Super Systems H2 Sensor User Manual

HYDROGEN (H2) SENSOR
(PART NUMBER 20624)
OPERATIONS MANUAL
Super Systems Inc.
7205 Edington Drive
Cincinnati, OH 45249
513-772-0060 800-666-4330
Fax: 513-772-9466
www.supersystems.com
Hydrogen (H2) Sensor Operations Manual
Super Systems Inc.
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Table of Contents
Introduction ........................................................................................................................................ 3
Features ............................................................................................................................................. 3
Specifications ..................................................................................................................................... 3
Switch Settings, Jumper Settings, and Connector Assignments .................................................... 5
Location of RS-485, DC Input, and Analog Output Terminals ...................................................... 5
Dip Switch Settings ........................................................................................................................ 5
Jumper Positions – Modbus RTU/ASCII ........................................................................................ 6
9-Pin Connector ............................................................................................................................. 7
Analog Output Jumpers ................................................................................................................. 7
Plumbing Connections ................................................................................................................... 8
Analog Output Assignments .......................................................................................................... 8
Calibrating and Configuring the Sensor using the H
Configuration Utility Software ..................... 9
2
Minimum Computer Requirements ............................................................................................... 9
Configuring Communications ........................................................................................................ 9
Overview Screen ............................................................................................................................. 9
Sensor Output Configuration ....................................................................................................... 10
Sensor Output Calibration ........................................................................................................... 10
Sensor Calibration ....................................................................................................................... 11
About ............................................................................................................................................. 12
Modifying Modbus Registers ....................................................................................................... 12
Calibrating the Sensor using Modbus Registers ........................................................................ 13
Performing a Zero Calibration ................................................................................................. 13
Performing a Span Calibration ................................................................................................ 13
Changing the 4-20mA Assignments using Modbus Registers ................................................... 13
Appendix 1: Modbus Register Map .................................................................................................. 14
Warranty ........................................................................................................................................... 16
Revision History ............................................................................................................................... 17
Hydrogen (H2) Sensor Operations Manual
Super Systems Inc.
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Introduction This sensor is designed to accurately measure Hydrogen through thermal conductivity technology. It is capable of providing additional computations based on the Hydrogen measurement, and it has multiple methods of digital and analog communications capabilities.

Features

Measures H
Calculates NH
from 0 to 100% with 0.01% resolution
2
, DA, and KN for nitrider applications
3
Two isolated analog outputs capable of outputting current (4-20 mA or 0-20 mA) as well as
voltage (2-10 VDC, 0-10 VDC, 1-5 VDC, or 0-5 VDC)
One RS-232 port with Modbus RTU or a simple ASCII protocol
One RS-485 port with Modbus RTU protocol
Wide power supply input range (9 to 30VDC)
Small physical size

Specifications

Hydrogen measurement
Range: 0 to 100%
Accuracy: ±0.01%
Repeatability: ±0.01%
Resolution: ±0.01%
Calculated Variables for simple nitrider applications
%NH
0 to 100%
3
%DA (dissociated ammonia) 0 to 100%
nitriding potential
K
N
Analog Outputs
Two isolated analog outputs with common supply; capable of outputting current (4-20 mA or
0-20 mA) as well as voltage (2-10 VDC, 0-10 VDC, 1-5 VDC, or 0-5 VDC)
Output variables: %H
, %NH3, %DA, and KN on either output
2
Adjustable range of PV: zero and span
Resolution: 0.005 mA
Accuracy: ±0.01% of range
Linearity: ±0.01%
Minimum load resistance: 0 Ohms
Maximum load resistance: 500 Ohms
Sample flow rate
1.5 to 2 cfh
RS-232 Serial Communications
Protocols: Modbus RTU or a simple ASCII
Baud rates: 9600, 19200, or 38400
Format: 8 bits No parity, 1 stop bit, No handshaking
Connection: DB-9F
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Super Systems Inc.
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RS-485 Serial Communications:
Protocol: Modbus RTU
Baud rates: 9600, 19200, or 38400.
Format: 8 bits No parity, 1 stop bit, No handshaking
Power requirement
9 to 30 volts DC @ 2 watts
Temperature and Humidity
Electronics Operating: 0 to 50 °C, RH 0 to 90% non-condensing
Sample gas: 0 to 70 °C, RH 0 to 90% non-condensing
Storage: -20 to 70 °C, RH 0 to 90% non-condensing
Dimensions:
See Figure 1.
Weight:
Material:
Figure 1 - H2 Sensor Dimensions
350 g
Stainless steel sensor housing
Hydrogen (H2) Sensor Operations Manual
Super Systems Inc.
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Wiring:
See Figure 2.
Figure 2 - H2 Sensor Wiring

