 4700 Sampler Installation Overview 2-1
2.2 Positioning the Sampler . . . . . . . . . . 2-1
2.3 Installing a Bottle Kit . . . . . . . . . . . . 2-5
2.3.1 Installing the Distributor
Arm and Discharge Tube . . . . 2-8
2.3.2 24 Bottles . . . . . . . . . . . . . . . 2-10
2.3.3 4 Bottles . . . . . . . . . . . . . . . . 2-12
2.3.4 2 Bottles . . . . . . . . . . . . . . . . 2-12
2.3.5 1 Bottle . . . . . . . . . . . . . . . . . 2-14
2.4 Attaching the Suction Line . . . . . . . 2-16
2.4.1 Vinyl Suction Line . . . . . . . . 2-17
2.4.2 FEP-lined Suction Line . . . . 2-19
2.5 Attaching a Strainer . . . . . . . . . . . . 2-19
2.5.1 Alternative to Strainers . . . . 2-22
2.5.2 Maximum Unanchored
2.6 Routing the Suction Line and
2.7 Connecting the Sampler to
Depth . . . . . . . . . . . . . . . . . . . 2-22
Strainer . . . . . . . . . . . . . . . . . . . . . . 2-23
External Devices . . . . . . . . . . . . . . . 2-23
2.7.1 Standard Isco Instrument
Connections . . . . . . . . . . . . . . 2-25
2.7.2 Other Device Connections . . 2-25
iii
2.8 Connecting Power . . . . . . . . . . . . . . 2-30
2.9 Configuring and Programming the
Sampler . . . . . . . . . . . . . . . . . . . . . . 2-31
2.10 Locking the Sampler . . . . . . . . . . . . 2-31
3. Programming
3.1 Control Panel Description . . . . . . . . . 3-1
3.2 Getting Started . . . . . . . . . . . . . . . . . 3-3
3.3 Configuring the Sampler . . . . . . . . . . 3-4
3.3.1 Set Clock . . . . . . . . . . . . . . . . . 3-5
3.3.2 Bottle and Sizes . . . . . . . . . . . 3-5
3.3.3 Suction Line . . . . . . . . . . . . . . 3-6
3.3.4 Liquid Detector . . . . . . . . . . . . 3-7
3.3.5 Flow Mode Sampling . . . . . . . 3-9
3.3.6 Enable Pin . . . . . . . . . . . . . . . 3-10
3.3.7 Refrigeration . . . . . . . . . . . . . 3-11
3.3.8 Output Pins . . . . . . . . . . . . . . 3-12
3.3.9 Tubing Life . . . . . . . . . . . . . . 3-14
3.3.10 Program Lock . . . . . . . . . . . . 3-16
3.3.11 Language . . . . . . . . . . . . . . . . 3-17
3.3.12 System IDs . . . . . . . . . . . . . . 3-18
3.3.13 Run Diagnostics . . . . . . . . . . 3-19
3.3.14 Exit Configuration . . . . . . . . 3-19
3.4 Sampling Program Overview . . . . . 3-19
3.5 Programming Steps . . . . . . . . . . . . . 3-26
3.5.1 Pacing . . . . . . . . . . . . . . . . . . 3-26
3.5.2 Sample Every __ Hours,
__ Minutes . . . . . . . . . . . . . . . 3-27
3.5.3 Sample Every __ Pulses . . . . 3-27
3.5.4 __ Bottles per Sample Event 3-31
3.5.5 Switch on Time or Number
of Samples . . . . . . . . . . . . . . . 3-32
3.5.6 Switch Bottles Every
__ Hours, __ Minutes . . . . . . 3-32
3.5.7 First Switch Time . . . . . . . . . 3-32
3.5.8 __Samples per Bottle . . . . . . 3-32
3.5.9 Run Continuously? . . . . . . . . 3-34
3.5.10 Enter Sample Volume
Use Defined Sample . . . . . . . 3-34
iv
Table of Contents
3.5.11 Volumes Dependent
on Flow? . . . . . . . . . . . . . . . . 3-35
3.5.12 Sample Volume __ ml . . . . . . 3-36
3.5.13 Flow Pulses, Analog Input . . 3-36
3.5.14 10 ml for Every __ Pulses . . . 3-36
3.5.15 Sample Volume at
20 mA: __ ml . . . . . . . . . . . . . 3-37
3.5.16 __ Composite Samples . . . . . 3-37
3.5.17 Suction Head . . . . . . . . . . . . . 3-38
3.5.18 No Delay to Start
Set Start Time . . . . . . . . . . . 3-39
3.5.19 First Sample At: . . . . . . . . . . 3-40
3.5.20 Start Flow Count At: . . . . . . 3-40
3.5.21 Maximum Run Time
3.6 Programming Examples . . . . . . . . . 3-41
__ Hours . . . . . . . . . . . . . . . . 3-40
3.6.1 Defining the Sample Volume 3-41
3.6.2 Time Paced Sampling
Program . . . . . . . . . . . . . . . . 3-44
3.6.3 Flow Paced Sampling
Program . . . . . . . . . . . . . . . . 3-47
3.6.4 Flow-proportional Constant Time Variable Volume
Program . . . . . . . . . . . . . . . . 3-51
4. Operation
4.1 Start a Sampler Program . . . . . . . . . 4-1
4.1.1 Start Time Delay . . . . . . . . . . 4-2
4.1.2 The Run State . . . . . . . . . . . . . 4-3
4.1.3 Completed Program . . . . . . . . 4-4
4.2 Pause or Stop a Running Program . . 4-4
4.3 Post Sampling Activities . . . . . . . . . . 4-5
4.3.1 View the Log . . . . . . . . . . . . . . 4-5
4.3.2 Remove Sample Bottles . . . . 4-10
4.4 Grab Samples . . . . . . . . . . . . . . . . . . 4-11
4.5 Calibrate Sample Volumes . . . . . . . 4-12
4.6 Operate the Pump Manually . . . . . . 4-15
v
5. Maintenance
5.1 Periodic Maintenance Checklist . . . . 5-1
5.1.1 Pump Inspection . . . . . . . . . . . 5-2
5.1.2 Pump Tube Replacement . . . . 5-4
5.1.3 Cleaning the Pump Rollers . . 5-7
5.1.4 Cleaning the Pump Housing . 5-7
5.1.5 Cleaning or Replacing
Wetted Parts . . . . . . . . . . . . . . 5-7
5.1.6 Sampler Cleaning Guidelines 5-9
vi
4700 Refrigerated
Sampler

