Shimadzu RID-10A User Manual
228-30179
DIFFERENTIAL REFRACTIVE DETECTOR
RID-1
OA
FOR
SHIMADZU
HIGH
-
PERFORMANCE
LIQUID
CHROMATOGRAPH
USER’S
MANUAL
Read the instruction manual thoroughly before you use the product. Keep
this
instruction
manual
with care
so
that you can use it any time you need it.
SHIMADZU
CORPORATION
CHROMATOGRAPHIC & SPECTROPHOTOMETRIC
INSTRUMENTS DIVISION
KYOTO,
3APAN
Copyright 0 Shimadzu Corporation
1995.
.
All rights are reserved, including those to reproduce
this
publication or
parts
thereof in any
form without permission in writing from Shimadzu Corporation.
Information in this publication is subject to change without notice and does not represent
a
commitment on the part of the vendor.
Any errors or omissions which may have occurred in this publication despite the utmost care
taken in its production will be corrected
as
soon
as
possible, but not necessarily immediately
upon detection.
Note that Shimadzu does not have any obligation concerning the effects resulting from the
application of the contents of this manual.
MS, MS
-
DOS, Microsoft and Visual Basic are registerd trademarks, and Windows is
a
trademark of Microsoft Corporation
in
the USA.
IBM is a registerd trademark
of
International Business Machines Corporation in the USA.
TrueType
is
a
registerd trademark of Apple Computer, Inc in the USA.
The
RID-1
OA
is the differential refractive index detector for the high-performance liquid
chromatograph.
In
order to operate the unit safely, strictly observe the following points.
1.
Do
not
use
the unit for any purpose other than the above mentioned analysis.
2.
Follow the procedures described in the instruction manual.
3.
Observe the warnings and cautions.
4.
Do
not disassemble
or
modify the unit without approval
from
Shimadzu. Failing to do
so
may lead to a dangerous situation or damage of the unit.
5.
For internal repair of the product, contact your Shimadzu Service Representative.
6.
The pink-color pages and the meshed parts are for our service engineers, and are not
intended for our clients.
Do
not attempt installation of the instruments
as
serious damage
could result.
WARNING IN
THE
INSTRUCTION MANUAL
This instruction stipulates the content of warnings as follows:
-1
Applied in a case that could result in death or serious injury.
-1
Applied in a case that could result in slight injury or physical
damage.
-1
Applied for improvement of operating efficiency or help in
understanding.
I
For safety
of
operation, this unit is provided with
the
A
mark
at the portion where special
When operating the
parts
where
this
mark
is
indicated, exercise
special
caution
after
reading
cautions are required.
the
manual.
Replacement
of
fuses
This
unit uses the
following
fuse. Be sure to replace the fuse
of
same
type
and
capacity.
Rated voltage
:
100-24OV
Part
NO.
072-01652-23 250V 5AT
I
CAUTION
I
Do
not bend the optical cable for remote control with the radius
of
35mm
or less.
Bending it with the radius smaller than 35mm may damage the cable,
whith may cause
malfunction
of
the
unit.
m
VAOS
I
AOX-022
VAOSI
A02
I
96-000ZE-822
26-0002€-822
VAOS
I
hpedea
A001
16-000Zf-822
a3NlOS
JaMOd
'ON
lred
8.
Solvent
not
usable
HFIPA
(Hexafluoroisopropyl alcohol) affects the materials used in the flow path and
deteriorate the strength of the material. In the worst case, pipe may explode and high
-
pressure solvent scatters.
As
it is very dangerous, never
use
HFIPA.
9.
Others
The equipment should not be exposed to direct sunlight or strong air currents.
It
is
also
recommended to install in a room where temperature fluctuation
is
small.
N
Liquid chromatography using flammable organic solvents as mobile phase requires proper care
against
fire,
explosion, etc. Pakcularly, among various possible accidents, those caused by static
electricity are difficult to anticipate, and tend to occur only with unexpected conditions which
often make countermeasures insufficient.
At a site where preparative liquid chromatography is practiced, a large amount of flammable
substances may be used. Therefore, once an accident happens, it could lead to tremendous
damage.
The mechanism of accident caused by static electrical discharge and preventive measures are
described below. Take due care in safety measures in handling of equipment.
1.
Mechanism
of
Static Electrical Discharge Accident (Example)
Accidents caused by static electricity take place through the following processes.