Switch Settings, Jumper Settings, and Connector Assignments

Location of RS-485, DC Input, and Analog Output Terminals

(Items “A” and “B” in Figure 2)
There are two terminal blocks on the H2 cell circuit board. Figure 2 shows their locations.
One block (“A”) contains the analog output terminals. Jumper settings on the circuit board are used to change whether resistance or voltage is generated. These jumper settings can be found in “Analog Output Jumpers” below.
Another block (“B”) contains the digital communications (RS-485) and power (DC) terminals.

Dip Switch Settings

(Item “C” in Figure 2)
The first three dip switches determine the Modbus address. The address can be set for any number between 1 and 8 using a binary numbering system where Bit #1 is the least significant bit and Bit #3 is the most significant bit. The diagram below describes the switch position for each possible address. The shaded area indicates the location of the switch.
Hydrogen (H2) Sensor Operations Manual
Super Systems Inc.
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ADDRESS 1
ADDRESS 2
ADDRESS 3
ADDRESS 4
1 O 1 O 1 O 1 O
2 N 2 N 2 N 2 N 3 3 3 3
4 4 4 4 ADDRESS 5
ADDRESS 6
ADDRESS 7
ADDRESS 8
1 O 1 O 1 O 1 O 2 N 2 N 2 N 2
N
3 3 3 3 4 4 4 4
Protocol
1 O 1 O
2 N 2 N
3 3 4 4
1 2 3
4
1 2 3
4
Figure 3 - Dip Switch Settings (#1, #2, #3)
The last dip switch (#4) indicates the communication protocol. The ‘Off’ position is Modbus RTU mode, and the ‘On’ position emulates the simple ASCII protocol of the previous version of the SSI Hydrogen Sensor. The diagram below describes the switch position for each protocol. The shaded area indicates the location of the switch.
Modbus RTU
Protocol
Previous SSI
Sensor
Figure 4 - Dip Switch Positions (#4)

Jumper Positions – Modbus RTU/ASCII

(Item “D” in Figure 2)
Four jumper terminals can be found on the board approximately 1.5” (3.81cm) to the left of the RS-485 connections (specifically, when looking at the board in the orientation shown in Figure
2). These jumpers determine the pins that transmit and receive data via RS-232 communication. The jumpers should be on Pins 2 and 3 for normal Modbus RTU operation (pin 2 is receiving and pin 3 is transmitting). The jumpers should be on Pins 1 and 4 if the sensor is being used to communicate via the simple ASCII protocol used on the previous version of the SSI Hydrogen Sensor (pin 2 is transmitting and pin 3 is receiving).
Modbus RTU Protocol
Simple ASCII Protocol
Figure 5 - Jumper Positions (Modbus RTU/ASCII)
Hydrogen (H2) Sensor Operations Manual
Super Systems Inc.
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JP2
JP4
JP3
JP5
Note the location of terminals #1 and #2, as well as the
Figure 7 – Analog Output
Terminal Block
#1
C
#2

9-Pin Connector

(Item “E” in Figure 2)
The sensor has a female 9-pin connector used for RS-232 communication. Only three of the nine pins are used, and their assignments are:
Pin #2: Transmit or Receive (Depends on jumper positioning) Pin #3: Transmit or Receive (Depends on jumper positioning) Pin #5: Ground