Section 1 Introduction

1.1 Features

The 4700 Series sampler features are identified in Figures 1-1 through 1-3 and described in Table 1-1.
1
2
3
4
5
6
9
Figure 1-1 4700 Sampler features (Front)
7
8
1-1
4700 Refrigerated Sampler
10
11
11
Figure 1-2 4700 Sampler features (Side)
12
13
14
Figure 1-3 4700 Sampler features (Back)
1-2
Section 1 Introduction
Table 1-1 4700 Sampler Features
Item Name Description
1 Control
Panel Cover
2 Control
Panel
3 Discharge
Tube
4 Distributor
Arm
5 Bottles Hold the collected
6 Bottle
Locator Rack
7 Refrigerator
Door
Protects the control panel display and keypad.
Supports user control and programming of sampler operation.
Carries liquid to the sample bottle. For 24, 4, 2, and 10 liter one-bottle configurations, the discharge tube is routed through the distributor arm. For the 20 liter one-bottle configuration the discharge tube is routed directly into the bottle.
Directs collected liquids to the bottle. Movement of the distributor is controlled by user-specified program settings.
samples.
Positions the bottles under the distributor.
Protects the collected samples inside the refrigerated compartment.
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4700 Refrigerated Sampler
Table 1-1 4700 Sampler Features
(Continued)
Item Name Description
8 Latch Secures the door. The
9Level
Adjustment Feet
10 Liquid
Detector and Pump
11 Lift Points If you must lift the sampler,
latch mechanism may be locked with a user-supplied padlock.
The sampler includes two level adjustment feet at the front of the sampler. Use these to keep the bottle rack or locating deck level inside the refrigerated compartment.
The non-wetted liquid detector senses when the liquid is at the pump to determine head height and sample volumes. The peristaltic pump collects sample liquid and performs suction line rinses.
it can be safely handled at these points. Lifting must be done by two people, one on each side, with the door closed and latched.
1-4
Section 1 Introduction
Table 1-1 4700 Sampler Features
(Continued)
Item Name Description
12 External
Device Connection
13 Refrigeration
Assembly
14 AC Mains
Line Cord
Supports connections to external devices such as a flow meter for sample pacing and enable signals, and connection to a personal computer for data collection.
Modular, corrosion-resistant refrigeration assembly cools the refrigerated compartment to a user-selected temperature of 1 to 9°C (34 to 48°F).
Connects to AC power source.
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4700 Refrigerated Sampler