When liquid is fed at high speed through a small
-
diameter
tube like the pipe of a liquid chromatograph, static electrical
charge occurs by friction between solid and liquid
as
shown in
Fig.
1.
Occurrence
of
Static
Electricity
1
$
-
Flowing liquid
A
Solid
body
A
:
Electric charge
moving with
flowing liquid
B
:
Electric charge
being fixed
to
the
solid surface.
Fig. 1 Occurrence
of
Static Electricity by Friction between Solid and Liquid
Charging and storage
of
static electricity
t
1
Energy release by
1
I
discharge
I
3.
Ignition
of
combustible
substances
f
When the charged liquid is collected in an insulated vessel,
the static charge accumulates gradually, and the voltage can
easily reach
a
few kilovolts.
If
some other conductive object
is
brought near the vessel,
electricity is discharged at a certain distance from the vessel
releasing heat energy.
If flammable gas of sufficient concentration exists nearby,
ignition is caused by this energy.
If
air drv
\
Liquid is flowing at high
speed
through a
small
diameter tube.
*Charge is easily accumulated if
bubbles are included in the liquid.
Insulated vessel
(like polyethylene)
Spark discharge
-
””;”oyc
I
Ill
/
Inflammable gas is stored in the
head space
of
the vessel.
(\
n\
Inflammable organic solvent is
charged
to
a great extent.
e
- - -
-
Floor covered
with
rubber, etc.,
provides unwanted insulation.
Fig. 2 Conditions which may cause Accidents
2.
Preventive Measures against Accidents
The principal preventive measure is the prevention of “charging and storage of static
electricity” among those items shown in “Mechanism
of
Static Electrical Discharge
Accident.” The preventive measures are shown below. It is recommended to exercise two
or more measures simultaneously.
3K
Particularly when a large quantity of flammable solvent is held in a large vessel,
be
sure
to observe the preventive measures
1,2,
and
3.
Preventive measure
1.
Use metallic (conductive) waste liquid vessel which is well grounded.
This
releases the
charge of the waste liquid and vessel to ground.
The following items are available.
(1)
Grounding
wire
with clip P/N
228-21353-91
(2)
Metallic
18
liter can
P/N
038-00044
(3)
Metallic 4 liter can
P/N
038-00043-01
3K
+E
Be sure to ground the vessel properly. Disconnecting of grounding wire or poor
grounding defeat the purpose of using
a
metallic vessel.
There are some metallic cans which have no conductivity
due
to
an
oxidized coating
or lacquer on their surface. Be
sure
to
confirm
the grounding
of
vessels by a tester
before application.
When a liquid with almost no conductivity (of
10-lOs/m or less) is discharged into the
vessel, it is necessary to
mix
it with another liquid with some conductivity. (The other
liquid can be placed in the vessel
in
advance.)
%
Preventive measure
2.
Minimize the clearance
of
both inlet and outlet
of
vessel to prevent flame from entering the
vessel.
(1)
Cap with three holes for
18
liter and 4 liter cans
(P/N
228-21
354-91)
is available.
Connect clip to metallic
Minimize clearance
by
attaching a cap.
ground the metallic vessel.
Metallic
18
litter can
(A
plated can is recommended.)
Static electricity
of
the liquid
is released via vessel.
Fig. 3 Anti-Static Electricity Measures for Vessel
Preventive measure
3.
Do
not approach the vessel with charged objects including the human body.
Charging prevention measures for human body
a)
b) Grounding
of
human body
c) Make
working floor conductive
Prevention of charging of shoes and clothes
Suitable products to be used for those measures a), b), and c) are available on the
market.
When persons who use no charge prevention measures approach dangerous sections,
they have to be grounded beforehand. (For example, they should contact grounded
metal by hand.)
%
Preventive measure
4.
Use pipes with inner diameter of
2mm
or more for waste liquid line for large flow rates.
3%
Inclusion
of
bubbles in the
tube
may increase the amount of charging by ten times.
Check that there is no inclusion
of
air
via
tube
joints.
Preventive measure
5.
When it is impossible to use a conductive vessel, use caution in the following points.
a)
Set the vessel
so
that the pipe outlet will be placed below the liquid
level
in the
vessel. Or, dip a grounded metal (ex. pipe connected
to
the main body of device) in
the liquid.
This
method is not effective
for
liquid with small conductivity (10-I0s/m
or
less).