Analog Output Jumpers

(Item “F” in Figure 2)
Jumpers near the analog output terminal block are used to determine whether a current or a voltage is produced. Figure 6 shows the locations of the four jumpers: JP2, JP3, JP4, and JP5.
V1
0-5V
Figure 6 - Layout of Analog Output Jumpers
0-5V
If all jumpers are OPEN, a 4-20mA signal is produced.
COMMON terminal, in Figure 7. #1 and COMMON, in combination, constitute loop 1, or the “left side” of the block. #2 and COMMON, in combination, constitute loop 2, or the “right side” of the block.
JP2 and JP3 are used for loop 1. JP4 and JP5 are used for loop 2.
V2
O M M O N
The following table shows how the jumpers are used to change settings for the analog outputs.
Hydrogen (H2) Sensor Operations Manual
Super Systems Inc.
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Applies to Loop 1 (#1 and COMMON)
Applies to Loop 2 (#2 and COMMON)
JP2
JP3
Resulting
Output
JP4
JP5
Resulting
Output
Open
Open
4-20mA
(current)
Open
Open
4-20mA
(current)
Closed
Open
2-10 VDC
Closed
Open
2-10 VDC
Open
Closed
4-20mA
(current)
Open
Closed
4-20mA
(current)
Closed
Closed
1-5 VDC
Closed
Closed
1-5 VDC
IMPORTANT: If Modbus register 43 is set to 0,
1-5 VDC becomes 0-5 VDC.
IMPORTANT: If Modbus register 44 is set to 0,
1-5 VDC becomes 0-5 VDC.
the above conditions are true. If Modbus register 43 is set to 1, the following changes take place (depending on jumper settings):
4-20mA becomes 0-20mA
2-10 VDC becomes 0-10 VDC
Table 1 - Analog Output Jumper Settings
the above conditions are true. If Modbus register 44 is set to 1, the following changes take place (depending on jumper settings):
4-20mA becomes 0-20mA
2-10 VDC becomes 0-10 VDC

Plumbing Connections

(Items “G” and “H” in Figure 2)
The sensor is provided with barb fittings (Items “G” and “H”) that are intended for use with 1/8” ID flexible tubing. Flow goes into “G” and out through “H”. The barb fittings can be removed at the user’s discretion, and any fitting with a 1/8” male pipe thread can be used in their place. If the fittings are going to be replaced with different fittings, they must be replaced while the stainless steel sensor block is still attached to the circuit board. Do not remove the sensor block since its alignment with the sensors is a critical function that should only be performed by a trained technician.
Analog Output Assignments There are two analog outputs on the sensor. The default settings result in Output 1 being set for Percent H2 (0-100%) and Output 2 being set for Percent Dissociation (0-100%). Both of these outputs can be configured for any of the following parameters:
Percent Hydrogen (H
)
2
Percent Dissociation (DA) Percent Ammonia (NH Nitriding Potential (K
)
3
)
N
External
In “External” output mode, no calculation is performed, and the output is set to match a specific value. Modifications to the Analog Output Assignments can be performed with the SSI H
Cell
2
Configuration Utility Software, which is described in the next section of this manual.
Hydrogen (H2) Sensor Operations Manual
Super Systems Inc.
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Calibrating and Configuring the Sensor using the H2 Configuration Utility Software

The simplest way to set up the analog outputs, calibrate the analog outputs, and calibrate the Hydrogen sensor is to use the SSi H
Configuration Utility software. This software provides a
2
simple to use graphical interface for performing the setup and calibration functions. It communicates via Modbus (either RS-232 or RS-485). This is set by moving dip switch #4 to the off position. To communicate via RS-232, use the 9-pin connector with the jumpers in positions 2 and 3. To communicate via RS-485, use the RT+ and RT- terminals on the 8 pin terminal strip.

Minimum Computer Requirements

Microsoft Windows XP/Vista/7
500 MHz CPU
128MB RAM
2MB hard disk storage space
1 RS-232 or RS-485 Serial Port
Configuring Communications Open the H2 Configurator and click Options  Settings to open the dialog that allows you to set the serial port, baud rate and target address of the H2 cell. (See
Figure 8.)
Figure 8 - Settings window
When using the RS-232 port, the baud rate should be set to 9600 and the address should be set to 250. 250 is an SSi broadcast address and any H
cell that sees the message will answer, so
2
while the 250 address should be used for RS-232 it should not be used for RS-485 if there are multiple SSi instruments on the same serial port. The Port setting may need to be adjusted to match the port on your PC that is connected to the H
cell. RS-232 communications use a
2
simple straight through cable to the DB9 connector.
Overview Screen The Overview screen (Figure 9) displays the current % H2 and the three buttons used to configure or calibrate the H2 cell.
Hydrogen (H2) Sensor Operations Manual
Super Systems Inc.
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Figure 9 - Overview screen
Sensor Output Configuration The Configuration screen (Figure 10) allows basic configuration of the H2 cell.
Figure 10 - Configuration screen
The Instrument Mode is the primary PV (Process Variable) setup. This is mainly used by the touch screen and normally does not need to be changed as the % H
is always available. The
2
output sources are the PVs that will be retransmitted via the selected output. The Output Zero is the PV value that will result in a 4 mA output and the output span value is the PV value that will result in a 20 mA output.
Sensor Output Calibration Output calibration calibrates the outputs. Each output can be zeroed and spanned. To perform this calibration a reliable measurement device capable of accurately measuring a 4-20mA signal will be required. An example screen is shown in Figure 11; a screen showing the success of an output calibration can be seen in Figure 12.
Hydrogen (H2) Sensor Operations Manual
Super Systems Inc.
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Figure 11 - Output Calibration screen
Figure 12 - Successful Output Calibration
The steps to performing an output cal are as follows:
Select an output and whether you are going to do a zero or a span.
Click Prep for Cal. The H
Measure the output current at the H
cell will set the output appropriately for measurement.
2
cell’s terminals and input that value into the box next
2
to ‘Measured Output mA’. For example, if you are performing a zero calibration and your measurement device is indicating 4.03mA, you would enter the value of 4.03 in the “Measured Output mA” box.
Click the Calibrate button to perform the calibration.
When the calibration is complete, the measurement device should display the target value.
For a zero calibration that would be 4.00mA, and for a span calibration that would be 20mA.