1.2 Specifications

Table 1-2 Specifications
General
Size (H×W×D):
Weight (empty):
Bottle Configurations:
Refrigerator Body:
Powe r Requirements:
Installation Category:
Pollution Degree:
130 × 72 × 84 cm 51 × 28 × 33 in
72 kg 159 lb
12 configurations available: 24, 1-liter PP or 350 ml glass; 4, 10-liter PE or glass; 2, 10-liter PE or glass; 1, 20-liter PE or glass; 1, 10-liter PE or glass; 24 ProPaks, 1-liter wedge; 1 ProPak, 10-liter round
Linear low-density polyethylene (LLDPE)
100 VAC ±10%, 50 Hz:
Running current 1.4 amperes Stalled current 21.3 amperes
115 VAC ±10%, 60 Hz:
Running current 1.4 amperes Stalled current 21.3 amperes
230 VAC ±10%, 50 Hz:
Running current 0.82 amperes Stalled current 17 amperes
II
3
1-6
Section 1 Introduction
Table 1-2 Specifications (Continued)
Maximum Altitude:
Humidity: 0 to 100%
Operational Temperature:
Pump
Intake Suction Tubing Length:
Material: Vinyl or FEP-lined polyethylene
Inside Diameter:
Pump Tubing Life:
Maximum Suction Lift:
Ty pi c a l Repeatability:
Typical Line Velocity at Head Height:
Liquid Presence Detector:
2,000 meters
–29 to 49 °C –20 to 120 °F
1 to 30 m 3 to 99 feet
9 mm
3
/8 inch
Typically 1,000,000 pump counts.
8.5 m 28 feet
±5 ml or ±5% of the average volume in a set.
0.9 m: 0.91 m/s
3.1 m: 0.87 m/s
4.6 m: 0.83 m/s
3 ft: 3.0 ft/s 10 ft: 2.9 ft/s 15 ft: 2.7 ft/s
Non-wetted, non-conductive sensor detects when liquid sample reaches the pump to automatically compensate for changes in head heights.
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4700 Refrigerated Sampler
Table 1-2 Specifications (Continued)
Controller
Enclosure Rating:
Program Memory:
Flow Meter Signal Inputs:
Digital Alarms: 4 programmable outputs; 5
Number of Composite Samples:
Internal Clock Accuracy:
Software
Sample Frequency:
Sampling Modes:
Programmable Sample Vol um es:
IP67 NEMA 4X, 6
Non-volatile ROM (Flash)
5 to 15 volt DC pulse or 25 millisecond isolated contact closure for Isco flow meters. 4-20 mA input for non-Isco flow meters.
VDC, 100 mA
Programmable from 1 to 999 samples.
1 minute per month, typical
1 minute to 99 hours 59 minutes, in 1-minute increments. 1 to 9,999 flow pulses.
Constant Time, constant volume Variable time, constant volume Constant time, variable volume
(Variable time and variable volume modes are controlled by an external flow meter signal)
10 to 9,990 ml in 1 ml increments.
1-8
Section 1 Introduction
Table 1-2 Specifications (Continued)
Sample Retries:
Rinse Cycles: Automatic rinsing of suction line
Controller Diagnostics:
If no sample is detected, up to 3 attempts; user selectable.
up to 3 rinses for each sample collection.
Tests for RAM, ROM, pump, display, and electrical components.
1-9
4700 Refrigerated Sampler
1-10
4700 Refrigerated
Sampler