Use
a
vessel
of
the
smallest possible capacity to minimize the damage by
fire
if it
should occur.
Prevent the
room
from
being
dry.
Humidity of
65% or
more has charge prevention
effects.
+E
b)
c)
a
1ChapterlI
General
1.1
Outline
..........................................................................................................
1-2
1.2
Features
........................................................................................................
1-3
1.3 Principle
of
Measurement
.............................................................................
1-4
1.4
Row Schematic
............................................................................................
1-6
1
Chapter2 1 Parts List
2.1 Parts and Accessories
...................................................................................
2-2
-1
Component Location and Function
3.1 Front View
....................................................................................................
3-2
3.2 Interior
of
Front Cover. Right Side
..............................................................
3-3
3.3 Rear View
.....................................................................................................
3-4
I
Chapter4 1 Installation
4.1 Basic Installation Requirements
...................................................................
4-2
4.2 Example
of
System Layout
..........................................................................
4-3
4.3
Stacking Modules
.........................................................................................
4-4
4.4 Electrical Connections
..................................................................................
4-5
4.6 Connecting the Recorder and Integrator
.......................................................
4-11
4.7
4.5 Plumbing Connections
..........................................
:
......................................
4-6
Connecting the Drain Tube
for
Solvent Leakage
...........................................
4-13
1-1
Operation
5.1
Precautions
for
Operation
.............................................................................
5-2
5.2 Fundamentals
of
Operation
..........................................................................
5-3
5.3 Plumbing
of
the Flow Selection Block
.........................................................
5-13
5.4
5.5
Creating and Executing
Tie
Programs
.......................................................
5-16
Additional Functions (AUX
-
FUNC)
............................................................
5-21
1
ChaDter
6
I
Initial Performance Test
6.1
System Performance Check
............................................................................
6-2
-1
Control from External Equipment
7.1 Connection with System Controller SCL-1 OA
.............................................
7-2
7.2 Control
form
the SCL-IOA
...........................................................................
7-3
7.3
Connecting External Input and Output Terminals
........................................
7-10
I
Chapter
8 1 Maintenance
8.1
Cleaning the Flow Lines
...............................................................................
8-2
8.2 Span Adjustment
..........................................................................................
8-3
8.3 Replacement
of
Fuse
....................................................................................
8-7
8.4 Periodical Cleaning
......................................................................................
8-8
1-1
Performance Verification
9.1 Component Validation
..................................................................................
9-2
9.1
.
1
Test Procedures
of
Stand-alone Unit
......................................................
9-3
9.1.2
Test Procedures Controlled
from
the
SCL
-
1
OA
......................................
9-5
9.2 System Validation
.........................................................................................
9-9
9.2.1 Test Procedure
of
Isocratic LC System
..................................................
9-9
1-1
Troubleshooting
10.1
10.2
Symptoms. Causes and Remedies
................................................................
10-2
List
of
Error
Messages
..................................................................................
10-4
-1
Specifications
...............................................................................
1 1 . 1
RID-1
OA
Specifications 11-2
[-I
Replacement Parts
12.1
Consumables
and
Repair
Parts
.....................................................................
12-2
12.2 Optional
Parts
...............................................................................................
12-4
rChapterl31
Reference
13.1 Solvent Characteristics
.................................................................................
13-2
.
Chapter
1
General
1.1
Outline
.....................................................................................................
1-2
1.2
Features
...................................................................................................
1-3
1.3
Principle
of
Measurement
.......................................................................
1-4
1.4
Flow
Schematic
.......................................................................................
1-6
1-1
RID-1OA
-
RID-1OA
is
the
differential refractive index detector for the high
performance liquid
chromatogaph developed as a module
of
the
LC
-
1
OA
series.
The
RID-10A
improves analysis productivity and convenience
of
use like a
UV
detector. Its shortened stabilization time, the fact that
it covers various applications from high sensitivity analysis to
sampling analysis preparation
and
more,
RID-1OA
is much
improved in convenience than conventional models.
Only handling instructions for
RID
- 1 OA
and related accessories
are
described
in
this
instruction manual.
For
handling instructions of
other components, please refer to the pertinent instruction manual.
1-2
-
RID-1OA
1.
Excellent
stability
Stabilization time after turning on the power has been shortened to
reduce the waiting time for
start
of
analysis. Excellent stability has
been realized by employing the dual temperature control structure
of
the optical system and by improving the thermal design.
