Shimadzu TOC-V CPH, TOC-V CPN User Manual
SHIMADZU
TOC-V Series
TOTAL ORGANIC CARBON
ANALYSER
Short-User Manual
TOC-V CPH/CPN
TOC-Control V
Version 2.00
Table of Content
I. TOC-Control V Main Menu
1. Measurement
1.1 Sample Table Editor
1.2 H/W Settings
1.3 Online Manual
2. Administration
2.1 System Administrator
2.2 Audit Trail
2.3 User Authentication
2.4 Others
II. Sample Table Editor
1. Create a calibration curve
2. Create a method
3. Create a sample run
4. Schedule File
4.1 Create a new schedule file
4.2 Export the sample table as schedule file
4.3 Insert a schedule
5. Vial Number
III. Analysis
1. Connect the system
2. Start the analysis
3. Sample Window
4. Edit Mode
5. Stop the analysis
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I. Main Menu
Parameter
Action/Description
Start TOC-Control V
Main Menu
STARTPROGRAMSTOC-Control V TOC-Control V or
double-click on the TOC-Control V icon (Desktop)
1 Measurement
1.1 Sample Table Editor
- to create and edit methods, calibration curves and sample measurement sequences.
Parameter
Action / Description
Start
Click on the “Sample Table Editor” button
User Name / Password
Enter exact user name and password
Sample Table Editor
Sample Table Editor opens to start the TOC instrument
1.2 H/W Settings
- to configure a new system
- to view or modify the instrument settings
Parameter
Action / Description
Start
Click on the “H/W Settings” button
User Name / Password
Enter exact user name and password
H/W Settings
H/W Settings opens
1.2.1 New System
- to configure a new instrument.
Parameter
Action / Description
Start
Click on the “Create a New Setting” button
Instrument Setup Wizard-1 : Basic System Information
Parameter
Action / Description
System
Enter a unique name (max. 32 characters)
Instrument serial
number
Enter the serial number of the TOC-instrument (mentioned on the
instrument label)
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User
Name of current user is automatically entered, if entered it cannot
be edited
Date of Creation
Current date is automatically entered and cannot be edited
Comment
Enter additional system information (optional)
Instrument Setup Wizard-2 : Instrument Options
Parameter
Action / Description
Oxidation
Select “Combustion”
Options
Select the installed instrument components (TOC, ASI, SSM,
Sparge Kit and 8-port Sampler)
[The selected options determine which Instrument Setup Wizard
screens will subsequently be displayed.]
Instrument Setup Wizard-3 : Instrument Parameters
Parameter
Action / Description
Catalyst type
Select the catalyst type (Regular, High Sense or TC/TN)
Tubing Diameter
Regular
Suspended Particle
Select the diameter size of the sample injection tubing.
0.5 mm diameter
0.8 mm diameter
Cell length
Select the cell of the NDIR detection
(Long as default, short for SSM measurements)
TC Furnace
This item sets the TC furnace temperature
Buzzer
If this item is selected, a buzzer will sound with the press of each
instrument key
Auto regeneration of
IC solution
If this item is selected, IC reagent will automatically be generated in
special situations (Please refer to the User Manual)
Enable ready status
check
Select this option to enable the Ready Status Check function
[recommended, thus software always verifies Ready Status of
instrument prior to starting measurement]
TN Power
If this item is selected, the power to the optional TNM-1 is turned
on.
Instrument Setup Wizard-4 : ASI parameters
Parameter
Action / Description
Tray Type
Select ASI tray type (24 ml, 40 ml or 125 ml vial)
Needle Type
Select the needle type. (only active if Sparge Kit was selected)
No of Needle Washes
Select the number of times (0-10) the outside of the needle to be
washed with dilution water, after each sample analysis
No of Flow Line
Washes
Select the number of times (0-10) the flow lines to be washed with
dilution water from the needle to the injection tube, at the
completion of the sample sequence
Rinse
Select this option to rinse the sampling needle with dilution water
between each sample.
Rinse after acid
addition
Select this option to rinse the sampling needle after each acid
addition.
Stirrer on
Select this option to use the magnetic stirrer. (if installed)
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Instrument Setup Wizard-5 : SSM parameters
Parameter
Action / Description
SSM TC Furnace ON
Select this option to heat the TC furnace of SSM
SSM IC Furnace ON
Select this option to heat the IC furnace of SSM
Instrument Setup Wizard-6 : Communication parameters
Parameter
Action / Description
Com Port
Select the communication port
Stop Bits and Parity
Cannot be edited by the user .
[determined by the hardware, automatically set based on Com Port]
[Finish] Button
The system configuration is created and the newly created system
configuration is displayed as an icon in the H/W Setting List
window.
1.2.2 H/W Setting List
- to view or modify instrument parameters of already defined systems
Parameter
Action / Description
Open
Select the “Instrument/System” icon and press “Open” to open the
instrument properties
Delete
Select the “Instrument/System” icon and press “Delete” to delete the
instrument system
Close
Press “Close” to close the H/W Setting List window.
1.3. Online Manual
- to open the user manual as PDF format
2 Administration
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2.1 System Administration
2.1.1 System Policy
- to check the security functions, activation of them is done during the installation
2.1.2 S/W Validation
- to verify that the TOC-Control V program files have not been modified since
installation
2.2 Audit Trail
2.2.1 Log Browser
- to open the audit trail database (please refer to the Administration Manual)
2.2.2 Add a Log Event
- to add an event to the Log Browser
2.3 User Authentication
2.3.1 User Account
- to create new user
- to edit user information of already registered users
- to deactivate accounts.
Parameter
Action/Description
Start
Click on User Accounts
User Name/Password
Enter exact user name and password
[first time: “Admin”, no password]
New User
Select UserNew
Change existing user
accounts
Select UserEdit
Parameter
Action/Description
User ID
(required item)
Enter a user name (maximum 32 characters). Spaces are the only
characters that cannot be used.
User Name
(required item)
Enter additional information about the account
(this field is optional max.128 characters)
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Password
(required item)
Enter the password for the new account. The limits for password
length and complexity can be changed. Please refer to the
Administration Menu
Confirm Password
(required item)
Enter the password again.
Company, Department,
Position, Tel, email
Enter additional information of user if required
User Level
Administrator
Main User
User
Guest
Detailed Access Rights
Select a radio button to establish the user level
[Each user level has a set of access rights that are selected by
default. Adaptation is possible, see detailed access rights.]
Add or remove access rights for main user, user and guests
Detailed Access Rights
Lists the functions that a user can access. Each of the four user
levels has a default list of access rights, displayed in this field.
The administrator can use this list to add or remove access rights for
main user, user and guests. Please refer to the Administration Menu
[OK]
Click on the OK button to create a new account
2.3.2 Change Password
- to change the password of user ID
2.4 Others
2.4.1 LIMS Settings
- The LIMS-related settings are used to establish a relationship between external
applications and TOC-Control V software. These applications run in the background
before an d after measurement
- Please refer to the Administration Manual
2.4.2 Database Manager
- The Database Manager enables export of the database file in .mdb format (Microsoft
Access)
- Please refer to the Administration Manual
2.4.3. Data Profile Viewer
- The data profile can be exported from TOC-Control V software and displayed. Each
row of the TOC-Control V sample table is output as an individual data profile
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