Section 2 Installation

2.1 4700 Sampler Installation Overview

The following sections provide general instructions for placing the sampler into operation. In typical applications, the steps are:
1. Position the sampler. (Section 2.2)
2. Install a bottle kit. (2.3)
3. Attach the suction line. (2.4)
4. Attach a strainer. (2.5)
5. Route the suction line and strainer. (2.6)
6. Connect external instruments. (2.7)
7. Connect power. (2.8)
8. Configure and program the sampler. (2.9)
9. Lock the sampler. (2.10)

2.2 Positioning the Sampler

There are a few considerations when selecting a site for the sampler. The foremost concern should be personal safety.
2-1
4700 Refrigerated Sampler
The installation and use of this product may subject you to dangerous working conditions that can cause you serious or fatal injuries. Take any necessary precautions before entering the worksite. Install and operate this product in accordance with all applicable safety and health regulations, and local ordinances.
WAR NING
If this product is used in a manner not specified in this manual, the protection provided by the equipment may be impaired.
WAR NING
This product has not been approved for use in hazardous locations as defined by the National Electrical Code.
WAR NING
The sampler is heavy. When lifting, use a two-person lift at the points identified in Table 1-1. When possible, move the sampler using a two-wheeled hand cart from the left or right side. To prevent damage to the refrigeration system, do not tip the sampler more than 45°.
Dangerous locations – If you must enter a manhole, confined space, or other dangerous location to install the suction line and strainer, observe standard safety precautions. Refer to
2-2
Section 2 Installation
Appendix B of the Installation and Operation guide for a discussion of safety considerations.
Support – The sampler should be installed on a surface capable of safely supporting the sampler, full liquid containers, and personnel.
AC Power – The mains line cord is the disconnect device should you need to remove power. Therefore, the electrical power outlet should be accessible.
Environmental – The sampler is designed for outdoor use. Refer to Table 1-2 for environmental specifications. When possible, avoid subjecting the sampler to chemical attacks and direct sunlight.
Avoid submersion – Although the control panel will resist damage (rated NEMA 4x, 6; IP 67), the refrigerator system and bottle compartment cannot prevent the liquid from entering. Liquid entering the refrigeration system might permanently damage the sampler; liquid entering the bottle compartment might contaminate the collected samples. Liquid entering the electrical compartment for the refrigeration system might result in a short circuit and possible shock hazard.
Liquid sample collection point – It is best to keep the distance between the sampler pump and the collection point as short as possible. The shorter distance will increase pumping efficiency and pump tubing life. Also, the pump inlet should be located above the liquid surface. Gravity will aid suction line rinses and allow
2-3
4700 Refrigerated Sampler
the line to drain, thereby reducing the possibility of sample cross-contamination. Refer to Table 1-2 for maximum suction line lengths and suction head heights.
Security – The location may need to provide some degree of security to prevent tampering or vandalism.
Accessibility – The sampler must be installed in a location where personnel can easily exchange bottles and perform routine service.
The sampler requires about 2600 square centimeters (925 in
2
) of floor space. Additional space must be allowed in front of the sampler, at its left and right sides, and above the sampler. Do not block access to these areas. Obstructions will make routine servicing activities difficult or impossible.
The back of the sampler may be placed against a wall as long as air at the bottom of the refrigerator can flow freely to surrounding air. Unrestricted air flow behind and around the sampler will keep the refrigeration system working efficiently.
Level surface – The sampler should be placed on a level surface and the feet on the refrigerator body should be adjusted to prevent tipping or spills. If the sampler is not level, the sample liquid may miss the bottle mouth.
To level the sampler, place a bubble level on the bottle rack or locating base, then adjust the feet. For one-bottle configurations, place the bubble level on the side rails of the refrigerated compartment.
2-4
Section 2 Installation
CAUTION
Do not tip the sampler on its side or back. Tipping the sampler more than 45° might cause oil to run into the compressor inlet, which can permanently damage the sampler.