-
0
r
t
By adapting the original four-partitioned photodiode,
this
equipment
now covers the wide dynamic range of various applications from
high
sensitive analysis to large scale preparation of high concentration
samples.
2.
Various
applications
3.
Safety measure
4.
Corresponding to the
LC-1OA
series
The standard model is equipped with a leak sensor which enables
automatic performance
of
operations such
as
stopping the pump in
the early stage of organic solvent leakage.
This
equipment is designed for the
LC
-
1
OA
series to have excellent
operability
as
a
component of the total system, including control
from the
SCL-1OA
and
data
processing in the
CLASS
workstation,
etc.
1-3
RID-1OA
-
The optical system of this unit is shown in following illustration.
The light radiated from the lamp passes through the lens slit and
through the cell in the form of parallel rays, which is then reflected
by
the
mirror and passed through the cell
to
form an image of the
slit
on
the photodiode.
The
flow
cell consists of the sample side and the reference side.
When
the refractive index
in
the sample side cell varies,
the
image
of the slit moves horizontally.
W
lamp
#
When refractive index
I
When refractive index
,
in the
flow
cell
vanes,
Samole
/
<\-&
~&zf
the
slit
moves.
Dhotodiode
This
unit has a photodiode partitioned in four
as
shown in the figure
below. When selecting a piece of photodiode to use among these
four, the unit is able to provide measurements for both analytical
and preparative work.
In
modes
P
and
L
In
mode
A
1
A
signal is processed
divided into up and down.
regarding
it
as
two
regarding
it
as
two
elements
A
signal is processed
divided into right and left.
Signal processing
in
mode
A
A
signal
is
processed using the right and left portions of the
photodiode
as
individual elements. Data processing is performed as
a two
-
partitioned photodiode divided into right and left.
When the refractive index in the
cell
varies,
the
balance of the incident
light intensity into right and left
parts
of
the photodiode changes. The
change
in
the right/left balance
is
converted into refractive index and
then can
be
recorded.
1-4
-
RID-1OA
1.3
Principle
of
Measurement
A-B
RIx
TOTAL
Signal processing in mode
P
-
E
a,
Signal processing is performed using the upper and lower parts of
L
Q
the photodiode
as
individual elements. Since the boundary between
the upper and lower parts
is
slanted against a horizontal line, when
an
image of the slit moves horizontally, the balance of the light
intensity
in
the upper/lower parts
of
the diode changes.
This
change
in balance is converted into refractive index. The change
of
the bal
-
ance against the variation
of
the
refractive index is one-twentieth
that
of
mode
A.
In
mode
A,
when the slit image goes beyond the
center line, measurement becomes impossible because the balance
value stops varying, while in mode
P,
measurement is possible
under
these
conditions enabling measurement of a sample with high
concentration.
A-B
TQTU
Signal processing in mode L (An optional
flow
selection
block
is necessary)
Signal processing is performed
as
the same
as
in mode
P,
using
each
of
the upper and lower parts of the diode
as
individual ele
-
ments. However, since the reference side with less flow line resis
-
tance is used
as
the sample cell, the image moves in the reverse
direction
of
that
of
mode
P.
Thus polarity is turned over
before
the
change in balance
is
converted into a refi-active index.
B-A
TOTAL
w.
A
1-5
RID-1OA
-
The diagram shows flow lines
in
the RID-10A.
At R flow
OFF
When the R flow switch is
OFT,
the solenoid valve is open at side
A.
The solvent passing through the sample cell flows into the outlet
port, not into the reference cell.
At
R
flow
ON
When the R flow switch
is
ON,
the solenoid valve is open at side
B.
The solvent passing through the sample cell flows into the outlet
port after passing through the reference cell. This
is
used to fill the
sample cell and the reference cell with solvent of equal refractive
index before starting the measurement.
R
flow
ON
Q
!
Outlet
port
Inlet
port
Tubing
volume (At R flow
OFF)
Inlet port to flow cell
63.5
pL
Flow cell volume
9pL
Flow cell to cell outlet port
280.2
pL
S:
Sample
R:
Reference
1-6
-
RID-1OA
Chapter
2
Parts List
c
v)
3
2.1
Parts
and
Accessories
..............................................................................
2-2
1
CONTENTS
1
2
-
1
RID-1OA
-
1
[Caution]
Part
Name
Signal cable
When connecting the flow line and performing maintenance, be
sure
to use the
parts
described on this page or
“1
2.1,
Consumable
and Repair
Parts
”.