Sensor Calibration

The sensor can be zeroed or spanned via Sensor Calibration (Figure 13). The gas should flow at a rate of 1.5 SCFH and the detected H
value needs to be steady before a calibration is
2
performed. To perform a Zero cal select Zero in the drop down box next to Calibrate. Enter the % H
of the supplied gas (for zero this will be 0.00%). Wait for the readings to come to
2
equilibrium and click Calibrate. To perform a Span cal select Span in the drop down list and repeat the process.
Hydrogen (H2) Sensor Operations Manual
Super Systems Inc.
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Figure 13 - Sensor Calibration screen
About The About screen (Figure 14) is access from the overview screen by clicking Help…About. The About screen provides release information about the H the firmware in the SSi H
cell.
2
Configuration utility and the revision of
2
Modifying Modbus Registers The setup parameters of the H2 sensor can also be modified by adjusting the Modbus registers. A list of all Modbus registers can be found in “Appendix 1: Modbus Register Map”. To make modifications, you must connect the sensor to a computer that uses SSI’s “Configurator” software. When communicating with Configurator, use a straight-through serial extension cable connecting the computer to the sensor. Set the baud rate in Configurator to 9600. On the sensor, set DIP Switch #4 to Off for Modbus communication, and be sure that the jumpers are on pins 2 and 3.
Figure 14 - "About" Screen
Hydrogen (H2) Sensor Operations Manual
Super Systems Inc.
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Calibrating the Sensor using Modbus Registers

Performing a Zero Calibration

1. Begin the flow of Zero gas (Nitrogen or Argon) at a rate of 1.5 SCFH.
2. Allow the readings from the sensor to stabilize.
3. Set Register #13 to 0 (equal to 0% H
).
2
4. Set Register 12 to 1.

Performing a Span Calibration

1. Begin the flow of Span gas (with a known %H
2. Allow the readings from the sensor to stabilize.
3. Set Register #13 to the H
value in the span gas. Multiply the gas value by 100 before
2
entering the number (i.e. if the gas has 40.13%H enter a 997 into Register 13).
4. Set Register 12 to 2.
Changing the 4-20mA Assignments using Modbus Registers Register 19 denotes the assignment for 4-20mA #1, and register 23 denotes the assignment of 4-20mA #2. The default value for #1 is %H
2
number into either register according to the following list:
0 = %H
2
1 = %DA
2 = %NH
3
3 = %Kn
4 = External Source
) at a rate of 1.5 SCFH.
2
, enter a 4013 or if the gas has 9.97% H2
2
, and #2 is #DA. To change the assignment, enter a
Hydrogen (H2) Sensor Operations Manual
Super Systems Inc.
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Register Functions and Default Values
#
Function
Default
0
Current firmware revision level
Varies
1
RS-232 communication mode (0=Modbus slave, 1=ASCII /Previous SSI Sensor)
DIP Sw.
2
RS-232 baud rate (0=9600, 1=19200, 2=38400)
0
3
RS-485 communication mode (0=Modbus slave, 1=Modbus master [NOT USED])
0
4
RS-485 baud rate (0=9600, 1=19200, 2=38400)
1
5
Temperature trim for thermistor 1 / ambient temperature
200
6
A/d counts for thermistor 1
Varies
7
Thermistor 1 temperature
Varies
8
%H2 A/D counts – High (Right justified: 0x00 byte, high byte, mid byte, low byte)
Varies
9
%H2 A/D counts – Low (Right justified: 0x00 byte, high byte, mid byte, low byte)
Varies
10
%H2 measured voltage
Varies
11
%H2 as found from a polynomial
Varies
12
%H2 sensor calibration (0=none, 1=zero cal, 2=span cal)
0
13
%H2 gas composition (value/100 = %H2/N2 balance)
0
14
Sensor Modbus address (important for slave communications only)
DIP Sw.
15
Model Number
4100
16
Set Factory Defaults (23205=Full, 23206=%H2, 23207=Loop 1, 23208 = Loop 2)
0
17
4-20mA #1 DAC output counts
Varies
18
4-20mA #2 DAC output counts
Varies
19
4-20mA #1 Source (0=%H2, 1=%DA, 2=%NH3, 3=Kn, 4= External)
0
20
4-20mA #1 Zero value
Varies
21
4-20mA #1 Span Value
10000
22
4-20mA #1 External current loop (Used only if register 19 = 4)
0
23
4-20mA #2 Source (0=%H2, 1=%DA, 2=%NH3, 3=Kn, 4= External)
1
24
4-20mA #2 Zero value
0
25
4-20mA #2 Span Value
1000
26
4-20mA #2 External current loop (Used only if register 23 = 4)
0
27
Enable Calibration of 4-20ma output (0=disable, 1=enable)
0
28
Calibrate 4-20mA output (1=#1 zero, 2=#1 span, 3=#2 zero, 4=#2 span)
0
29
4-20mA calibration value (4000 to 20000 for 4-20mA)
0
30
Calibration result codes (9-12=successes, 13-16=failures, 20=no cal specified)
0
31
Percent DA value
Varies
32
Percent NH3 value
Varies
33
Super Kn value
Varies
34
%N2 flow
0
35
%NH3 flow
0
36
%DA flow
0