2.3 Installing a Bottle Kit

The 4700 sampler can hold 1, 2, 4, and 24 bottles. Each of these bottle configurations are supplied as a kit (see Table 2-1), which is normally ordered with the sampler or when you desire to change the bottle configuration.
Table 2-1 Bottle Kits
Part Number Description
68-4700-003 24-bottle Configuration. Includes
68-4700-004 24-bottle Configuration. Includes
68-4700-017 24-Container ProPak
24 polypropylene 1-liter wedge shaped bottles with caps, retaining ring, bottle rack and two discharge tubes.
24 glass 350-ml round bottles with PTFE lined caps, retaining rings, bottle rack and two discharge tubes.
Configuration. Includes 25 holders, 100 bags, retaining ring, bottle rack and instruction sheet.
2-5
4700 Refrigerated Sampler
Table 2-1 Bottle Kits (Continued)
Part Number Description
68-4700-005 4-bottle Configuration. Includes
68-4700-006 4-bottle Configuration. Includes
68-4700-007 2-bottle Configuration. Includes
68-4700-008 2-bottle Configuration. Includes
68-4700-009 1-bottle Configuration. Includes
68-4700-010 1-bottle Configuration. Includes
four polyethylene 10-liter round bottles with caps, locating base and two discharge tubes.
four glass 10-liter round bottles with PTFE lined caps, locating base and two discharge tubes.
two polyethylene 10-liter round bottles, locating base, caps and two discharge tubes.
two glass 10-liter round bottles with PTFE lined caps, locating base, and two discharge tubes.
one polyethylene 2.5-gallon (10-liter) round bottle, locating base, two caps and two discharge tubes.
on glass 2.5-gallon (10-liter) round bottle, two PTFE lined caps, locating base, and two discharge tubes.
2-6
Section 2 Installation
Table 2-1 Bottle Kits (Continued)
Part Number Description
68-4700-018 Single ProPak Configuration for
68-4700-011 1-bottle Configuration. Includes
68-4700-012 1-bottle Configuration. Includes
If you have selected a multi-bottle kit, first install the distributor arm and discharge tube (Section 2.3.1), then refer to the instructions for your selected bottle configuration:
• 24 Bottle configurations – section 2.3.2
• 4 Bottle configurations – section 2.3.3
• 2 Bottle configurations – section 2.3.4
4700 and 6700 Series FR Refrigerated Sampler. Includes one composite ProPak holder with cap, 100 ProPak bags, two discharge tubes and an instruction sheet.
one polyethylene 20-liter round bottle, two caps and two discharge tubes.
one glass 20-liter round bottle, two PTFE lined caps and two discharge tubes.
If you have selected a single (composite) bottle kit, refer to the instructions in section 2.3.5.
For first-time use of the sampler, or if you have changed the bottle kit, be sure to configure the software for the new bottle kit (section 3.3.2).
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4700 Refrigerated Sampler
2.3.1 Installing the Distributor Arm and
Discharge Tube
The distributor arm ships with the sampler installed on its mounting shaft inside the refrigerator (Figure 2-1). It is generally easier to install the discharge tube with the arm removed, then you can reinstall the distributor arm. To do so:
1. Remove the knurled nut that secures the distributor arm.
Figure 2-1 Installing the distributor arm and
discharge tube
2. Pull the distributor arm downward to remove it from the keyed shaft.
3. Thread the discharge tube through the body of the distributor arm.
4. Insert the end of the discharge tube into the outlet hole on the distributor arm.
2-8
Section 2 Installation
CAUTION
The discharge tube should not extend below the hole in the distributor arm. This could cause the distributor to fail if the excess tubing catches a bottle.
5. Pull on the loose end of the discharge tube
to remove any slack. The tube should follow the contour of the distributor arm.
6. Push the distributor arm up onto the keyed
shaft and secure it with the knurled nut.
7. Push the loose end of the discharge tube
onto the bulkhead fitting in the top-front corner of the refrigerator.
8. Inspect the discharge tube:
CAUTION
An incorrectly installed discharge tube can cause the distributor arm to fail. It can also cross-contaminate samples. To prevent these problems, inspect the discharge tube as described in the following steps.
a. Manually rotate the arm to make sure
that the tube does not obstruct its movement. If the tube obstructs arm movement, re-route the discharge tubing.
b. The discharge tube must slope
downward from the bulkhead fitting to the arm throughout the range of arm motion. Otherwise, liquid might pool in
2-9
4700 Refrigerated Sampler
the tube and cross-contaminate samples. Note that the discharge tube has a natural curve. Should the tube create a low spot where liquid can pool, twist the end of the tube connected to the bulkhead fitting so that the natural curve holds the tube in a downward sloping position. Then, retest the tube at other arm positions.