Normal
function
of
the system
is
not
,guaranteed
when
other
parts
are
used.
Parts
No.
Quantity
228-25089-92
1
This equipment consists of the following components. Upon
unpacking,
confirm that all
parts
listed below
are
included
in
your
shipment.
0
RID-IOA
Main Body
Power supply cord
(
120V)
(220-240V)
Optical cable
0
Standard Accessories
071-608 14-
01
1
07 1-608 14-06
070
-
92025-5
1
1
sus
tubing
Teflon tubing
228-22310-00 lm
228-22305-00
50
crn
228- 18495-03 2m
Remote
cable
I
228-28253-91
I
1
Locking plate
Instruction
manual
SC
Coil
ASSY
(220-24OV)
Syringe
Syringe adapter
228-15672-91
Coupling 1.6C
228-16004-03
Male nut PEEK
228- 18565
228
-
1875
1
1
228-301 78
1
228-34050-9
1
1
Drain tubino
kit
I
228-18495-03
I
1
I
2-2
-
RID-1OA
-
Chapter
3
Component Location
and Function
3.1
Front
View
...............................................................................................
3-2
3.2
Interior
of
Front Cover,
Right
Side
.........................................................
3-3
3.3
Rear View
................................................................................................
3-4
c
0
(D
0
0
-
c
3-1
RID-1OA
-
w
S
Q,
c
0
E
s
0
I
RID-1OA
I
Front cover
The front cover is opened for mounting
and
dismounting of
flow
cell
and
piping.
~ ~~
I
No-
I
Description
7
Function
~~~
1-0
I
controipanel
I
Performs
parasnetex
setting
and
displays
set
values.
I
@
I
Front cover opening
button
1
Press
this
button
to
open the front cover.
3-2
0
RID-1OA
ON
I
I%
OFF0
No.
0
0
0
Description Function
Refer
to
page
Cell inlet
port
Connects the
tube
from
column.
4-8
I II
@I
@
@
@
HI1
I
Cell outlet
port
Tube
holder
Connection
port
for leak
tube
Normally
COM~C~S
back
pressure
tube
(03mm
ID.
x
Im).
4-9
Secures
the connected
tube.
Connects the leak
tube
to
this
port.
4-13
Solvent
leak
sensor
Detects
solvent leaks and
outputs
an
error signal.
10-4
n
I
\
/
S
0
0
E
3
LL
-
c
3-3
RID-1OA
-
E
0
0
E
3
LL
.-
c
No.
3
6
6
@
c9
‘c,
E
Q
Description
Function
Refer
to
page
This
is
the connector for
SCL-IOA.
7-2
7
-
16
REMOTE
connector
External
input and output
texminals
Grounding terminal
Power supply cord connector
Fuse holder
These terminals connect
external equipment.
This
terminal
is
used
for grounding.
The power supply
cord
is
connected here.
4-8
Two fuses
are
provided
in
this
holder.
8-7
r
I---
I
i
Ta2
I
I
I
\
I
I
3-4
-
RID-1OA
Chapter
4
Installation
~~~ ~~~~ ~
(,,NTENTs
1
4.1
Basic Installation Requirements
.............................................................
4-2
4.2
Example
of
System Layout
....................................................................
4-3
4.3
Stacking Modules
...................................................................................
4-4
4.4
Electrical Connections
............................................................................
4-5
4.5
Plumbing Connections
...........................................................................
4-6
4.6
Connecting the Recorder
and
Integrator
................................................
4
-
1 1
4.7
Connecting the
Drain
Tube for Solvent Leakage
...................................
4-13
4-1
RID-1OA
-
Basic Installation Requirements
pAGiiiq
To
take full advantage of the RID-1OA’s performance capabilities
and
to
ensure its operational stability over a long service life,
verify that
the
selected installation site satisfies the following
requirements.
1.
Ventilation
2.
Fire
3.
Sink
Ventilate the room where
the
high-perfomance liquid chromatograph
is located since the solvent used is flammable
andor toxic.
Never use
fre in the same room where the high performance liquid
chromatograph is installed. Also, avoid installation in the same
room of other devices which may spark.
Always
keep
a
fire
extinguisher nearby
in
case of accident.
Install a sink nearby for flushing eyes
or
skin which have been in
contact with solvent.
4.
Corrosive gas and dust
Avoid installation in a place exposed to corrosive
gases
or dust.