Appendix 1: Modbus Register Map

Hydrogen (H2) Sensor Operations Manual
Super Systems Inc.
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Register Functions and Default Values
#
Function
Default
37
Process variable mode (0=H2, 1=DA, 2=NH3, 3=KN)
0
38
Process variable value
Varies
39
%H2 mantissa
Varies
40
%H2 exponent
Varies
41
Force theoretical current loop values
0
42
Minimum H2 value
0
Hydrogen (H2) Sensor Operations Manual
Super Systems Inc.
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Warranty

Limited Warranty for Super Systems Products:
The Limited Warranty applies to new Super Systems Inc. (SSI) products purchased direct from SSI or from an authorized SSI dealer by the original purchaser for normal use. SSI warrants that a covered product is free from defects in materials and workmanship, with the exceptions stated below.
The limited warranty does not cover damage resulting from commercial use, misuse, accident, modification or alteration to hardware or software, tampering, unsuitable physical or operating environment beyond product specifications, improper maintenance, or failure caused by a product for which SSI is not responsible. There is no warranty of uninterrupted or error-free operation. There is no warranty for loss of data—you must regularly back up the data stored on your product to a separate storage product. There is no warranty for product with removed or altered identification labels. SSI DOES NOT PROVIDE ANY OTHER WARRANTIES OF ANY KIND, INCLUDING, BUT NOT LIMITED TO, THE IMPLIED WARRANTIES OR CONDITIONS OF MERCHANTABILITY AND FITNESS FOR A PARTICULAR PURPOSE. SOME JURISDICTIONS DO NOT ALLOW THE LIMITATION OF IMPLIED WARRANTIES, SO THIS LIMITATION MAY NOT APPLY TO YOU. SSI is not responsible for returning to you product which is not covered by this limited warranty.
If you are having trouble with a product, before seeking limited warranty service, first follow the troubleshooting procedures that SSI or your authorized SSI dealer provides.
SSI will replace the PRODUCT with a functionally equivalent replacement product, transportation prepaid after PRODUCT has been returned to SSI for testing and evaluation. SSI may replace your product with a product that was previously used, repaired and tested to meet SSI specifications. You receive title to the replaced product at delivery to carrier at SSI shipping point. You are responsible for importation of the replaced product, if applicable. SSI will not return the original product to you; therefore, you are responsible for moving data to another media before returning to SSI, if applicable. Data Recovery is not covered under this warranty and is not part of the warranty returns process. SSI warrants that the replaced products are covered for the remainder of the original product warranty or 90 days, whichever is greater.
Super Systems Inc.
Page 17 of 17
Rev.
Description
Date
MCO #
A
Previous Release
B
Changes made to reflect changes in board
setting analog outputs to volts.
11/1/2013
2132

Revision History

Hydrogen (H2) Sensor Operations Manual
design. Changed pinout. Added content for
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