2.3.2 24 Bottles

The 24 bottle configurations use a rack to hold and align the containers. To install the bottles in the refrigerator using the rack:
1. Place the uncapped bottles in the rack.
2. If you are using 350 ml glass bottles, compress the retaining ring and place it in the center of the bottles. Release the ring and the outward force of the ring will secure the bottles. (The polypropylene and
®
ProPak
bottles do not use a retaining ring.)
Note
Bottles caps can be stored in the center of the bottle rack.
3. Locate the back of the rack (arrow, Figure 2-2). This end has a notch that fits a key on the rear wall of the refrigerator.
4. Lift and insert the back of the rack into the refrigerated compartment.
2-10
Section 2 Installation
Figure 2-2 Insert the keyed end first so that it
faces the back of the refrigerated compartment
Figure 2-3 The 24-bottle rack is held in place
by a latch on the left side
2-11
4700 Refrigerated Sampler
Note
There are four metal guides along the sidewall of the refrigerator, two on each side. The front two guides fit along the left and right sides of the rack. The back two guides run along the top of the rack to prevent the rack from tipping forward.
5. Slide the rack along the guides. Push the rack in until the left-side latch (inset, Figure 2-3) secures the rack.

2.3.3 4 Bottles

The four bottle configuration uses a locating base to hold and align the bottles. To install the base and bottles:
1. Slide the locating base into the bottom of the refrigerated compartment (Figure 2-4). Note that the arrow must be pointing toward the back of the refrigerator.
2. Insert the four uncapped bottles into the numbered holes in the locating base.
Note
Bottle caps can be stored between the bottles.

2.3.4 2 Bottles

The two bottle configuration uses a locating base to hold and align the bottles. To install the base and bottles:
1. Slide the locating base into the bottom of the refrigerated compartment (Figure 2-4). Note that the arrow must be pointing toward the back of the refrigerator.
2-12
Section 2 Installation
Figure 2-4 Installing the locating base
2. Insert the two uncapped bottles into the
holes numbered “1” and “2” in the locating base.
Note
When the sampler controller is configured for two bottles (section 3), samples will only be distributed to bottles 1 and 2. If you place the bottles in positions 3 or 4 the liquid will miss the bottle.
Note
Bottle caps can be stored between the bottles.
2-13
4700 Refrigerated Sampler

2.3.5 1 Bottle

If your one-bottle configuration has a 10 liter (2.5 gallon) polyethylene, glass, or ProPak bottle, use a locating base to hold and align the bottle. If your one-bottle configuration has a 20 liter (5 gallon) glass or polyethylene bottle, simply place the bottle in the center of the refrigerator; no rack or locating base is required.
Refer to the instructions for your bottle size. 10 liter bottle – To install the locating base
and 10 liter bottle:
1. Slide the locating base into the bottom of the refrigerated compartment (Figure 2-4). Note that the arrow must be pointing toward the back of the refrigerator.
2. Insert the bottle into the hole numbered “1” in the locating base.
Note
When the sampler controller is configured for a single 10 liter bottle (section 3), samples will only be distributed to bottle 1. If you place the bottle in any other position liquid will miss the bottle.
20 liter bottle – To install the 20 liter bottle: The distributor arm should be removed to
prevent it from being an obstruction while you replace the bottle. To remove the arm:
1. Remove the knurled nut that secures the distributor arm.
2. Pull the distributor arm downward to remove it from the keyed shaft.
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