5.
Electromagnetic noise
Avoid locations subject to intense magnetic or electromagnetic
fields. Use
an
additional noise filter if power line noise interferes.
6.
Space requirements
This system is designed to be used on a table
or
stand, preferably a
solid and flat surface with
a
depth of 60cm
or
more.
See
“4.2,
Example of System Layout” for typical confi,o;urations of systems
and installation space.
7.
Others
Select
an
installation site with
the
following parameters to maintain
full performance of the system.
(1)
Maintain
room temperature within
4--35”C,
without extreme
fluctuations.
(2)
Avoid direct output of a heater or a cooler.
(3)
Avoid exposure to direct sunlight.
(4)
Avoid locations subject to strong vibrations
or
prolonged
weak vibrations.
(5)
Maintain relative humidity within
45-85%.
4-2
-
RID-1OA
Example
of
System
Layout
Example
of
liquid chromatograph system layout using this equip
-
ment
and
space requirements
are
shown below.
Detector
(RI
0-1QA)
Column oven (CTO-1OA)
Manual injector
(7725)
Pump (LC-IOAD)
Reservoir
box
Chrornatopac (C-RGA)
Degasser
(D
G
U -1
06)
Option
bpx
S
[Caution/
Each component
of
the
LC-1OA
has a little clearance at the bot-
tom. Be careful to keep fingers clear when installing the unit.
4-3
RID-1OA
-
RID-1OA may
be
stacked on the pump (LC-IOASLC-lOAD/
LC- 1 OAT/LC- 1 OAi) or the column oven (CTO
-
1
ON
1 OAC). The
equipment can
be
stacked and locked for safety in case of
an
earthquake, etc. using the supplied locking plate.
(1) Refer to the figure below and remove the screws fastening
the equipment cover.
(2)
Attach the mounting plate using the removed screws.
Tighten the
mounting
plate
using the removed screws.
4-4
-
RID-1OA
piEG@-[
Check the following points before connecting power supply.
Supply voltage and capacity
lOOV 150VA 228-32000-91
120V
150VA 228-32000-92
220
-
240V 150VA 228-32000-94
~ ~~~~~~~
When the power supply
is
not stable or the capacity insufficient,
satisfactory performance is not possible. Verify the total power
supply for the system before preparing the power supply.
0
Verify that the power switch of the main unit is
turned
OFF.
1.
Connection
to
outlet
(1)
Connect the female connector of the power supply cord
supplied with the unit to the power supply cord connector at
the rear
of
the unit, and plug the male connector into a power
supply outlet.
The supplied power cord is a three
-
conductor (3-prong) type.
When connecting to a
twoconductor (2-prong) type power
supply outlet, use the provided power supply adapter.
(2)
2.
Grounding
(1)
(2)
When the three
-
conductor type power supply outlet
is
used,
the unit is grounded by the power supply cord.
When the
two-conductor type power supply outlet is used,
the unit is not grounded.
In
this
case, ground
from
the
grounding terminal on the
rear
panel of the unit.
piiGi@l
To
prevent electric shock and to secure safe operation of the
system, always ground the unit.
4-5
RID-1OA
-
F
-
7
umbing
Connections
This section describes proper connection in a typical
flow
line as
shown
in the figure below:
1.
Flow
line in the system
Refer to the column oven instruction manual for installation
of
the
manual injector and column oven. When the column oven is
not
used, an injector holder and a column holder are optionally
available for installation of the manual injector and the column.
2.
Connecting the solvent delivery pump and manual injector
Connection of the solvent delivery pump and the manual injector
are described below.
Cut the
SUS
pipe
(1.6
x
0.3 supplied
as
a liquid pump
accessory) to the necessary length for the pump outlet and
injector port
2.
Install
the male nut and ferrule to both ends of the
SUS
pipe.
Attach the male nut
1.6MN
and ferrule
1.6F
(accessories of
the pump)
to
the pump outlet side, and the male nut and
ferrule (accessories of the manual injector) to the manual
injector.
Connect
an
end of the
SUS
pipe to the pump outlet and the
other end to the injector.
(Notel
Connect the
drain
tube to the manual injector ports 5 and
6.
Adjust the tip of the
drain
tube to meet the needle port of the
injector.
For all connections of the manual injector, use the male nut and
ferrule supplied
as
the manual injector accessory.
4-6
-
RID-1OA
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